CN108149089A - A kind of preparation of 6D16 aluminum alloy materials hot rolled plate - Google Patents

A kind of preparation of 6D16 aluminum alloy materials hot rolled plate Download PDF

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Publication number
CN108149089A
CN108149089A CN201711218088.4A CN201711218088A CN108149089A CN 108149089 A CN108149089 A CN 108149089A CN 201711218088 A CN201711218088 A CN 201711218088A CN 108149089 A CN108149089 A CN 108149089A
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casting
dispensing
product
soaking
refining
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CN201711218088.4A
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曹晓国
曹旷
曹洪正
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DALISHEN ALUMINUM Co Ltd
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DALISHEN ALUMINUM Co Ltd
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Priority to CN201711218088.4A priority Critical patent/CN108149089A/en
Publication of CN108149089A publication Critical patent/CN108149089A/en
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    • CCHEMISTRY; METALLURGY
    • C22METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22CALLOYS
    • C22C21/00Alloys based on aluminium
    • C22C21/06Alloys based on aluminium with magnesium as the next major constituent
    • C22C21/08Alloys based on aluminium with magnesium as the next major constituent with silicon
    • CCHEMISTRY; METALLURGY
    • C22METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22CALLOYS
    • C22C1/00Making non-ferrous alloys
    • C22C1/02Making non-ferrous alloys by melting
    • C22C1/026Alloys based on aluminium
    • CCHEMISTRY; METALLURGY
    • C22METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22CALLOYS
    • C22C1/00Making non-ferrous alloys
    • C22C1/06Making non-ferrous alloys with the use of special agents for refining or deoxidising
    • CCHEMISTRY; METALLURGY
    • C22METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22CALLOYS
    • C22C21/00Alloys based on aluminium
    • C22C21/02Alloys based on aluminium with silicon as the next major constituent
    • CCHEMISTRY; METALLURGY
    • C22METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22FCHANGING THE PHYSICAL STRUCTURE OF NON-FERROUS METALS AND NON-FERROUS ALLOYS
    • C22F1/00Changing the physical structure of non-ferrous metals or alloys by heat treatment or by hot or cold working
    • C22F1/04Changing the physical structure of non-ferrous metals or alloys by heat treatment or by hot or cold working of aluminium or alloys based thereon
    • C22F1/043Changing the physical structure of non-ferrous metals or alloys by heat treatment or by hot or cold working of aluminium or alloys based thereon of alloys with silicon as the next major constituent
    • CCHEMISTRY; METALLURGY
    • C22METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22FCHANGING THE PHYSICAL STRUCTURE OF NON-FERROUS METALS AND NON-FERROUS ALLOYS
    • C22F1/00Changing the physical structure of non-ferrous metals or alloys by heat treatment or by hot or cold working
    • C22F1/04Changing the physical structure of non-ferrous metals or alloys by heat treatment or by hot or cold working of aluminium or alloys based thereon
    • C22F1/047Changing the physical structure of non-ferrous metals or alloys by heat treatment or by hot or cold working of aluminium or alloys based thereon of alloys with magnesium as the next major constituent
    • CCHEMISTRY; METALLURGY
    • C22METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22FCHANGING THE PHYSICAL STRUCTURE OF NON-FERROUS METALS AND NON-FERROUS ALLOYS
    • C22F1/00Changing the physical structure of non-ferrous metals or alloys by heat treatment or by hot or cold working
    • C22F1/04Changing the physical structure of non-ferrous metals or alloys by heat treatment or by hot or cold working of aluminium or alloys based thereon
    • C22F1/05Changing the physical structure of non-ferrous metals or alloys by heat treatment or by hot or cold working of aluminium or alloys based thereon of alloys of the Al-Si-Mg type, i.e. containing silicon and magnesium in approximately equal proportions

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  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Mechanical Engineering (AREA)
  • Metallurgy (AREA)
  • Organic Chemistry (AREA)
  • Physics & Mathematics (AREA)
  • Thermal Sciences (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Manufacture And Refinement Of Metals (AREA)

Abstract

The present invention is a kind of preparation of 6D16 aluminum alloy materials hot rolled plate, and preparation method includes the following steps:(1)Dispensing:Dispensing includes the raw material of following mass percent:Si≤1.2, Fe≤0.6, Cu≤0.3, Mn≤1.0, Mg≤1.6, Zn≤0.4, Ti≤0.10, Zr≤0.10, other≤0.15, surplus Al,(2)Melting(3)Refining is stood(4)Online processing(5)Casting(6)Soaking pit soaking(7)Sawing milling face(8)Heating furnace(9)Hot rolling(10)Heavy pruning(11)Performance detection.The present invention can make full use of Heat transmission composite waste, high magnesium alloy waste material and other waste recoveries to recycle, and can economize on resources, and for raw material needed for the production of tool and mould product, provide alternative product, reduce production cost.

Description

A kind of preparation of 6D16 aluminum alloy materials hot rolled plate
Technical field
The invention belongs to aluminum alloy materials manufacture fields, particularly relate to a kind of 6D16 aluminum alloy materials hot rolled plate Preparation.
Background technology
With enterprise's production Heat transmission composite material, the output increased of high magnesium alloy materials, the amount of waste material is also corresponding Increase, and waste material is difficult to digestibility and utilization, how to utilize Heat transmission composite waste, waste material of skimming, high magnesium alloy to greatest extent Waste material, saw milling mix the recyclings such as waste material, are current problems, therefore are badly in need of a kind of novel aluminum alloy of research and development and come These waste materials are digested, the essential element of waste material is the multiple elements such as Si, Fe, Cu, Mn, Mg, Zn.
Invention content
To solve the above-mentioned problems, the present invention provides a kind of preparation of 6D16 aluminum alloy materials hot rolled plate, using compared with Heavy Heat transmission composite waste, waste material of skimming, high magnesium alloy waste material, saw milling mix waste material and carry out alloying component proportioning, really Determine chemical composition formula, exploitation is suitable for the application of plate product similar in tools production or replacement performance.
In order to achieve the above object, the present invention is achieved by the following technical solutions:
The present invention is a kind of preparation of 6D16 aluminum alloy materials hot rolled plate, and the preparation method includes the following steps:
(1)Dispensing:Dispensing includes the raw material of following mass percent:Si≤1.2, Fe≤0.6, Cu≤0.3, Mn≤1.0, Mg ≤ 1.6, Zn≤0.4, Ti≤0.10, Zr≤0.10, other≤0.15, surplus Al;
(2)Melting:Above-mentioned dispensing is packed into stove, after igniting is completed in shove charge, when dispensing part is melted, 40kg is uniformly added into and covers Lid agent treats that dispensing just all melts, is uniformly added into 40kg slagging agents immediately, and before refining, after being sufficiently stirred, sampling carries out ingredient Analysis, 710 DEG C~740 DEG C of smelting temperature;
(3)Refining is stood:To step(2)Product after melting is refined using N2+Cl2 methods, refining time 20 minutes, pressure 0.6 ~1.0MPa, 710 DEG C~740 DEG C of refining temperature, time of repose 20 minutes;
(4)Online processing:Product grains after refining treatment are refined, crystal grain refinement feeds silk speed using Al-5Ti-B refinements 280-320cm/min is spent, online degasification uses SDF birotor degasification, 300~400rpm of rotor speed, and on-line filtration uses 30ppi+40ppi twin-stages foamed ceramic filter plate filters;
(5)Casting:To step(4)Product carry out semi-continuous casting, casting speed 40-60mm/min, casting 680-730 DEG C, Cooling water pressure 150-200Pa, cools down 510 × 1600 × 6130mm of specification after ingot casting shaping, and the ingot casting after casting answers surface, ruler Very little, appearance should conform to quality requirements;
(6)Soaking pit soaking:By 450-480 DEG C of product soaking metal temperature after casting, soaking time 5-10 hours;
(7)Sawing milling face:A mouthful bottom sawing 250mm is poured by cast the product after soaking, and sawing is taken a sample to check chemical composition Analysis, single side milling amount are more than 10mm, remove the part of surface scale, coarse grains, milling face thickness The ingot casting thickness 470- 490mm;
(8)Heating furnace:Metal temperature behind milling face is heated to 460-490 DEG C, heating time 6-9 hour;
(9)Hot rolling:By the ingot casting after heating in 3300mm four-high reversing mills, it is rolled down to finished product thickness 20mm, finishing temperature 280-330℃;
(10)Heavy pruning:By precision saw according to required trimmed size size, shearing samples performance detection;
(11)Performance detection:Mechanics properties testing is carried out on omnipotent mechanics machine, obtains testing result.
The beneficial effects of the invention are as follows:The present invention utilizes existing production equipment, technical conditions, does not need to increase investment, Give full play to the potential of production equipment;Heat transmission composite waste, high magnesium alloy waste material and other waste recoveries can be made full use of It recycles, can economize on resources, reduce the discharge environmental protection of carbon dioxide, create economic benefit for enterprise, social benefit has Profound significance;For raw material needed for the production of tool and mould product, alternative product is provided, reduces production cost.
Specific embodiment
In order to deepen the understanding of the present invention, the present invention is described in further detail below in conjunction with embodiment, the reality It applies example to be only used for explaining the present invention, protection scope of the present invention is not formed and is limited.
As shown in the Examples, the present invention is a kind of preparation of 6D16 aluminum alloy materials hot rolled plate, the preparation method packet Include following steps:
(1)Dispensing:Heat transmission compound material, waste material of skimming, high magnesium alloy waste material, saw milling material are collected as dispensing;According to chemical composition Control requirement, dispensing include the raw material of following mass percent:Si≤1.2, Fe≤0.6, Cu≤0.3, Mn≤1.0, Mg≤ 1.6, Zn≤0.4, Ti≤0.10, Zr≤0.10, other≤0.15, surplus Al;Wherein other refer to impurity element, such as:B、 Bi, Ca, Sb, Be etc.;
(2)Melting:Above-mentioned dispensing is packed into stove, after igniting is completed in shove charge, when dispensing part is melted, 40kg is uniformly added into and covers Lid agent treats that dispensing just all melts, is uniformly added into 40kg slagging agents immediately, and before refining, after being sufficiently stirred, sampling passes through DF- 100E direct-reading spectrometers carry out constituent analysis, 710 DEG C~740 DEG C of smelting temperature;
(3)Refining is stood:To step(2)Product after melting is refined using N2+Cl2 methods, refining time about 20 minutes, pressure 0.6~1.0MPa, 710 DEG C~740 DEG C of refining temperature, time of repose 20 minutes;
(4)Online processing:Product grains after refining treatment are refined, crystal grain refinement feeds silk speed using Al-5Ti-B refinements 280-320cm/min is spent, online degasification uses SDF birotor degasification, 300~400rpm of rotor speed, and on-line filtration uses 30ppi+40ppi twin-stages foamed ceramic filter plate filters;
(5)Casting:To step(4)Product carry out semi-continuous casting, casting speed 40-60mm/min, casting 680-730 DEG C, Cooling water pressure 150-200Pa, cools down 510 × 1600 × 6130mm of specification after ingot casting shaping, and the ingot casting after casting answers surface, ruler Very little, appearance should conform to quality requirements;
(6)Soaking pit soaking:By 450-480 DEG C of product soaking metal temperature after casting, soaking time 5-10 hours;
(7)Sawing milling face:By mouthful bottom sawing 250mm that pours of the product after casting soaking, it is straight that sawing sampling passes through DF-100E It reads spectrometer and checks chemical composition analysis, single side milling amount is more than 10mm, removes the part of surface scale, coarse grains, milling Face thickness The ingot casting thickness 470-490mm;
(8)Heating furnace:Metal temperature behind milling face is heated to 460-490 DEG C, heating time 6-9 hour;
(9)Hot rolling:By the ingot casting after heating in 3300mm four-high reversing mills, it is rolled down to finished product thickness 20mm, finishing temperature 280-330℃;
(10)Heavy pruning:By precision saw according to required trimmed size size, shearing samples performance detection;It is cut out in the present embodiment Size such as following table:
(11)Performance detection:Mechanics properties testing is carried out on the omnipotent mechanics machines of TY-8000 50KN, obtains testing result. According to national standard on omnipotent mechanics machine《GB/T 228.1-2010 metal material stretching test part 1s:Room temperature is tried Proved recipe method》Carry out mechanics properties testing;Case hardness carries out hardness determination on MICROMET-3 Vickers, is detected As a result, normative reference《GB/T3880.2-2012, general industry aluminium and aluminium alloy plate, band part 2:Mechanical property》.
The testing result of the present embodiment such as following table
Alloy designations Supply status Thickness/mm Tensile strength/MPa Yield strength/MPa Elongation percentage/% Hardness/HB
6D16 H112 20.0 170~176 102~108 18~23 52~56
Comparative alloy detection data see the table below 2
By data above it can be seen that:The 6D16 Mechanical Properties of Aluminum Alloys testing results of the present invention, the mechanical property with 6 line aluminium alloys Energy index approaches, and 6D16 can substitute the production of 6061-H112,6082-H112,3003-H112/O, 5052-O hot-rolled thick plank completely Product.

Claims (1)

1. a kind of preparation of 6D16 aluminum alloy materials hot rolled plate, it is characterised in that:The preparation method includes the following steps:
(1)Dispensing:Dispensing includes the raw material of following mass percent:Si≤1.2, Fe≤0.6, Cu≤0.3, Mn≤1.0, Mg ≤ 1.6, Zn≤0.4, Ti≤0.10, Zr≤0.10, other≤0.15, surplus Al;
(2)Melting:Above-mentioned dispensing is packed into stove, after igniting is completed in shove charge, when dispensing part is melted, 40kg is uniformly added into and covers Lid agent treats that dispensing just all melts, is uniformly added into 40kg slagging agents immediately, and before refining, after being sufficiently stirred, sampling carries out ingredient Analysis, 710 DEG C~740 DEG C of smelting temperature;
(3)Refining is stood:To step(2)Product after melting is refined using N2+Cl2 methods, refining time 20 minutes, pressure 0.6 ~1.0MPa, 710 DEG C~740 DEG C of refining temperature, time of repose 20 minutes;
(4)Online processing:Product grains after refining treatment are refined, crystal grain refinement feeds silk speed using Al-5Ti-B refinements 280-320cm/min is spent, online degasification uses SDF birotor degasification, 300~400rpm of rotor speed, and on-line filtration uses 30ppi+40ppi twin-stages foamed ceramic filter plate filters;
(5)Casting:To step(4)Product carry out semi-continuous casting, casting speed 40-60mm/min, casting 680-730 DEG C, Cooling water pressure 150-200Pa, cools down 510 × 1600 × 6130mm of specification after ingot casting shaping, and the ingot casting after casting answers surface, ruler Very little, appearance should conform to quality requirements;
(6)Soaking pit soaking:By 450-480 DEG C of product soaking metal temperature after casting, soaking time 5-10 hours;
(7)Sawing milling face:A mouthful bottom sawing 250mm is poured by cast the product after soaking, and sawing is taken a sample to check chemical composition Analysis, single side milling amount are more than 10mm, remove the part of surface scale, coarse grains, milling face thickness The ingot casting thickness 470- 490mm;
(8)Heating furnace:Metal temperature behind milling face is heated to 460-490 DEG C, heating time 6-9 hour;
(9)Hot rolling:By the ingot casting after heating in 3300mm four-high reversing mills, it is rolled down to finished product thickness 20mm, finishing temperature 280-330℃;
(10)Heavy pruning:By precision saw according to required trimmed size size, shearing samples performance detection;
(11)Performance detection:Mechanics properties testing is carried out on omnipotent mechanics machine, obtains testing result.
CN201711218088.4A 2017-11-28 2017-11-28 A kind of preparation of 6D16 aluminum alloy materials hot rolled plate Pending CN108149089A (en)

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Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109722576A (en) * 2019-01-10 2019-05-07 大力神铝业股份有限公司 A kind of ingot casting process of preparing of ultra-low residue stress aluminum alloy materials
CN111961898A (en) * 2020-09-15 2020-11-20 昆明冶金研究院有限公司 Method for preparing aluminum-magnesium-silicon alloy by recycling waste resources
CN113186433A (en) * 2021-03-24 2021-07-30 辽宁忠旺集团有限公司 6082 aluminum alloy and process for casting to replace deformed extrusion rod by using same
CN115319413A (en) * 2022-08-17 2022-11-11 山东南山铝业股份有限公司 Production method of circulating grade-keeping 5-series beverage bottom cover material

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104294194A (en) * 2013-07-16 2015-01-21 大力神铝业股份有限公司 Manufacturing method for improving cupping value of 3104 aluminum alloy strip
CN104294113A (en) * 2013-07-16 2015-01-21 大力神铝业股份有限公司 Method for manufacturing aluminium alloy sheet for automobile fuel tank
CN104294112A (en) * 2013-07-16 2015-01-21 大力神铝业股份有限公司 Production method of aluminum alloy foil for aviation lunch box

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104294194A (en) * 2013-07-16 2015-01-21 大力神铝业股份有限公司 Manufacturing method for improving cupping value of 3104 aluminum alloy strip
CN104294113A (en) * 2013-07-16 2015-01-21 大力神铝业股份有限公司 Method for manufacturing aluminium alloy sheet for automobile fuel tank
CN104294112A (en) * 2013-07-16 2015-01-21 大力神铝业股份有限公司 Production method of aluminum alloy foil for aviation lunch box

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109722576A (en) * 2019-01-10 2019-05-07 大力神铝业股份有限公司 A kind of ingot casting process of preparing of ultra-low residue stress aluminum alloy materials
CN111961898A (en) * 2020-09-15 2020-11-20 昆明冶金研究院有限公司 Method for preparing aluminum-magnesium-silicon alloy by recycling waste resources
CN113186433A (en) * 2021-03-24 2021-07-30 辽宁忠旺集团有限公司 6082 aluminum alloy and process for casting to replace deformed extrusion rod by using same
CN115319413A (en) * 2022-08-17 2022-11-11 山东南山铝业股份有限公司 Production method of circulating grade-keeping 5-series beverage bottom cover material

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Application publication date: 20180612

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