CN108187356B - Take vertical double-tube pass circulating fluidized bed evaporimeter of baffle - Google Patents

Take vertical double-tube pass circulating fluidized bed evaporimeter of baffle Download PDF

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CN108187356B
CN108187356B CN201810158651.1A CN201810158651A CN108187356B CN 108187356 B CN108187356 B CN 108187356B CN 201810158651 A CN201810158651 A CN 201810158651A CN 108187356 B CN108187356 B CN 108187356B
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plate
partition plate
solid particle
fluidized bed
tube
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CN108187356A (en
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姜峰
李娜
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Tianjin University
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Tianjin University
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    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D1/00—Evaporating
    • B01D1/0082—Regulation; Control
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D1/00—Evaporating
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D1/00—Evaporating
    • B01D1/0094—Evaporating with forced circulation
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D1/00—Evaporating
    • B01D1/30—Accessories for evaporators ; Constructional details thereof

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  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)
  • Devices And Processes Conducted In The Presence Of Fluids And Solid Particles (AREA)

Abstract

The invention belongs to the technical field of evaporators, and discloses a vertical double-tube-pass circulating fluidized bed evaporator with a partition plate, which comprises a heating chamber and an evaporation chamber, wherein the heating chamber is divided into an ascending bed and a descending bed, the partition plate is arranged in the evaporation chamber, and a mixed working medium consisting of solid particles and liquid-phase working medium pure water is added into the heating chamber and the evaporation chamber for forced circulation; the upper part of the partition board is provided with a solid particle distribution board, the solid particle distribution board comprises a side board fixedly connected with the partition board and a main board vertically connected to the top of the side board, and the main board is horizontally arranged and positioned above the descending bed; the mainboard is provided with the round hole that the multirow is gradually grow from inside to outside as solid particle passway mouth. The invention has simple structure and convenient processing, can prevent and remove scale and strengthen heat transfer on line, and the particle distribution device can effectively improve the particle distribution condition of the downer, can uniformly distribute solid particles in the tube bundle of the downer, and is beneficial to further improving the effects of strengthening heat transfer and preventing and removing scale.

Description

Take vertical double-tube pass circulating fluidized bed evaporimeter of baffle
Technical Field
The invention belongs to the technical field of evaporators, and particularly relates to a heat transfer enhancement, scale prevention and removal technology applied to a vertical double-tube-pass circulating evaporator with a partition plate.
Background
The vertical double-tube-pass circulating evaporator with the partition plate is generally applied to industrial production of sodium sulfide and the like. As the operation time is prolonged, suspended substances or crystals in the material are concentrated on the wall surface of the tube bundle, and scale is formed. The heat transfer coefficient in the heat exchange pipe is reduced due to the generation of dirt, the heat transfer rate is reduced, and the heat exchange equipment needs to be shut down and cleaned periodically, so that the production capacity is seriously reduced. At present, the methods for preventing and removing scale adopted by this type of evaporator mainly include physical methods and chemical methods, such as: the method adopts a high-pressure water gun for cleaning, chemical scale inhibitors and the like, but the methods have the defects of influencing production, increasing operation cost, polluting environment and the like due to parking, and can not fundamentally solve the scaling problem of equipment. The fluidized bed heat exchange antiscaling energy-saving technology combines the fluidized bed technology and the heat exchange process, and the fluidized solid particles move randomly to shear and collide continuously to heat the wall surface, so as to destroy the flowing and heat transferring boundary layer, reduce heat transferring resistance, raise heat transferring efficiency, prolong the scaling inducing period effectively and have obvious antiscaling and descaling effects and reinforced heat transferring effect. The technology is implemented in a physical process, the scale prevention and removal mechanism is irrelevant to the types of materials, the application prospect is wide, and the online enhanced heat transfer and scale prevention and removal of heat exchange equipment can be realized. In the implementation process of the fluidized bed heat exchange anti-scaling energy-saving technology, the distribution of solid particles in the tube bundle can influence the collision and shearing of the particles on the wall surface of the heating tube, and further influence the effects of heat transfer enhancement, scale prevention and removal, so that the uniform distribution of the particles in the tube bundle is the premise for realizing the good operation of the technology.
Disclosure of Invention
The invention aims to solve the technical problems of heat transfer performance reduction and wall surface scaling in long-term use of a vertical double-tube-pass circulating type evaporator with a partition plate, provides a vertical double-tube-pass circulating fluidized bed evaporator with a partition plate, applies a fluidized bed heat exchange anti-scaling energy-saving technology to the vertical double-tube-pass circulating type evaporator, and aims at solving the problems that particles on one side of an upper bed in the fluidized bed evaporator are uniformly distributed and particles in a lower bed are not uniformly distributed.
In order to solve the technical problems, the invention is realized by the following technical scheme:
a vertical double-tube pass circulating fluidized bed evaporator with a partition plate comprises a heating chamber and an evaporation chamber arranged above the heating chamber, wherein the heating chamber is divided into an ascending bed and a descending bed, the partition plate is arranged in the evaporation chamber, and a mixed working medium consisting of solid particles and liquid-phase working medium pure water is added into the heating chamber and the evaporation chamber to carry out forced circulation;
a solid particle distribution plate is arranged at the upper part of the partition plate, the solid particle distribution plate comprises a side plate fixedly connected to the partition plate and a main plate vertically connected to one side of the top of the side plate, and the main plate is horizontally arranged and positioned above the descending bed;
the mainboard is the semi-circular plate body, the mainboard is provided with three to four rows of round holes as solid particle passway mouth, the same and the centre of a circle of each row of round hole diameter of solid particle passway mouth is at same radial semicircle equipartition, and the diameter of each row of round hole is followed the mainboard is radial from inside to outside crescent.
Preferably, the solid particles are polyoxymethylene particles, which are spherical with a diameter of 2.0-5.5mm and a density of 1390kg/m3(ii) a GranuleThe addition amount of the granules is 0.5-2.0 percent, and the circulating flow rate is 10.66-19.14m3/h。
Preferably, the height of the partition is 0.05 to 0.2 m.
Preferably, the side plate is a strip-shaped plate body, and the side plate is vertically connected to the lower part of the straight edge of the main plate; the circle center of the semicircular plate body of the main plate is superposed with the top center point of the side plate.
Preferably, the rows of circular holes of the solid particle passage openings are arranged at equal center distances.
Preferably, the diameter of the semicircular plate body of the main plate is 250-280mm, no hole is formed in the radius range of 40-50mm, the other part of the semicircular plate body is provided with four rows of round holes as the solid particle passage ports, the circle centers of the four rows of round holes from inside to outside are respectively arranged on the semicircular arcs with the radius of 48-53mm, 60-65mm, 85-90mm and 115-120mm, and the diameters of the semicircular arc are respectively 7-9mm, 11-13mm, 18-22mm and 22-26 mm.
Preferably, the side plate is provided with a clamping groove which is opened downwards and is used for being inserted into the upper part of the partition plate so as to fix the solid particle distribution plate.
The invention has the beneficial effects that:
the invention has simple structure and convenient processing, and the mixed working medium replaces pure water to carry out forced circulation in the evaporator, and the circulating fluidized bed evaporator can play the effects of online scale prevention and removal and heat transfer enhancement; and the solid particle distribution plate is arranged on the partition plate, so that the particle distribution condition of the downer in the vertical double-tube-pass circulating fluidized bed evaporator with the partition plate can be effectively improved, solid particles can be uniformly distributed in a tube bundle of the downer, the heating wall surface of each tube of the downer is sheared and collided, the boundary layer of flowing and heat transfer is damaged, and further the effects of enhancing heat transfer and preventing and removing scale are further improved.
Drawings
FIG. 1 is a schematic structural view of a vertical double-pass circulating fluidized bed evaporator with baffles according to the present invention;
in fig. 1: 1. a circulation pump; 2. a particle collector; 3. an electromagnetic flow meter; 4. an end socket inner partition plate; 5. an ascending bed; 6. a downer; 7. a heating chamber; 8. an evaporation chamber; 9. a partition plate; 10. a solid particle distribution plate.
FIG. 2 is a schematic diagram of the configuration of the solid particle distribution plate of FIG. 1;
in fig. 2: 101. a main board; 102. a side plate; 103. a solid particle passage port.
Detailed Description
In order to further understand the contents, features and effects of the present invention, the following embodiments are illustrated and described in detail with reference to the accompanying drawings:
as shown in figure 1, the embodiment discloses a vertical double-tube pass circulating fluidized bed evaporator with a partition, which is composed of a heating chamber 7 and an evaporation chamber 8, wherein the evaporation chamber 8 is positioned above the heating chamber 7, the heating chamber 7 can be divided into an ascending bed 5 and a descending bed 6 by a seal head inner partition plate 4, a partition 9 is arranged in the evaporation chamber 8, and fluid flows through the ascending bed 5 of the heating chamber 7 to enter the evaporation chamber 8 and passes through the partition 9 in the evaporation chamber 8 to enter the descending bed 6 of the heating chamber 7. Wherein the height of the partition board 9 is 0.05-0.2 m.
In order to solve the problems of scaling and reduced heat transfer performance caused by long-term operation of a vertical double-tube-pass circulating evaporator with a partition plate, the invention adopts a mixed working medium consisting of solid particles and liquid-phase working medium pure water to replace the pure water to carry out forced circulation in the evaporator. Wherein the solid particles are preferably polyoxymethylene particles, the polyoxymethylene particles are spherical, the diameter of the polyoxymethylene particles is 2.0-5.5mm, and the density of the polyoxymethylene particles is 1390kg/m3(ii) a The addition of the particles is 0.5-2.0%, and the circulation flow is 10.66-19.14m3The minimum flow rate in the evaporator at which the polyoxymethylene particles can be circulated and fluidized is 10.66m3Per hour, when the circulating flow is higher than 19.14m3At/h, a large number of bubbles enter the evaporator. In this embodiment, the height of the partition 9 is 0.15m, the amount of the polyoxymethylene particles added is 0.5%, and the amount of the particles added is the percentage of the volume of the bulk of the added particles to the volume of the liquid.
Since the solid particles are uniformly mixed in the end socket and enter the ascending bed 5, the solid particles are uniformly distributed in the ascending bed 5, and the particles in the descending bed 6 have to have a higher horizontal velocity to enter the tube bundle far away from the partition plate 9, so more particles enter the tube bundle near the partition plate 9. The invention designs a solid particle distribution plate 10, wherein the solid particle distribution plate 10 is fixed on a partition plate 9 and is positioned above one side of a downer 6 in an evaporation chamber 8, so that solid particles can be uniformly distributed in the downer 6.
As shown in fig. 2, the solid particle distribution plate 10 includes a main plate 101 and a side plate 102, and the main plate 101 and the side plate 102 are fixedly connected together at a right angle. The main plate 101 is a semicircular plate body, the side plate 102 is a strip-shaped plate body, and the side plate 102 is vertically connected to the lower part of the straight edge of the main plate 101. The center of the semicircular plate body of the main plate 101 coincides with the center point of the top of the side plate 102, and is located at the center of the evaporation chamber. The main board 101 is provided with three to four rows of round holes as solid particle passage ports 103, the diameter of each row of round holes is the same, the circle centers of the round holes are uniformly distributed on a semicircular arc with the same radius, and the diameter of each row of round holes is gradually increased from inside to outside along the radial direction of the main board 101. For example, the main plate 101 is a semicircular plate with a diameter of 260mm, no hole is formed in a radius range of 46mm, four rows of circular holes are arranged in the rest part as the solid particle passage ports 103, the centers of the four rows of circular holes from inside to outside are respectively arranged on a semicircular arc with a radius of 50mm, 65mm, 90mm and 117mm, and the diameters of the four rows of circular holes are respectively 8mm, 12mm, 20mm and 24 mm. The side plate 102 has a slot with a lower opening, that is, the longitudinal section of the side plate 102 is in an inverted U shape, and the slot is used for being inserted into the upper part of the partition plate 9 to fix the solid particle distribution plate 10. The solid particle distribution plate 10 is mounted by its side plates 102 on the upper part of the partition 9, while its main plate 10 is horizontally disposed above the side of the downer 6 in the evaporation chamber 8.
Generally, the diameter of the semicircular plate body of the main plate 101 is 250-280mm, no hole is formed in the radius range of 40-50mm, the circle centers of the four rows of circular holes from inside to outside are respectively arranged on the semicircular arcs with the radius of 48-53mm, 60-65mm, 85-90mm and 115-120mm, and the diameters of the semicircular arc are respectively 7-9mm, 11-13mm, 18-22mm and 22-26 mm.
The solid particles thus pass through the upgoing bed 5 into the evaporation chamber 8, over the partition 9, are redistributed by the solid particle distribution plate 10 and then into the downgoing bed 6. When the solid particle distribution plate 10 is not reinforced, the solid particles tend to enter the tube bundle close to the partition plate 9 and the center of the evaporation chamber 8, so that the solid particles can be uniformly distributed in the downer 6 by the design that no hole is formed in the center of the solid particle distribution plate 10, the solid particle channel 103 is formed in the rest part of the solid particle distribution plate, and the diameter of the circular hole of the solid particle channel 103 is gradually increased from inside to outside along the radial direction of the main plate 101.
When the device works, the circulating pump 1 is started, the liquid-solid two phases circularly flow, solid particles frequently impact the pipe wall, fluid enters the ascending bed 5 from bottom to top, passes through the partition plate 9 and passes through the solid particle distribution plate 10 to be redistributed and uniformly flows into the pipe bundle of the descending bed 6. The circulating flow is adjusted by a frequency converter, and is measured by an electromagnetic flowmeter. The circulating flow rate has obvious influence on the circulating fluidization state of the solid particles, and the circulating flow rate in the experiment is 10.66-19.14m3When the circulation flow rate is changed within the above range, the uniformity of the distribution can be improved by 90% at most, compared with the unreinforced particle distribution plate.
Although the preferred embodiments of the present invention have been described above with reference to the accompanying drawings, the present invention is not limited to the above-described embodiments, which are merely illustrative and not restrictive, and those skilled in the art can make various changes and modifications within the spirit and scope of the present invention without departing from the spirit and scope of the appended claims.

Claims (6)

1. A vertical double-tube pass circulating fluidized bed evaporator with a partition plate comprises a heating chamber and an evaporation chamber arranged above the heating chamber, wherein the heating chamber is divided into an ascending bed and a descending bed, and the evaporation chamber is internally provided with the partition plate;
a solid particle distribution plate is arranged at the upper part of the partition plate, the solid particle distribution plate comprises a side plate fixedly connected to the partition plate and a main plate vertically connected to one side of the top of the side plate, and the main plate is horizontally arranged and positioned above the descending bed;
the main board is a semicircular plate body, three to four rows of round holes are arranged on the main board and used as solid particle channel ports, the diameter of each row of round holes of the solid particle channel ports is the same, the circle centers of the round holes are uniformly distributed on a semicircular arc with the same radius, and the diameter of each row of round holes is gradually increased from inside to outside along the radial direction of the main board;
the diameter of the semicircular plate body of the main plate is 250-280mm, no hole is formed in the radius range of 40-50mm, the other part is provided with four rows of round holes as the solid particle passage ports, the circle centers of the four rows of round holes from inside to outside are respectively arranged on the semicircular arcs where the radius of the four rows of round holes is 48-53mm, 60-65mm, 85-90mm and 115-120mm, and the diameters of the four rows of round holes are respectively 7-9mm, 11-13mm, 18-22mm and 22-26 mm.
2. The vertical double-tube-pass circulating fluidized bed evaporator with the partition plate according to claim 1, wherein the solid particles are polyoxymethylene particles which are spherical and have a diameter of 2.0-5.5mm and a density of 1390kg/m3(ii) a The addition of the particles is 0.5-2.0%, and the circulation flow is 10.66-19.14m3/h。
3. The vertical double-tube-pass circulating fluidized bed evaporator with the partition plate according to claim 1, wherein the height of the partition plate is 0.05-0.2 m.
4. The vertical double-tube-pass circulating fluidized bed evaporator with the partition plate according to claim 1, wherein the side plate is a long-strip-shaped plate body and is vertically connected to the lower part of the straight edge of the main plate; the circle center of the semicircular plate body of the main plate is superposed with the top center point of the side plate.
5. The vertical double-tube-pass circulating fluidized bed evaporator with the partition plate according to claim 1, wherein the rows of the circular holes of the solid particle passage openings are arranged at equal center distances.
6. The vertical, dual-tube-pass circulating fluidized bed evaporator with partition plate according to claim 1, wherein the side plate has a downwardly open slot for inserting into the upper portion of the partition plate to fix the solid particle distribution plate.
CN201810158651.1A 2018-02-23 2018-02-23 Take vertical double-tube pass circulating fluidized bed evaporimeter of baffle Active CN108187356B (en)

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CN108187356B true CN108187356B (en) 2020-08-07

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Publication number Priority date Publication date Assignee Title
CN109399745A (en) * 2018-12-17 2019-03-01 广东上典环境保护工程有限公司 One kind is from descaling evaporator and its operation method
CN110448928A (en) * 2019-07-15 2019-11-15 天津大学 A kind of air-liquid-solid downlink cycle fluidized bed evaporation device and its operating method
CN110448927A (en) * 2019-07-15 2019-11-15 天津大学 A kind of metabisulfite solution recirculating fluidized bed vaporising device and its operating method

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