CN108126411A - A kind of filter method and filter plant of honeysuckle distillate - Google Patents
A kind of filter method and filter plant of honeysuckle distillate Download PDFInfo
- Publication number
- CN108126411A CN108126411A CN201611090248.7A CN201611090248A CN108126411A CN 108126411 A CN108126411 A CN 108126411A CN 201611090248 A CN201611090248 A CN 201611090248A CN 108126411 A CN108126411 A CN 108126411A
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- China
- Prior art keywords
- filter
- filter paper
- paper pulp
- filtering tank
- distillate
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- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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- 241000205585 Aquilegia canadensis Species 0.000 title claims abstract description 26
- 238000000034 method Methods 0.000 title claims abstract description 19
- 241000196324 Embryophyta Species 0.000 title claims abstract description 10
- 238000001914 filtration Methods 0.000 claims abstract description 58
- 229920001131 Pulp (paper) Polymers 0.000 claims abstract description 40
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 18
- 239000012634 fragment Substances 0.000 claims abstract description 11
- 239000003513 alkali Substances 0.000 claims abstract description 6
- 238000004080 punching Methods 0.000 claims abstract description 6
- 239000002002 slurry Substances 0.000 claims abstract description 6
- 239000007788 liquid Substances 0.000 claims description 22
- 230000000740 bleeding effect Effects 0.000 claims description 18
- 238000005192 partition Methods 0.000 claims description 15
- 238000009826 distribution Methods 0.000 claims description 7
- 239000004744 fabric Substances 0.000 claims description 6
- 238000004451 qualitative analysis Methods 0.000 claims description 5
- 230000000694 effects Effects 0.000 abstract description 9
- 238000010521 absorption reaction Methods 0.000 abstract description 2
- 230000003204 osmotic effect Effects 0.000 abstract description 2
- 239000000463 material Substances 0.000 description 6
- 239000000706 filtrate Substances 0.000 description 5
- 238000004519 manufacturing process Methods 0.000 description 3
- 239000000047 product Substances 0.000 description 3
- 238000010025 steaming Methods 0.000 description 3
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 2
- 238000005516 engineering process Methods 0.000 description 2
- 238000005352 clarification Methods 0.000 description 1
- 230000000052 comparative effect Effects 0.000 description 1
- 230000006835 compression Effects 0.000 description 1
- 238000007906 compression Methods 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- 239000003814 drug Substances 0.000 description 1
- 235000013399 edible fruits Nutrition 0.000 description 1
- 238000010438 heat treatment Methods 0.000 description 1
- 238000007689 inspection Methods 0.000 description 1
- 238000005259 measurement Methods 0.000 description 1
- 239000008213 purified water Substances 0.000 description 1
- 230000035939 shock Effects 0.000 description 1
- 239000000243 solution Substances 0.000 description 1
- 239000012085 test solution Substances 0.000 description 1
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D37/00—Processes of filtration
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D29/00—Filters with filtering elements stationary during filtration, e.g. pressure or suction filters, not covered by groups B01D24/00 - B01D27/00; Filtering elements therefor
- B01D29/01—Filters with filtering elements stationary during filtration, e.g. pressure or suction filters, not covered by groups B01D24/00 - B01D27/00; Filtering elements therefor with flat filtering elements
- B01D29/05—Filters with filtering elements stationary during filtration, e.g. pressure or suction filters, not covered by groups B01D24/00 - B01D27/00; Filtering elements therefor with flat filtering elements supported
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D2239/00—Aspects relating to filtering material for liquid or gaseous fluids
- B01D2239/10—Filtering material manufacturing
Abstract
The invention discloses a kind of filter methods and filter plant of honeysuckle distillate, the filter method includes making filter paper pulp, make filter paper cake and filtering three big step of distillate, wherein, filter paper pulp is that filter paper is broken into after paper fragment to mix with piece alkali to be made by steam punching slurry again, and filter paper cake is in filter plant（Filtering tank）Fully compacting is formed again after the middle hot-water soak by filter paper pulp, and finally honeysuckle distillate is slowly added into filtering tank, is filtered using manufactured filter paper cake.Mode present invention employs naturally osmotic is filtered, and filter paper cake is made again after filter paper chopping is made filter paper pulp, filter paper cake can be by most muddy object absorption wherein, its good filtration effect, the distillate after filtering can be made to reach ideal clarity, and simple for process, it is easily operated.
Description
Technical field
The present invention relates to distilled liquid of honeysuckle production technical field, more specifically more particularly to a kind of honeysuckle distillate
Filter method and filter plant.
Background technology
In the production technology of the distilled liquid of honeysuckle, there are the process being filtered together to honeysuckle distillate, filter effect
Quality directly influence the clarity of product, good filtration effect, product clarity is just high；Filter effect is bad, product clarification
Degree is just low.At present, the filtering of honeysuckle distillate is filtered always using sheet frame, and filter material is mostly selected used in plate-frame filtering
One layer of filter cloth adds one layer of filter paper, and in this way under the compression shock of pump, liquid has passed through filter material quickly, and the effect of filtering is undesirable；
If increasing the thickness of filter material, filter material is easily blocked, it is difficult to pass through to make filtrate, filters the difficulty of change；If but increase the pressure of pump,
Filter material can be punctured again, the effect of filtering is not achieved.Moreover, found in production using plate-frame filtering, no matter which kind of filter selected
Material is all difficult that slightly cloudy liquid is filled into ideal clarity.
Invention content
It is an object of the invention in view of the above shortcomings of the prior art, provide a kind of filtering side of honeysuckle distillate
Method promotes filter effect, the filtrate after filtering is made to reach ideal clarity.
To achieve the above object, present invention employs following technical solutions：
A kind of filter method of honeysuckle distillate, includes the following steps：
（1）Make filter paper pulp：The middling speed qualitative analysis filter paper that specification is 60 × 60cm is put into shredder and is broken into paper fragment, then
Paper fragment and piece alkali are added to by weight the ratio for 10 ︰ 1 in plastic barrel, seals in backward plastic barrel and is passed through steam
Punching slurry 2-3 days, then the filter paper pulp that steam treatment is crossed is poured into filter bag, rinsed repeatedly with clear water for several times, until test paper detects
It is in neutrality, filter paper pulp completes；
（2）Make filter paper cake：A filter cloth for being less than 10 mesh is taken to be laid on the intermediate bulkhead in filtering tank, is set on the partition board
Filter paper pulp is poured into filtering tank and is equably laid on partition board by the hole of regular distribution, and patting filter paper pulp makes it build in fact；
The liquid valve of filtering pot bottom, while the air bleeding valve of crack filtering tank side are then shut off, 80-100 DEG C is added in into filtering tank
Hot water filter paper pulp is totally submerged, impregnate 20-30 minute after, close air bleeding valve, open liquid valve release hot water, finally will filter
Paper pulp is fully compacted, and the filter paper cake of 6-8cm thickness is made；
（3）Filter distillate：Honeysuckle distillate is slowly added into filtering tank, opens liquid valve, is controlled and filtered with air bleeding valve
Speed is filtered in 20L/min, and one piece of filter paper cake can filter the honeysuckle distillate of 1000L or so.
The present invention also provides the filter plant for realizing above-mentioned filter method, the filter plant includes filtering tank, described
Intermediate bulkhead is equipped in filtering tank, the partition board is equipped with the hole of regular distribution, in the filtering tank side concordant with partition board bottom surface
Portion is equipped with air bleeding valve, and liquid valve is equipped in filtering pot bottom.
Compared with prior art, the advantage of the invention is that：Mode present invention employs naturally osmotic is filtered, will
Filter paper cake is made after making filter paper pulp in filter paper chopping again, and filter paper cake can be by most muddy object absorption wherein, filtering effect
Fruit is good, and the distillate after filtering can be made to reach ideal clarity.
Description of the drawings
Fig. 1 is the structure diagram of filter plant of the present invention；
In figure：1- filtering tanks；2- partition boards；3- air bleeding valves；4- liquid valves.
Specific embodiment
For a better understanding of the present invention, the content that the present invention is furture elucidated with reference to the accompanying drawings and embodiments, but this
The content of invention is not limited solely to the following examples.
Embodiment 1
A kind of filter method of honeysuckle distillate, includes the following steps：
（1）Make filter paper pulp：The middling speed qualitative analysis filter paper that specification is 60 × 60cm is put into shredder and is broken into paper fragment, is taken
8Kg paper fragments are added in the plastic barrel that volume is 80L, are added 0.8Kg piece alkali, are sealed and steaming is passed through in backward plastic barrel
Vapour punching slurry 2-3 days, then the filter paper pulp that steam treatment is crossed is poured into filter bag, rinsed repeatedly with clear water for several times, until test paper is examined
Survey is in neutrality, and filter paper pulp completes；
（2）Make filter paper cake：A filter cloth for being less than 10 mesh is taken to be laid on the intermediate bulkhead 2 in filtering tank 1, the partition board 2
The hole of regular distribution is equipped with, filter paper pulp is poured into filtering tank 1 and is equably laid on partition board 2, patting filter paper pulp makes
It builds real；The liquid valve 4 of filtering pot bottom, while the air bleeding valve 3 of crack filtering tank side are then shut off, is added into filtering tank 1
Enter 85 DEG C of hot water to be totally submerged filter paper pulp, after impregnating 30 minutes, close air bleeding valve 3, open liquid valve 4 and release hot water, most
Filter paper pulp is fully compacted afterwards, the filter paper cake of 6cm thickness is made；
（3）Filter distillate：Honeysuckle distillate is slowly added into filtering tank 1, liquid valve 4 is opened, was controlled with air bleeding valve 3
Filtering velocity degree is filtered for 20L/min, and one piece of filter paper cake can filter the honeysuckle distillate of 1000L or so.
Embodiment 2
A kind of filter method of honeysuckle distillate, includes the following steps：
（1）Make filter paper pulp：The middling speed qualitative analysis filter paper that specification is 60 × 60cm is put into shredder and is broken into paper fragment, is taken
10Kg paper fragments are added in the plastic barrel that volume is 80L, are added 1Kg piece alkali, are sealed and steaming is passed through in backward plastic barrel
Vapour punching slurry 2-3 days, then the filter paper pulp that steam treatment is crossed is poured into filter bag, rinsed repeatedly with clear water for several times, until test paper is examined
Survey is in neutrality, and filter paper pulp completes；
（2）Make filter paper cake：A filter cloth for being less than 10 mesh is taken to be laid on the intermediate bulkhead 2 in filtering tank 1, the partition board 2
The hole of regular distribution is equipped with, filter paper pulp is poured into filtering tank 1 and is equably laid on partition board 2, patting filter paper pulp makes
It builds real；The liquid valve 4 of filtering pot bottom, while the air bleeding valve 3 of crack filtering tank side are then shut off, is added into filtering tank 1
Enter 90 DEG C of hot water to be totally submerged filter paper pulp, after impregnating 25 minutes, close air bleeding valve 3, open liquid valve 4 and release hot water, most
Filter paper pulp is fully compacted afterwards, the filter paper cake of 8cm thickness is made；
（3）Filter distillate：Honeysuckle distillate is slowly added into filtering tank 1, liquid valve 4 is opened, was controlled with air bleeding valve 3
Filtering velocity degree is filtered for 20L/min, and one piece of filter paper cake can filter the honeysuckle distillate of 1000L or so.
Embodiment 3
A kind of filter method of honeysuckle distillate, includes the following steps：
（1）Make filter paper pulp：The middling speed qualitative analysis filter paper that specification is 60 × 60cm is put into shredder and is broken into paper fragment, is taken
10Kg paper fragments are added in the plastic barrel that volume is 80L, are added 1Kg piece alkali, are sealed and steaming is passed through in backward plastic barrel
Vapour punching slurry 2-3 days, then the filter paper pulp that steam treatment is crossed is poured into filter bag, rinsed repeatedly with clear water for several times, until test paper is examined
Survey is in neutrality, and filter paper pulp completes；
（2）Make filter paper cake：A filter cloth for being less than 10 mesh is taken to be laid on the intermediate bulkhead 2 in filtering tank 1, the partition board 2
The hole of regular distribution is equipped with, filter paper pulp is poured into filtering tank 1 and is equably laid on partition board 2, patting filter paper pulp makes
It builds real；The liquid valve 4 of filtering pot bottom, while the air bleeding valve 3 of crack filtering tank side are then shut off, is added into filtering tank 1
Enter 100 DEG C of hot water to be totally submerged filter paper pulp, impregnate after twenty minutes, close air bleeding valve 3, open liquid valve 4 and release hot water, most
Filter paper pulp is fully compacted afterwards, the filter paper cake of 8cm thickness is made；
（3）Filter distillate：Honeysuckle distillate is slowly added into filtering tank 1, liquid valve 4 is opened, was controlled with air bleeding valve 3
Filtering velocity degree is filtered for 20L/min, and one piece of filter paper cake can filter the honeysuckle distillate of 1000L or so.
The measure of filtrate clarity
Each 5g of filtrate sample of embodiment 1-3 acquisitions is weighed respectively, the hydrochloric acid of 5mL37% concentration and 50mL water is added in, shakes up, and is mixed
Heating 5 minutes is closed, lets cool, is then diluted to 100 mL with purified water, as test solution, press《People's Republic of China's medicine
Allusion quotation》Four annex 0902 of version in 2015《Clarity inspection technique》, it is compared with No. 0.5 turbidity standard, measurement result is as follows
Shown in table：
| Comparative example | Embodiment 1 | Embodiment 2 | Embodiment 3 | |
| Clarity | No. 0.5 turbidity standard | It is shallower than the turbidity of No. 0.5 turbidity standard | It is shallower than the turbidity of No. 0.5 turbidity standard | It is shallower than the turbidity of No. 0.5 turbidity standard |
After filter method filtering of the honeysuckle distillate it can be seen from result in table by the present invention, the clarity of filtrate
It is shallower than the turbidity of No. 0.5 turbidity standard, and the method for the present invention is simple for process, easily operated, good filtration effect can make
Distillate after filter reaches ideal clarity.
Claims (2)
1. a kind of filter method of honeysuckle distillate, it is characterised in that：Include the following steps：
（1）Make filter paper pulp：The middling speed qualitative analysis filter paper that specification is 60 × 60cm is put into shredder and is broken into paper fragment, then
Paper fragment and piece alkali are added to by weight the ratio for 10 ︰ 1 in plastic barrel, seals in backward plastic barrel and is passed through steam
Punching slurry 2-3 days, then the filter paper pulp that steam treatment is crossed is poured into filter bag, rinsed repeatedly with clear water for several times, until test paper detects
It is in neutrality, filter paper pulp completes；
（2）Make filter paper cake：A filter cloth for being less than 10 mesh is taken to be laid on the intermediate bulkhead in filtering tank, is set on the partition board
Filter paper pulp is poured into filtering tank and is equably laid on partition board by the hole of regular distribution, and patting filter paper pulp makes it build in fact；
The liquid valve of filtering pot bottom, while the air bleeding valve of crack filtering tank side are then shut off, 80-100 DEG C is added in into filtering tank
Hot water filter paper pulp is totally submerged, impregnate 20-30 minute after, close air bleeding valve, open liquid valve release hot water, finally will filter
Paper pulp is fully compacted, and the filter paper cake of 6-8cm thickness is made；
（3）Filter distillate：Honeysuckle distillate is slowly added into filtering tank, opens liquid valve, is controlled and filtered with air bleeding valve
Speed is filtered in 20L/min, and one piece of filter paper cake can filter the honeysuckle distillate of 1000L or so.
2. a kind of filter plant for realizing above-mentioned filter method, the filter plant includes filtering tank, it is characterised in that：The mistake
Intermediate bulkhead is equipped in filter tank, the partition board is equipped with the hole of regular distribution, in the filtering tank side concordant with partition board bottom surface
Equipped with air bleeding valve, liquid valve is equipped in filtering pot bottom.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201611090248.7A CN108126411A (en) | 2016-12-01 | 2016-12-01 | A kind of filter method and filter plant of honeysuckle distillate |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201611090248.7A CN108126411A (en) | 2016-12-01 | 2016-12-01 | A kind of filter method and filter plant of honeysuckle distillate |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN108126411A true CN108126411A (en) | 2018-06-08 |
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201611090248.7A Pending CN108126411A (en) | 2016-12-01 | 2016-12-01 | A kind of filter method and filter plant of honeysuckle distillate |
Country Status (1)
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| CN (1) | CN108126411A (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN114112770A (en) * | 2021-11-17 | 2022-03-01 | 超威电源集团有限公司 | Method for detecting uniformity of lead paste of negative electrode of lead-acid storage battery |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US5200072A (en) * | 1990-08-16 | 1993-04-06 | Ahlstrom Screen Plates Inc. | Screen plates and methods of manufacture |
| CN203777800U (en) * | 2014-04-23 | 2014-08-20 | 铜陵金典电子科技有限公司 | Negative pressure suction filtration separation device |
-
2016
- 2016-12-01 CN CN201611090248.7A patent/CN108126411A/en active Pending
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US5200072A (en) * | 1990-08-16 | 1993-04-06 | Ahlstrom Screen Plates Inc. | Screen plates and methods of manufacture |
| CN203777800U (en) * | 2014-04-23 | 2014-08-20 | 铜陵金典电子科技有限公司 | Negative pressure suction filtration separation device |
Non-Patent Citations (2)
| Title |
|---|
| 《浙江中草药制剂技术》编写组: "《浙江中草药制剂技术》", 28 February 1978 * |
| 徐艺立等: "深层吸附过滤法在中药水溶液精制中的应用", 《中国药业》 * |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN114112770A (en) * | 2021-11-17 | 2022-03-01 | 超威电源集团有限公司 | Method for detecting uniformity of lead paste of negative electrode of lead-acid storage battery |
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| PB01 | Publication | ||
| PB01 | Publication | ||
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| SE01 | Entry into force of request for substantive examination | ||
| RJ01 | Rejection of invention patent application after publication |
Application publication date: 20180608 |
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| RJ01 | Rejection of invention patent application after publication |