CN108070508A - A kind of solid material continuous distillation plant and distillating method - Google Patents
A kind of solid material continuous distillation plant and distillating method Download PDFInfo
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- CN108070508A CN108070508A CN201711374405.1A CN201711374405A CN108070508A CN 108070508 A CN108070508 A CN 108070508A CN 201711374405 A CN201711374405 A CN 201711374405A CN 108070508 A CN108070508 A CN 108070508A
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- distillation
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- C—CHEMISTRY; METALLURGY
- C12—BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
- C12H—PASTEURISATION, STERILISATION, PRESERVATION, PURIFICATION, CLARIFICATION OR AGEING OF ALCOHOLIC BEVERAGES; METHODS FOR ALTERING THE ALCOHOL CONTENT OF FERMENTED SOLUTIONS OR ALCOHOLIC BEVERAGES
- C12H6/00—Methods for increasing the alcohol content of fermented solutions or alcoholic beverages
- C12H6/02—Methods for increasing the alcohol content of fermented solutions or alcoholic beverages by distillation
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- General Engineering & Computer Science (AREA)
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- Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)
Abstract
The present invention relates to a kind of solid material continuous distillation plant and distillating methods.Solid material continuous distillation plant, including：Screw feeding device, the screw feeding device includes spiral mesh roll body, spiral mesh its periphery is provided with multiple independent, closing distillation stations, and the solid material overturns multiple independent, closing the distillation stations set through spiral mesh its periphery forward in spiral mesh roller and realizes continuous still.The continuous still of solid material can be achieved in the present invention, and material contacts fully in the state of relative loose with steam in distillation process, is conducive to material distillation completely, material utilization is high.
Description
Technical field
The invention belongs to retort fields, and in particular to a kind of solid material continuous distillation plant and distillating method.
Background technology
The characteristics of traditional intermittent teaming bucket distillation is that rice steamer bottom heating residual water generates steam, high-temperature steam by rice steamer comb on it is quiet
Contact of the fermented grain material that state uniformly dispenses with material generates physical and chemical effect, so as to progressively by the alcohol in fermented grain and various low
Boilers gasify, and generate alcohol in high concentration steam, win to obtain the wine liquid of different qualities by classification after condensation.During this
There are the problem of be：In the static distillation process of fermented grain, since steam and fermented grain being needed to come into full contact with, it is necessary to which fermented grain dispensed
Try one's best in journey uniformity, no matter but manually dispensed in actual mechanical process or equipment dispense all be difficult accomplish it is complete equal
It is even；Separately due to needing to obtain the wine liquid of high concentration, so can must be more thick and solid fermented grain heap so that steam can be with more materials
It contacts and absorbs to saturation alcohol and other low-boiling point materials as far as possible so as to improve out wine concentration, but the extruding that solid accumulation is brought
It is incomplete in distillation process that power has been further exacerbated by local fermented grain；Simultaneously because the open working side of intermittent teaming bucket distillation
Formula needs repeatedly loaded steamer to go out rice steamer in production process, and work efficiency is relatively low, equipment sealing and preventive means deficiency, thus alcohol into
Point volatilization loss, the loss shifted repeatedly of material is difficult to avoid that.
The content of the invention
The technical problems to be solved by the invention are in view of the deficiencies of the prior art and provide a kind of solid material continuous steaming
Distillation unit and distillating method.The continuous still of the achievable solid material of the present invention, material is in the shape of relative loose in distillation process
Under state and steam contact is abundant, is conducive to material distillation completely, material utilization is high.
To achieve the above object, the technical solution that the present invention takes is as follows：
A kind of solid material continuous distillation plant is provided, including：Screw feeding device, the screw feeding device include
Spiral mesh roll body, spiral mesh its periphery are provided with multiple independent, closing distillation stations, and the solid material exists
Multiple independent, closing the distillation stations set through spiral mesh its periphery forward are overturn in spiral mesh roller to realize continuously
Distillation.
By said program, the spiral mesh its periphery is correspondingly arranged upper chamber and lower chamber respectively, upper chamber and
Lower chamber corresponds to the distillation station of one closing of composition.
By said program, the upper chamber and lower chamber are preferably semi-loop, are symmetrically installed in outside spiral mesh roller
Week.
By said program, pressure sensor is provided in the middle part of each upper chamber and lower chamber.
By said program, each upper chamber distilled in workshop section and lower chamber number are multiple, each upper chamber and lower gas
Room is mutually independent, and each upper chamber is connected with the adjacent lower chamber being located at thereafter by external pipe, each distills workshop section
In each lower chamber in addition to the first lower chamber be equipped with force (forcing) pump；The last one upper chamber of each distillation workshop section is equipped with exhaust pump,
Remaining upper chamber is pumped equipped with return-air.
By said program, the solid material continuous distillation plant further includes steam conveying main pipeline, steam conveying master
Multiple steam conveying branches are provided on pipeline, each steam conveying branch is connected with the lower chamber of each distillation station, and each steam is defeated
Branch road is sent to be equipped with steam control valve；When the lower chamber of each distillation workshop section has multiple, the steam conveying branch and each steaming
The first lower chamber for evaporating workshop section is connected.
By said program, each vapor inlet port in the solid material continuous distillation plant is provided with steam flow biography
Sensor and temperature sensor.
By said program, the screw feeding device includes the helical blade being provided at its inner portion, and solid material is in spiral shell
The overturning conveying forward in spiral mesh roller under the action of vane piece.Compared to other traditional plate chain type conveying device conveyings
More efficient, rotary structure can realize good mechanical seal, reach more preferably continuous still effect.
By said program, the charging rate of the screw feeding device is adjustable.
By said program, the mesh aperture of the spiral mesh roller is less than the grain size of solid material, and solid material exists
Not material leakage in continuous process of distillation.
By said program, the solid material continuous distillation plant further includes the cylindrical case with heat insulation function, spiral shell
Rotation mesh roller and distillation station are located in cylindrical case, form full-closed structure.
By said program, the solid material continuous distillation plant further include with each distillation station be correspondingly arranged it is cold
Solidifying collection device.
A kind of solid material continuous distillation process is provided, solid material is sent into screw feeding device, solid material is in spiral shell
Constantly overturning conveying forward in mesh roller is revolved, is passed through steam to lower chamber when distillation starts, steam passes through under differential pressure action
Mesh on spiral mesh roller, which enters in spiral mesh roller to be sufficiently mixed to contact with material, completes a distillation station workshop section
It extracts, material completes the extraction of each distillation station section successively by each distillation station in lasting overturning transmission process afterwards.
By said program, when the upper chamber and lower chamber that distill station area are multiple, when distillation starts under first
Gas chamber is passed through steam, and steam enters by the mesh on spiral mesh roller in spiral mesh roller to be sufficiently mixed with solid material
Discharge is pumped by the return-air of the first upper chamber after contact, then through external pipe be delivered to adjacent lower chamber and pressurized pump it is appropriate plus
Pressure output, so as to which the solid material again with spiral mesh roller contacts mixing, and so on so that solid material is relatively loose
With the steam of the reciprocal gradual flowing between lower chamber and upper chamber sufficiently mix and contact so as to complete in the state of dissipating
Into the extraction of a distillation station workshop section.
By said program, the flow of steam at monitoring distillation station section in distillation process, temperature, the pressure of upper lower chamber and
Pressure differential, and need such as vapor (steam) temperature, distillation degree etc. adjusted according to technique, it can specifically be adjusted by adjusting steam
Valve, force (forcing) pump and return-air pump are realized and adjusted.
By said program, the charging rate for needing to adjust solid material according to technique is further included in distillation process.
Fermented grain accumulation of thick in traditional liquor production process, dispenses uneven, and the distillation of local fermented grain is not exclusively, it is necessary to repeatedly
Loaded steamer goes out rice steamer, and work efficiency is relatively low, equipment sealing and preventive means deficiency, so that the volatilization loss of alcoholic content, material are repeatedly
The loss of transfer is difficult to avoid that.It is analyzed with reference to its operating feature, studies carefully the essence of its distillation process, be to need to allow steam and foot
Enough fermented grains sufficiently contact, so as to using the heat of steam cause alcohol in fermented grain and other low boiling point fragrance matters by
It is discharged after step gasification with steam, the wine liquid of concentration needed for generation after condensed device condensation.On this basis, the present invention proposes
State continuous distillation method.
Beneficial effects of the present invention
Continuous distillation plant and distillating method provided by the invention, by taking solid material fermented grain as an example, with traditional liquor production process
Middle fermented grain distillation process is compared, and is had the following advantages：
1st, solid material is overturn during conveying in spiral mesh roller relatively loose in continuous still provided by the invention
With the steam of the reciprocal gradual flowing between lower chamber and upper chamber sufficiently mix and contact so as to complete in the state of dissipating
Into distillation, fermented grain distillation is complete, may be such that the remaining utility in fermented grain is few；
2nd, continuous still provided by the invention be by formula continuous still, it is efficient there is no interval and stand-by period；
3rd, wine process control is plucked, by adjusting the different length for distilling workshop sections and the temperature of input steam, pressure, flow, material
Conveying speed etc. may be such that the wine of the required vinosity of different workshop section's outputs and concentration, the flow and temperature of steam, material it is defeated
Send speed and pressure etc. that can be obtained very by the combination temperatures such as steam control valve, arrangements for speed regulation, pressure and flow sensor
Good control；
4th, volatilizing, leakage loss is small, and distillation can carry out under the conditions of totally-enclosed, and spiral mesh roller is convenient for using good machinery
Formula sealing can minimize the volatilization leakage loss of low boiling point active principle；
5th, enclosed structure is convenient for good external sealing thermal insulation measure, can drop steam and radiation heat loss in distillation process
Extremely minimum, thermal losses is small.
Description of the drawings
Fig. 1 is the solid material continuous distillation plant schematic diagram of the present invention.In figure：1. 2. upper chamber of condensate recycling device
3. 7. exhaust pump of spiral mesh roller 4. lower chamber, 5. steam control valve, 6. force (forcing) pump, 8. return-air pumps, 9 steam pipelines
Road, 10 steam conveying branch, 11 cylindrical cases.
Fig. 2 is the side view of the solid material continuous distillation plant of the present invention.
Specific embodiment
As shown in Figure 1, solid material continuous distillation plant, including screw feeding device, the screw feeding device bag
Spiral mesh roller 3 and helical blade are included, the spiral mesh roller mesh aperture is less than solid material grain size, solid material
The not material leakage in continuous process of distillation, spiral mesh its periphery are provided with five sections of distillation station sections, every section of distillation station section by
The multiple upper chambers 2 and lower chamber 4 for being correspondingly arranged at spiral mesh its periphery form, every section distillation station section in upper chamber and
The number of lower chamber is 3, and each upper chamber and lower chamber are mutually independent, each upper chamber and it is adjacent be located at thereafter under
Gas chamber is connected by external pipe, and each each lower chamber distilled in station section in addition to the first lower chamber is equipped with force (forcing) pump 6, each
The last one upper chamber for distilling station section is equipped with exhaust pump 7, remaining upper chamber is equipped with return-air and pumps 8.The spiral charging dress
The charging rate put is adjustable；The solid material continuous distillation plant further includes steam conveying main pipeline 9, steam conveying main pipeline
On be provided with multiple steam conveying branches 10, each steam conveying branch is connected with each the first lower chamber for distilling station, steam
It conveys branch road and is equipped with steam control valve 6.
Further, each vapor inlet port in distillation zone in the solid material continuous distillation plant is provided with steam stream
Pressure sensor is provided in the middle part of quantity sensor and temperature sensor, each upper chamber and lower chamber.
Further, the solid material continuous distillation plant further includes the cylindrical case 11 with heat insulation function, spiral shell
Revolve mesh roller and distillation station（Lower chamber, upper chamber, external pipe, force (forcing) pump, return-air pump and exhaust pump etc.）It is located at tubular
In shell, full-closed structure is formed.
Further, the condensation that the solid material continuous distillation plant is further included with each distillation station is correspondingly arranged
Collection device 1.
The technique that solid material continuous still is carried out using above-mentioned solid material continuous distillation plant, by solid cooking wine a word used in place name
Screw feeding device to be sent into, starts screw feeding device, constantly overturning conveys wine a word used in place name forward in spiral mesh roller, while to
First lower chamber is passed through steam, and steam enters by the mesh on spiral mesh roller in spiral mesh roller under differential pressure action
It is sufficiently mixed with solid material after contacting and discharge is pumped by the return-air of the first upper chamber, then adjacent lower gas is delivered to through external pipe
Room and the appropriate pressurization output of pressurized pump, so as to which the solid material again with spiral mesh roller contacts mixing, and so on, make
Steam back and forth passed through from each lower chamber and upper chamber, steam from each lower chamber and upper chamber be reciprocated through during with continue
The loose solid material of overturning conveying comes into full contact with so that the target component in solid material is sufficiently distilled extraction, completes
One distills the extraction of station workshop section, and material completes each steaming successively by each distillation station in lasting overturning transmission process afterwards
Evaporate the extraction of station section.
Workshop section's quantity, either simplex segment length, each workshop section's gas chamber quantity can be distilled with reference to fermented grain in above-mentioned continuous distillation plant
The characteristics of demand of wine is plucked in segmentation in journey, is adjusted according to each technique needs.Each workshop section can be according to different quality and concentration
Demand carry out length adjustment, so as to realize segmentation win on the basis of meet the needs of to different quality and concentration.Each
Distillation workshop section is not limited to the length of the signal in diagram, and the length of each workshop section can be adjusted according to actual process demand, regulates and controls each work
The length combination mode of section.In addition, steam flow, temperature, the pressure of upper lower chamber and pressure differential, reflow's cycle in distillation process
And material conveying speed etc., it can be also adjusted flexibly according to the process requirements of different workshop sections, it specifically can be by being fed to spiral
Pump pressure and the number of upper lower chamber that the charging rate of device, the aperture of steam control valve, force (forcing) pump and return-air pump etc. are adjusted
Section is realized, from there through control so that distillation ingredient and concentration are effectively controlled.
Claims (11)
1. a kind of solid material continuous distillation plant, it is characterised in that：It includes：Screw feeding device, spiral charging
Device includes spiral mesh roll body, and spiral mesh its periphery is provided with multiple independent, closing distillation stations, described solid
State material overturns multiple independent, closing the distillation stations set through spiral mesh its periphery forward in spiral mesh roller
Realize continuous still.
2. solid material continuous distillation plant according to claim 1, it is characterised in that：Outside the spiral mesh roller
It is correspondingly arranged upper chamber and lower chamber week respectively, upper chamber and lower chamber correspond to the distillation station of one closing of composition.
3. solid material continuous distillation plant according to claim 2, it is characterised in that：The upper chamber and lower chamber are
Semi-loop is symmetrically installed in spiral mesh its periphery；Pressure sensor is provided in the middle part of each upper chamber and lower chamber.
4. solid material continuous distillation plant according to claim 2, it is characterised in that：Upper gas in each distillation workshop section
Room and lower chamber number are multiple, and each upper chamber and lower chamber are mutually independent, each upper chamber and adjacent are located at thereafter
Lower chamber connected by external pipe, each each lower chamber distilled in workshop section in addition to the first lower chamber is equipped with force (forcing) pump；Often
The last one upper chamber of a distillation workshop section is equipped with exhaust pump, remaining upper chamber is pumped equipped with return-air.
5. solid material continuous distillation plant according to claim 1, it is characterised in that：The solid material continuous steaming
Distillation unit further includes steam conveying main pipeline, and multiple steam conveying branches, each steam conveying are provided on steam conveying main pipeline
Branch is connected with the lower chamber of each distillation station, and each steam conveying branch road is equipped with steam control valve；Under the distillation workshop section
When gas chamber has multiple, the steam conveying branch is connected with the first upper chamber of each distillation workshop section；The solid material is continuous
Each vapor inlet port in distillation zone in distilling apparatus is provided with steam flow sensor and temperature sensor.
6. solid material continuous distillation plant according to claim 1, it is characterised in that：The spiral mesh roller
Mesh aperture is less than the grain size of solid material, solid material not material leakage in continuous process of distillation.
7. solid material continuous distillation plant according to claim 1, it is characterised in that：The solid material continuous steaming
Distillation unit further includes the cylindrical case with heat insulation function, and spiral mesh roller and distillation station are located in cylindrical case, are formed
Full-closed structure.
8. solid material continuous distillation plant according to claim 1, it is characterised in that：The screw feeding device bag
Include the helical blade being provided at its inner portion, solid material overturns forward under the action of helical blade in spiral mesh roller defeated
It send；The charging rate of the screw feeding device is adjustable；
The condensate collection device that the solid material continuous distillation plant is further included with each distillation station is correspondingly arranged.
9. based on the solid material continuous distillation process of solid material continuous distillation plant described in claim 1, feature exists
In：Solid material is sent into screw feeding device, starts screw feeding device, solid material in spiral mesh roller constantly to
Preceding overturning conveying, while steam is passed through to lower chamber, steam enters under differential pressure action by the mesh on spiral mesh roller
The extraction for contacting and completing a distillation station workshop section is sufficiently mixed in spiral mesh roller with material, material is defeated in lasting overturning afterwards
During sending the extraction of each distillation station section is completed by each distillation station successively.
10. technique according to claim 9, it is characterised in that：When the upper chamber and lower chamber in distillation station area are more
When a, steam is passed through to the first lower chamber when distillation starts, steam enters spiral mesh by the mesh on spiral mesh roller
It is sufficiently mixed in roller with solid material after contacting and discharge is pumped by the return-air of the first upper chamber, then be delivered to through external pipe adjacent
Lower chamber and the appropriate pressurization output of pressurized pump, so as to which the solid material again with spiral mesh roller contacts mixing, so
Back and forth so that the steam of solid material reciprocal gradual flowing in the state of relative loose and between lower chamber and upper chamber into
The extraction of a distillation station workshop section is completed in row sufficiently mixing and contact.
11. technique according to claim 10, it is characterised in that：The solid material is wine a word used in place name material；Distillation process
The flow of steam, temperature, the pressure and pressure differential of upper lower chamber at middle monitoring distillation station section, and according to technique need to its into
Row is adjusted；The charging rate of solid material is adjusted in distillation process as needed.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201711374405.1A CN108070508A (en) | 2017-12-19 | 2017-12-19 | A kind of solid material continuous distillation plant and distillating method |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201711374405.1A CN108070508A (en) | 2017-12-19 | 2017-12-19 | A kind of solid material continuous distillation plant and distillating method |
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| Publication Number | Publication Date |
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| CN108070508A true CN108070508A (en) | 2018-05-25 |
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201711374405.1A Pending CN108070508A (en) | 2017-12-19 | 2017-12-19 | A kind of solid material continuous distillation plant and distillating method |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110042035A (en) * | 2019-04-29 | 2019-07-23 | 北京百漾酒业科技股份有限公司 | A kind of continuous distillation plant and method of white wine |
| CN114752443A (en) * | 2022-03-27 | 2022-07-15 | 郭勇 | Cosmetic raw material distillation extraction separator |
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| CN103215137A (en) * | 2013-05-08 | 2013-07-24 | 宜宾学院 | Method for continuously distilling aromatic oil by subsectional temperature control |
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| CN107384720A (en) * | 2017-08-31 | 2017-11-24 | 潘建军 | A kind of segment reflux solid continuous distillation machine and its distillating method |
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2017
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Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN201351159Y (en) * | 2009-02-12 | 2009-11-25 | 黄亚东 | Continuous distillation equipment for producing distilled spirits by solid-state fermentation method |
| CN201781923U (en) * | 2010-09-13 | 2011-04-06 | 南宁市创宇茶叶机械有限公司 | Drum type superheated steam fixation machine |
| CN103215137A (en) * | 2013-05-08 | 2013-07-24 | 宜宾学院 | Method for continuously distilling aromatic oil by subsectional temperature control |
| CN105685273A (en) * | 2014-11-27 | 2016-06-22 | 贵州开阳蓝芝茶叶开发有限责任公司 | Steam enzyme deactivation device for summer and autumn tea |
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110042035A (en) * | 2019-04-29 | 2019-07-23 | 北京百漾酒业科技股份有限公司 | A kind of continuous distillation plant and method of white wine |
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| CN114752443A (en) * | 2022-03-27 | 2022-07-15 | 郭勇 | Cosmetic raw material distillation extraction separator |
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