CN108164883A - A kind of uvioresistant PVC glove and its manufacturing method - Google Patents
A kind of uvioresistant PVC glove and its manufacturing method Download PDFInfo
- Publication number
- CN108164883A CN108164883A CN201810101003.2A CN201810101003A CN108164883A CN 108164883 A CN108164883 A CN 108164883A CN 201810101003 A CN201810101003 A CN 201810101003A CN 108164883 A CN108164883 A CN 108164883A
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- parts
- uvioresistant
- pvc
- sand
- auxiliary agent
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L27/00—Compositions of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by a halogen; Compositions of derivatives of such polymers
- C08L27/02—Compositions of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by a halogen; Compositions of derivatives of such polymers not modified by chemical after-treatment
- C08L27/04—Compositions of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by a halogen; Compositions of derivatives of such polymers not modified by chemical after-treatment containing chlorine atoms
- C08L27/06—Homopolymers or copolymers of vinyl chloride
-
- A—HUMAN NECESSITIES
- A41—WEARING APPAREL
- A41D—OUTERWEAR; PROTECTIVE GARMENTS; ACCESSORIES
- A41D19/00—Gloves
- A41D19/0055—Plastic or rubber gloves
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2201/00—Properties
- C08L2201/08—Stabilised against heat, light or radiation or oxydation
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2201/00—Properties
- C08L2201/10—Transparent films; Clear coatings; Transparent materials
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/03—Polymer mixtures characterised by other features containing three or more polymers in a blend
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- Chemical & Material Sciences (AREA)
- Health & Medical Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Organic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Textile Engineering (AREA)
- Gloves (AREA)
Abstract
Present invention is disclosed a kind of uvioresistant PVC glove and its manufacturing methods, are made of the raw material of following weight fraction:100 parts of PVC powder, 10 15 parts of 78 82 parts of DOP, TXIB, 10 15 parts of D70,2 2.5 parts of stabilizer, 2 2.5 parts of epoxidized soybean oil, 5 10 parts of uvioresistant auxiliary agent, wherein, uvioresistant auxiliary agent is made of the raw material of following weight fraction:12 15 parts of fluorine carbon emulsion, 2 (2 ' hydroxyl, 3 ' tertiary butyl, 5 ' aminomethyl phenyl) 25 parts of 5 chlorobenzotriazoles, 58 parts of 2 hydroxyl, 4 methoxy benzophenone, 34 parts of ceramic powder.The present invention have good anti-ultraviolet property, duration long, it is wearing comfort, at low cost, the UV resistant agent of use does not influence the transparency of product, and the initial coloring of PVC glove is not also influenced, simple production process, easy to operate.
Description
Technical field
The present invention relates to a kind of uvioresistant PVC glove and its manufacturing methods, belong to plastic gloves technical field..
Background technology
Relatively easy, material cost is relatively low, wearing is convenient, comfortable feel, acidproof since its production technology has for PVC glove
Alkali, isolation effect are good, will not cause skin allergy, the characteristics of price is cheap so that quickly growing for PVC glove, it is commonly used
In fields such as medical treatment, electronics processing, food processing, scientific research, fast foods.In certain processing spaces, the both hands of operator can contact purple
Outside line, and PVC glove function currently on the market is single does not have uvioresistant this characteristic.Therefore, for the prior art
Deficiency, design a kind of uvioresistant PVC glove, it appears meaningful.
Invention content
The purpose of the present invention is exactly to solve the above-mentioned problems in the prior art, provides a kind of uvioresistant effect
Good, wearing comfort, duration long uvioresistant PVC glove and its manufacturing method.
The present invention technical solution be:A kind of uvioresistant PVC glove, is made of the raw material of following weight fraction:
100 parts of PVC powder
78-82 parts of DOP
10-15 parts of TXIB
10-15 parts of D70
2-2.5 parts of stabilizer
2-2.5 parts of epoxidized soybean oil
5-10 parts of uvioresistant auxiliary agent;
Wherein, uvioresistant auxiliary agent is made of the raw material of following weight fraction:12-15 parts of fluorine carbon emulsion, 2- (2 '-hydroxyl -3 ' -
Tertiary butyl -5 '-aminomethyl phenyl) -5- is benzotriazole 2-5 parts chloro-, 5-8 parts of ESCALOL 567, ceramic powder 3-4
Part.
Further, above-mentioned uvioresistant PVC glove, it is preferable that be made of the raw material of following weight fraction:
100 parts of PVC powder
80 parts of DOP
10 parts of TXIB
10 parts of D70
2 parts of stabilizer
2 parts of epoxidized soybean oil
8 parts of uvioresistant auxiliary agent,
Wherein, uvioresistant auxiliary agent is made of the raw material of following weight fraction:12 parts of fluorine carbon emulsion, 2- (2 '-hydroxyls -3 '-Te Ding
Base -5 '-aminomethyl phenyl) 5 parts of the chloro- benzotriazole of -5-, 6 parts of ESCALOL 567,3 parts of ceramic powder.
Further, above-mentioned uvioresistant PVC glove, it is preferable that be made of the raw material of following weight fraction:
100 parts of PVC powder
80 parts of DOP
15 parts of TXIB
15 parts of D70
2.5 parts of stabilizer
2.5 parts of epoxidized soybean oil
10 parts of uvioresistant auxiliary agent
Wherein, uvioresistant auxiliary agent is made of the raw material of following weight fraction:12 parts of fluorine carbon emulsion, 2- (2 '-hydroxyls -3 '-Te Ding
Base -5 '-aminomethyl phenyl) 2 parts of the chloro- benzotriazole of -5-, 5 parts of ESCALOL 567,4 parts of ceramic powder.
Further, above-mentioned uvioresistant PVC glove, wherein:The stabilizer is calcium stearate and/or stearic acid
Zinc.
The invention also discloses a kind of manufacturing methods of uvioresistant PVC glove, include the following steps:
(1) Primary batching system:Will DOP, epoxidized soybean oil and uvioresistant auxiliary agent mix after stir, then sequentially add PVC powder, steady
Determine agent, TXIB thinners are stirred, obtain Primary batching system;
(2) standing and defoaming:By Primary batching system standing and defoaming, then filter slurry;
(3) second batch:D70 thinners are added in the material being prepared to step (2), are stirred evenly;
(4) single-steeping:It is added in hopper after the second batch that step (3) is prepared is filtered, fingerprint is preheated to 60
It is impregnated after~70 DEG C, dipping temperature is 46~50 DEG C;
(5) leaching slurry:Hand after dipping is touched and carries out leaching slurry, leaching slurry 5-10 minutes;
(6) primary plasticizing:Fingerprint after dipping is put into oven, is toasted 18~20 minutes at 180~200 DEG C;
(7) sand is soaked:Hand is touched to be put into sand material and is impregnated, sand material viscosity is 600-800Pa.s, and the leaching sand time is 5-10 minutes;
(8) sand is drenched:Hand after leaching sand is touched and carries out leaching sand, the leaching sand time is 2-5 minutes;
(9) secondary plasticizing:Fingerprint after double-steeping is entered in oven, 7~9min is toasted at 190~220 DEG C;
(10) fingerprint after secondary plasticizing is obtained into PVC glove after volume lip, demoulding, inspection, sorting.
The prominent substantive distinguishing features of the present invention and significant progress are mainly reflected in:The present invention has good uvioresistant
Performance, duration long, it is wearing comfort, at low cost, the UV resistant agent of use does not influence the transparency of product, to PVC glove
Initial coloring also do not influence, it is simple production process, easy to operate.
Specific embodiment
Below to the present invention specific embodiment be described in further detail so that technical solution of the present invention be more readily understood and
It grasps.
A kind of uvioresistant PVC glove, is made of the raw material of following weight fraction:
100 parts of PVC powder
78-82 parts of DOP
10-15 parts of TXIB
10-15 parts of D70
2-2.5 parts of stabilizer
2-2.5 parts of epoxidized soybean oil
5-10 parts of uvioresistant auxiliary agent;
Wherein:DOP and epoxidized soybean oil are plasticizer, and plasticizer plays the role of following:1)Intermolecular polyvinyl chloride resin is with very strong
Van der Waals force is combined, and rigidity is very strong, and flexibility is insufficient, plasticizer is filled between macromolecular, makes molecule mutual
Activity is easier to, and reduces the crystallinity of polymer molecular chain, that is, increases the plasticity of polyvinyl chloride resin.2)Improve the elongation of PVC
Rate, circumnutating property and flexibility, and hardness, modulus, softening temperature and brittle temperature all decline, so as to adapt to the need of glove industry
It asks.Epoxidized soybean oil is suitable epoxy plasticiser, and it is to capture PVC to decomposite HCL to play stable mechanism, however epoxy soybean
Oily use level has bleeding when big, layering, muddy can occur when it is cold, epoxidation is different or soybean oil epoxidation is uneven
Weighing apparatus, PART EPOXY, part do not aoxidize, cause polarity different, so as to be layered, therefore the ratio of epoxidized soybean oil should not mistake
Height, preferably 2-2.5 parts in this programme.
TXIP and D70 is thinner, and effect is to reduce viscosity, changes PVC paste Resin Flow matter, convenient for gloves control gram
Weight and thickness, while also function to plasticization, and TXIB is bigger than DOP volatility, remained in after processing the part on PVC glove surface compared with
It is few, therefore finished surface is dryer and comfortableer, it is not easy to pollute, the cleaning of appearance can be kept for a long time.
Since polyvinyl chloride resin begins at 100 degree or more to decomposite HCL, stability is poor.Its mechanism is:It is first in polyvinyl chloride resin
It first generates free radicals, free radical attack resin generates double bond, and the CL of the presence excitation ortho position C of double bond releases HCL, this is PVC
Degradation.PVC degradations have Domino effect:If aerobic presence, i.e., the discoloration of resin into carbonyl, can be deepened and promote chain
Fracture and the effusion of HCL.Therefore stabilizer is needed to absorb the HCL that discharges in PVC processing, and prevent to occur in the presence of oxygen from
Dynamic catalytic action.Meanwhile stabilizer has good dissolubility with PVC.Stabilizer is preferably calcium stearate and/or stearic acid
Zinc.
Uvioresistant auxiliary agent is made of the raw material of following weight fraction:12-15 parts of fluorine carbon emulsion, 2- (2 '-hydroxyls -3 '-spy
Butyl -5 '-aminomethyl phenyl) -5- is benzotriazole 2-5 parts chloro-, 5-8 parts of ESCALOL 567, ceramic powder 3-4
Part.
A kind of manufacturing method of uvioresistant PVC glove of the present invention is as follows:
(1) Primary batching system:Will DOP, epoxidized soybean oil and uvioresistant auxiliary agent mix after stir, then sequentially add PVC powder, steady
Determine agent, TXIB thinners are stirred, obtain Primary batching system;
(2) standing and defoaming:By Primary batching system standing and defoaming, then filter slurry;
(3) second batch:D70 thinners are added in the material being prepared to step (2), are stirred evenly;
(4) single-steeping:It is added in hopper after the second batch that step (3) is prepared is filtered, fingerprint is preheated to 60
It is impregnated after~70 DEG C, dipping temperature is 46~50 DEG C;
(5) leaching slurry:Hand after dipping is touched and carries out leaching slurry, leaching slurry 5-10 minutes;
(6) primary plasticizing:Fingerprint after dipping is put into oven, is toasted 18~20 minutes at 180~200 DEG C;
(7) sand is soaked:Hand is touched to be put into sand material and is impregnated, sand material viscosity is 600-800Pa.s, and the leaching sand time is 5-10 minutes;
(8) sand is drenched:Hand after leaching sand is touched and carries out leaching sand, the leaching sand time is 2-5 minutes;
(9) secondary plasticizing:Fingerprint after double-steeping is entered in oven, 7~9min is toasted at 190~220 DEG C;
(10) fingerprint after secondary plasticizing is obtained into PVC glove after volume lip, demoulding, inspection, sorting.
Embodiment 1
A kind of uvioresistant PVC glove, is made of the raw material of following weight fraction:
100 parts of PVC powder
80 parts of DOP
10 parts of TXIB
10 parts of D70
2 parts of stabilizer
2 parts of epoxidized soybean oil
8 parts of uvioresistant auxiliary agent,
Wherein, uvioresistant auxiliary agent is made of the raw material of following weight fraction:12 parts of fluorine carbon emulsion, 2- (2 '-hydroxyls -3 '-Te Ding
Base -5 '-aminomethyl phenyl) 5 parts of the chloro- benzotriazole of -5-, 6 parts of ESCALOL 567,3 parts of ceramic powder.
PVC glove manufacturing method is as follows:
(1) Primary batching system:Will DOP, epoxidized soybean oil and uvioresistant auxiliary agent mix after stir, then sequentially add PVC powder, steady
Determine agent, TXIB thinners are stirred, obtain Primary batching system;
(2) standing and defoaming:By Primary batching system standing and defoaming, then filter slurry;
(3) second batch:D70 thinners are added in the material being prepared to step (2), are stirred evenly;
(4) single-steeping:It is added in hopper after the second batch that step (3) is prepared is filtered, fingerprint is preheated to 65
It is impregnated after DEG C, dipping temperature is 50 DEG C;
(5) leaching slurry:Hand after dipping is touched and carries out leaching slurry, leaching slurry 5 minutes;
(6) primary plasticizing:Fingerprint after dipping is put into oven, is toasted 20 minutes at 180 DEG C;
(7) sand is soaked:Hand is touched to be put into sand material and is impregnated, sand material viscosity is 800Pa.s, and the leaching sand time is 5 minutes;
(8) sand is drenched:Hand after leaching sand is touched and carries out leaching sand, the leaching sand time is 2 minutes;
(9) secondary plasticizing:Fingerprint after double-steeping is entered in oven, 8min is toasted at 200 DEG C;
(10) fingerprint after secondary plasticizing is obtained into PVC glove after volume lip, demoulding, inspection, sorting.
Embodiment 2
A kind of uvioresistant PVC glove, is made of the raw material of following weight fraction:
100 parts of PVC powder
80 parts of DOP
15 parts of TXIB
15 parts of D70
2.5 parts of stabilizer
2.5 parts of epoxidized soybean oil
10 parts of uvioresistant auxiliary agent
Wherein, uvioresistant auxiliary agent is made of the raw material of following weight fraction:12 parts of fluorine carbon emulsion, 2- (2 '-hydroxyls -3 '-Te Ding
Base -5 '-aminomethyl phenyl) 2 parts of the chloro- benzotriazole of -5-, 5 parts of ESCALOL 567,4 parts of ceramic powder.
PVC glove manufacturing method is as follows:
(1) Primary batching system:Will DOP, epoxidized soybean oil and uvioresistant auxiliary agent mix after stir, then sequentially add PVC powder, steady
Determine agent, TXIB thinners are stirred, obtain Primary batching system;
(2) standing and defoaming:By Primary batching system standing and defoaming, then filter slurry;
(3) second batch:D70 thinners are added in the material being prepared to step (2), are stirred evenly;
(4) single-steeping:It is added in hopper after the second batch that step (3) is prepared is filtered, fingerprint is preheated to 70
It is impregnated after DEG C, dipping temperature is 47 DEG C;
(5) leaching slurry:Hand after dipping is touched and carries out leaching slurry, leaching slurry 5 minutes;
(6) primary plasticizing:Fingerprint after dipping is put into oven, is toasted 18 minutes at 200 DEG C;
(7) sand is soaked:Hand is touched to be put into sand material and is impregnated, sand material viscosity is 700Pa.s, and the leaching sand time is 5 minutes;
(8) sand is drenched:Hand after leaching sand is touched and carries out leaching sand, the leaching sand time is 2 minutes;
(9) secondary plasticizing:Fingerprint after double-steeping is entered in oven, 7min is toasted at 220 DEG C;
(10) fingerprint after secondary plasticizing is obtained into PVC glove after volume lip, demoulding, inspection, sorting.
The PVC glove that is produced of the present invention have good anti-ultraviolet property, duration long, wearing comfort, cost
Low, the UV resistant agent of use does not influence the transparency of product, and the initial coloring of PVC glove is not also influenced, production
It is simple for process, easy to operate.
Certainly, representative instance only of the invention more than, in addition to this, the present invention can also have other a variety of specific implementations
Mode, all technical solutions formed using equivalent substitution or equivalent transformation, is all fallen within the scope of protection of present invention.
Claims (5)
1. a kind of uvioresistant PVC glove, it is characterised in that:It is made of the raw material of following weight fraction:
100 parts of PVC powder
78-82 parts of DOP
10-15 parts of TXIB
10-15 parts of D70
2-2.5 parts of stabilizer
2-2.5 parts of epoxidized soybean oil
5-10 parts of uvioresistant auxiliary agent;
Wherein, uvioresistant auxiliary agent is made of the raw material of following weight fraction:12-15 parts of fluorine carbon emulsion, 2- (2 '-hydroxyl -3 ' -
Tertiary butyl -5 '-aminomethyl phenyl) -5- is benzotriazole 2-5 parts chloro-, 5-8 parts of ESCALOL 567, ceramic powder 3-4
Part.
2. uvioresistant PVC glove according to claim 1, it is characterised in that:It is made of the raw material of following weight fraction:
100 parts of PVC powder
80 parts of DOP
10 parts of TXIB
10 parts of D70
2 parts of stabilizer
2 parts of epoxidized soybean oil
8 parts of uvioresistant auxiliary agent,
Wherein, uvioresistant auxiliary agent is made of the raw material of following weight fraction:12 parts of fluorine carbon emulsion, 2- (2 '-hydroxyls -3 '-Te Ding
Base -5 '-aminomethyl phenyl) 5 parts of the chloro- benzotriazole of -5-, 6 parts of ESCALOL 567,3 parts of ceramic powder.
3. uvioresistant PVC glove according to claim 1, it is characterised in that:It is made of the raw material of following weight fraction:
100 parts of PVC powder
80 parts of DOP
15 parts of TXIB
15 parts of D70
2.5 parts of stabilizer
2.5 parts of epoxidized soybean oil
10 parts of uvioresistant auxiliary agent
Wherein, uvioresistant auxiliary agent is made of the raw material of following weight fraction:12 parts of fluorine carbon emulsion, 2- (2 '-hydroxyls -3 '-Te Ding
Base -5 '-aminomethyl phenyl) 2 parts of the chloro- benzotriazole of -5-, 5 parts of ESCALOL 567,4 parts of ceramic powder.
4. a kind of uvioresistant PVC glove according to claim 1, it is characterised in that:The stabilizer is calcium stearate
And/or zinc stearate.
5. a kind of manufacturing method of uvioresistant PVC glove, it is characterised in that:Include the following steps,
(1) Primary batching system:Will DOP, epoxidized soybean oil and uvioresistant auxiliary agent mix after stir, then sequentially add PVC powder, steady
Determine agent, TXIB thinners are stirred, obtain Primary batching system;
(2) standing and defoaming:By Primary batching system standing and defoaming, then filter slurry;
(3) second batch:D70 thinners are added in the material being prepared to step (2), are stirred evenly;
(4) single-steeping:It is added in hopper after the second batch that step (3) is prepared is filtered, fingerprint is preheated to 60
It is impregnated after~70 DEG C, dipping temperature is 46~50 DEG C;
(5) leaching slurry:Hand after dipping is touched and carries out leaching slurry, leaching slurry 5-10 minutes;
(6) primary plasticizing:Fingerprint after dipping is put into oven, is toasted 18~20 minutes at 180~200 DEG C;
(7) sand is soaked:Hand is touched to be put into sand material and is impregnated, sand material viscosity is 600-800Pa.s, and the leaching sand time is 5-10 minutes;
(8) sand is drenched:Hand after leaching sand is touched and carries out leaching sand, the leaching sand time is 2-5 minutes;
(9) secondary plasticizing:Fingerprint after double-steeping is entered in oven, 7~9min is toasted at 190~220 DEG C;
(10) fingerprint after secondary plasticizing is obtained into PVC glove after volume lip, demoulding, inspection, sorting.
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CN201810101003.2A CN108164883A (en) | 2018-02-01 | 2018-02-01 | A kind of uvioresistant PVC glove and its manufacturing method |
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CN201810101003.2A CN108164883A (en) | 2018-02-01 | 2018-02-01 | A kind of uvioresistant PVC glove and its manufacturing method |
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Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN112029208A (en) * | 2020-08-07 | 2020-12-04 | 百通达科技(东台)有限公司 | Oil-resistant polyvinyl chloride gloves and preparation process thereof |
CN112063069A (en) * | 2020-08-05 | 2020-12-11 | 百通达科技(东台)有限公司 | Ultraviolet-resistant polyvinyl chloride gloves and preparation process thereof |
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CN103720083A (en) * | 2012-10-15 | 2014-04-16 | 无锡新亚安全用品有限公司 | Method for manufacturing anti-skid rubber glove |
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Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN112063069A (en) * | 2020-08-05 | 2020-12-11 | 百通达科技(东台)有限公司 | Ultraviolet-resistant polyvinyl chloride gloves and preparation process thereof |
CN112029208A (en) * | 2020-08-07 | 2020-12-04 | 百通达科技(东台)有限公司 | Oil-resistant polyvinyl chloride gloves and preparation process thereof |
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