CN108201902A - TMRadThe insulating box of tester - Google Patents

TMRadThe insulating box of tester Download PDF

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Publication number
CN108201902A
CN108201902A CN201611168580.0A CN201611168580A CN108201902A CN 108201902 A CN108201902 A CN 108201902A CN 201611168580 A CN201611168580 A CN 201611168580A CN 108201902 A CN108201902 A CN 108201902A
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CN
China
Prior art keywords
side wall
insulating box
babinet
box according
air inlet
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
CN201611168580.0A
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Chinese (zh)
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CN108201902B (en
Inventor
费轶
徐伟
张帆
王振刚
刘静如
贾学五
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
China Petroleum and Chemical Corp
Sinopec Qingdao Safety Engineering Institute
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China Petroleum and Chemical Corp
Sinopec Qingdao Safety Engineering Institute
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Application filed by China Petroleum and Chemical Corp, Sinopec Qingdao Safety Engineering Institute filed Critical China Petroleum and Chemical Corp
Priority to CN201611168580.0A priority Critical patent/CN108201902B/en
Publication of CN108201902A publication Critical patent/CN108201902A/en
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    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01LCHEMICAL OR PHYSICAL LABORATORY APPARATUS FOR GENERAL USE
    • B01L1/00Enclosures; Chambers
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01LCHEMICAL OR PHYSICAL LABORATORY APPARATUS FOR GENERAL USE
    • B01L7/00Heating or cooling apparatus; Heat insulating devices
    • B01L7/50Cryostats
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N33/00Investigating or analysing materials by specific methods not covered by groups G01N1/00 - G01N31/00

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  • Health & Medical Sciences (AREA)
  • Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Clinical Laboratory Science (AREA)
  • Biochemistry (AREA)
  • Physics & Mathematics (AREA)
  • Analytical Chemistry (AREA)
  • Medicinal Chemistry (AREA)
  • General Health & Medical Sciences (AREA)
  • General Physics & Mathematics (AREA)
  • Immunology (AREA)
  • Pathology (AREA)
  • Food Science & Technology (AREA)
  • Engineering & Computer Science (AREA)
  • Apparatus Associated With Microorganisms And Enzymes (AREA)
  • Sampling And Sample Adjustment (AREA)

Abstract

The present invention relates to TMRadThe insulating box of tester.The insulating box includes the babinet for accommodating laboratory sample, air inlet runner is provided in babinet and goes out flow channel, the entrance of air inlet runner is both formed in the outlet for going out flow channel on the first side wall, the multiple distributing fins being arranged in parallel, multiple distributing fins are spaced apart and are mounted in the opposite circumferential side wall of babinet and towards the internal stretch of babinet by supporting rod respectively in the axial direction.Be provided with multiple distributing fins in the insulating box of the present invention, these distributing fins can guide hot-air insulating box formed multiple small circulation and and then enable chemicals thermally equivalent in insulating box, so as to obtain accurate TMRadData.

Description

TMRadThe insulating box of tester
Technical field
The present invention relates to chemicals field of storage, more particularly to TMRadThe insulating box of tester.
Background technology
It is widely recognized at present, the hazardous chemicals such as peroxide, self reactive substances are in storage and transportational process The tendency for the reaction that may decompose is respectively provided with, this decomposable process sometimes results in very serious safety problem.
It has been found that environment temperature may influence the speed of decomposition reaction, and the speed of decomposition reaction will influence chemicals Speed is thermally generated in parcel post.When being thermally generated radiating rate of the speed more than parcel post, there is heat accumulation in parcel post.The accumulation Heat can further promote the progress of decomposition reaction.When parcel post is stacked on a large scale, due to the blocking heat-blocking action of outer layer parcel post, The heat-transfer environment of internal layer parcel post is similar to adiabatic environment.In this case, chemicals decomposition reaction in parcel post is investigated to reach most The time of big reaction rate, i.e. TMRad, to instructing chemical producting safety storage and transport process extremely important.
In the adiabatic environment for usually using the insulating box simulation above-mentioned in the lab, to obtain the change in insulating box The TMR of productadData.However, usually insulating box is conducted heat using natural convection air, this leads to each of the chemicals in insulating box A part can touch the air-flow of different temperatures, i.e. the uneven heating of chemicals is even, so as to cause obtained TMRadData are not Accurately.
Invention content
In view of the above-mentioned problems, the present invention proposes a kind of TMRadThe insulating box of tester.It is set in the insulating box of the present invention Multiple distributing fins are equipped with, these distributing fins can guide hot-air to form multiple small circulation in insulating box and and then make constant temperature Chemicals in case can thermally equivalent, so as to obtain accurate TMRadData.
TMR according to the present inventionadThe insulating box of tester includes the babinet for accommodating laboratory sample, is set in babinet There is air inlet runner and go out flow channel, the entrance of air inlet runner is both formed in the outlet for going out flow channel on the first side wall;It is parallel to set The multiple distributing fins put, multiple distributing fins are spaced apart and are mounted on the opposite of babinet by supporting rod respectively in the axial direction Circumferential side wall on and towards the internal stretch of babinet.
Insulating box according to the present invention, hot-air are entered through air inlet runner inside insulating box.It is spaced apart with wall box Multiple distributing fins the guiding of hot-air that script is flowed along babinet wall can be divided into multiply tributary and be further formed office The small circulation in portion.These small circulation have identical temperature and laboratory sample are heated in all directions, thus test Sample realizes thermally equivalent on the whole, this is extremely favourable to obtain more accurate TMRadData.
In one embodiment, multiple distributing fins are parallel with the first side wall.
In one embodiment, multiple distributing fins are configured to include towards the inclined-plane of the first side wall and opposite with inclined-plane The sphenoid faced directly, the small end of sphenoid is towards the circumferential side wall of babinet, and big end is towards the inside of babinet.Distributing fin it is oblique Face contributes to hot-air tributary to form circulation.In a preferred embodiment, inclined-plane and the angle faced directly are the first acute angle, the One acute angle is between 15 ° to 25 °, preferably 20 °.The first so small acute angle will not stop the flowing of hot-air so that by more Multiple small circulation that a distributing fin is formed are essentially identical, this helps to be evenly heated laboratory sample.Further, since air Density very little, so small the first acute angle is enough hot-air tributary is guided to form small circulation.
In one embodiment, be axially distant from the direction of the first side wall, multiple distributing fins and corresponding circumferential side wall it Between gap be gradually reduced.As stream of hot air is along the flowing of babinet wall, the distributing fin of upstream constantly intercepts stream of hot air, The stream of hot air for reaching downstream is caused to tail off.Therefore, the distributing fin in downstream is configured closer to side wall, helps to be formed Multiple small circulation it is identical.
In one embodiment, air inlet runner and go out flow channel and be spaced apart by the guide part of bent, guide part includes The cylindrical portion that is connected with the first side wall and the guide plate for being connected and being parallel to the first side wall with cylindrical portion;In guide plate and first Air inlet runner is formd between side wall, cylindrical portion forms out flow channel, and multiple distributing fins are in the downstream of guide plate.According to This structure, stream of hot air can be flowed directly to through air inlet runner at the circumferential side wall of babinet under the guiding of guide part, and by Multiple distributing fins form multiple small circulation.Finally, these small circulation bring together from go out flow channel outflow.
In one embodiment, the end structure of guide plate is into the inclined-plane towards air inlet runner, inclined-plane and guide plate it is outer The angle on surface is the second acute angle.In a preferred embodiment, the second acute angle is between 15 ° to 25 °, preferably 20 °.This Second acute angle of kind angle reduces stream of hot air to the resistance of the circumferential side wall of babinet, and then help to be formed by distributing fin Hot-air circulation.
In one embodiment, the supporting rack of support laboratory sample is additionally provided in babinet, the height of supporting rack is more than The height of distributing fin.By setting supporting rack, just without laboratory sample is in direct contact cabinet wall and is placed, so as to fulfill The various pieces of laboratory sample are carried out it is equal, be uniformly heated up, help to obtain more accurate TMRadData.
In one embodiment, babinet is cuboid, is not had on the first side wall and rear wall with the first side wall face Multiple distributing fins are set, distributing fin is provided on remaining side wall.It has been found that it is set on remaining side wall After distributing fin, rear wall can push the small circulation of the hot-air of most downstream to laboratory sample.In the case, if on rear wall It is also provided with multiple distributing fins and does not contribute to the small circulation of thermal control gas of most downstream and flow to test specimen, its stream can be interfered on the contrary It is dynamic, be unfavorable for carrying out the various pieces of laboratory sample it is equal, be uniformly heated up.
Compared with prior art, the advantage of the invention is that:Multiple distributing fins are provided in the insulating box of the present invention, These distributing fins can guide hot-air to form multiple small circulation in insulating box and and then make the chemicals in insulating box uniform It is heated, so as to obtain accurate TMRadData.
Description of the drawings
The invention will be described in more detail below based on embodiments and refering to the accompanying drawings.Wherein:
Fig. 1 schematically shows TMR according to an embodiment of the inventionadThe structure of the insulating box of tester;
Fig. 2 is the A direction views of Fig. 1;
Fig. 3 schematically shows the TMR in Fig. 1adThe hot-air field of flow of the insulating box of tester;
Fig. 4 is the enlarged view of the part B in Fig. 1;And
Fig. 5 schematically shows the cross section of distributing fin with enlarged view.
In the accompanying drawings, identical component uses identical reference numeral.Attached drawing is not according to practical ratio.
Specific embodiment
The present invention will be further described with reference to the accompanying drawings.
Fig. 1 shows TMR according to the present invention with one embodimentadThe structure of the insulating box 10 of tester.Such as Fig. 1 institutes Show, insulating box 10 includes the babinet 11 of generally cuboid.The inside of babinet 11 forms the space for accommodating laboratory sample 2.
There is air inlet runner 201 in 11 internal structure of babinet and go out flow channel 202.The entrance 21 and outlet of air inlet runner 201 The outlet 22 of runner 202 is formed on the first side wall 1 of babinet 11.Oriented babinet 11 is installed in the circumferential side wall 12 of babinet 11 Extend internally multiple distributing fins 204, be not provided with distributing fin on the first side wall 1 of babinet 11 and rear wall 13.These Distributing fin 204 is parallel to each other and preferably parallel with the first side wall 1 (that is, generally along circumferential direction), and axially between 15 It separates.In addition, these distributing fins 204 are mounted in circumferential side wall 12 (i.e. in water conservancy diversion wing by supporting rod 14 spaced apart There are gaps 16 between piece 204 and circumferential side wall 12) so that the hot-air from air inlet runner 201 can by gap 16 and Circumferentially internal flow of the side wall 12 to babinet 11.
Fig. 2 schematically shows entrance 21 and outlet 22 on the first side wall 1.With reference to Fig. 1 and Fig. 2 it is found that inlet air flow Road 201 with flow channel 202 is gone out is formed by the interval of guide part 25 of bent.Specifically, guide part 25 includes tubular Portion 251 and the guide plate 252 being connected with cylindrical portion 251.The generally tablet of guide plate 252 is filled and is had in the middle and tubular Thus guide plate 252 can be generally vertically mounted together by 251 matched circular hole of portion with cylindrical portion 251.In the first side wall 1 On offer through-hole 23.The diameter of cylindrical portion 251 is less than the diameter of through-hole 23 and is connected by multiple connecting rods 24 with the first side wall 1 It is connected to together, so as to which guide part 25 to be installed to the inside of babinet 11.It sees on the whole, guide plate 252 is substantially parallel to One side wall 1 is simultaneously spaced apart with the first side wall 1 and circumferential side wall 12.In this way, cylindrical portion 251 forms out flow channel 202, it is being oriented to Air inlet runner 201 is formd between plate 252 and the first side wall 1.In this case, multiple in circumferential side wall 12 lead Stream fin 204 is in the downstream of guide plate 252.
In the insulating box 10 for using the present invention, laboratory sample 100 is put into the inside of babinet 11 first, then by into The entrance 21 of flow channel 201 feeds hot-air to the inside of babinet 11.Hot-air flows to circumferential under the guiding of air inlet runner 201 Side wall 12, and form the stream stock 30 of circumferentially downstream (or inside of babinet 11) flowing of side wall 12;Mounted on circumferential side wall Multiple distributing fins 204 on 12 respectively can form multiply tributary 33 since flow interception part hot-air in stock 30, and into one Step promotes these multiply tributaries 33 to be respectively formed local small circulation 31;Finally, these small circulation 31 converge into exhaust stream 32 through going out Flow channel 202 leaves babinet 11, as shown in Figure 3.These small circulation 31 and exhaust stream 32 have identical temperature and each Laboratory sample 100 is heated in direction, and thus laboratory sample 100 realizes thermally equivalent on the whole, this is extremely favourable to obtain More accurate TMRadData.
The end structure of guide plate 252 is into the inclined-plane 19 towards air inlet runner 201.The appearance on inclined-plane 19 and guide plate 252 The angle in face 200 is the second acute angle 101, as shown in Figure 4.Preferably, the second acute angle 101 is between 15 ° to 25 °, more preferably 20°.Second acute angle 101 helps that stream of hot air is guided to reduce gas-flow resistance to circumferential side wall 12.
Also as shown in Figure 1 and Figure 5, distributing fin 204 is constructed similarly to sphenoid, including inclined-plane 51 and faces 55 directly. In installation condition, inclined-plane 51 is towards the first side wall 1, and the small end 52 of distributing fin 204 is towards circumferential side wall 12, big end 53 Towards the inside of babinet 11.It inclined-plane 51 and faces 55 directly and forms the first acute angle 54.Preferably, the first acute angle 54 15 ° to 25 ° it Between, more preferably 20 °.In this way, the distance L between distributing fin 204 and the first side wall 1 is in the direction far from circumferential side wall 12 On be gradually reduced, this contributes to tributary 33 to churn along inclined-plane 51 to come and form small circulation 31.For adjacent water conservancy diversion Special case between fin 204 is also in this way, which is not described herein again.If the angle of the first acute angle 54 is excessive, can prevent Small circulation 31 is formed, therefore should not be configured to the angle of the first acute angle 54 to be more than 25 °.And when the angle of the first acute angle 54 is less than At 15 °, then tributary 33 cannot be promoted to churn and come, and then small circulation 31 should not be formed.
In addition, also as shown in figure 5, rear wall 13 is mainly used for pushing the small circulation of the hot-air in downstream to laboratory sample 100, because This does not need to set distributing fin 204 on rear wall 13.
It is also preferred that the direction of the first side wall 1 is axially distant from, multiple distributing fins 204 and corresponding circumferential side wall 12 Between gap 16 be gradually reduced.As stream of hot air is along the wall flowing of babinet 11, the distributing fin 204 of upstream is constantly cut Stream of hot air is taken, the stream of hot air for reaching downstream is caused to tail off.Therefore, the distributing fin in downstream 204 is configured closer to week To side wall 12, contribute to the multiple small circulation to be formed identical in flow velocity, air pressure etc., so as to improve to laboratory sample 100 heating consistency.
Preferably, the supporting rack 17 of support laboratory sample 100 is also provided in babinet 11, the height of supporting rack 17 is more than The height of distributing fin 204.Inner wall of each face of laboratory sample 100 not with babinet 11 is contacted (that is, generally outstanding as a result, Dummy status), hot-air small circulation multiple in this way the various pieces of laboratory sample 100 can be carried out it is equal, be uniformly heated up, Help to obtain more accurate TMRadData.
In this application, direction term " upstream " and " downstream " are using the flow direction of hot-air as reference.
Although by reference to preferred embodiment, invention has been described, in the situation for not departing from the scope of the present invention Under, various improvement can be carried out to it and component therein can be replaced with equivalent.Especially, it to be rushed as long as there is no structures Prominent, items technical characteristic mentioned in the various embodiments can be combined in any way.The invention is not limited in texts Disclosed in specific embodiment, but all technical solutions including falling within the scope of the appended claims.

Claims (10)

1.TMRadThe insulating box of tester, including for accommodating the babinet of laboratory sample, air inlet is provided in the babinet Runner is both formed in the outlet for going out flow channel on the first side wall with flow channel, the entrance of the air inlet runner is gone out,
The multiple distributing fins being arranged in parallel, the multiple distributing fin are spaced apart and are pacified respectively by supporting rod in the axial direction In the opposite circumferential side wall of the babinet and towards the internal stretch of the babinet.
2. insulating box according to claim 1, which is characterized in that the multiple distributing fin is put down with the first side wall Row.
3. insulating box according to claim 2, which is characterized in that the multiple distributing fin is configured to include towards institute State the inclined-plane of the first side wall and the sphenoid faced opposite with the inclined-plane, the small end of the sphenoid is towards the babinet Circumferential side wall, big end is towards the inside of the babinet.
4. insulating box according to claim 3, which is characterized in that the inclined-plane is first sharp with the angle faced directly Angle, first acute angle is between 15 ° to 25 °, preferably 20 °.
5. insulating box according to any one of claims 1 to 4, which is characterized in that be axially distant from the first side wall Direction, the gap between the multiple distributing fin and corresponding circumferential side wall is gradually reduced.
6. the insulating box according to any one of claim 1 to 5, which is characterized in that the air inlet runner and the outlet Runner is spaced apart by the guide part of bent, the guide part include the cylindrical portion that is connected with the first side wall and with it is described Cylindrical portion is connected and is parallel to the guide plate of the first side wall,
The air inlet runner is formd between the guide plate and the first side wall, the cylindrical portion forms the outlet Runner, the multiple distributing fin are in the downstream of the guide plate.
7. insulating box according to claim 6, which is characterized in that the end structure of the guide plate is into towards the air inlet The inclined-plane of runner, the angle on the inclined-plane and the outer surface of the guide plate is the second acute angle.
8. insulating box according to claim 7, which is characterized in that second acute angle is between 15 ° to 25 °, preferably 20°。
9. the insulating box according to any one of claim 1 to 8, which is characterized in that branch is additionally provided in the babinet The supporting rack of the laboratory sample is supportted, the height of shown supporting rack is more than the height of the distributing fin.
10. the insulating box according to any one of claim 1 to 9, which is characterized in that the babinet is cuboid, The first side wall and with being not provided with distributing fin on the rear wall of the first side wall face, is provided with institute on remaining side wall State multiple distributing fins.
CN201611168580.0A 2016-12-16 2016-12-16 TMRadConstant temperature box of tester Active CN108201902B (en)

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Application Number Priority Date Filing Date Title
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CN108201902B CN108201902B (en) 2020-06-26

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110456287A (en) * 2019-08-05 2019-11-15 厦门多彩光电子科技有限公司 A kind of thermostat
CN111486742A (en) * 2020-04-23 2020-08-04 中国空气动力研究与发展中心高速空气动力研究所 Natural convection enhanced heat exchange structure based on semi-closed flow channel

Citations (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR920000701B1 (en) * 1989-03-27 1992-01-20 박순홍 Usual humiditor
JP2009216357A (en) * 2008-03-12 2009-09-24 Nagano Science Kk Temperature controlled bath
CN104152663A (en) * 2014-07-18 2014-11-19 新疆金风科技股份有限公司 Heating furnace of annular component
CN204122133U (en) * 2014-08-04 2015-01-28 广州赛宝计量检测中心服务有限公司 A kind of temperature test chamber by heating liquid and constant temperature
CN204170745U (en) * 2014-10-16 2015-02-25 广西师范大学 A kind of air bath thermostat
CN204365328U (en) * 2014-12-29 2015-06-03 广州威锘浦环境试验设备有限公司 Calm simulated environmental test device
CN205042489U (en) * 2015-08-31 2016-02-24 广州市汉迪环境试验设备有限公司 Calm constant temperature test case
CN105413763A (en) * 2015-12-06 2016-03-23 重庆阿泰可试验设备有限公司 High temperature high humidity constant temperature constant humidity test box
CN205435766U (en) * 2016-02-24 2016-08-10 东莞市剑乔试验设备有限公司 Air duct structure for constant temperature and constant humidity test box

Patent Citations (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR920000701B1 (en) * 1989-03-27 1992-01-20 박순홍 Usual humiditor
JP2009216357A (en) * 2008-03-12 2009-09-24 Nagano Science Kk Temperature controlled bath
CN104152663A (en) * 2014-07-18 2014-11-19 新疆金风科技股份有限公司 Heating furnace of annular component
CN204122133U (en) * 2014-08-04 2015-01-28 广州赛宝计量检测中心服务有限公司 A kind of temperature test chamber by heating liquid and constant temperature
CN204170745U (en) * 2014-10-16 2015-02-25 广西师范大学 A kind of air bath thermostat
CN204365328U (en) * 2014-12-29 2015-06-03 广州威锘浦环境试验设备有限公司 Calm simulated environmental test device
CN205042489U (en) * 2015-08-31 2016-02-24 广州市汉迪环境试验设备有限公司 Calm constant temperature test case
CN105413763A (en) * 2015-12-06 2016-03-23 重庆阿泰可试验设备有限公司 High temperature high humidity constant temperature constant humidity test box
CN205435766U (en) * 2016-02-24 2016-08-10 东莞市剑乔试验设备有限公司 Air duct structure for constant temperature and constant humidity test box

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110456287A (en) * 2019-08-05 2019-11-15 厦门多彩光电子科技有限公司 A kind of thermostat
CN111486742A (en) * 2020-04-23 2020-08-04 中国空气动力研究与发展中心高速空气动力研究所 Natural convection enhanced heat exchange structure based on semi-closed flow channel

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