CN108121317A - A kind of ECS hot spot multiple unit control systems for preparing alkynol based compound - Google Patents
A kind of ECS hot spot multiple unit control systems for preparing alkynol based compound Download PDFInfo
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- CN108121317A CN108121317A CN201810121352.0A CN201810121352A CN108121317A CN 108121317 A CN108121317 A CN 108121317A CN 201810121352 A CN201810121352 A CN 201810121352A CN 108121317 A CN108121317 A CN 108121317A
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- 150000001875 compounds Chemical class 0.000 title claims abstract description 32
- 238000003860 storage Methods 0.000 claims abstract description 88
- 238000001914 filtration Methods 0.000 claims abstract description 49
- 238000002156 mixing Methods 0.000 claims abstract description 44
- 239000002994 raw material Substances 0.000 claims abstract description 28
- 239000003054 catalyst Substances 0.000 claims abstract description 16
- 238000006243 chemical reaction Methods 0.000 claims abstract description 14
- -1 ketone compound Chemical class 0.000 claims abstract description 13
- HSFWRNGVRCDJHI-UHFFFAOYSA-N alpha-acetylene Natural products C#C HSFWRNGVRCDJHI-UHFFFAOYSA-N 0.000 claims abstract description 11
- 125000002534 ethynyl group Chemical group [H]C#C* 0.000 claims abstract description 11
- 239000000047 product Substances 0.000 claims description 71
- 230000002950 deficient Effects 0.000 claims description 30
- 239000010865 sewage Substances 0.000 claims description 15
- 238000004821 distillation Methods 0.000 claims description 11
- 238000010438 heat treatment Methods 0.000 claims description 4
- 238000005303 weighing Methods 0.000 claims description 3
- 230000005611 electricity Effects 0.000 claims description 2
- 239000000706 filtrate Substances 0.000 claims description 2
- 150000001345 alkine derivatives Chemical class 0.000 claims 1
- 238000012797 qualification Methods 0.000 claims 1
- 238000003915 air pollution Methods 0.000 abstract description 2
- 238000002360 preparation method Methods 0.000 description 7
- 238000005516 engineering process Methods 0.000 description 4
- 238000000034 method Methods 0.000 description 3
- 239000000203 mixture Substances 0.000 description 3
- 239000000126 substance Substances 0.000 description 3
- 238000010586 diagram Methods 0.000 description 2
- 230000007613 environmental effect Effects 0.000 description 2
- 238000003754 machining Methods 0.000 description 2
- 230000035484 reaction time Effects 0.000 description 2
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 1
- 239000007795 chemical reaction product Substances 0.000 description 1
- 230000006835 compression Effects 0.000 description 1
- 238000007906 compression Methods 0.000 description 1
- 230000007547 defect Effects 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 229910001873 dinitrogen Inorganic materials 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 238000005265 energy consumption Methods 0.000 description 1
- 235000021050 feed intake Nutrition 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 238000012544 monitoring process Methods 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
Classifications
-
- G—PHYSICS
- G05—CONTROLLING; REGULATING
- G05B—CONTROL OR REGULATING SYSTEMS IN GENERAL; FUNCTIONAL ELEMENTS OF SUCH SYSTEMS; MONITORING OR TESTING ARRANGEMENTS FOR SUCH SYSTEMS OR ELEMENTS
- G05B19/00—Programme-control systems
- G05B19/02—Programme-control systems electric
- G05B19/418—Total factory control, i.e. centrally controlling a plurality of machines, e.g. direct or distributed numerical control [DNC], flexible manufacturing systems [FMS], integrated manufacturing systems [IMS] or computer integrated manufacturing [CIM]
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C29/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring
- C07C29/36—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring increasing the number of carbon atoms by reactions with formation of hydroxy groups, which may occur via intermediates being derivatives of hydroxy, e.g. O-metal
- C07C29/38—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring increasing the number of carbon atoms by reactions with formation of hydroxy groups, which may occur via intermediates being derivatives of hydroxy, e.g. O-metal by reaction with aldehydes or ketones
- C07C29/42—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring increasing the number of carbon atoms by reactions with formation of hydroxy groups, which may occur via intermediates being derivatives of hydroxy, e.g. O-metal by reaction with aldehydes or ketones with compounds containing triple carbon-to-carbon bonds, e.g. with metal-alkynes
-
- G—PHYSICS
- G05—CONTROLLING; REGULATING
- G05B—CONTROL OR REGULATING SYSTEMS IN GENERAL; FUNCTIONAL ELEMENTS OF SUCH SYSTEMS; MONITORING OR TESTING ARRANGEMENTS FOR SUCH SYSTEMS OR ELEMENTS
- G05B2219/00—Program-control systems
- G05B2219/20—Pc systems
- G05B2219/26—Pc applications
- G05B2219/2629—Assembly line
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02A—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
- Y02A50/00—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE in human health protection, e.g. against extreme weather
- Y02A50/20—Air quality improvement or preservation, e.g. vehicle emission control or emission reduction by using catalytic converters
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P90/00—Enabling technologies with a potential contribution to greenhouse gas [GHG] emissions mitigation
- Y02P90/02—Total factory control, e.g. smart factories, flexible manufacturing systems [FMS] or integrated manufacturing systems [IMS]
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- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Engineering & Computer Science (AREA)
- Manufacturing & Machinery (AREA)
- Quality & Reliability (AREA)
- Physics & Mathematics (AREA)
- General Physics & Mathematics (AREA)
- Automation & Control Theory (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
The present invention relates to the ECS hot spot multiple unit control systems for preparing alkynol based compound, the first meter is equipped with after first raw material storage still, the second meter is equipped with after second raw material storage still, the 3rd meter is equipped with after catalyst storage kettle, mixing kettle is connected after first meter and the second meter, mixed acetylene and ketone compound and catalyst enter cryogenic high pressure macro reactor and are reacted, first product after reaction enters first product storage still, first product in first product storage still is distilled and filtered into poly- filtering hot spot rectifier unit system in meditation, qualified finished product enters qualified finished room, further comprise the polynary middle control platform of ECS hot spots, an ECS controller is designed between multiple components, all ECS controllers are all connected with the polynary middle control platform of ECS hot spots.It can realize the pipelining of alkynol based compound, and efficient, safe and environment-friendly, reduction air pollution and energy loss.
Description
Technical field
The invention belongs to technical field of compound preparation, are related to a kind of compound preparation system, and in particular to a kind of to prepare
The ECS hot spot multiple unit control systems of alkynol based compound.
Background technology
With the requirement of development of chemical industry, the chemical industry technology for developing green safe environmental protection is chemical industry technology row
Needed for industry.
At present, existing alkynol based compound preparation process is as follows：It is replaced using acetylene and ketone compound below 100 DEG C
Form controllable acetylenic ketone compound；Then again by press pump under 45 DEG C, the protection of 1-2.5 pressure nitrogen gas by-OH foundation group
（Catalyst）It squeezes into isothermal reaction kettle, when reaction 6-8 is small, forms first product；Finally, first product is kept the temperature at 25 DEG C is stored into centainly
Into in next step after quantity, qualified alkynol based compound is distilled out.
But existing preparation process fully relies on manual control safety and danger coefficient, stability is poor, and it is hidden to there is safety
Suffer from.Meanwhile the control such as temperature is unstable, affects product quality, and is difficult to meet the requirements in environmental protection, energy consumption etc..
In view of the above-mentioned technological deficiency of the prior art, there is an urgent need to develop a kind of new to prepare setting for alkynol based compound
Standby and method.
The content of the invention
The defects of it is an object of the invention to overcome the prior art, provides a kind of ECS hot spots for preparing alkynol based compound
Multiple unit control system, the problem of which solving traditional artificial technology controlling and process safety and high danger coefficient, and improve the life of product
The guarantee of yield and quality and safety coefficient, so as to save comprehensive cost for enterprise.
To achieve these goals, the present invention provides following technical solution：
A kind of ECS hot spot multiple unit control systems for preparing alkynol based compound, the first raw material storage still including storing acetylene,
The second raw material storage still of ketone compound and the catalyst storage kettle of storage catalyst are stored, is set after the first raw material storage still
It is equipped with after having the first meter, the second raw material storage still after the second meter, the catalyst storage kettle equipped with the 3rd meter
Measuring device connects mixing kettle after first meter and the second meter, by the acetylene after the mixing kettle mixing weighing and
Ketone compound, which is characterized in that through the mixed acetylene of the mixing kettle and ketone compound and through the 3rd meter
Catalyst after amount enters cryogenic high pressure macro reactor and is reacted, first after the cryogenic high pressure macro reactor reaction
Product enter first product storage still and are stored, the first product in the first product storage still into it is in meditation it is poly- filtering hot spot rectifier unit system into
Row distillation and filtering, the qualified finished product after the quiet poly- filtering hot spot rectifier unit system distillation and filtering enter qualified finished product
Warehouse, further comprises the polynary middle control platform of ECS hot spots, first meter and the second meter and the mixing kettle it
Between, the mixing kettle and the cryogenic high pressure macro reactor, the 3rd meter and the cryogenic high pressure macro reactor
Between, between the cryogenic high pressure macro reactor and the first product storage still, the first product storage still and the quiet poly- filtering
It is designed between hot spot rectifier unit system, between the quiet poly- filtering hot spot rectifier unit system and the qualified finished room
One ECS controller, and all ECS controllers are all connected with the polynary middle control platform of the ECS hot spots.
Further, wherein, the defective products after the quiet poly- filtering hot spot rectifier unit system distillation and filtering enters
Defective products storage still is stored, and the defective products in the defective products storage still enters the mixing kettle to be recycled,
And between the quiet poly- filtering hot spot rectifier unit system and the defective products storage still, the defective products storage still with it is described mixed
Also an ECS controller is respectively equipped between conjunction kettle, and the two ECS controllers are also all flat with the polynary middle control of the ECS hot spots
Platform is connected.
Further, wherein, the cryogenic high pressure macro reactor is line style mixing low temp high-pressure reactor, is used
Infrared microwave multipoint heating mode, temperature are controlled between 32-42 DEG C, and pressure is in 2-3 pas/second.
Yet further, wherein, the quiet poly- filtering hot spot rectifier unit system includes vibration of ultrasonic wave filter, distillation
Device and the far infrared microwave thermal control hot spot on distiller, pass through the far infrared microwave thermal on the distiller
Control hot spot is heated to 95 DEG C of -105 DEG C of progress constant temperature distillation reactions, is then filtered and produced by the vibration of ultrasonic wave filter
Product, the qualified products obtained.
In addition, the ECS hot spot multiple unit control systems for preparing alkynol based compound of the present invention further comprise electrical management
System, and between the first raw material storage still and first meter, the second raw material storage still with described second meter
Between measuring device, between first meter and second meter and the mixing kettle, the mixing kettle and the low temperature
Between high pressure macro reactor, between the 3rd meter and the cryogenic high pressure macro reactor, the cryogenic high pressure it is micro-
Change between reactor and the first product storage still, the first product storage still and the quiet poly- filtering hot spot rectifier unit system it
Between, between the quiet poly- filtering hot spot rectifier unit system and the qualified finished room, the quiet poly- filtering hot spot rectifying fills
Put between system and the defective products storage still, between the defective products storage still and the mixing kettle, the electrical management system
Be designed with a power-supply controller of electric between system and the polynary middle control platform of the ECS hot spots, all power-supply controller of electric all with it is described
Electric power management system is connected.
Further, wherein, the electric power management system and the ECS hot spots it is polynary it is middle control platform between set there are one
ECS controllers, and the ECS controllers are also connected with the polynary middle control platform of the ECS hot spots.
Furthermore the ECS hot spot multiple unit control systems for preparing alkynol based compound of the invention further comprise fire-fighting sewage
Management system, and the electric power management system, fire-fighting sewage management system, the first raw material storage still, the second raw material storage still and
Be designed with a fire-fighting controller in the polynary middle control platform of ECS hot spots, all fire-fighting controllers all with the fire-fighting sewage pipe
Reason system is connected.
Further, wherein, between first meter and second meter and the mixing kettle, described mix
Between kettle and the cryogenic high pressure macro reactor, between the 3rd meter and the cryogenic high pressure macro reactor, institute
State between cryogenic high pressure macro reactor and the first product storage still, the first product storage still with it is described it is quiet it is poly- filtering hot spot rectifying
Between apparatus system, between the quiet poly- filtering hot spot rectifier unit system and the qualified finished room, the quiet poly- filtering
It is designed between hot spot rectifier unit system and the defective products storage still, between the defective products storage still and the mixing kettle
One fire-fighting controller, all fire-fighting controllers are all connected with the fire-fighting sewage management system.
Further, wherein, it is equipped between the fire-fighting sewage management system and the polynary middle control platform of the ECS hot spots
One ECS controller, and the ECS controllers are also connected with the polynary middle control platform of the ECS hot spots.
Yet further, wherein, set between the quiet poly- filtering hot spot rectifier unit system and the qualified finished room
There is the 4th meter.
Compared with existing preparation system, the ECS hot spots multiple unit control system for preparing alkynol based compound tool of the invention
There are following advantageous effects：
1st, it gets up all machining control points by controlling data control in ECS, realizes low-voltage safety control circuit system, really
The shortcomings that ensuring safety, overcoming manual control.
2nd, it uses line style cryogenic high pressure macro reactor and quiet poly- filtering hot spot rectifier unit system, realizes alkynol base
The pipelining of compound, and this method it is efficient, it is safe and environment-friendly, reduce air pollution and energy loss.
Description of the drawings
Fig. 1 is the composition schematic diagram of the ECS hot spot multiple unit control systems for preparing alkynol based compound of the present invention.
Specific embodiment
The present invention is further described with reference to the accompanying drawings and examples, and the content of embodiment is not as the guarantor to the present invention
Protect the limitation of scope.
Fig. 1 shows the composition schematic diagram of the ECS hot spot multiple unit control systems for preparing alkynol based compound of the present invention.Such as
A kind of polynary control system of ECS hot spots for preparing alkynol based compound similar with existing preparation system shown in Fig. 1, of the invention
System also includes the first raw material storage still of storing acetylene（A raw material storage stills in Fig. 1）, storage ketone compound the second raw material storage
Deposit kettle（B raw material storage stills in Fig. 1）With the catalyst storage kettle of storage catalyst.Also, after the first raw material storage still
Equipped with being equipped with the second meter after the first meter, the second raw material storage still, the 3rd be equipped with after the catalyst storage kettle
Meter.First meter is used to measure the amount of the acetylene of reaction.Second meter is used to measure reaction
The amount of ketone compound.3rd meter is used for metered catalyst, such as the amount of-OH foundation group.First meter and
Mixing kettle is connected after second meter, passes through the acetylene and ketone compound after the mixing kettle mixing weighing.
It is different from existing preparation system, in the present invention, through the mixed acetylene of the mixing kettle and ketone compound with
And the catalyst after the 3rd meter metering enters cryogenic high pressure macro reactor and is reacted.Wherein, the low temperature
High pressure macro reactor is line style mixing low temp high-pressure reactor, uses infrared microwave multipoint heating mode, and temperature control exists
Between 32-42 DEG C, pressure is in 2-3 pas/second.
First product after the cryogenic high pressure macro reactor reaction enters first product storage still and is stored.The first product storage
The first product deposited in kettle is distilled and filtered into poly- filtering hot spot rectifier unit system in meditation.The quiet poly- filtering hot spot rectifying dress
Putting system includes vibration of ultrasonic wave filter, distiller and the far infrared microwave thermal control hot spot on distiller.It is logical
The far infrared microwave thermal control hot spot crossed on the distiller is heated to 95 DEG C of -105 DEG C of progress constant temperature distillation reactions, then
By the vibration of ultrasonic wave filter filtering product, the qualified products obtained.
Qualified finished product after the quiet poly- filtering hot spot rectifier unit system distillation and filtering enters qualified finished room.
Defective products after the quiet poly- filtering hot spot rectifier unit system distillation and filtering enters defective products storage still and is stored, institute
The defective products in defective products storage still is stated into the mixing kettle to be recycled,
Meanwhile in the present invention, the ECS hot spot multiple unit control systems for preparing alkynol based compound further comprise ECS heat
The polynary middle control platform of point.Also, between first meter and the second meter and the mixing kettle, the mixing kettle and institute
It states between cryogenic high pressure macro reactor, the 3rd meter and the cryogenic high pressure macro reactor, the cryogenic high pressure
Between macro reactor and the first product storage still, the first product storage still and the quiet poly- filtering hot spot rectifier unit system it
Between, between the quiet poly- filtering hot spot rectifier unit system and the qualified finished room be designed with an ECS controller, and institute
Some ECS controllers are all connected with the polynary middle control platform of the ECS hot spots.
In addition, it is described it is quiet it is poly- filtering hot spot rectifier unit system and the defective products storage still between, the defective products store up
It deposits and an ECS controller is also respectively equipped between kettle and the mixing kettle, and the two ECS controllers are also all warm with the ECS
The polynary middle control platform of point is connected.
In this way, it gets up all machining control points by controlling data control in ECS, low-voltage safety control circuit is realized
System, it is ensured that safety, the shortcomings that overcoming manual control.
Meanwhile in the present invention, it is, for example, the macro reactor of 20L by feedstock transportation to volume by streamline compression pump
In, and conveyance conduit monitors reaction rate and temperature whenever and wherever possible in ESC monitoring control devices, controls the speed of reaction mass
Degree is come the safety that reduces manually and feed intake.When small compared with traditional reaction kettle reaction time 6-8, and contracted significantly using macro reactor
The short reaction time, it is only necessary to which when 2-4 is small, and reaction rate is also quickly, so as to save the loss of personnel cost and material.
Furthermore in the present invention, the ECS hot spot multiple unit control systems for preparing alkynol based compound of the invention further wrap
Include electric power management system.And between the first raw material storage still and first meter, the second raw material storage still with
Between second meter, between first meter and second meter and the mixing kettle, the mixing kettle
Between the cryogenic high pressure macro reactor, between the 3rd meter and the cryogenic high pressure macro reactor, it is described
Between cryogenic high pressure macro reactor and the first product storage still, the first product storage still fills with the quiet poly- filtering hot spot rectifying
Put between system, between the quiet poly- filtering hot spot rectifier unit system and the qualified finished room, the quiet poly- filtering heat
Between point rectifier unit system and the defective products storage still, between the defective products storage still and the mixing kettle, the electricity
A power-supply controller of electric, all power-supply controller of electric are designed between power management system and the polynary middle control platform of the ECS hot spots
All it is connected with the electric power management system.In this way, the control of power supply is convenient for, so as to control heating.
Preferably, ECS is controlled there are one being set between the electric power management system and the polynary middle control platform of the ECS hot spots
Device, and the ECS controllers are also connected with the polynary middle control platform of the ECS hot spots.
Furthermore the ECS hot spot multiple unit control systems for preparing alkynol based compound of the invention further comprise fire-fighting sewage
Management system.And the electric power management system, fire-fighting sewage management system, the first raw material storage still, the second raw material storage still and
Be designed with a fire-fighting controller in the polynary middle control platform of ECS hot spots, all fire-fighting controllers all with the fire-fighting sewage pipe
Reason system is connected.
And, it is preferable that between first meter and second meter and the mixing kettle, the mixing kettle
Between the cryogenic high pressure macro reactor, between the 3rd meter and the cryogenic high pressure macro reactor, it is described
Between cryogenic high pressure macro reactor and the first product storage still, the first product storage still fills with the quiet poly- filtering hot spot rectifying
Put between system, between the quiet poly- filtering hot spot rectifier unit system and the qualified finished room, the quiet poly- filtering heat
One is designed between point rectifier unit system and the defective products storage still, between the defective products storage still and the mixing kettle
A fire-fighting controller, all fire-fighting controllers are all connected with the fire-fighting sewage management system.
In this way, it is controlled and is managed convenient for offseting bilge water resisting.
It is highly preferred that being set between the fire-fighting sewage management system and the polynary middle control platform of the ECS hot spots, there are one ECS
Controller, and the ECS controllers are also connected with the polynary middle control platform of the ECS hot spots.
Finally, it is preferable that the is equipped between the quiet poly- filtering hot spot rectifier unit system and the qualified finished room
Four meters.In this way, obtain the amount of qualified finished product convenient for metering.
The above embodiment of the present invention is only intended to clearly illustrate example of the present invention, and is not to the present invention
Embodiment restriction.For those of ordinary skill in the art, can also make on the basis of the above description
Other various forms of variations or variation.Here all embodiments can not be exhaustive.Every skill for belonging to the present invention
The obvious changes or variations that art scheme is extended out is still in the row of protection scope of the present invention.
Claims (10)
1. a kind of ECS hot spot multiple unit control systems for preparing alkynol based compound, the first raw material storage including storing acetylene
The catalyst storage kettle of kettle, the second raw material storage still for storing ketone compound and storage catalyst, the first raw material storage still
Be equipped with the first meter afterwards, the second meter, the catalyst storage kettle are equipped with after the second raw material storage still after be equipped with the
Three meters connect mixing kettle after first meter and the second meter, pass through the second after the mixing kettle mixing weighing
Alkynes and ketone compound, which is characterized in that through the mixed acetylene of the mixing kettle and ketone compound and through the described 3rd metering
Catalyst after device metering enters cryogenic high pressure macro reactor and is reacted, after the cryogenic high pressure macro reactor reaction
First product enter first product storage still and stored, the first product in the first product storage still is into poly- filtering hot spot rectifier unit system in meditation
System is distilled and filtered, and the qualified finished product after the quiet poly- filtering hot spot rectifier unit system distillation and filtering enters qualification
Finished room further comprises the polynary middle control platform of ECS hot spots, first meter and the second meter and the mixing kettle
Between, the mixing kettle and the cryogenic high pressure macro reactor, the 3rd meter react with the cryogenic high pressure macro
Between device, between the cryogenic high pressure macro reactor and the first product storage still, the first product storage still quiet gathered with described
It is all set between filter hot spot rectifier unit system, between the quiet poly- filtering hot spot rectifier unit system and the qualified finished room
There are one ECS controllers, and all ECS controllers are all connected with the polynary middle control platform of the ECS hot spots.
2. the ECS hot spot multiple unit control systems according to claim 1 for preparing alkynol based compound, which is characterized in that warp
Defective products after the quiet poly- filtering hot spot rectifier unit system distillation and filtering enters defective products storage still and is stored, described
Defective products in defective products storage still enters the mixing kettle to be recycled, and the quiet poly- filtering hot spot rectifier unit
An ECS is also respectively equipped between system and the defective products storage still, between the defective products storage still and the mixing kettle
Controller, and the two ECS controllers are also all connected with the polynary middle control platform of the ECS hot spots.
3. the ECS hot spot multiple unit control systems according to claim 2 for preparing alkynol based compound, which is characterized in that institute
Cryogenic high pressure macro reactor is stated as line style mixing low temp high-pressure reactor, uses infrared microwave multipoint heating mode, temperature
Control is between 32-42 DEG C, and pressure is in 2-3 pas/second.
4. the ECS hot spot multiple unit control systems according to claim 3 for preparing alkynol based compound, which is characterized in that institute
Stating quiet poly- filtering hot spot rectifier unit system includes vibration of ultrasonic wave filter, distiller and the far infrared on distiller
Microwave thermal control hot spot, by the far infrared microwave thermal control hot spot on the distiller be heated to 95 DEG C -105 DEG C into
Row constant temperature distillation reaction, then by the vibration of ultrasonic wave filter filtering product, the qualified products obtained.
5. the ECS hot spot multiple unit control systems according to claim 4 for preparing alkynol based compound, which is characterized in that into
One step include electric power management system, and between the first raw material storage still and first meter, second raw material storage
Deposit between kettle and second meter, between first meter and second meter and the mixing kettle, it is described
Between mixing kettle and the cryogenic high pressure macro reactor, the 3rd meter and the cryogenic high pressure macro reactor it
Between, between the cryogenic high pressure macro reactor and the first product storage still, the first product storage still and the quiet poly- filtering heat
Between point rectifier unit system, between the quiet poly- filtering hot spot rectifier unit system and the qualified finished room, it is described quiet
Between poly- filtering hot spot rectifier unit system and the defective products storage still, the defective products storage still and the mixing kettle it
Between, the electric power management system and the ECS hot spots it is polynary it is middle control platform between be designed with a power-supply controller of electric, all electricity
Source controller is all connected with the electric power management system.
6. the ECS hot spot multiple unit control systems according to claim 5 for preparing alkynol based compound, which is characterized in that institute
State ECS controllers there are one being set between electric power management system and the polynary middle control platform of the ECS hot spots, and the ECS controllers
It is connected with the polynary middle control platform of the ECS hot spots.
7. the ECS hot spot multiple unit control systems according to claim 6 for preparing alkynol based compound, which is characterized in that into
One step include fire-fighting sewage management system, and the electric power management system, fire-fighting sewage management system, the first raw material storage still,
A fire-fighting controller is designed in second raw material storage still and the polynary middle control platform of ECS hot spots, all fire-fighting controllers are all
It is connected with the fire-fighting sewage management system.
8. the ECS hot spot multiple unit control systems according to claim 7 for preparing alkynol based compound, which is characterized in that institute
It states between the first meter and second meter and the mixing kettle, the mixing kettle is reacted with the cryogenic high pressure macro
Between device, between the 3rd meter and the cryogenic high pressure macro reactor, the cryogenic high pressure macro reactor and institute
State between first product storage still, between the first product storage still and the quiet poly- filtering hot spot rectifier unit system, described quiet gathered
Filter between hot spot rectifier unit system and the qualified finished room, the quiet poly- filtering hot spot rectifier unit system with it is described not
A fire-fighting controller is designed between non-defective unit storage still, between the defective products storage still and the mixing kettle, all disappears
Proof controller is all connected with the fire-fighting sewage management system.
9. the ECS hot spot multiple unit control systems according to claim 8 for preparing alkynol based compound, which is characterized in that institute
It states and is set between fire-fighting sewage management system and the polynary middle control platform of the ECS hot spots there are one ECS controllers, and the ECS is controlled
Device is also connected with the polynary middle control platform of the ECS hot spots.
10. the ECS hot spot multiple unit control systems for preparing alkynol based compound according to any one of claim 1-9,
It is characterized in that, the 4th meter is equipped between the quiet poly- filtering hot spot rectifier unit system and the qualified finished room.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810121352.0A CN108121317A (en) | 2018-02-07 | 2018-02-07 | A kind of ECS hot spot multiple unit control systems for preparing alkynol based compound |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810121352.0A CN108121317A (en) | 2018-02-07 | 2018-02-07 | A kind of ECS hot spot multiple unit control systems for preparing alkynol based compound |
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| CN105924330A (en) * | 2016-06-29 | 2016-09-07 | 西南化工研究设计院有限公司 | Reactor and reaction system for synthesizing methylbutynol |
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| US4847440A (en) * | 1987-09-04 | 1989-07-11 | Huels Aktiengesellschaft | Method of manufacturing propynol |
| CN1769254A (en) * | 2004-10-29 | 2006-05-10 | 中国石油化工股份有限公司 | Method for synthesizing alkynol by ketone and acetylene |
| CN101503635A (en) * | 2009-03-06 | 2009-08-12 | 武汉奥泰自动化工程有限责任公司 | Control device for oxygenation intermittent coal gas preparation |
| CN102830625A (en) * | 2012-09-10 | 2012-12-19 | 江苏科技大学 | Process control system and method based on neural network predictive control |
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| CN103896737A (en) * | 2014-03-31 | 2014-07-02 | 南京工业大学 | Method for preparing propargyl alcohol by utilizing microstructure reactor |
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Application publication date: 20180605 |