CN108163993A - Preparation and the polluted water body repairing method that phosphorus denitrogenates particulate vector are consolidated in a kind of algal control - Google Patents
Preparation and the polluted water body repairing method that phosphorus denitrogenates particulate vector are consolidated in a kind of algal control Download PDFInfo
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- CN108163993A CN108163993A CN201711365928.XA CN201711365928A CN108163993A CN 108163993 A CN108163993 A CN 108163993A CN 201711365928 A CN201711365928 A CN 201711365928A CN 108163993 A CN108163993 A CN 108163993A
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- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F3/00—Biological treatment of water, waste water, or sewage
- C02F3/34—Biological treatment of water, waste water, or sewage characterised by the microorganisms used
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- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F2101/00—Nature of the contaminant
- C02F2101/10—Inorganic compounds
- C02F2101/105—Phosphorus compounds
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- C—CHEMISTRY; METALLURGY
- C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
- C02F2101/00—Nature of the contaminant
- C02F2101/10—Inorganic compounds
- C02F2101/16—Nitrogen compounds, e.g. ammonia
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Abstract
Preparation and the polluted water body repairing method that phosphorus denitrogenates particulate vector are consolidated in a kind of algal control, belong to water-treatment technology field.Algal control consolidate phosphorus denitrogenate particulate carrier materials composition include 20~45 parts of iron powder, 10~25 parts of active carbon powder, 1~5 part of catalyst M, 0.2~2 part of polyvinyl alcohol, 10~18 parts of portland-pozzolana, 0.5~5 part of fruit peel, 0.5~5 part of grain husk, one kind of 0.5~5 part of biomass or its arbitrary combination；Preparation method is the particle for being mixed, being pressed into 0.2~15mm by material composition feeding, by drying, is cured.The particle of preparation, which is put into contaminated water body, can have the effect of algal control, solid phosphorus, denitrogenate, water body blue-green alge after reparation is suppressed completely, and the blue-green alge for having more than 85% is killed, total tp removal rate is up to more than 90%, nitrogen removal rate is up to more than 85%, and it is harmless to biological nontoxics such as water body Mesichthyes, zooplankters, it has broad application prospects.
Description
Technical field
The present invention relates to a kind of algal controls to consolidate preparation and the polluted water body repairing method that phosphorus denitrogenates particulate vector, belongs to water process
Technical field.
Background technology
At present, China's majority urban water-body eutrophication is serious, and " green congee " phenomenon is apparent.It is analyzed main reason is that city
The nourishment source of city's water body (city inland river and inland lake) mostly come from by after city domestic sewage and Industrial Wastewater Treatment again
Unboiled water, but recycled water enter water body after its pollutant can constantly be enriched with, eventually lead to nitrogen, phosphorus, organic matter in urban water-body water quality
It is exceeded；Another reason be by a large amount of nutritive salt of the modes such as atmospheric sedimentation, rain drop erosion, heavy metal, organic matter again into
Enter urban water system, so as to cause the collapse of the urban water system ecological balance, exacerbate water body eutrophication and, algae is spread unchecked.
Mainly there are dystopy treatment technology and in-situ treatment technology to the method for urban water-body eutrophication pollution reparation now.
Polluted-water mainly will be guided to sewage treatment plant after Sediment Dredging and carries out strange land processing by dystopy treatment technology, and wherein bed mud is dredged
It is to dig out river and lake contaminated sediments using waterpower or mechanical means to dredge, and is released by removing bed mud reduction pollutant
It puts.Though this method can obtain relatively thorough effect in a short time, the time, slightly long body eutrophication can occur repeatedly；Separately
Outside, since showering need to excavate bed mud, transfer water body, required engineering equipment is more, costly, and the structure of destructible bed mud is led
The destruction of the city eutrophication water ecosystem is caused, later stage recovery needs the long period.In view of the foregoing, dystopy processing skill
Art is generally applied in laboratory simulation experiment or the relatively small water remediation of Polluted area area more.And in-situ treatment technology
Mobile bed mud and water body position are not required to, cuts off the dirt of pollution sources by taking certain measures that pollutant is prevented to enter water body first
Then dye approach reduces the pollutant load in river, water body in lake and bed mud by using physics, chemistry and biological method
And pollutant solubility, toxicity and migration can be reduced simultaneously.It is sent out by the comparison of dystopy treatment technology and in-situ control technology
Existing, urban water-body in-situ control technology has that investment smaller, operation are more easy to and secondary pollution is less etc. excellent with respect to showering technology
Point is the inevitable requirement and development trend of urban water-body eutrophication remedy and sustainable development.However domestic water body in-situ is repaiied
Recovering technology is limited the problems such as developing high pollutant concentration still in by water body and bed mud and complicated component.
Mainly have at present with regard to the removal of Measures of Algae in Water Body simultaneously：Dispensing algae removal method, adds copper sulphate, chlorine, sodium hypochlorite etc.,
But these methods are of high cost, while can also be with the ecosystem of influence water body；Solid-liquid isolation method, it is direct by micro-filtration, sand filtration etc.
Filtering；Air supporting and reinforced deposition etc..These methods are usually invested big, of high cost, elimination and are not thorough.
According to《Water prevention and cure of pollution action plan》, will there is the rich battalion such as prominent total nitrogen, the total phosphorus influenced on quality of water environment
Fosterization index incorporate basin, regional pollution object prediction emission the binding indicator system, and be distinctly claimed stringent control
The total nitrogen of eutrophication, total phosphorus index.Clear understanding arrives people, controls city eutrophicated polluted water, improves municipal water
Ecological environment ensures water quality safety, realizes urban ecology civilization, has been the task of top priority.Therefore the high, pollution to eutrophic extent
Serious river and lake realize that science, stabilization, quick repair process are one of China's key subjects urgently to be resolved hurrily at present,
And it especially needs that new technology and methods is researched and developed effectively to reduce nitrogen, phosphorus, heavy metal and the chemical oxygen demand in eutrophication water
The polluters such as amount.
In short, solve the problems, such as that it is many that polluted water body still has from algal grown is inhibited at present；It gets dirty in removal
P (phosphorus), N (nitrogen) etc. in water body are contaminated, there is also numerous limitations.
Invention content
The object of the present invention is to provide that can reduce total phosphorus in water, total nitrogen, inhibit algal grown or kill algae so as to
Preparation and polluted water body repairing method that phosphorus denitrogenates particulate vector are consolidated in a kind of algal control that control blue-green alge is spread unchecked.
A kind of algal control consolidates phosphorus and denitrogenates particulate vector, and material composition includes iron powder, active carbon powder, catalyst M, polyethylene
Alcohol, portland-pozzolana and fruit peel, grain husk, one kind of biomass or its arbitrary combination；
Material forms weight proportion：20~45 parts of iron powder, 10~25 parts of active carbon powder, catalyst M1~5 part, poly- second
0.2~2 part of enol, 10~18 parts of portland-pozzolana, 0.5~5 part of fruit peel, 0.5~5 part of grain husk, biomass 0.5~
5 parts.
Catalyst M is one in palladium catalyst powder, catalyst manganese powder, catalyst titanium valve, catalyst copper powder, catalyst magnesium powder
The combination of kind or its arbitrary catalyst.
The preparation method that phosphorus denitrogenates particulate vector is consolidated in a kind of algal control, contains following steps；
Step 1: by composition and proportioning feeding mixing；
Composition and weight proportion are：20~45 parts of iron powder, 10~25 parts of active carbon powder, catalyst M1~5 part are gathered
0.2~2 part of vinyl alcohol, 10~18 parts of portland-pozzolana, 0.5~5 part of fruit peel, 0.5~5 part of grain husk, biomass 0.5
~5 parts；
Step 2: plus water hydraulic produce the particle of 0.2~15mm；
Step 3: the particle of preparation is placed in 110 ± 2 DEG C of drying box, in H2Under the protection of/CO gas, dry 1~
2h；
Step 4: finally particles are cooled to room temperatures.
The pollution waters restoration application method that phosphorus denitrogenates particulate vector is consolidated in a kind of algal control, contains following steps；By preparation
Algal control, which consolidates phosphorus and denitrogenates particulate vector and direct plunge into contaminated water body or be put into container, to be positioned over again in contaminated water body,
Consolidate that phosphorus denitrogenates the continuous haptoreaction of particulate vector and algal control consolidates phosphorus and denitrogenates particulate vector and exists by contaminated water body and algal control
The algal control constantly discharged in water consolidates phosphorus except the biomembrane on nitrogen and its surface acts on, and blue-green alge in water body is made to be pressed down completely
System, and be killed, total phosphorus and total nitrogen are removed, and water body is made to be repaired and purified.
Algal control consolidate phosphorus denitrogenate particulate vector dosage in water body added as 0.5 according to the pollution level of polluted water body~
2.5kg/m3。
By algal control consolidate phosphorus denitrogenate particulate vector launch to carry out in polluted water body except algae, dephosphorization, denitrogenation application.
The algal control prepared consolidates phosphorus and denitrogenates particulate vector, bulk density≤1200Kg/m3, simple Compressive Strength >=0.25Mpa,
Specific surface area >=400m2/ g, porosity of=60%.
Beneficial effects of the present invention：
The present invention provides a kind of algal controls to consolidate preparation and its restorative procedure to polluted-water that phosphorus denitrogenates particulate vector, makes
Consolidate phosphorus with algal control of the present invention and denitrogenate particulate vector, have and blue-green alge is inhibited to grow and is killed, while can be by total phosphorus in water
It is removed with total nitrogen, thoroughly the blue-green alge of solution polluted water body spreads unchecked the eutrophication with water body, the water body blue-green alge after reparation
It is suppressed completely, and the blue-green alge for having more than 85% is killed, total tp removal rate is up to more than 90%, and nitrogen removal rate is up to 85%
More than, and it is harmless to biological nontoxics such as water body Mesichthyes, zooplankters, it has broad application prospects.
The river system repair technology that phosphorus denitrogenates class is consolidated in present invention research and development algal control, for reducing the eutrophy of polluted water body
Change, influence to have important practical significance caused by cyanobacterial bloom
Specific embodiment
Obviously, those skilled in the art belong to the guarantor of the present invention based on many modifications and variations that spirit of the invention is done
Protect range.
Those skilled in the art of the present technique are appreciated that unless otherwise defined all terms used herein are (including technology art
Language and scientific terminology) there is the meaning identical with the general understanding of the those of ordinary skill in fields of the present invention.
For ease of the understanding to the embodiment of the present invention, it will be further explained explanation below, and each embodiment is not
Form the restriction to the embodiment of the present invention.
Embodiment 1：
Algal control, which consolidates phosphorus and denitrogenates the preparation method of particulate vector, to be included：
Step 1: algal control consolidate phosphorus denitrogenate the material of particulate vector by：40 parts of iron powder, 20 parts of active carbon powder, catalyst M 4
Part, 1.5 parts of polyvinyl alcohol, 16 parts of portland-pozzolana, 0.5 part of 3 parts of fruit peel, 1.5 parts of grain husk, biomass mixing；
Catalyst M is one in palladium catalyst powder, catalyst manganese powder, catalyst titanium valve, catalyst copper powder, catalyst magnesium powder
Kind or its arbitrary combination.
Step 2: plus water hydraulic produce the particle of 10mm；
Step 3: the particle of preparation is placed in 110 ± 2 DEG C of drying box, in H2Under the protection of gas, dry 1.5h；
Step 4: finally particles are cooled to room temperatures.
Step 5: phosphorus is consolidated in algal control prepared by step 1 to step 4 denitrogenates particulate vector by 2kg/m3It is directly thrown into leaf
Green element a is 238.2 (chl-a)/μ g/L, TP (total phosphorus) is that 2.75mg/L, TN (total nitrogen) are in the contaminated water bodys of 23.3mg/L,
By the haptoreaction of 3 days, last water body was purified, and water Determination of Chlorophyll a drops to 28.3 (chl-a)/μ g/L, was led to
It crosses FDA-PI fluorescent stainings to be killed using more than 90% blue-green alge of fluorescence microscope, total tp removal rate is up to 99%, total nitrogen
Removal rate is biological without side-effects up to 94%, and to water body Mesichthyes, zooplankter etc..
Embodiment 2：
Algal control, which consolidates phosphorus and denitrogenates the preparation method of particulate vector, to be included：
Step 1: algal control consolidate phosphorus denitrogenate the material of particulate vector by：35 parts of iron powder, 20 parts of active carbon powder, catalyst M 3
Part, 1 part of polyvinyl alcohol, 18 parts of portland-pozzolana, 1 part of 5 parts of fruit peel, 2 parts of grain husk, biomass mixing；Catalyst M is
Palladium catalyst powder, catalyst manganese powder, catalyst titanium valve, catalyst copper powder, one kind in catalyst magnesium powder or its arbitrary catalyst
Combination.
Step 2: plus water hydraulic produce the particle of 15mm；
Step 3: the particle of preparation is placed in 110 ± 2 DEG C of drying box, in H2Under the protection of gas, dry 1.5h；
Step 4: finally particles are cooled to room temperatures.
Step 5: phosphorus is consolidated in algal control prepared by step 1 to step 4 denitrogenates particulate vector by 2.5kg/m3It is directly thrown into
Chlorophyll a is 1099.3 (chl-a)/μ g/L, TP 1.39mg/L, TN are in the contaminated water bodys of 4.6mg/L, is passed through 10 days
Haptoreaction, last water body are purified, and water Determination of Chlorophyll a drops to 20 (chl-a)/μ g/L hereinafter, being contaminated by FDA-PI fluorescence
Color is killed using more than 85% blue-green alge of fluorescence microscope, total tp removal rate up to 99%, nitrogen removal rate up to 90%, and
It is without side-effects to the biology such as water body Mesichthyes, zooplankter.
Embodiment 3：
Algal control, which consolidates phosphorus and denitrogenates the preparation method of particulate vector, to be included：
Step 1: algal control consolidate phosphorus denitrogenate the material of particulate vector by：45 parts of iron powder, 20 parts of active carbon powder, catalyst M 5
Part, 2 parts of polyvinyl alcohol, 18 parts of portland-pozzolana, 3 parts of 3 parts of fruit peel, 5 parts of grain husk, biomass mixing；Catalyst M is
Palladium catalyst powder, catalyst manganese powder, catalyst titanium valve, catalyst copper powder, one kind in catalyst magnesium powder or its arbitrary catalyst
Combination.
Step 2: plus water hydraulic produce the particle of 5mm；
Step 3: the particle of preparation is placed in 110 ± 2 DEG C of drying box, in H2Under the protection of gas, dry 1h；
Step 4: finally particles are cooled to room temperatures.
Step 5: phosphorus is consolidated in algal control prepared by step 1 to step 4 denitrogenates particulate vector by 1.0kg/m3It is directly thrown into
Chlorophyll a is 310.6 (chl-a)/μ g/L, TP 0.29mg/L, TN are in the contaminated water bodys of 2.1mg/L, passes through 5 days connect
Reaction is touched, last water body is purified, and water Determination of Chlorophyll a drops to 30 (chl-a)/μ g/L hereinafter, by FDA-PI fluorescent stainings
It is killed using more than 95% blue-green alge of fluorescence microscope, for total tp removal rate up to 99%, nitrogen removal rate is and right up to 85%
The biology such as water body Mesichthyes, zooplankter is without side-effects.
Embodiment 4：
Algal control, which consolidates phosphorus and denitrogenates the preparation method of particulate vector, to be included：
Step 1: algal control consolidate phosphorus denitrogenate the material of particulate vector by：20 parts of iron powder, 10 parts of active carbon powder, catalyst M1
Part, 0.2 part of polyvinyl alcohol, 10 parts of portland-pozzolana, 0.5 part of 0.5 part of fruit peel, 0.5 part of grain husk, biomass mixing；
Catalyst M for palladium catalyst powder, catalyst manganese powder, catalyst titanium valve, catalyst copper powder, one kind in catalyst magnesium powder or its
The combination of meaning catalyst.
Step 2: plus water hydraulic produce the particle of 5mm；
Step 3: the particle of preparation is placed in 110 ± 2 DEG C of drying box, in H2Under the protection of gas, dry 1h；
Step 4: finally particles are cooled to room temperatures.
Step 5: phosphorus is consolidated in algal control prepared by step 1 to step 4 denitrogenates particulate vector by 1.0kg/m3It is directly thrown into
Chlorophyll a is 310.6 (chl-a)/μ g/L, TP 0.29mg/L, TN are in the contaminated water bodys of 2.1mg/L, passes through 5 days connect
Reaction is touched, last water body is purified, and water Determination of Chlorophyll a drops to 30 (chl-a)/μ g/L hereinafter, by FDA-PI fluorescent stainings
It is killed using more than 95% blue-green alge of fluorescence microscope, for total tp removal rate up to 99%, nitrogen removal rate is and right up to 85%
The biology such as water body Mesichthyes, zooplankter is without side-effects.
Embodiment 5：
Algal control, which consolidates phosphorus and denitrogenates the preparation method of particulate vector, to be included：
Step 1: algal control consolidate phosphorus denitrogenate the material of particulate vector by：45 parts of iron powder, 25 parts of active carbon powder, catalyst M5
Part, 2 parts of polyvinyl alcohol, 18 parts of portland-pozzolana, 5 parts of 5 parts of fruit peel, 5 parts of grain husk, biomass mixing；Catalyst M is
Palladium catalyst powder, catalyst manganese powder, catalyst titanium valve, catalyst copper powder, one kind in catalyst magnesium powder or its arbitrary catalyst
Combination.
Step 2: plus water hydraulic produce the particle of 5mm；
Step 3: the particle of preparation is placed in 110 ± 2 DEG C of drying box, in H2Under the protection of gas, dry 1h；
Step 4: finally particles are cooled to room temperatures.
Step 5: phosphorus is consolidated in algal control prepared by step 1 to step 4 denitrogenates particulate vector by 1.0kg/m3It is directly thrown into
Chlorophyll a is 310.6 (chl-a)/μ g/L, TP 0.29mg/L, TN are in the contaminated water bodys of 2.1mg/L, passes through 5 days connect
Reaction is touched, last water body is purified, and water Determination of Chlorophyll a drops to 20 (chl-a)/μ g/L hereinafter, by FDA-PI fluorescent stainings
It is killed using more than 95% blue-green alge of fluorescence microscope, for total tp removal rate up to 99%, nitrogen removal rate is and right up to 85%
The biology such as water body Mesichthyes, zooplankter is without side-effects.
As described above, the embodiment of the present invention is explained in detail, as long as but essentially without this hair of disengaging
Bright inventive point and effect can have many deformations, this will be readily apparent to persons skilled in the art.Therefore, this
The variation of sample is also integrally incorporated within protection scope of the present invention.
Claims (5)
1. phosphorus is consolidated in a kind of algal control denitrogenates particulate vector, it is characterised in that：Material composition includes iron powder, active carbon powder, catalyst
M, polyvinyl alcohol, portland-pozzolana and fruit peel, grain husk, one kind of biomass or its arbitrary combination；
Material forms weight proportion：20~45 parts of iron powder, 10~25 parts of active carbon powder, catalyst M1~5 part, polyvinyl alcohol
0.2~2 part, 10~18 parts of portland-pozzolana, 0.5~5 part of fruit peel, 0.5~5 part of grain husk, 0.5~5 part of biomass.
2. phosphorus is consolidated in a kind of algal control according to claim 1 denitrogenates particulate vector, it is characterised in that catalyst M is palladium catalyst
The combination of powder, catalyst manganese powder, catalyst titanium valve, catalyst copper powder, one kind in catalyst magnesium powder or its arbitrary catalyst.
3. the preparation method that phosphorus denitrogenates particulate vector is consolidated in a kind of algal control, it is characterised in that contains following steps；
Step 1: by composition and proportioning feeding mixing；
Composition and weight proportion are：20~45 parts of iron powder, 10~25 parts of active carbon powder, 1~5 part of catalyst M, poly- second
0.2~2 part of enol, 10~18 parts of portland-pozzolana, 0.5~5 part of fruit peel, 0.5~5 part of grain husk, biomass 0.5~
5 parts；
Step 2: plus water hydraulic produce the particle of 0.2~15mm；
Step 3: the particle of preparation is placed in 110 ± 2 DEG C of drying box, in H2Under the protection of/CO gas, dry 1~2h；
Step 4: finally particles are cooled to room temperatures.
4. the pollution waters restoration application method that phosphorus denitrogenates particulate vector is consolidated in a kind of algal control, it is characterised in that contains following steps；
By the algal control of preparation consolidate phosphorus denitrogenate particulate vector direct plunge into contaminated water body or be put into be positioned over again in container it is contaminated
Water body in, consolidate that phosphorus denitrogenates the continuous haptoreaction of particulate vector and algal control is consolidated phosphorus and denitrogenated by contaminated water body and algal control
The algal control that grain carrier constantly discharges in water consolidates phosphorus except the biomembrane on nitrogen and its surface acts on, and makes blue-green alge in water body complete
It is suppressed, and is killed, total phosphorus and total nitrogen are removed, and water body is made to be repaired and purified.
5. pollution waters restoration application method according to claim 4, it is characterised in that algal control consolidates phosphorus and denitrogenates particulate vector
Dosage is added according to the pollution level of polluted water body as 0.5~2.5kg/m in water body3。
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110937693A (en) * | 2019-12-09 | 2020-03-31 | 苏亮星 | Preparation method and application of bacterium-fixing sustained-release granules capable of efficiently removing nitrogen |
| CN113145118A (en) * | 2021-04-15 | 2021-07-23 | 北京京华清源环保科技有限公司 | Catalytic particle carrier for synchronously removing nitrogen, phosphorus and fluorine and preparation method thereof |
| CN113277605A (en) * | 2021-05-31 | 2021-08-20 | 杭州师范大学 | Modified biochar algistat and application and preparation method thereof |
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| CN104761024A (en) * | 2015-04-22 | 2015-07-08 | 湖北泉盛环保科技有限公司 | Efficient heterogeneous catalytic oxidation ferric-carbon micro-electrolysis packing and preparation method thereof |
| CN104920465A (en) * | 2015-06-23 | 2015-09-23 | 上海金布梯环保科技发展有限公司 | Algae growth inhibiting composition and preparation method and application thereof |
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| CN103145234A (en) * | 2013-03-22 | 2013-06-12 | 北京交通大学 | Aerobic bio-particle carrier for directly removing ammonia nitrogen from sewage with low carbon nitrogen ratio and preparation method thereof |
| CN104761024A (en) * | 2015-04-22 | 2015-07-08 | 湖北泉盛环保科技有限公司 | Efficient heterogeneous catalytic oxidation ferric-carbon micro-electrolysis packing and preparation method thereof |
| CN104920465A (en) * | 2015-06-23 | 2015-09-23 | 上海金布梯环保科技发展有限公司 | Algae growth inhibiting composition and preparation method and application thereof |
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110937693A (en) * | 2019-12-09 | 2020-03-31 | 苏亮星 | Preparation method and application of bacterium-fixing sustained-release granules capable of efficiently removing nitrogen |
| CN110937693B (en) * | 2019-12-09 | 2022-08-05 | 苏亮星 | Preparation method and application of bacterium-fixing sustained-release granules capable of efficiently removing nitrogen |
| CN113145118A (en) * | 2021-04-15 | 2021-07-23 | 北京京华清源环保科技有限公司 | Catalytic particle carrier for synchronously removing nitrogen, phosphorus and fluorine and preparation method thereof |
| CN113145118B (en) * | 2021-04-15 | 2023-04-28 | 北京京华清源环保科技有限公司 | Synchronous denitrification dephosphorization defluorination catalytic particle carrier and preparation method thereof |
| CN113277605A (en) * | 2021-05-31 | 2021-08-20 | 杭州师范大学 | Modified biochar algistat and application and preparation method thereof |
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Application publication date: 20180615 |