CN108127092A - A kind of coverture and its preparation process - Google Patents

A kind of coverture and its preparation process Download PDF

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Publication number
CN108127092A
CN108127092A CN201611090644.XA CN201611090644A CN108127092A CN 108127092 A CN108127092 A CN 108127092A CN 201611090644 A CN201611090644 A CN 201611090644A CN 108127092 A CN108127092 A CN 108127092A
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CN
China
Prior art keywords
parts
coverture
diatomite
preparation process
lime stone
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201611090644.XA
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Chinese (zh)
Inventor
苏伟
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Super Peculiar Non-Ferrous Metal Additive Factory Of Tongshan County
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Super Peculiar Non-Ferrous Metal Additive Factory Of Tongshan County
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Super Peculiar Non-Ferrous Metal Additive Factory Of Tongshan County filed Critical Super Peculiar Non-Ferrous Metal Additive Factory Of Tongshan County
Priority to CN201611090644.XA priority Critical patent/CN108127092A/en
Publication of CN108127092A publication Critical patent/CN108127092A/en
Pending legal-status Critical Current

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Classifications

    • BPERFORMING OPERATIONS; TRANSPORTING
    • B22CASTING; POWDER METALLURGY
    • B22DCASTING OF METALS; CASTING OF OTHER SUBSTANCES BY THE SAME PROCESSES OR DEVICES
    • B22D11/00Continuous casting of metals, i.e. casting in indefinite lengths
    • B22D11/10Supplying or treating molten metal
    • B22D11/11Treating the molten metal
    • B22D11/111Treating the molten metal by using protecting powders
    • CCHEMISTRY; METALLURGY
    • C21METALLURGY OF IRON
    • C21CPROCESSING OF PIG-IRON, e.g. REFINING, MANUFACTURE OF WROUGHT-IRON OR STEEL; TREATMENT IN MOLTEN STATE OF FERROUS ALLOYS
    • C21C7/00Treating molten ferrous alloys, e.g. steel, not covered by groups C21C1/00 - C21C5/00
    • C21C7/005Treating molten ferrous alloys, e.g. steel, not covered by groups C21C1/00 - C21C5/00 using exothermic reaction compositions

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  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Materials Engineering (AREA)
  • Metallurgy (AREA)
  • Organic Chemistry (AREA)
  • Mechanical Engineering (AREA)
  • Solid-Sorbent Or Filter-Aiding Compositions (AREA)

Abstract

The invention discloses a kind of coverture of coverture technical field, the formula of the coverture is as follows:Lime stone:30~60 parts;Diatomite:10~20 parts;Expanded vermiculite:5~10 parts;Expanded graphite:4~7 parts;Exothermic mixture:2~4 parts;Calcirm-fluoride:3~8 parts, the present invention has the characteristics that using expanded vermiculite and expanded graphite compared with highly expanded ability, make coverture that can be unfolded rapidly after ladle is put into, and then achieve the purpose that quickly and effectively to cover molten steel surface, the present invention is after addition expanded vermiculite and expanded graphite, a separation layer can also be formed in the slag blanket of molten steel surface, the heat dissipation capacity of molten steel can effectively be reduced, improve the insulation effect of coverture, add suitable aluminium powder, coke blacking and coal dust are as exothermic mixture, improve the calorific value of coverture, the heat loss of molten steel in ladle is made up using heat caused by the chemical reaction of exothermic mixture.

Description

A kind of coverture and its preparation process
Technical field
The present invention relates to coverture technical field, specially a kind of coverture and its preparation process.
Background technology
The initial use purpose of thermal-insulating covering agent is very simple, exactly in order to keep the temperature, to prevent molten steel from transporting and pouring into a mould Temperature declines excessive in the process.But with raising of the people to the quality requirement of steel, the function of molten steel insulation coverture tends to Diversification and functionalization.It specifically includes:Heat preservation prevents secondary oxidation of the air to molten steel, adsorbs the field trash to float in molten steel. Meanwhile also require thermal-insulating covering agent that molten steel cannot be made to generate pollution with the element reaction in molten steel or molten steel in itself.
When pouring into a mould carbon aluminium-killed steel and high-alloy steel, the non-gold for how reducing and eliminating the aggregation of molten steel face will necessarily be encountered The problem of belonging to field trash, if the non-metallic inclusion in tundish molten steel cannot be eliminated in time, necessarily affect the table of strand Face and subcutaneous quality, to come into operation for this purpose, we have proposed a kind of covertures and its preparation process, to solve the above problems.
Invention content
The purpose of the present invention is to provide a kind of coverture and its preparation processes, mentioned above in the background art to solve If the non-metallic inclusion in tundish molten steel cannot be eliminated in time, the surface of strand and asking for subcutaneous quality are necessarily affected Topic.
To achieve the above object, the present invention provides following technical solution:A kind of coverture, the formula of the coverture are as follows:
Lime stone:30~60 parts;
Diatomite:10~20 parts;
Expanded vermiculite:5~10 parts;
Expanded graphite:4~7 parts;
Exothermic mixture:2~4 parts;
Calcirm-fluoride:3~8 parts.
Preferably, the exothermic mixture is the mixture of aluminium powder, coke blacking and coal dust, wherein aluminium powder:Coke blacking:Coal dust= 0.8:1.2:1.9。
A kind of preparation process of coverture, the preparation process of the coverture are as follows:S1:By 30~60 parts Lime stone and 10~20 parts of diatomite material are sieved, and the lime stone and diatomite for choosing a diameter of 20~30mm are used as system Standby raw material;
S2:Lime stone after screening and diatomite are put into blender, sequentially add 5~10 parts expanded vermiculite, 4~ In 7 parts of expanded graphite, 2~4 parts of exothermic mixture and 3~8 parts of calcirm-fluoride to blender, powder is sufficiently stirred by blender It is uniformly mixed it after broken;
S3:By in feedstock transportation to comminutor after fully mixed, by the atomizer being mounted on inside comminutor Atomized water is generated by high-pressure hydraulic pump, raw material is squirted;
S4:Raw material is agglomerated into corase particles after being contacted with water, controls the rotating speed of granulation disc, and raw material contacts the coarse grain to be formed with water Son is rotated in granulation disc, squeezes and is brought together, forms graininess semi-finished product;
S5:The graininess semi-finished product prepared in step S4 are handled by heat drying, by its water content control 3~ Between 5%;
S6:Semi-finished product after being dried in step S5 are sieved, choose range conduct of the grain size in 10~15mm Finished product coverture.
Preferably, in the step S2, the proportioning between lime stone and diatomite is 3:1, the rotating speed of wherein blender is 800~1200r/min, mixing time are 10~15min.
Preferably, in the step S3, the pressure of high-pressure hydraulic pump is controlled between 0.6~0.8MPa.
Preferably, in the step S4, the rotating speed of granulation disc is 700~900r/min, and pass through wind inside comminutor Machine forms negative pressure.
Preferably, in the step S5, heating temperature is 120~150 DEG C, and 8~12min of continuous heating time.
Compared with prior art, the beneficial effects of the invention are as follows:The present invention has using expanded vermiculite and expanded graphite The characteristics of compared with highly expanded ability, makes coverture that can be unfolded rapidly, and then reach and quickly and effectively cover after ladle is put into The purpose of molten steel surface, the present invention can also be formed after addition expanded vermiculite and expanded graphite in the slag blanket of molten steel surface One separation layer can effectively reduce the heat dissipation capacity of molten steel, improve the insulation effect of coverture, add suitable aluminium powder, coke blacking With coal dust as exothermic mixture, the calorific value of coverture is improved, steel is made up using heat caused by the chemical reaction of exothermic mixture The heat loss of molten steel in packet.
Description of the drawings
Fig. 1 is work flow diagram of the present invention.
Specific embodiment
Below in conjunction with the attached drawing in the embodiment of the present invention, the technical solution in the embodiment of the present invention is carried out clear, complete Site preparation describes, it is clear that described embodiment is only part of the embodiment of the present invention, instead of all the embodiments.It is based on Embodiment in the present invention, those of ordinary skill in the art are obtained every other without making creative work Embodiment shall fall within the protection scope of the present invention.
Embodiment one
A kind of coverture, the formula of the coverture are as follows:
Lime stone:30 parts;
Diatomite:10 parts;
Expanded vermiculite:5 parts;
Expanded graphite:4 parts;
Exothermic mixture:2 parts, exothermic mixture is the mixture of aluminium powder, coke blacking and coal dust, wherein aluminium powder:Coke blacking:Coal dust= 0.8:1.2:1.9;
Calcirm-fluoride:3~8 parts.
The present invention also provides a kind of preparation process of coverture, the preparation process of the coverture is as follows: S1:30 parts of lime stone and 10 parts of diatomite material are sieved, the lime stone and diatomite for choosing a diameter of 20mm are made To prepare raw material;
S2:Lime stone after screening and diatomite are put into blender, sequentially add 5 parts expanded vermiculite, 4 parts swollen In swollen graphite, 2 parts of exothermic mixture and 3 parts of calcirm-fluoride to blender, by blender be sufficiently stirred crushing after make its mixing Uniformly, the proportioning between lime stone and diatomite is 3:1, the wherein rotating speed of blender is 800r/min, and mixing time is 10min;
S3:By in feedstock transportation to comminutor after fully mixed, by the atomizer being mounted on inside comminutor Atomized water is generated by high-pressure hydraulic pump, raw material is squirted, the pressure of high-pressure hydraulic pump is controlled between 0.6MPa;
S4:Raw material is agglomerated into corase particles after being contacted with water, controls the rotating speed of granulation disc, and raw material contacts the coarse grain to be formed with water Son is rotated in granulation disc, squeezes and is brought together, forms graininess semi-finished product, the rotating speed of granulation disc is 700r/min, and be granulated Negative pressure is formed by wind turbine inside machine;
S5:The graininess semi-finished product prepared in step S4 are handled by heat drying, by its water content control 3% Between, heating temperature is 120 DEG C, and continuous heating time 8min;
S6:Semi-finished product after being dried in step S5 are sieved, choose grain size in the range of 10mm as finished product Coverture.
Embodiment two
A kind of coverture, the formula of the coverture are as follows:
Lime stone:60 parts;
Diatomite:20 parts;
Expanded vermiculite:10 parts;
Expanded graphite:7 parts;
Exothermic mixture:4 parts, exothermic mixture is the mixture of aluminium powder, coke blacking and coal dust, wherein aluminium powder:Coke blacking:Coal dust= 0.8:1.2:1.9;
Calcirm-fluoride:8 parts.
The present invention also provides a kind of preparation process of coverture, the preparation process of the coverture is as follows: S1:60 parts of lime stone and 20 parts of diatomite material are sieved, the lime stone and diatomite for choosing a diameter of 30mm are made To prepare raw material;
S2:Lime stone after screening and diatomite are put into blender, sequentially add 10 parts expanded vermiculite, 7 parts In expanded graphite, 4 parts of exothermic mixture and 8 parts of calcirm-fluoride to blender, by blender be sufficiently stirred crushing after make it mixed It closes uniformly, the proportioning between lime stone and diatomite is 3:1, the wherein rotating speed of blender is 1200r/min, and mixing time is 15min;
S3:By in feedstock transportation to comminutor after fully mixed, by the atomizer being mounted on inside comminutor Atomized water is generated by high-pressure hydraulic pump, raw material is squirted, the pressure of high-pressure hydraulic pump is controlled between 0.8MPa;
S4:Raw material is agglomerated into corase particles after being contacted with water, controls the rotating speed of granulation disc, and raw material contacts the coarse grain to be formed with water Son is rotated in granulation disc, squeezes and is brought together, forms graininess semi-finished product, the rotating speed of granulation disc is 900r/min, and be granulated Negative pressure is formed by wind turbine inside machine;
S5:The graininess semi-finished product prepared in step S4 are handled by heat drying, by its water content control 5% Between, heating temperature is 150 DEG C, and continuous heating time 12min;
S6:Semi-finished product after being dried in step S5 are sieved, choose grain size in the range of 15mm as finished product Coverture.
Embodiment three
A kind of coverture, the formula of the coverture are as follows:
Lime stone:40 parts;
Diatomite:15 parts;
Expanded vermiculite:8 parts;
Expanded graphite:5 parts;
Exothermic mixture:3 parts, exothermic mixture is the mixture of aluminium powder, coke blacking and coal dust, wherein aluminium powder:Coke blacking:Coal dust= 0.8:1.2:1.9;
Calcirm-fluoride:6 parts.
The present invention also provides a kind of preparation process of coverture, the preparation process of the coverture is as follows: S1:40 parts of lime stone and 15 parts of diatomite material are sieved, the lime stone and diatomite for choosing a diameter of 25mm are made To prepare raw material;
S2:Lime stone after screening and diatomite are put into blender, sequentially add 8 parts expanded vermiculite, 5 parts swollen In swollen graphite, 3 parts of exothermic mixture and 6 parts of calcirm-fluoride to blender, by blender be sufficiently stirred crushing after make its mixing Uniformly, the proportioning between lime stone and diatomite is 3:1, the wherein rotating speed of blender is 1000r/min, and mixing time is 13min;
S3:By in feedstock transportation to comminutor after fully mixed, by the atomizer being mounted on inside comminutor Atomized water is generated by high-pressure hydraulic pump, raw material is squirted, the pressure of high-pressure hydraulic pump is controlled between 0.7MPa;
S4:Raw material is agglomerated into corase particles after being contacted with water, controls the rotating speed of granulation disc, and raw material contacts the coarse grain to be formed with water Son is rotated in granulation disc, squeezes and is brought together, forms graininess semi-finished product, the rotating speed of granulation disc is 800r/min, and be granulated Negative pressure is formed by wind turbine inside machine;
S5:The graininess semi-finished product prepared in step S4 are handled by heat drying, by its water content control 4% Between, heating temperature is 130 DEG C, and continuous heating time 10min;
S6:Semi-finished product after being dried in step S5 are sieved, choose grain size in the range of 13mm as finished product Coverture.
It although an embodiment of the present invention has been shown and described, for the ordinary skill in the art, can be with Understanding without departing from the principles and spirit of the present invention can carry out these embodiments a variety of variations, modification, replace And modification, the scope of the present invention is defined by the appended.

Claims (7)

1. a kind of coverture, it is characterised in that:The formula of the coverture is as follows:
Lime stone:30~60 parts;
Diatomite:10~20 parts;
Expanded vermiculite:5~10 parts;
Expanded graphite:4~7 parts;
Exothermic mixture:2~4 parts;
Calcirm-fluoride:3~8 parts.
2. a kind of coverture according to claim 1, it is characterised in that:The exothermic mixture is aluminium powder, coke blacking and coal dust Mixture, wherein aluminium powder:Coke blacking:Coal dust=0.8:1.2:1.9.
3. a kind of preparation process of coverture:It is characterized in that:The preparation process of the coverture is as follows:
S1:30~60 parts of lime stone and 10~20 parts of diatomite material are sieved, choose a diameter of 20~30mm's Lime stone and diatomite, which are used as, prepares raw material;
S2:Lime stone after screening and diatomite are put into blender, sequentially add 5~10 parts expanded vermiculite, 4~7 parts Expanded graphite, in 2~4 parts of exothermic mixture and 3~8 parts of calcirm-fluoride to blender, crushing is sufficiently stirred by blender After make its be uniformly mixed;
S3:By in feedstock transportation to comminutor after fully mixed, passed through by being mounted on the atomizer inside comminutor High-pressure hydraulic pump generates atomized water, and raw material is squirted;
S4:Raw material is agglomerated into corase particles after being contacted with water, controls the rotating speed of granulation disc, and raw material contacts the corase particles to be formed with water and exists It rotates, squeeze and brings together in granulation disc, form graininess semi-finished product;
S5:The graininess semi-finished product prepared in step S4 are handled by heat drying, by its water content control 3~5% Between;
S6:Semi-finished product after being dried in step S5 are sieved, choose grain size in the range of 10~15mm as finished product Coverture.
4. a kind of preparation process of coverture according to claim 3, it is characterised in that:In the step S2, lime stone Proportioning between diatomite is 3:1, the wherein rotating speed of blender is 800~1200r/min, and mixing time is 10~15min.
5. a kind of preparation process of coverture according to claim 3, it is characterised in that:In the step S3, high pressure water The pressure of pump is controlled between 0.6~0.8MPa.
6. a kind of preparation process of coverture according to claim 3, it is characterised in that:In the step S4, granulation disc Rotating speed for 700~900r/min, and negative pressure is formed by wind turbine inside comminutor.
7. a kind of preparation process of coverture according to claim 3, it is characterised in that:In the step S5, heating temperature Spend is 120~150 DEG C, and 8~12min of continuous heating time.
CN201611090644.XA 2016-12-01 2016-12-01 A kind of coverture and its preparation process Pending CN108127092A (en)

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Application Number Priority Date Filing Date Title
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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109332608A (en) * 2018-11-27 2019-02-15 沈劲松 Metallurgical industry thermal-insulating covering agent for heat product
CN111100967A (en) * 2020-01-13 2020-05-05 北京科技大学 Foaming agent, tundish covering agent and preparation method and application thereof

Citations (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH01210157A (en) * 1988-02-15 1989-08-23 Sumitomo Metal Ind Ltd Method for preventing surface longitudinal crack on continuous cast slab
JPH03226341A (en) * 1990-01-30 1991-10-07 Shinagawa Refract Co Ltd Exothermic type mold powder for continuous casting
CN1759958A (en) * 2005-03-22 2006-04-19 浙江湖州红鹰企业集团有限公司 Heat preservation agent in use for molded casting, and producing technique
CN102554141A (en) * 2012-02-24 2012-07-11 上海市机械制造工艺研究所有限公司 Heating covering agent for casting steel piece
CN103173591A (en) * 2013-03-07 2013-06-26 西安建筑科技大学 Foundry ladle covering agent
CN103801666A (en) * 2014-02-24 2014-05-21 江苏苏南重工机械科技有限公司 High-performance heat-preservation covering agent for thick slab and preparing method of high-performance heat-preservation covering agent
CN104275447A (en) * 2014-10-08 2015-01-14 吴江市液铸液压件铸造有限公司 Heating covering agent and preparation method thereof
CN104308106A (en) * 2014-10-08 2015-01-28 吴江市液铸液压件铸造有限公司 Steel ladle covering agent

Patent Citations (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH01210157A (en) * 1988-02-15 1989-08-23 Sumitomo Metal Ind Ltd Method for preventing surface longitudinal crack on continuous cast slab
JPH03226341A (en) * 1990-01-30 1991-10-07 Shinagawa Refract Co Ltd Exothermic type mold powder for continuous casting
CN1759958A (en) * 2005-03-22 2006-04-19 浙江湖州红鹰企业集团有限公司 Heat preservation agent in use for molded casting, and producing technique
CN102554141A (en) * 2012-02-24 2012-07-11 上海市机械制造工艺研究所有限公司 Heating covering agent for casting steel piece
CN103173591A (en) * 2013-03-07 2013-06-26 西安建筑科技大学 Foundry ladle covering agent
CN103801666A (en) * 2014-02-24 2014-05-21 江苏苏南重工机械科技有限公司 High-performance heat-preservation covering agent for thick slab and preparing method of high-performance heat-preservation covering agent
CN104275447A (en) * 2014-10-08 2015-01-14 吴江市液铸液压件铸造有限公司 Heating covering agent and preparation method thereof
CN104308106A (en) * 2014-10-08 2015-01-28 吴江市液铸液压件铸造有限公司 Steel ladle covering agent

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109332608A (en) * 2018-11-27 2019-02-15 沈劲松 Metallurgical industry thermal-insulating covering agent for heat product
CN111100967A (en) * 2020-01-13 2020-05-05 北京科技大学 Foaming agent, tundish covering agent and preparation method and application thereof

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