CN108158834A - A kind of preparation method of salt for foot bath, shower and dissipation - Google Patents

A kind of preparation method of salt for foot bath, shower and dissipation Download PDF

Info

Publication number
CN108158834A
CN108158834A CN201810179619.1A CN201810179619A CN108158834A CN 108158834 A CN108158834 A CN 108158834A CN 201810179619 A CN201810179619 A CN 201810179619A CN 108158834 A CN108158834 A CN 108158834A
Authority
CN
China
Prior art keywords
salt
nacl
shower
dissipation
preparation
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201810179619.1A
Other languages
Chinese (zh)
Inventor
张继森
徐增山
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Jilin Light Salt Melting Biological Technology Co Ltd
Original Assignee
Jilin Light Salt Melting Biological Technology Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Jilin Light Salt Melting Biological Technology Co Ltd filed Critical Jilin Light Salt Melting Biological Technology Co Ltd
Priority to CN201810179619.1A priority Critical patent/CN108158834A/en
Publication of CN108158834A publication Critical patent/CN108158834A/en
Pending legal-status Critical Current

Links

Classifications

    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
    • A61K8/20—Halogens; Compounds thereof
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q11/00—Preparations for care of the teeth, of the oral cavity or of dentures; Dentifrices, e.g. toothpastes; Mouth rinses
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q17/00—Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
    • A61Q17/005—Antimicrobial preparations
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00—Preparations for care of the skin
    • A61Q19/10—Washing or bathing preparations
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D9/00—Compositions of detergents based essentially on soap
    • C11D9/04—Compositions of detergents based essentially on soap containing compounding ingredients other than soaps
    • C11D9/06—Inorganic compounds
    • C11D9/08—Water-soluble compounds
    • C11D9/10—Salts

Landscapes

  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Chemical & Material Sciences (AREA)
  • Animal Behavior & Ethology (AREA)
  • General Health & Medical Sciences (AREA)
  • Public Health (AREA)
  • Veterinary Medicine (AREA)
  • Inorganic Chemistry (AREA)
  • Dermatology (AREA)
  • Oral & Maxillofacial Surgery (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Wood Science & Technology (AREA)
  • Organic Chemistry (AREA)
  • Birds (AREA)
  • Epidemiology (AREA)
  • Cosmetics (AREA)

Abstract

The present invention relates to a kind of preparation methods of the salt for foot bath, shower and dissipation, party's genealogy of law utilizes high-purity caustic alkali, such as KOH, to fusion method, high-purity salt carries out calcining modification at high temperature, has prepared a kind of with biological affinity and optically active NaCl [(K+,O2‑):(F2 +)AH] salt crystalline flour end, NaCl [(K of the present invention+,O2‑):(F2 +)AH] salt crystalline substance powder-product preparation method do not have " three wastes " discharge, equipment is simple and energy consumption is low and efficient, which can stablize storage in normal temperature environment, it is contemplated that the product salt can be in foot bath, shower and dissipation（It such as gargles, wash eye）And the fields such as salt soap and toothpaste preparation are with a wide range of applications.

Description

A kind of preparation method of salt for foot bath, shower and dissipation
Technical field
The invention belongs to melt the application production field of high purity N aCl product salt materials, it is used for more particularly to one kind The preparation method of the salt of foot bath, shower and dissipation, the product salt can be widely applied for foot bath, shower and dissipation and salt soap and The daily chemical products manufacturing field such as toothpaste.
Background technology
People just have been found that those salt for being derived from the making of seawater Gu method have more body than purified salt a long time ago Benefit.It is inspired by this, the salt for being derived from deep-sea is most already refined into maintenance of the bath salt for skin by Greek.Even to this day, Beautiful bath salt in beauty has deduced various culture of taking a shower：It adds in the bath salt of hot spring mineralogical composition, add in the bath of champignon essence oil Salt, the bath salt ... for adding in plant granule, throughout each corner of people's life.People have been accustomed to being washed with various salt Face, foot bath and shower to promote the soft and smooth exquisiteness of skin, boost metabolism, anti-inflammatory, sterilization, rapid healing minor cut or wound, dispel it is more Excess oil fat and cuticula repair rough epidermis and restrain coarse pore.The level of consumption of health-care salt has become weighing apparatus Measure one of scale of countries in the world standard of living height.Nowadays, it is not only a kind of fashion to eat salt less and be mostly used salt, even more a kind of text Change, and have changed into the theory that people keep fit.
Research in the processed NaCl crystal of special process technology it has been shown that by that can generate a large amount of defect center： One anion vacancy captures an electronics and is known as F colour centers, is known as F there are one cation impurity beside F colour centersAColour center; Two adjacent anion vacancies capture an electronics and are known as F2 +Colour center；F2 +It is known as (F there are one anionic impurity beside colour center2 + ) HColour center;In (F2 +) HIt is known as (F there are one cation impurity beside colour center2 +)AHOr (F2 + ) HAColour center.
Invention content
The object of the present invention is to provide a kind of preparation method of the salt for foot bath, shower and dissipation, party's genealogy of law utilizes High-purity caustic alkali, such as KOH, to fusion method, high-purity salt carries out calcining modification at high temperature, has prepared a kind of affine with biology Power and optically active NaCl [(K+, O2-):(F2 +)AH] salt crystalline flour end.
A kind of salt for foot bath, shower and dissipation --- NaCl [(K+, O2-):(F2 +)AH] salt crystalline flour end preparation side Method, this method include the following steps：
1., weigh the melting salt powder of 60 mesh of 3g KOH and 10 kg, be put into quartz-ceramics vessel and be placed into after mixing In electric furnace；In 30 minutes, 1000 are heated to from room temperature0C, then Temperature fall to 8000C；Again in 20 minutes from 800 0C is warming up to 10000C, then Temperature fall is to room temperature, you can obtain NaCl (K+, OH-) salt crystalline substance.
2., the NaCl (K that 1. obtain step+,OH-) salt crystalline substance is put into quartz-ceramics vessel, is placed in electric furnace, in CO gas In atmosphere 800 are heated in 20 minutes0C and calcining at constant temperature 4~6 hours, take out after Temperature fall to room temperature, you can obtain NaCl [(K+, O2-):(F2 +)AH] salt crystalline substance；Finally by NaCl [(K+, O2-):(F2 +)AH] salt crystalline substance grind into powder, it is moulded after crossing 60 mesh screens Material bag is packaged and stored in drying and is protected from light place.
The present invention has the advantages that：
1st, NaCl [(K of the present invention+, O2-):(F2 +)AH] salt crystalline substance powder-product preparation method do not have " three wastes " discharge, equipment letter List and energy consumption are low and efficient, which can stablize storage in normal temperature environment, it is contemplated that the product salt can bathe Foot, shower and dissipation（It such as gargles, wash eye）And the fields such as salt soap and toothpaste preparation are with a wide range of applications.
2nd, NaCl [(K of the present invention+, O2-):(F2 +)AH] salt crystalline substance by adulterate OH-Ion is introduced into NaCl lattices, then Cause OH by means of high-temperature calcination and protection of reducing atmosphere-Dehydration is converted to O2-, so as to promote stable (F2 +)AHDefect is formed.
3rd, salt crystalline flour end of the present invention can emit visible ray, provable NaCl [(K under near ultraviolet excitation+, O2-): (F2 +)AH] fault of construction stability（As shown in Figure 1）.
4th, salt crystalline flour end hygroscopicity of the present invention declines so that the 60 purposes salt powder can for a long time be stablized in normal temperature environment In the presence of.
5th, by O in salt crystalline substance powder preparing processes of the present invention2- It is introduced into lattice, 0.9~10% salt crystalline substance powder aqueous solution pH Value stabilization shows the alkalescent identical with the skin of people between 7.4~9, the salting liquid is caused to keep traditional dissipation work( The affinity to organism can be also added outside.It is known that object cell line is made of protein, therefore cell surface contains ammonia Base（——NH2）And carbonyl（——C=O）.Again since the salt contains O2-Ion, therefore OH can be generated when being dissolved in water-Ion, And OH-Ion can be with --- NH2And --- C=O forms hydrogen bond；In addition K+Keratoprotein is enabled to soften, therefore when life After object is impregnated using the salting liquid, in organism skin surface, the water conservation of one layer of Subnano-class absorption is formed as shown in Figure 2 Layer.Due to the OH in the protective film of this layer " fine and close salt deposit "-And K+Collective effect function so that the salt than commonsense method prepare Salt moisturizing and dissipation performance it is more preferable, more longlasting；After the aqueous solution containing the salt is used to take a shower, people can be allowed to feel pleasant satisfied Meaning；Long-time service can sterilize and skin surface softness can be made fine and smooth.
6th, salt crystalline flour end dissipation of the present invention and moisture-keeping functions are the maximum features of novelty salt crystalline substance, this assigns the salt crystalline substance and possesses It is widely applied value：8~10% salting liquid is cracked to heel, foot odour and some skin diseases all have well more Cooperation is used；0.9% or so the solution understands that the peculiar smell in oral cavity is made to the moistening protection at canthus, nasal cavity and as mouthwash With apparent；The bath soap moisture retention processed with the salt is apparent, with rear skin refreshing；Tooth paste product cleans the teeth makes us very full with comfort Meaning.
Description of the drawings
Fig. 1 is present invention NaCl [(K under 340 nm near ultraviolet excitations+, O2-):(F2 +)AH] salt powder luminous light Spectrogram.
Fig. 2 is that the present invention is applied to skin surface absorption " salt deposit " signal in foot bath, shower and dissipation and salt soap product Figure.
Specific embodiment
A kind of salt for foot bath, shower and dissipation --- NaCl [(K+, O2-):(F2 +)AH] salt crystalline flour end preparation side Method, this method include the following steps：
1., weigh the melting salt powder of 60 mesh of 3g KOH and 10 kg, be put into quartz-ceramics vessel and be placed into after mixing In electric furnace；In 30 minutes, 1000 are heated to from room temperature0C, then Temperature fall to 8000C；Again in 20 minutes from 800 0C is warming up to 10000C, then Temperature fall is to room temperature, you can obtain NaCl (K+, OH-) salt crystalline substance.
2., the NaCl (K that 1. obtain step+,OH-) salt crystalline substance is put into quartz-ceramics vessel, is placed in electric furnace, in CO gas In atmosphere 800 are heated in 20 minutes0C and calcining at constant temperature 4~6 hours, take out after Temperature fall to room temperature, you can obtain NaCl [(K+, O2-):(F2 +)AH] salt crystalline substance；Finally by NaCl [(K+, O2-):(F2 +)AH] salt crystalline substance grind into powder, it is moulded after crossing 60 mesh screens Material bag is packaged and stored in drying and is protected from light place.
Step 1. described in fuse salt powder raw material system derive from a kind of melting recrystallization method prepare high purity salt（> 99.9%）, referring to ZL 201710160188, prepared by the product in X patents.
As shown in attached drawing 1：Pass through NaCl [(K under 340 nm near ultraviolet excitations+, O2-):(F2 +)AH] salt powder shine Spectrogram can be seen that：In NaCl [(K+, O2-):(F2 +)AH] crystal energy gap in have existed defect level.These defect energy Grade is so that salt crystalline substance oxidation -- reduction potential declines.This is that the salt crystalline substance has photochemically reactive important evidence.
Application Example
1st, the configuration of foot bath salting liquid：10 kg water are taken, add in 1kg NaCl [(K+, O2-):(F2 +)AH] the existing foot bath solution of salt.
2nd, bath salt solution allocation：100 kg water are taken, add in 0.8 kg NaCl [(K+, O2-):(F2 +)AH] the existing bath salt of salt Solution.
As shown in attached drawing 2：By by NaCl [(K+, O2-):(F2 +)AH] salt crystalline flour end be applied to foot bath, shower and dissipation And skin surface absorption " salt deposit " schematic diagram can be seen that in salt soap product：The salt crystalline substance can form one layer of cause in skin surface Close water-retaining property " film of salt ", this for keeping skin surface iuntercellular humidity, harmful bacteria activity being inhibited to play for a long time Key effect.

Claims (1)

1. a kind of preparation method of salt for foot bath, shower and dissipation, it is characterised in that：The salt refers to NaCl [(K+, O2-): (F2 +)AH] salt crystalline flour end, preparation method includes the following steps：
1., weigh the melting salt powder of 60 mesh of 3g KOH and 10 kg, be put into quartz-ceramics vessel and be placed into after mixing In electric furnace；In 30 minutes, 1000 are heated to from room temperature0C, then Temperature fall to 8000C；Again in 20 minutes from 800 0C is warming up to 10000C, then Temperature fall obtain NaCl (K to room temperature+, OH-) salt crystalline substance；
2., the NaCl (K that 1. obtain step+,OH-) salt crystalline substance is put into quartz-ceramics vessel, is placed in electric furnace, in CO atmosphere 800 are heated in 20 minutes0C and calcining at constant temperature 4~6 hours, take out after Temperature fall to room temperature, you can obtain NaCl [(K+, O2-):(F2 +)AH] salt crystalline substance；Finally by NaCl [(K+, O2-):(F2 +)AH] salt crystalline substance grind into powder, cross polybag after 60 mesh screens It is packaged and stored in drying and is protected from light place.
CN201810179619.1A 2018-03-05 2018-03-05 A kind of preparation method of salt for foot bath, shower and dissipation Pending CN108158834A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201810179619.1A CN108158834A (en) 2018-03-05 2018-03-05 A kind of preparation method of salt for foot bath, shower and dissipation

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201810179619.1A CN108158834A (en) 2018-03-05 2018-03-05 A kind of preparation method of salt for foot bath, shower and dissipation

Publications (1)

Publication Number Publication Date
CN108158834A true CN108158834A (en) 2018-06-15

Family

ID=62511447

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201810179619.1A Pending CN108158834A (en) 2018-03-05 2018-03-05 A kind of preparation method of salt for foot bath, shower and dissipation

Country Status (1)

Country Link
CN (1) CN108158834A (en)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110713196A (en) * 2019-12-05 2020-01-21 吉林省光盐健道健康管理集团有限公司 Preparation of low-sodium NaCl K by using melt recrystallization technology+Method for preparing salt

Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4386936A (en) * 1979-02-01 1983-06-07 Ppg Industries Canada Ltd. Production of potassium chloride using pond crystallization
CN101575104A (en) * 2008-05-08 2009-11-11 闫涛 Salt crystal processing technology and product

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4386936A (en) * 1979-02-01 1983-06-07 Ppg Industries Canada Ltd. Production of potassium chloride using pond crystallization
CN101575104A (en) * 2008-05-08 2009-11-11 闫涛 Salt crystal processing technology and product

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
李宝让: "《纳米熔盐合成技术》", 30 September 2014 *

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110713196A (en) * 2019-12-05 2020-01-21 吉林省光盐健道健康管理集团有限公司 Preparation of low-sodium NaCl K by using melt recrystallization technology+Method for preparing salt
CN110713196B (en) * 2019-12-05 2021-12-31 吉林省光盐健道健康管理集团有限公司 Preparation of low-sodium NaCl K by using melt recrystallization technology+Method for preparing salt

Similar Documents

Publication Publication Date Title
CN107032615B (en) Biological ceramic glaze with good biocompatibility and bioactivity and production method thereof
CN101199469B (en) Process for preparing lava pearl beauty mask
CN101085906A (en) Multifunctional far infrared negative ions material and preparing method thereof
US20170275196A1 (en) Porous and non-porous bodies
CN102550752A (en) Health-care florists chrysanthemum tea
CN103504049A (en) Soothing tea
CN108158834A (en) A kind of preparation method of salt for foot bath, shower and dissipation
CN101684042B (en) Nano-selenium ceramic ball, preparation method and application thereof
CN105476934A (en) Mask of which deionized water solvent is replaced with peony hydrosol and preparation method of mask
KR20060108282A (en) Method of producting of the facial cream preparing biovital-water using material radiating far 0infared and mineral
CN106266585A (en) A kind of Chinese medicine treating oral disease and preparation method thereof
CN102631581B (en) Medicament for treating agrypnia and production method thereof
CN102451390A (en) Traditional Chinese medicine formula for treating insomnia
CN108503354A (en) Function bionics compound bio piezoceramic material
CN103431259A (en) Rana japonica oil oral liquid
CN107660928A (en) A kind of mattress and its production technology with healthcare function
CN102972564A (en) Cherokee rose fruit night sweat-relieving health-care tea
CN102335109A (en) Floristic sterilizing and mite removing facial cleanser
CN105919365B (en) A kind of ventilative cotton-wadded quilt for improving sleep quality
CN104224663A (en) Whitening facial mask
CN111714437A (en) Beautifying liquid for removing freckles and wrinkles and preparation method thereof
CN103637927B (en) Tooth powder and preparation method thereof
CN108277113A (en) A kind of rose slag perfumed soap and preparation method thereof
CN103125651A (en) Manufacturing method of macule-removing flower tea
CN1528264A (en) Black mud for producing beauty, thinning and skin-care articles

Legal Events

Date Code Title Description
PB01 Publication
PB01 Publication
SE01 Entry into force of request for substantive examination
SE01 Entry into force of request for substantive examination
RJ01 Rejection of invention patent application after publication
RJ01 Rejection of invention patent application after publication

Application publication date: 20180615