CN108158878B - 一种防脱发洗发水及其制备方法 - Google Patents

一种防脱发洗发水及其制备方法 Download PDF

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CN108158878B
CN108158878B CN201711425318.4A CN201711425318A CN108158878B CN 108158878 B CN108158878 B CN 108158878B CN 201711425318 A CN201711425318 A CN 201711425318A CN 108158878 B CN108158878 B CN 108158878B
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朱浩奇
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Hangzhou New Picture Biotechnology Co ltd
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Abstract

本发明公开了一种防脱发洗发水及其制备方法,该洗发水是由以下重量百分比的组分组成:香波基质70‑90%、中草药提取液10‑30%;香波基质由聚氧乙烯月桂醇醚硫酸钠、无患子皂苷、脂肪醇聚氧乙烯醚磷酸酯钾盐、鲸蜡硬脂基葡糖苷、椰油酰基谷氨酸三乙醇胺盐、椰油酸二乙醇酰胺、聚季铵盐‑7、阳离子瓜尔胶、双吡啶硫酮、甜菜碱水杨酸盐、水等原料制成;中草药提取液由红花、扶芳藤、蔷薇根、透骨草、柠条子、山核桃叶、梓白皮、旱莲草、侧柏叶、桑白皮、芝麻花等原料制成。本发明洗发水具有清洁去屑,杀螨止痒,护发固发,养发生发的特性,对于防止头发脱落和促进头发生长具有显著的效果,且不含酒精和硅油,安全可靠。

Description

一种防脱发洗发水及其制备方法
发明领域
本发明涉及一种洗发水及其制备方法,具体地说是涉及一种防脱发洗发水及其制备方法。
背景技术
头螨是一种寄生在头皮上的嗜脂性微小寄生虫,肉眼看不到,但头螨对头发的危害不容忽视。由于头螨喜欢吃头皮油脂,啃食发根为生,并且分泌解脂酵素,所以会侵蚀皮脂腺,阻塞毛囊生长,令毛囊萎缩,引起脱发或秃头,直到谢顶,预防头螨性脱发比治疗更重要。所以,在日常生活中要注意个人卫生,经常使用洗发水洗发,清除头皮油污垢,避免螨虫的滋生。但是现有市场上的洗发水含酒精或硅油,给头螨提供生长繁衍的机会。因此,需开发一种全新的不含酒精和硅油的防脱发洗发水。
发明内容
为解决上述技术问题,本发明的目的在于提供一种防脱发洗发水及其制备方法。本发明洗发水具有清洁去屑,杀螨止痒,护发固发,养发生发的特性,对于防止头发脱落和促进头发生长具有显著的效果,且不含酒精和硅油,安全可靠。
为实现上述目的,本发明所采取的技术方案为:
一种防脱发洗发水,该洗发水是由以下重量百分比的组分组成:香波基质 70-90%、中草药提取液10-30%;
所述香波基质由下列重量份的原料制成:聚氧乙烯月桂醇醚硫酸钠15-20份、无患子皂苷10-15份、脂肪醇聚氧乙烯醚磷酸酯钾盐10-15份、鲸蜡硬脂基葡糖苷5-10份、椰油酰基谷氨酸三乙醇胺盐8-14份、椰油酸二乙醇酰胺6-12、聚季铵盐-7 4-8份、阳离子瓜尔胶3-6份、双吡啶硫酮1-2份、甜菜碱水杨酸盐1-2份、水70-80份;
所述中草药提取液由下列重量份的原料制成:红花15-25份、扶芳藤10-20份、蔷薇根10-20份、透骨草10-20份、柠条子5-15份、山核桃叶5-15份、梓白皮10-20份、旱莲草 5-15份、侧柏叶5-15份、桑白皮10-20份、芝麻花10-20份。
一种防脱发洗发水的制备方法,包括以下步骤:
(1)香波基质的制备:
(1.1)取相当于总量1/3-1/4的水,水浴加热至50-60℃,在机械搅拌下依次加入无患子皂苷、鲸蜡硬脂基葡糖苷和阳离子瓜尔胶,搅拌至完全溶解,得混合料A;
(1.2)取余下的水,水浴加热至55-65℃,在机械搅拌下依次加入聚氧乙烯月桂醇醚硫酸钠、脂肪醇聚氧乙烯醚磷酸酯钾盐、椰油酰基谷氨酸三乙醇胺盐和聚季铵盐-7,搅拌至完全溶解,得混合料B;
(1.3)将混合料A加入混合料B中,在机械搅拌下依次加入椰油酸二乙醇酰胺、双吡啶硫酮和甜菜碱水杨酸盐,充分搅拌均匀,得香波基质;
(2)中草药提取液的制备:
(2.1)将红花、扶芳藤、蔷薇根、透骨草、柠条子、山核桃叶、梓白皮、旱莲草、侧柏叶、桑白皮、芝麻花混合均匀,粉碎,过60-80目筛后加入相当于药粉质量4-6倍的体积分数为80%的乙醇溶液,使药粉充分湿润膨胀后,分次均匀填装于渗漉筒内,加入体积分数为80%的乙醇溶液浸没药粉1-2cm,浸渍20-30min,缓慢渗漉,流速控制在2-3 mL/min,先收集相当于药粉重量70-80%的初漉液,另器保存,继续渗漉,待有效成分完全漉出,收集续漉液,将续漉液与初漉液混合,得到渗漉液,备用;
(2.2)将步骤(2.1)渗漉提取后的药渣加入相当于药渣质量8-10倍的体积分数为85%的乙醇溶液中,加热回流提取2次,每次提取2-3h,合并两次提取液,过滤,得到滤液,备用;
(2.3)将步骤(2.1)得到的渗漉液与步骤(2.2)得到的滤液混合,然后在搅拌下加体积分数为90%的乙醇溶液使混合液含醇量为55-60%,离心分离,取上清液,将沉淀加入相当于沉淀质量3-5倍量的体积分数为90%的乙醇溶液中,双频超声波交替处理20-30min,静置过夜,取上清液,将两次上清液合并,减压回收乙醇,浓缩至原来体积的2/4-3/4,得中草药提取液;
(3)洗发水的制备:
将香波基质和中草药提取液按照配方配比混合,水浴加热至50-55℃,磁力搅拌20-30min,待温度冷却至常温后取样检测,合格后灌装,包装,即得成品。
优选地,步骤(1.1)中所述机械搅拌的转速为400-500r/min。
优选地,步骤(1.2)中所述机械搅拌的转速为300-400r/min。
优选地,步骤(1.3)中所述机械搅拌的转速为500-600r/min。
优选地,步骤(2.3)中所述离心分离的条件为:离心转速为4000-5000r/min,离心时间为15-25min。
优选地,步骤(2.3)中所述双频超声波交替处理的条件为:双频超声波交替频率为30-50KHz/80-100KHz,双频超声波交替工作时间为5-10s,超声波功率为150-300W。
优选地,步骤(3)中所述磁力搅拌的条件为:功率为200-300W,转速为300-400r/min。
本发明中草药提取液中各中草药的药理如下:
红花:味辛,性温,具有活血通经,散瘀止痛之功效,
扶芳藤:为卫矛科植物扶芳藤的带叶茎枝,具有舒筋活络、止血消瘀、行气活血的功效;
蔷薇根:为蔷薇科蔷薇属植物野蔷薇的根,具有清热解毒、祛风除湿、活血调经的功效;
透骨草:味辛,性温,具有祛风除湿、舒筋活血、散瘀消肿、解毒止痛之功效;
上述红花、扶芳藤、蔷薇根、透骨草之间相互协同作用,能够起到行气活血、通窍生发的功效,扩张毛细血管,减少头皮毛细血管脂肪粘附,软化血管,增加头皮血液流动和供血,促进表皮代谢,使毛囊毛基质的代谢废物能够迅速穿过毛细血管进入血液代谢出体外,改善毛囊状态,促进头发生长;
柠条子:为豆科植物中间锦鸡儿的种子,味苦,性平,具有燥湿解毒,杀虫止痒之功效;
山核桃叶:味苦、涩,性凉;具有清热解毒、杀虫止痒的功效
梓白皮:为紫葳科植物梓的根皮或树皮的韧皮部,味苦,性寒,具有清热利湿、降逆止吐、杀虫止痒之功效;
上述柠条子、山核桃叶、梓白皮之间相互协同作用,能够起到杀螨止痒的作用,有效防止头发中螨虫的滋生与繁殖,可以有效预防头螨性脱发。
旱莲草:味甘酸,性凉,有凉血、止血、消肿、强壮之功效,据《唐本草》、《本草纲目》及《滇南本草》等记载:旱莲草“乌须发,益肾阴”,“固齿、乌须”,“汁涂发霉,生速而繁”;
侧柏叶:味苦、涩,性寒,具有凉血止血、化痰止咳、生发乌发的功效;《本草纲目》中记载其“烧取汁涂头,黑润鬓发”,用侧柏叶治疗脱发首见于唐代《千金要方》之鬓发堕落令生长方法;
桑白皮:味甘、辛,性寒,内服能泻肺平喘、利水消肿,外用可治“发鬓堕落,发槁不泽”,因此古人说它,“煮汁染褐色,久不落”;
芝麻花:味甘,性平,有生发,消肿的作用,对于治疗脱发有显著的效果;
上述旱莲草、侧柏叶、桑白皮、芝麻花之间相互协同作用,具有固发养发,生发护发的作用,对于防止脱发、促进头发生长有很好的效果。
本发明的有益效果:
本发明洗发水采用香波基质和中草药提取液相互复合制得而成,其中香波基质采用聚氧乙烯月桂醇醚硫酸钠、无患子皂苷、脂肪醇聚氧乙烯醚磷酸酯钾盐、鲸蜡硬脂基葡糖苷、椰油酰基谷氨酸三乙醇胺盐、椰油酸二乙醇酰胺等原料相互协同作用,具有亲肤能力好,渗透力强,去屑止痒效果好,去油脂清洁效果好等优点;中草药提取液采用红花、扶芳藤、蔷薇根、透骨草、柠条子、山核桃叶、梓白皮、旱莲草、侧柏叶等原料配伍,具有营养和疗效双重作用,能够增加头皮、头发和毛囊对营养的吸收,表现出较好的固发护发、养发生发的作用,还具有杀螨止痒、活血行气、通窍生发的功效,可以刺激毛囊生长,能活化头皮细胞,并加强头皮血液循环,对于抑制螨虫滋生、防止脱发、促进头发生长具有很好的效果,且本发明洗发水不含酒精和硅油,安全可靠。
(2)本发明中草药提取液制备过程中,先采用渗漉法提取,滤渣再采用乙醇回流提取法提取,这样处理可以显著提高有效成分的提取率,两次提取液合并后加入乙醇溶液先进行离心分离,沉淀再加入乙醇溶液双频超声波交替处理后进行醇沉,这样可以显著提高有效成分的纯度,从而保证中草药提取液的药效。
具体实施方式
下面结合具体实施例对本发明所述技术方案作进一步的说明。
实施例1:
一种防脱发洗发水,该洗发水是由以下重量百分比的组分组成:香波基质 70%、中草药提取液30%;
所述香波基质由下列重量份的原料制成:聚氧乙烯月桂醇醚硫酸钠15份、无患子皂苷10份、脂肪醇聚氧乙烯醚磷酸酯钾盐10份、鲸蜡硬脂基葡糖苷5份、椰油酰基谷氨酸三乙醇胺盐8份、椰油酸二乙醇酰胺6、聚季铵盐-7 4份、阳离子瓜尔胶3份、双吡啶硫酮1份、甜菜碱水杨酸盐1份、水70份;
所述中草药提取液由下列重量份的原料制成:红花15份、扶芳藤10份、蔷薇根10份、透骨草10份、柠条子5份、山核桃叶5份、梓白皮10份、旱莲草 5份、侧柏叶5份、桑白皮10份、芝麻花10份。
一种防脱发洗发水的制备方法,包括以下步骤:
(1)香波基质的制备:
(1.1)取相当于总量1/4的水,水浴加热至50℃,在转速为400r/min的机械搅拌下依次加入无患子皂苷、鲸蜡硬脂基葡糖苷和阳离子瓜尔胶,搅拌至完全溶解,得混合料A;
(1.2)取余下的水,水浴加热至55℃,在转速为300r/min的机械搅拌下依次加入聚氧乙烯月桂醇醚硫酸钠、脂肪醇聚氧乙烯醚磷酸酯钾盐、椰油酰基谷氨酸三乙醇胺盐和聚季铵盐-7,搅拌至完全溶解,得混合料B;
(1.3)将混合料A加入混合料B中,在转速为500r/min的机械搅拌下依次加入椰油酸二乙醇酰胺、双吡啶硫酮和甜菜碱水杨酸盐,充分搅拌均匀,得香波基质;
(2)中草药提取液的制备:
(2.1)将红花、扶芳藤、蔷薇根、透骨草、柠条子、山核桃叶、梓白皮、旱莲草、侧柏叶、桑白皮、芝麻花混合均匀,粉碎,过60目筛后加入相当于药粉质量4倍的体积分数为80%的乙醇溶液,使药粉充分湿润膨胀后,分次均匀填装于渗漉筒内,加入体积分数为80%的乙醇溶液浸没药粉1cm,浸渍20min,缓慢渗漉,流速控制在2mL/min,先收集相当于药粉重量70%的初漉液,另器保存,继续渗漉,待有效成分完全漉出,收集续漉液,将续漉液与初漉液混合,得到渗漉液,备用;
(2.2)将步骤(2.1)渗漉提取后的药渣加入相当于药渣质量8倍的体积分数为85%的乙醇溶液中,加热回流提取2次,每次提取2h,合并两次提取液,过滤,得到滤液,备用;
(2.3)将步骤(2.1)得到的渗漉液与步骤(2.2)得到的滤液混合,然后在搅拌下加体积分数为90%的乙醇溶液使混合液含醇量为55%,在转速为5000r/min的条件下离心分离15min,取上清液,将沉淀加入相当于沉淀质量3倍量的体积分数为90%的乙醇溶液中,在双频超声波交替频率为50KHz/100KHz,双频超声波交替工作时间为10s,超声波功率为300W的条件下双频超声波交替处理20min,静置过夜,取上清液,将两次上清液合并,减压回收乙醇,浓缩至原来体积的2/4,得中草药提取液;
(3)洗发水的制备:
将香波基质和中草药提取液按照配方配比混合,水浴加热至50℃,在功率为300W,转速为400r/min的条件下磁力搅拌20min,待温度冷却至常温后取样检测,合格后灌装,包装,即得成品。
实施例2:
一种防脱发洗发水,该洗发水是由以下重量百分比的组分组成:香波基质80%、中草药提取液20%;
所述香波基质由下列重量份的原料制成:聚氧乙烯月桂醇醚硫酸钠18份、无患子皂苷12份、脂肪醇聚氧乙烯醚磷酸酯钾盐12份、鲸蜡硬脂基葡糖苷8份、椰油酰基谷氨酸三乙醇胺盐11份、椰油酸二乙醇酰胺9、聚季铵盐-7 6份、阳离子瓜尔胶4.5份、双吡啶硫酮1.5份、甜菜碱水杨酸盐1.5份、水75份;
所述中草药提取液由下列重量份的原料制成:红花20份、扶芳藤15份、蔷薇根15份、透骨草15份、柠条子10份、山核桃叶10份、梓白皮15份、旱莲草 10份、侧柏叶10份、桑白皮15份、芝麻花15份。
一种防脱发洗发水的制备方法,包括以下步骤:
(1)香波基质的制备:
(1.1)取相当于总量1/3的水,水浴加热至55℃,在转速为450r/min的机械搅拌下依次加入无患子皂苷、鲸蜡硬脂基葡糖苷和阳离子瓜尔胶,搅拌至完全溶解,得混合料A;
(1.2)取余下的水,水浴加热至60℃,在转速为350r/min的机械搅拌下依次加入聚氧乙烯月桂醇醚硫酸钠、脂肪醇聚氧乙烯醚磷酸酯钾盐、椰油酰基谷氨酸三乙醇胺盐和聚季铵盐-7,搅拌至完全溶解,得混合料B;
(1.3)将混合料A加入混合料B中,在转速为550r/min的机械搅拌下依次加入椰油酸二乙醇酰胺、双吡啶硫酮和甜菜碱水杨酸盐,充分搅拌均匀,得香波基质;
(2)中草药提取液的制备:
(2.1)将红花、扶芳藤、蔷薇根、透骨草、柠条子、山核桃叶、梓白皮、旱莲草、侧柏叶、桑白皮、芝麻花混合均匀,粉碎,过70目筛后加入相当于药粉质量5倍的体积分数为80%的乙醇溶液,使药粉充分湿润膨胀后,分次均匀填装于渗漉筒内,加入体积分数为80%的乙醇溶液浸没药粉1.5cm,浸渍25min,缓慢渗漉,流速控制在2.5 mL/min,先收集相当于药粉重量75%的初漉液,另器保存,继续渗漉,待有效成分完全漉出,收集续漉液,将续漉液与初漉液混合,得到渗漉液,备用;
(2.2)将步骤(2.1)渗漉提取后的药渣加入相当于药渣质量9倍的体积分数为85%的乙醇溶液中,加热回流提取2次,每次提取2.5h,合并两次提取液,过滤,得到滤液,备用;
(2.3)将步骤(2.1)得到的渗漉液与步骤(2.2)得到的滤液混合,然后在搅拌下加体积分数为90%的乙醇溶液使混合液含醇量为58%,在转速为4500r/min的条件下离心分离20min,取上清液,将沉淀加入相当于沉淀质量4倍量的体积分数为90%的乙醇溶液中,在双频超声波交替频率为40KHz/90KHz,双频超声波交替工作时间为8s,超声波功率为250W的条件下双频超声波交替处理25min,静置过夜,取上清液,将两次上清液合并,减压回收乙醇,浓缩至原来体积的3/4,得中草药提取液;
(3)洗发水的制备:
将香波基质和中草药提取液按照配方配比混合,水浴加热至52℃,在功率为250W,转速为350r/min的条件下磁力搅拌25min,待温度冷却至常温后取样检测,合格后灌装,包装,即得成品。
实施例3:
一种防脱发洗发水,该洗发水是由以下重量百分比的组分组成:香波基质 90%、中草药提取液10%;
所述香波基质由下列重量份的原料制成:聚氧乙烯月桂醇醚硫酸钠20份、无患子皂苷15份、脂肪醇聚氧乙烯醚磷酸酯钾盐15份、鲸蜡硬脂基葡糖苷10份、椰油酰基谷氨酸三乙醇胺盐14份、椰油酸二乙醇酰胺12、聚季铵盐-7 8份、阳离子瓜尔胶6份、双吡啶硫酮2份、甜菜碱水杨酸盐2份、水80份;
所述中草药提取液由下列重量份的原料制成:红花25份、扶芳藤20份、蔷薇根20份、透骨草20份、柠条子15份、山核桃叶15份、梓白皮20份、旱莲草 15份、侧柏叶15份、桑白皮20份、芝麻花20份。
一种防脱发洗发水的制备方法,包括以下步骤:
(1)香波基质的制备:
(1.1)取相当于总量1/3的水,水浴加热至60℃,在转速为500r/min的机械搅拌下依次加入无患子皂苷、鲸蜡硬脂基葡糖苷和阳离子瓜尔胶,搅拌至完全溶解,得混合料A;
(1.2)取余下的水,水浴加热至65℃,在转速为400r/min的机械搅拌下依次加入聚氧乙烯月桂醇醚硫酸钠、脂肪醇聚氧乙烯醚磷酸酯钾盐、椰油酰基谷氨酸三乙醇胺盐和聚季铵盐-7,搅拌至完全溶解,得混合料B;
(1.3)将混合料A加入混合料B中,在转速为600r/min的机械搅拌下依次加入椰油酸二乙醇酰胺、双吡啶硫酮和甜菜碱水杨酸盐,充分搅拌均匀,得香波基质;
(2)中草药提取液的制备:
(2.1)将红花、扶芳藤、蔷薇根、透骨草、柠条子、山核桃叶、梓白皮、旱莲草、侧柏叶、桑白皮、芝麻花混合均匀,粉碎,过80目筛后加入相当于药粉质量6倍的体积分数为80%的乙醇溶液,使药粉充分湿润膨胀后,分次均匀填装于渗漉筒内,加入体积分数为80%的乙醇溶液浸没药粉2cm,浸渍30min,缓慢渗漉,流速控制在3 mL/min,先收集相当于药粉重量80%的初漉液,另器保存,继续渗漉,待有效成分完全漉出,收集续漉液,将续漉液与初漉液混合,得到渗漉液,备用;
(2.2)将步骤(2.1)渗漉提取后的药渣加入相当于药渣质量10倍的体积分数为85%的乙醇溶液中,加热回流提取2次,每次提取3h,合并两次提取液,过滤,得到滤液,备用;
(2.3)将步骤(2.1)得到的渗漉液与步骤(2.2)得到的滤液混合,然后在搅拌下加体积分数为90%的乙醇溶液使混合液含醇量为60%,在转速为4000r/min的条件下离心分离25min,取上清液,将沉淀加入相当于沉淀质量5倍量的体积分数为90%的乙醇溶液中,在双频超声波交替频率为30KHz/80KHz,双频超声波交替工作时间为5s,超声波功率为150W的条件下双频超声波交替处理30min,静置过夜,取上清液,将两次上清液合并,减压回收乙醇,浓缩至原来体积的3/4,得中草药提取液;
(3)洗发水的制备:
将香波基质和中草药提取液按照配方配比混合,水浴加热至55℃,在功率为200W,转速为300r/min的条件下磁力搅拌30min,待温度冷却至常温后取样检测,合格后灌装,包装,即得成品。
以上所述仅为本发明的优选实施例而已,并不用于限制本发明,对于本领域的技术人员来说,本发明可以有各种更改和变化。凡在本发明的精神和原则之内,所作的任何修改、等同替换、改进等,均应包含在本发明的保护范围之内。

Claims (7)

1.一种防脱发洗发水,其特征在于,该洗发水是由以下重量百分比的组分组成:香波基质70-90%、中草药提取液10-30%;
所述香波基质由下列重量份的原料制成:聚氧乙烯月桂醇醚硫酸钠15-20份、无患子皂苷10-15份、脂肪醇聚氧乙烯醚磷酸酯钾盐10-15份、鲸蜡硬脂基葡糖苷5-10份、椰油酰基谷氨酸三乙醇胺盐8-14份、椰油酸二乙醇酰胺6-12、聚季铵盐-74-8份、阳离子瓜尔胶3-6份、双吡啶硫酮1-2份、甜菜碱水杨酸盐1-2份、水70-80份;
所述中草药提取液由下列重量份的原料制成:红花15-25份、扶芳藤10-20份、蔷薇根10-20份、透骨草10-20份、柠条子5-15份、山核桃叶5-15份、梓白皮10-20份、旱莲草5-15份、侧柏叶5-15份、桑白皮10-20份、芝麻花10-20份;
所述的防脱发洗发水的制备方法,包括以下步骤:
(1)香波基质的制备:
(1.1)取相当于总量1/3-1/4的水,水浴加热至50-60℃,在机械搅拌下依次加入无患子皂苷、鲸蜡硬脂基葡糖苷和阳离子瓜尔胶,搅拌至完全溶解,得混合料A;
(1.2)取余下的水,水浴加热至55-65℃,在机械搅拌下依次加入聚氧乙烯月桂醇醚硫酸钠、脂肪醇聚氧乙烯醚磷酸酯钾盐、椰油酰基谷氨酸三乙醇胺盐和聚季铵盐-7,搅拌至完全溶解,得混合料B;
(1.3)将混合料A加入混合料B中,在机械搅拌下依次加入椰油酸二乙醇酰胺、双吡啶硫酮和甜菜碱水杨酸盐,充分搅拌均匀,得香波基质;
(2)中草药提取液的制备:
(2.1)将红花、扶芳藤、蔷薇根、透骨草、柠条子、山核桃叶、梓白皮、旱莲草、侧柏叶、桑白皮、芝麻花混合均匀,粉碎,过60-80目筛后加入相当于药粉质量4-6倍的体积分数为80%的乙醇溶液,使药粉充分湿润膨胀后,分次均匀填装于渗漉筒内,加入体积分数为80%的乙醇溶液浸没药粉1-2cm,浸渍20-30min,缓慢渗漉,流速控制在2-3mL/min,先收集相当于药粉重量70-80%的初漉液,另器保存,继续渗漉,待有效成分完全漉出,收集续漉液,将续漉液与初漉液混合,得到渗漉液,备用;
(2.2)将步骤(2.1)渗漉提取后的药渣加入相当于药渣质量8-10倍的体积分数为85%的乙醇溶液中,加热回流提取2次,每次提取2-3h,合并两次提取液,过滤,得到滤液,备用;
(2.3)将步骤(2.1)得到的渗漉液与步骤(2.2)得到的滤液混合,然后在搅拌下加体积分数为90%的乙醇溶液使混合液含醇量为55-60%,离心分离,取上清液,将沉淀加入相当于沉淀质量3-5倍量的体积分数为90%的乙醇溶液中,双频超声波交替处理20-30min,静置过夜,取上清液,将两次上清液合并,减压回收乙醇,浓缩至原来体积的2/4-3/4,得中草药提取液;
(3) 洗发水的制备:
将香波基质和中草药提取液按照配方配比混合,水浴加热至50-55℃,磁力搅拌20-30min,待温度冷却至常温后取样检测,合格后灌装,包装,即得成品。
2.根据权利要求1所述的防脱发洗发水,其特征在于,步骤(1.1)中所述机械搅拌的转速为400-500r/min。
3.根据权利要求1所述的防脱发洗发水,其特征在于,步骤(1.2)中所述机械搅拌的转速为300-400r/min。
4.根据权利要求1所述的防脱发洗发水,其特征在于,步骤(1.3)中所述机械搅拌的转速为500-600r/min。
5.根据权利要求1所述的防脱发洗发水,其特征在于,步骤(2.3)中所述离心分离的条件为:离心转速为4000-5000r/min,离心时间为15-25min。
6.根据权利要求1所述的防脱发洗发水,其特征在于,步骤(2.3)中所述双频超声波交替处理的条件为:双频超声波交替频率为30-50KHz/80-100KHz,双频超声波交替工作时间为5-10s,超声波功率为150-300W。
7.根据权利要求1所述的防脱发洗发水,其特征在于,步骤(3)中所述磁力搅拌的条件为:功率为200-300W,转速为300-400r/min。
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