CN108192736A - The equipment and its process of normal temperature and pressure distillation extraction agilawood essential oil - Google Patents
The equipment and its process of normal temperature and pressure distillation extraction agilawood essential oil Download PDFInfo
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- CN108192736A CN108192736A CN201810158188.0A CN201810158188A CN108192736A CN 108192736 A CN108192736 A CN 108192736A CN 201810158188 A CN201810158188 A CN 201810158188A CN 108192736 A CN108192736 A CN 108192736A
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- Prior art keywords
- reaction kettle
- water
- heat exchange
- steam
- water tank
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Classifications
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/02—Recovery or refining of essential oils from raw materials
- C11B9/027—Recovery of volatiles by distillation or stripping
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/02—Recovery or refining of essential oils from raw materials
- C11B9/022—Refining
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- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Fats And Perfumes (AREA)
Abstract
The invention discloses the equipment and its process that a kind of normal temperature and pressure distills extraction agilawood essential oil, it is characterized in inlet water tank coupled reaction kettle water supply pump, reaction kettle water supply pump is connected to the burning steam water layer of reaction kettle by reaction kettle water inlet pipe, reaction kettle has reaction kettle air outlet pipe to connect heat exchange head tower, connection heat exchange bottom tower under heat exchange head tower, connection compression cooler bin under the bottom of towe of heat exchange bottom, it compresses and oil water separator is housed under cooler bin, reaction kettle intracavity bottom is equipped with steam heat exchanger plate, steam heat exchanger plate has steam (vapor) outlet, electric-heating assembly is housed under steam heat exchanger plate, electric-heating assembly connects electric cabinet.Advantage is:Heating distillation is directly carried out to agalloch eaglewood plant with steam and obtains quality height, high degree of automation is not guarded manually, automatic heating humidification, and oil yield is high, oil quality is high, pure, and value is high, and equipment investment is few, save labor power saving, easy to install and use, and operation is easy, securely and reliably.
Description
Technical field
The invention belongs to distillation equipment, the equipment of especially a kind of normal temperature and pressure distillation extraction agilawood essential oil and
Its process.
Background technology
There are many existing agalloch eaglewood steam oil equipment, and traditional distillation is that olla heating distillation takes oil, recently also useful pressure cooker
The device and method of distillation are heated, it is equipment, simple for process, it is easily mastered and operates.But these device and method steam rates are low,
Oil quality is not pure enough, and oily fragrance is also not strong enough.Existing public technology application number:CN201410519611, denomination of invention:
A kind of agilawood essential oil distills extraction element, including distillation still, oil water separator and condenser, has further included blender, has carried out
During distillation, the substance in distillation still can be stirred using blender.The equipment construction of existing public technology, technical characteristic
It is formed with the structure of the present invention, technical characteristic is to differ, and is not also similar.
Invention content
It steams and gives off a strong fragrance the purpose of the present invention is to provide a kind of steam generated with 100 DEG C of hot water, quality
Pure, oil yield is high, and equipment is simple, is easy to make, easy to install and use, and operation is easy, saving of labor's power saving, production cost
The equipment and its process of a kind of low normal temperature and pressure distillation extraction agilawood essential oil.
The technical solution of the present invention is in this way:A kind of equipment of normal temperature and pressure distillation extraction agilawood essential oil,
Including rack, reaction kettle, electric cabinet, heat exchange head tower, heat exchange bottom tower, compression cooler bin, reaction kettle water inlet pipe, first
Water-oil separating return duct, wind turbine cooling and compression cooling connecting tube, oil water separator, inlet water tank, water tank inlet, cooling for reflux
Pipe, wind turbine water tank, reaction kettle air outlet pipe, cooling water supply pump, the first cooling feed pipe, cools back water pipe, is second cold cooling blower
But feed pipe, wind turbine cool back water pipe, wind turbine water tank connecting pipe, reaction kettle water supply pump, the second water-oil separating return duct, steam heat
Power board, reaction kettle side wall, burns steam water layer, electric-heating assembly, discharge port, head cover, universal wheel and manhole at steam (vapor) outlet, special
Sign is 11 coupled reaction kettle water supply pump 23 of inlet water tank, and reaction kettle water supply pump 23 is connected to reaction kettle 2 by reaction kettle water inlet pipe 7
Burning steam water layer 28, reaction kettle 2 has reaction kettle air outlet pipe 16 to connect heat exchange head tower 4, and connection heat is handed under heat exchange head tower 4
Refoot tower 5, connection compression cooler bin 6 under heat exchange bottom tower 5, equipped with oil water separator 10, reaction kettle under compression cooler bin 6
2 intracavity bottoms are equipped with steam heat exchanger plate 25, and steam heat exchanger plate 25 has steam (vapor) outlet 26, is equipped under steam heat exchanger plate 25
Electric-heating assembly 29, electric-heating assembly 29 connect electric cabinet 3.
There are wind turbine water tank connecting pipe 22, the connection cooling water supply pump of inlet water tank 11 between wind turbine water tank 15 and cooling blower 14
17, cooling water supply pump 17 has the first cooling feed pipe 18 connection heat exchange head tower 4, and heat exchange head tower 4 cools back water pipe 19 and connects
Tap into water tank 11.
Second cooling feed pipe 20, which connects heat exchange bottom tower 5 and cooling blower 14, wind turbine water tank 15, wind turbine cooling backwater
Pipe 21 connects heat exchange bottom tower 5.
Oil water separator 10 passes through the second water-oil separating return duct 24,8 pipe therein of the first water-oil separating return duct
Coupled reaction kettle 2.
Steam heat exchanger plate 25 has steam (vapor) outlet 26 uniformly distributed, and steam (vapor) outlet 26 is there are one more than.
Reaction kettle 2 pushes up upper outlet equipped with head cover 31, and the electric-heating assembly 29 of reaction kettle 2 is electrothermal tube and/or electric hot plate, is reacted
There is discharge port 30 in 2 lower section of kettle.
Reaction kettle 2, electric cabinet 3, heat exchange head tower 4, heat exchange bottom tower 5, compression cooler bin 6, oil water separator 10, water inlet
Case 11, cooling blower 14, wind turbine water tank 15, cooling water supply pump 17 and reaction kettle water supply pump 23 are installed in rack 1.
Agalloch eaglewood raw material is locked after being put into from 2 top opening of reaction kettle with head cover 31, and agalloch eaglewood raw material is in 2 inner cavity of reaction kettle, instead
It is steam heat exchanger plate 25 to answer under 2 inner cavity of kettle, enter from reaction kettle water supply pump 23 burn the water temperature of steam water layer 28 60 DEG C with
On, it is peace and quiet water to burn steam water, and the steam of reaction kettle 2 connects heat exchange head tower 4 by reaction kettle air outlet pipe 16 and enters, and pass through
Heat exchange bottom tower 5 enters compression cooler bin 6, enters the separation precipitation agalloch eaglewood essence of oil water separator 10 by compressing cooler bin 6 later
Oil.
Reaction kettle 2, heat exchange head tower 4, heat exchange bottom tower 5, compression cooler bin 6, inlet water tank 11, wind turbine water tank 15, cooling
Wind turbine 14 is equipped with Wen Sheng, the humidity of each former component of survey meter monitoring, electric appliance overload, overheat, overcurrent, disconnected phase, water tank, water
With appliance circuit short trouble, survey meter is all connected to electric cabinet 3, and electric cabinet 3 is equipped with alarm.
Compared with the prior art, the present invention has the advantages of:Heating distillation is directly carried out to agalloch eaglewood plant with steam and obtains quality
Height, high degree of automation are not guarded manually, and automatic heating humidification, oil yield is high, and oil quality is high, pure, and value is high, equipment
Small investment, save labor power saving, easy to install and use, and operation is easy, securely and reliably, can extract and is used for again while extracting essential oil
Beauty skin steeps foot relaxing tendons and activating collaterals, the distilled water byproduct of moisturizing beauty treatment.
Description of the drawings
Fig. 1 is the overall structure installation assembling schematic front view of the present invention.
Fig. 2 is the overall structure installation assembling schematic rear view of the present invention.
Fig. 3, which is that the overall structure installation assembling of the present invention is right, regards schematic diagram.
Fig. 4 is the overall structure installation assembling left view schematic diagram of the present invention.
Fig. 5 is the overall structure installation assembling schematic top plan view of the present invention.
Fig. 6 is overall structure installation the first stereoscopic schematic diagram of assembling of the present invention.
Fig. 7 is overall structure installation the second stereoscopic schematic diagram of assembling of the present invention.
Fig. 8 is the steam power board main view schematic cross-sectional view of the present invention.
Fig. 9 is the schematic top plan view by Fig. 8 of the present invention.
Reference numeral:Rack 1, electric cabinet 3, heat exchange head tower 4, heat exchange bottom tower 5, compresses cooler bin 6, is anti-reaction kettle 2
Answer kettle water inlet pipe 7, the first water-oil separating return duct 8, wind turbine cooling and compression cooling connecting tube 9, oil water separator 10, inlet water tank
11st, water tank inlet 12, cool back flow tube 13, cooling blower 14, wind turbine water tank 15, reaction kettle air outlet pipe 16, cooling water supply pump
17th, the first cooling feed pipe 18, cool back water pipe 19, second and cool down that feed pipe 20, wind turbine cool back water pipe 21, wind turbine water tank connects
Take over 22, reaction kettle water supply pump 23, the second water-oil separating return duct 24, steam heat exchanger plate 25, steam (vapor) outlet 26, reaction kettle side
Wall 27 burns steam water layer 28, electric-heating assembly 29, discharge port 30, head cover 31, universal wheel 32, manhole 33.
Specific embodiment
The present invention is described in further detail below in conjunction with the accompanying drawings
Embodiment 1, it is according to the present invention to form structure and generate steam steam oil principle with conventional heat up water:Each part is integrally fixed at
Put agalloch eaglewood raw material in rack, in reaction kettle into;Water tank is connected by water supply pump and reaction kettle water inlet pipe, is passed through by water pump anti-
Answer kettle water inlet pipe that water is pumped into reaction kettle;Reaction kettle is connect by reaction kettle air outlet pipe with cold water pipe, and cold water pipe is by water inlet pipe(Packet
Include water supply pump), return pipe and water tank connect;Cooling tube outlet is directly connected to wind turbine cooling tube import, wind turbine cooling tube
Outlet is connect, while wind turbine cooling tube is connect respectively by water inlet pipe with return pipe with wind turbine by connecting tube with compression cooler bin;
Compress coolant outlet connection oil water separator.
Embodiment 2, joins skilful attached drawing, reaction kettle 2, electric cabinet 3, heat exchange head tower 4, heat exchange bottom tower 5, compression cooler bin 6,
Oil water separator 10, inlet water tank 11, cooling blower 14, wind turbine water tank 15, cooling water supply pump 17, second cool down feed pipe 20 and anti-
Kettle water supply pump 23 is answered to be mounted on rack 1.2 inner cavity bottom of reaction kettle has steam heat exchanger plate 25, and steam heat exchanger plate 25 has steam
Outlet 26 is uniformly distributed, and steam (vapor) outlet 26 has under steam heat exchanger plate 25 there are one more than and burns steam water layer 28.Electric-heating assembly 29 is pacified
Under the burning steam water layer 28 of reaction kettle 2.2 inner cavity of reaction kettle puts agalloch eaglewood raw material into, agalloch eaglewood raw material granulate through crushing or
Powdery, sheet.2 bottom surface of reaction kettle is equipped with electric-heating assembly 29, and electric-heating assembly 29 connects electricity, and have temperature adjustment tune with electric cabinet 3
The thermoelectric control switch and warning circuit of heat, thermo-electronic switch and warning circuit element are outsourcing piece, also can designed, designed.Reaction kettle
2 have head cover 31 above, and 2 top of reaction kettle has reaction kettle outlet pipe 16 to connect heat exchange head tower 4, is heat under heat exchange head tower 4
Bottom tower 5 is exchanged to communicate.Heat exchange head tower 4 and heat exchange bottom tower 5 are tubulars.Oil water separator 10 has the second water-oil separating return duct
24 connect and mounted on 2 top of reaction kettle, and oil water separator 10 can also have the connection of the first water-oil separating return duct 8 to be mounted on reaction
2 bottom of kettle, the first water-oil separating return duct 8 and the second water-oil separating return duct 24 in use can only open one of pipe,
Without opening two pipes simultaneously.2 bottom of reaction kettle has the connection cooling water supply pump 17 of reaction kettle water inlet pipe 7 to communicate, inlet water tank 11
There is water tank inlet 12 to connect external water pipe to supply water.The connection of reaction kettle water inlet pipe 7 is burnt steam water layer 28 and is communicated.Wind turbine water tank 15 has
It cools back flow tube 13 and is connect with heat exchange bottom tower 5 and communicated, wind turbine water tank 15 has water tank to connect with fan connecting tube 22 to communicate, cool down
Wind turbine 14 has the second cooling feed pipe 20 to connect with heat exchange head tower 4 to communicate.Wind turbine water tank 15 have wind turbine cool back water pipe 21 with
The connection of heat exchange bottom tower 5 communicates.Heat exchange head tower 4 cools back water pipe 19 and is communicated with inlet water tank 11.Heat exchange head tower 4 has first
Cooling feed pipe 18 is communicated with cooling water supply pump 17, and cooling water supply pump 17 is connect with inlet water tank 11 to be communicated.Reaction kettle water supply pump 23
It is communicated with the burning steam water layer 28 of reaction kettle 2, reaction kettle water supply pump 23 is communicated with inlet water tank 11.There is universal quadrangle under rack 1
Wheel 32.Manhole 33 is arranged at 2 bottom of reaction kettle.Heat exchange bottom tower 5 is cooled back water pipe 21 and is connected by the second cooling feed pipe 20, wind turbine
Cooling blower 14, the connection compression cooler bin 6 of cooling blower 14, there is pipeline connection between wind turbine water tank 15 and cooling blower 14.Heat
The beneath installation compression cooler bin 6 of bottom tower 5 is exchanged, compresses and oil water separator 10 is installed under cooler bin 6, under oil water separator 10
There is essential oil mouth and go out to distill the mouth of a river.Oil water separator 10 goes out to distill the mouth of a river and the first water-oil separating return duct 8 or the second oil
Water separation return duct 24 communicates.
Embodiment 3, agalloch eaglewood raw material are put into 2 inner cavity of reaction kettle, top cover 31, from water tank inlet from 2 top opening of reaction kettle
12 add in 60 DEG C of clear water to inlet water tank 11, and the reacted kettle water supply pump 23 of water and reaction kettle water inlet pipe 7 of inlet water tank 11 enter reaction
The burning steam water layer 28 of kettle 2,29 electrified regulation of electric-heating assembly burns the water of 28 the inside of steam water layer, clear in steam water layer 28 when burning
Water temperature reaches the steam generated at 100 DEG C and enters 2 inner cavity of reaction kettle from steam (vapor) outlet 26, and agalloch eaglewood raw material is heated and is distilled.It is heavy
The oil-water-gas that perfume material is evaporated out enters heat exchange head tower 4, heat exchange bottom tower 5, oil-water-gas quilt from reaction kettle air outlet pipe 16
Enter oil water separator 10 after heat exchange, oil water separator 10 is precipitated essential oil from distilled water.Reaction kettle 2, heat exchange head tower 4,
Heat exchange bottom tower 5, compression cooler bin 6, oil water separator 10, inlet water tank 11, cooling blower 14, wind turbine water tank 15, cooling are supplied water
Pump 17, reaction kettle water supply pump 23 and burning steam water layer 28 are mounted on survey meter, for temperature detection, visit wet and spy water, survey meter
Electric cabinet 3 is all connected to, electric cabinet 3 is equipped with alarm, when appliance circuit element failure alarm equipment alarm.
Claims (9)
1. a kind of equipment of normal temperature and pressure distillation extraction agilawood essential oil, including rack, reaction kettle, electric cabinet, heat exchange head tower, heat
Exchange bottom tower, compression cooler bin, reaction kettle water inlet pipe, the first water-oil separating return duct, wind turbine cooling and compression cooling connecting tube,
Oil water separator, water tank inlet, cools back flow tube, cooling blower, wind turbine water tank, reaction kettle air outlet pipe, cooling confession at inlet water tank
Water pump, the first cooling feed pipe, cool back water pipe, the second cooling feed pipe, wind turbine cools back water pipe, wind turbine water tank connecting pipe,
Reaction kettle water supply pump, the second water-oil separating return duct, steam heat exchanger plate, steam (vapor) outlet, reaction kettle side wall, burn steam water layer,
Electric-heating assembly, discharge port, head cover, universal wheel and manhole, it is characterised in that 11 coupled reaction kettle water supply pump 23 of inlet water tank, reaction kettle
Water supply pump 23 is connected to the burning steam water layer 28 of reaction kettle 2 by reaction kettle water inlet pipe 7, and reaction kettle 2 has reaction kettle air outlet pipe 16
Heat exchange head tower 4 is connected, heat exchange bottom tower 5 is connected under heat exchange head tower 4, compression cooler bin is connected under heat exchange bottom tower 5
6, compression cooler bin 6 is beneath equipped with oil water separator 10, and 2 intracavity bottom of reaction kettle is equipped with steam heat exchanger plate 25, and steam heat is handed over
Changing plate 25 has steam (vapor) outlet 26, electric-heating assembly 29 is housed, electric-heating assembly 29 connects electric cabinet 3 under steam heat exchanger plate 25.
2. the equipment of normal temperature and pressure distillation extraction agilawood essential oil described in accordance with the claim 1, it is characterised in that wind turbine water tank 15
There is wind turbine water tank connecting pipe 22 between cooling blower 14, the connection cooling water supply pump 17 of inlet water tank 11, cooling water supply pump 17 has the
One cooling feed pipe 18 connects heat exchange head tower 4, and heat exchange head tower 4 cools back water pipe 19 and connects inlet water tank 11.
3. the equipment of normal temperature and pressure distillation extraction agilawood essential oil described in accordance with the claim 1, it is characterised in that the second cooling supplies
Water pipe 20 connects heat exchange bottom tower 5 and cooling blower 14, and wind turbine water tank 15 has wind turbine to cool back the connection heat exchange of water pipe 21 bottom tower
5。
4. the equipment of normal temperature and pressure distillation extraction agilawood essential oil described in accordance with the claim 1, it is characterised in that oil water separator
10 pass through the second water-oil separating return duct 24,8 pipe coupled reaction kettle 2 therein of the first water-oil separating return duct.
5. the equipment of normal temperature and pressure distillation extraction agilawood essential oil described in accordance with the claim 1, it is characterised in that steam heat exchange
Plate 25 has steam (vapor) outlet 26 uniformly distributed, and steam (vapor) outlet 26 is there are one more than.
6. the equipment of normal temperature and pressure distillation extraction agilawood essential oil described in accordance with the claim 1, it is characterised in that on the top of reaction kettle 2
Outlet is equipped with head cover 31, and the electric-heating assembly 29 of reaction kettle 2 is electrothermal tube and/or electric hot plate, and there is discharge port 30 in 2 lower section of reaction kettle.
7. the equipment of normal temperature and pressure distillation extraction agilawood essential oil described in accordance with the claim 1, it is characterised in that reaction kettle 2, electricity
Control case 3, heat exchange head tower 4, heat exchange bottom tower 5, compression cooler bin 6, oil water separator 10, inlet water tank 11, cooling blower 14, wind
Machine water tank 15, cooling water supply pump 17 and reaction kettle water supply pump 23 are installed in rack 1.
8. the process of a kind of normal temperature and pressure distillation extraction agilawood essential oil, it is characterised in that agalloch eaglewood raw material is from 2 top opening of reaction kettle
It is locked after being put into head cover 31, agalloch eaglewood raw material is steam heat exchanger plate 25 under 2 inner cavity of reaction kettle in 2 inner cavity of reaction kettle,
Enter the water temperature for burning steam water layer 28 at 60 DEG C or more from reaction kettle water supply pump 23, burn steam water for peace and quiet water, the steaming of reaction kettle 2
Vapour connects heat exchange head tower 4 by reaction kettle air outlet pipe 16 and enters, and passes through heat exchange bottom tower 5 and enter compression cooler bin 6, later
Enter the separation precipitation agilawood essential oil of oil water separator 10 by compressing cooler bin 6.
9. according to the process of the normal temperature and pressure distillation extraction agilawood essential oil described in claim 8 or 1, it is characterised in that reaction
Kettle 2, heat exchange head tower 4, heat exchange bottom tower 5, compression cooler bin 6, inlet water tank 11, wind turbine water tank 15, cooling blower 14 are equipped with
Wen Sheng, the humidity of each former component of survey meter monitoring, electric appliance overload, overheat, overcurrent, disconnected phase, water tank, water and appliance circuit are short
Road failure, survey meter are all connected to electric cabinet 3, and electric cabinet 3 is equipped with alarm.
Priority Applications (1)
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CN201810158188.0A CN108192736A (en) | 2018-02-25 | 2018-02-25 | The equipment and its process of normal temperature and pressure distillation extraction agilawood essential oil |
Applications Claiming Priority (1)
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CN201810158188.0A CN108192736A (en) | 2018-02-25 | 2018-02-25 | The equipment and its process of normal temperature and pressure distillation extraction agilawood essential oil |
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CN108192736A true CN108192736A (en) | 2018-06-22 |
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ID=62593666
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CN201810158188.0A Pending CN108192736A (en) | 2018-02-25 | 2018-02-25 | The equipment and its process of normal temperature and pressure distillation extraction agilawood essential oil |
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Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN108542997A (en) * | 2018-07-22 | 2018-09-18 | 秦乐 | A kind of burn and scald anti-inflammation liquid and its manufacturing technique method |
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CN206502795U (en) * | 2017-02-28 | 2017-09-19 | 湖北好雨时节农业发展有限责任公司 | Distillation extraction element for producing rose |
CN206872771U (en) * | 2017-06-28 | 2018-01-12 | 陕西博秦生物工程有限公司 | A kind of movable plant essential oil extracting device |
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Publication number | Priority date | Publication date | Assignee | Title |
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CN201347427Y (en) * | 2008-09-28 | 2009-11-18 | 中华全国供销合作总社南京野生植物综合利用研究院 | Combined distillation equipment of natural spice essential oil |
CN205740948U (en) * | 2016-06-12 | 2016-11-30 | 黑龙江省科学院自然与生态研究所 | A kind of plants essential oil extraction equipment |
CN106398869A (en) * | 2016-07-21 | 2017-02-15 | 甘肃农业大学 | An efficient cooking kettle suitable for essence oil extraction through a water vapor method |
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CN206502795U (en) * | 2017-02-28 | 2017-09-19 | 湖北好雨时节农业发展有限责任公司 | Distillation extraction element for producing rose |
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