CN108059450A - A kind of environment-friendly type dichroite-mullite kiln furnitures and preparation method thereof - Google Patents
A kind of environment-friendly type dichroite-mullite kiln furnitures and preparation method thereof Download PDFInfo
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- CN108059450A CN108059450A CN201711437792.9A CN201711437792A CN108059450A CN 108059450 A CN108059450 A CN 108059450A CN 201711437792 A CN201711437792 A CN 201711437792A CN 108059450 A CN108059450 A CN 108059450A
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- C04B35/00—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
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- C04B35/01—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on oxide ceramics
- C04B35/16—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on oxide ceramics based on silicates other than clay
- C04B35/18—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on oxide ceramics based on silicates other than clay rich in aluminium oxide
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- C04B2235/32—Metal oxides, mixed metal oxides, or oxide-forming salts thereof, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
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Abstract
A kind of environment-friendly type cordierite-mullite kiln furnitures include the raw material of following parts by weight：25 35 parts of waste old ceramics, 12 22 parts of cordierite-mullite clinker, wash ball clay 30 45, 10 15 parts of andalusite, 8 13 parts of talcum powder, 5 15 parts of kyanite, industrial 5 12 parts of alpha-aluminium oxide powder, with waste old ceramics, cordierite-mullite clinker, andalusite is aggregate, introduce washing ball clay, talcum powder, kyanite, industrial alpha-aluminium oxide powder forms the solids of the kiln furnitures composite material of the present invention for host material, 25 35% are reached to the utilization rate of waste old ceramics, reduce the waste to resource, also reduce the production cost of kiln furniture material, cordierite-mullite kiln furnitures product density obtained is low, light weight, strength at normal temperature is high, apparent porosity is high, good thermal shock stability, energy-efficient performance is good.
Description
Technical field
The invention belongs to kiln furniture material fields, and in particular to a kind of environment-friendly type dichroite-mullite kiln furnitures and its preparation side
Method.
Background technology
To being used to support the kiln furnitures of burnt product in kiln, it is desirable that the characteristics of its thermal shock resistance will be got well, low energy consumption, violet are blue or green
Stone-mullite material since its coefficient of expansion is low, high temperature resistance is used as by force high-grade kiln furniture material, but due to cordierite,
Mullite material cost is just very high and synthetic material to burn till that rate is low, cause the production cost of dichroite-mullite kiln furnitures it is high,
Waste material is more, and development is restricted；In addition the body of existing cordierite-mullite kiln furniture materials is close for 1.75-2.15g/cm3, production
Product weight is big, heat absorption is just more, and the fuel consumed when being used to raw materials for production and in kiln is big.
Waste old ceramics are the waste materials generated in Production of Ceramics production process or have lost the ceramics of use value, common
Processing method is degrade processing and landfill, causes the waste of material, while certain harmful effect is also caused to environment, is needed
Further improve.
The content of the invention
The shortcomings that the purpose of the present invention is overcoming the prior art, provide a kind of environment-friendly type dichroite-mullite kiln furnitures and its
Preparation method.
The present invention adopts the following technical scheme that：
A kind of environment-friendly type dichroite-mullite kiln furnitures include the raw material of following parts by weight：25-35 parts of waste old ceramics, violet are blue or green
Stone -12-22 parts of Mullite grogs, washing ball clay 30-45,10-15 parts of andalusite, 8-13 parts of talcum powder, 5-15 parts of kyanite,
Industry -5-12 parts of alpha-alumina.
Further, the waste old ceramics are according to metering percentage meter, including following chemical composition：Al2O3：20-
28%th, SiO2：70-75%, K2O：2-5%.
Further, the granularity of the waste old ceramics is 0-0.5um.
Further, Chun Du≤96% of the industry-alpha-alumina.
A kind of production method of environment-friendly type dichroite-mullite kiln furnitures, includes the following steps：
(1), batch mixing：After the raw material of dichroite-mullite kiln furnitures is weighed by its parts by weight, batch mixer stirring 10- is put into
15min, places into edge runner plus water-powered roller presses 20-25min；
(2), ageing mixture：The mixture that step (1) obtains is fitted into hopper at a temperature of 35-40 DEG C, preserves 28-36h；
(3), compression moulding：According to the shape for the kiln furnitures product to be made, kiln furnitures product green compact are made；
(4), it is dry：Green compact obtained are put into air humidity as 50-80%, temperature is dry under conditions of being 50-90 DEG C
Then 18-30h is transferred to air humidity as 25-40%, under conditions of temperature is 105-115 DEG C, dry 42-54h is finally transferred to
Air humidity is 15-20%, under conditions of temperature is 120-130 DEG C, dry 24-36h；
(5), fire：Dried green compact are sent into kiln, 8-12h is fired at a temperature of 1300-1350 DEG C, are obtained
Dichroite-mullite kiln furnitures product.
Further, the water added in the step (1) is the 15-18% of raw mixture.
Further, the ruler of kiln furnitures product green compact is calculated in the step (3) by the loss on ignition of mixture 0.8-1.2%
It is very little.
From the above-mentioned description of this invention, compared with prior art, the beneficial effects of the invention are as follows：It is prepared by the present invention
Dichroite-mullite kiln furnitures using waste old ceramics, dichroite-mullite clinker, andalusite as aggregate, introduce washing ball clay,
Talcum powder, kyanite, industry-alpha-alumina form the solids of the kiln furnitures composite material of the present invention for host material, to useless
The utilization rate of old ceramics reaches 25-35%, reduces the waste to resource, also reduces the production cost of kiln furniture material, is made
Dichroite-mullite kiln furnitures product density is low, light weight, strength at normal temperature height, apparent porosity height, good thermal shock stability,
Energy-efficient performance is good.
Specific embodiment
Below by way of specific embodiment, the invention will be further described.
Embodiment 1
A kind of environment-friendly type dichroite-mullite kiln furnitures include the raw material of following parts by weight：25 parts of waste old ceramics, cordierite-
22 parts of Mullite grogs, 30 parts of ball clay of washing, 10 parts of andalusite, 13 parts of talcum powder, 5 parts of kyanite, industry-alpha-alumina
5 parts；
Wherein, waste old ceramics are according to metering percentage meter, including following chemical composition：Al2O3：20%th, SiO2：75%th,
K2O：5%.
The granularity of waste old ceramics is 0-0.5um；
Chun Du≤96% of industry-alpha-alumina；
The production method of above-mentioned environment-friendly type dichroite-mullite kiln furnitures, includes the following steps：
(1), batch mixing：After the raw material of dichroite-mullite kiln furnitures is weighed by its parts by weight, batch mixer stirring is put into
10min, places into edge runner plus water-powered roller presses 25min, wherein the water added in is the 15% of raw mixture；
(2), ageing mixture：The mixture that step (1) obtains is fitted into hopper at a temperature of 40 DEG C, preserves 28h；
(3), compression moulding：According to the shape for the kiln furnitures product to be made, kiln furnitures product green compact are made, wherein, kiln furnitures
The size of product green compact is calculated by the loss on ignition of mixture 1.2%；
(4), it is dry：Green compact obtained are put into air humidity as 80%, dry 18h under the conditions of at a temperature of 90 °C, so
After be transferred to air humidity as 25%, under conditions of temperature is 105 DEG C, dry 54h is finally transferred to air humidity as 20%, temperature
Under conditions of 130 DEG C, drying is for 24 hours；
(5), fire：Dried green compact are sent into kiln, fire 12h at a temperature of 1300 DEG C, obtain cordierite-
Mullite kiln furnitures product.
Environment-friendly type dichroite-mullite kiln furnitures obtained obtain following performance parameter through experiment：
Density：2.0g/cm3；
The coefficient of expansion：22.14*10-7k-1；
The anti-folding of room temperature：13.2MPa；
Apparent porosity：62.67%；
The anti-folding (1250 DEG C of * 0.5h) of high temperature：15.4MPa；
Dichroite-mullite kiln furnitures of the prior art obtain following performance parameter through experiment：
Density：2.15g/cm3；
The coefficient of expansion：23.14*10-7k-1；
The anti-folding of room temperature：12.4MPa；
Apparent porosity：58.34%；
The anti-folding (1250 DEG C of * 0.5h) of high temperature：14.6MPa；
By above-mentioned test data, the obtained environment-friendly type dichroite-mullite kiln furnitures of the present invention are compared with the prior art
In dichroite-mullite kiln furnitures, product density is low, light weight, strength at normal temperature are high, apparent porosity is high, thermal shock resistance
Well, energy-efficient performance is good.
Embodiment 2
A kind of environment-friendly type dichroite-mullite kiln furnitures include the raw material of following parts by weight：35 parts of waste old ceramics, cordierite-
12 parts of Mullite grogs, 45 parts of ball clay of washing, 15 parts of andalusite, 8 parts of talcum powder, 15 parts of kyanite, industry-alpha-alumina
12 parts；
Wherein, waste old ceramics are according to metering percentage meter, including following chemical composition：Al2O3：28%th, SiO2：70%th,
K2O：2%.
The granularity of waste old ceramics is 0-0.5um；
Chun Du≤96% of industry-alpha-alumina；
The production method of above-mentioned environment-friendly type dichroite-mullite kiln furnitures, includes the following steps：
(1), batch mixing：After the raw material of dichroite-mullite kiln furnitures is weighed by its parts by weight, batch mixer stirring is put into
15min, places into edge runner plus water-powered roller presses 20min, wherein the water added in is the 15% of raw mixture；
(2), ageing mixture：The mixture that step (1) obtains is fitted into hopper at a temperature of 35 DEG C, preserves 36h；
(3), compression moulding：According to the shape for the kiln furnitures product to be made, kiln furnitures product green compact are made, wherein, kiln furnitures
The size of product green compact is calculated by the loss on ignition of mixture 0.8%；
(4), it is dry：Green compact obtained are put into air humidity as 50%, temperature dry 30h under conditions of being 50 DEG C, so
After be transferred to air humidity as 40%, under conditions of temperature is 115 DEG C, dry 42h is finally transferred to air humidity as 15%, temperature
Under conditions of 120 DEG C, dry 36h；
(5), fire：Dried green compact are sent into kiln, fire 8h at a temperature of 1350 DEG C, obtain cordierite-
Mullite kiln furnitures product.
Environment-friendly type dichroite-mullite kiln furnitures obtained obtain following performance parameter through experiment：
Density：1.98g/cm3；
The coefficient of expansion：22.16*10-7k-1；
The anti-folding of room temperature：13.7MPa；
Apparent porosity：62.78%；
The anti-folding (1250 DEG C of * 0.5h) of high temperature：15.5MPa；
Dichroite-mullite kiln furnitures of the prior art obtain following performance parameter through experiment：
Density：2.15g/cm3；
The coefficient of expansion：23.14*10-7k-1；
The anti-folding of room temperature：12.4MPa；
Apparent porosity：58.34%；
The anti-folding (1250 DEG C of * 0.5h) of high temperature：14.6MPa；
By above-mentioned test data, the obtained environment-friendly type dichroite-mullite kiln furnitures of the present invention are compared with the prior art
In dichroite-mullite kiln furnitures, product density is low, light weight, strength at normal temperature are high, apparent porosity is high, thermal shock resistance
Well, energy-efficient performance is good.
Embodiment 3
A kind of environment-friendly type dichroite-mullite kiln furnitures include the raw material of following parts by weight：30 parts of waste old ceramics, cordierite-
17 parts of Mullite grogs, 36 parts of ball clay of washing, 12 parts of andalusite, 11 parts of talcum powder, 10 parts of kyanite, industry-Alpha-alumina
8 parts of powder；
Wherein, waste old ceramics are according to metering percentage meter, including following chemical composition：Al2O3：23%th, SiO2：73%th,
K2O：4%.
The granularity of waste old ceramics is 0-0.5um；
Chun Du≤96% of industry-alpha-alumina；
The production method of above-mentioned environment-friendly type dichroite-mullite kiln furnitures, includes the following steps：
(1), batch mixing：After the raw material of dichroite-mullite kiln furnitures is weighed by its parts by weight, batch mixer stirring is put into
12min, places into edge runner plus water-powered roller presses 22min, wherein the water added in is the 15% of raw mixture；
(2), ageing mixture：The mixture that step (1) obtains is fitted into hopper at a temperature of 47 DEG C, preserves 22h；
(3), compression moulding：According to the shape for the kiln furnitures product to be made, kiln furnitures product green compact are made, wherein, kiln furnitures
The size of product green compact is calculated by the loss on ignition of mixture 1.0%；
(4), it is dry：Green compact obtained are put into air humidity as 65%, temperature dry 25h under conditions of being 75 DEG C, so
After be transferred to air humidity as 32%, under conditions of temperature is 112 DEG C, dry 46h is finally transferred to air humidity as 18%, temperature
Under conditions of 125 DEG C, dry 30h；
(5), fire：Dried green compact are sent into kiln, fire 8h at a temperature of 1320 DEG C, obtain cordierite-
Mullite kiln furnitures product.
Environment-friendly type dichroite-mullite kiln furnitures obtained obtain following performance parameter through experiment：
Density：1.97g/cm3；
The coefficient of expansion：22.19*10-7k-1；
The anti-folding of room temperature：13.8MPa；
Apparent porosity：62.88%；
The anti-folding (1250 DEG C of * 0.5h) of high temperature：15.6MPa；
Dichroite-mullite kiln furnitures of the prior art obtain following performance parameter through experiment：
Density：2.15g/cm3；
The coefficient of expansion：23.14*10-7k-1；
The anti-folding of room temperature：12.4MPa；
Apparent porosity：58.34%；
The anti-folding (1250 DEG C of * 0.5h) of high temperature：14.6MPa；
By above-mentioned test data, the obtained environment-friendly type dichroite-mullite kiln furnitures of the present invention are compared with the prior art
In dichroite-mullite kiln furnitures, product density is low, light weight, strength at normal temperature are high, apparent porosity is high, thermal shock resistance
Well, energy-efficient performance is good.
The foregoing is only a preferred embodiment of the present invention, therefore the scope that the present invention is implemented cannot be limited with this, i.e.,
According to the equivalent changes and modifications that scope of the present invention patent and description are made, it all should still belong to what patent of the present invention covered
In the range of.
Claims (7)
1. a kind of environment-friendly type dichroite-mullite kiln furnitures, it is characterised in that：Include the raw material of following parts by weight：Waste old ceramics 25-
35 parts, 12-22 parts of dichroite-mullite clinker, washing ball clay 30-45,10-15 parts of andalusite, 8-13 parts of talcum powder, aquamaine
5-15 parts of stone, industry -5-12 parts of alpha-alumina.
2. a kind of environment-friendly type dichroite-mullite kiln furnitures according to claim 1, it is characterised in that：The waste old ceramics
According to metering percentage meter, including following chemical composition：Al2O3：20-28%, SiO2：70-75%, K2O：2-5%.
3. a kind of environment-friendly type dichroite-mullite kiln furnitures according to claim 1, it is characterised in that：The waste old ceramics
Granularity be 0-0.5um.
4. a kind of environment-friendly type dichroite-mullite kiln furnitures according to claim 1, it is characterised in that：Industry-α-the oxygen
Change Chun Du≤96% of aluminium powder.
5. a kind of production method of environment-friendly type dichroite-mullite kiln furnitures, it is characterised in that：Include the following steps：
(1), batch mixing：After the raw material of dichroite-mullite kiln furnitures is weighed by its parts by weight, batch mixer stirring 10- is put into
15min, places into edge runner plus water-powered roller presses 20-25min；
(2), ageing mixture：The mixture that step (1) obtains is fitted into hopper at a temperature of 35-40 DEG C, preserves 28-36h；
(3), compression moulding：According to the shape for the kiln furnitures product to be made, kiln furnitures product green compact are made；
(4), it is dry：Green compact obtained are put into air humidity as 50-80%, temperature dry 18- under conditions of being 50-90 DEG C
Then 30h is transferred to air humidity as 25-40%, under conditions of temperature is 105-115 DEG C, dry 42-54h is finally transferred to air
Humidity is 15-20%, under conditions of temperature is 120-130 DEG C, dry 24-36h；
(5), fire：Dried green compact are sent into kiln, 8-12h is fired at a temperature of 1300-1350 DEG C, it is blue or green to obtain violet
Stone-mullite kiln furnitures product.
6. a kind of production method of environment-friendly type dichroite-mullite kiln furnitures according to claim 5, it is characterised in that：Institute
State the 15-18% that the water added in step (1) is raw mixture.
7. a kind of production method of environment-friendly type dichroite-mullite kiln furnitures according to claim 5, it is characterised in that：Institute
State the size for calculating kiln furnitures product green compact in step (3) by the loss on ignition of mixture 0.8-1.2%.
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| CN201711437792.9A CN108059450B (en) | 2017-12-26 | 2017-12-26 | Environment-friendly cordierite-mullite kiln furniture and manufacturing method thereof |
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Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109320224A (en) * | 2018-10-26 | 2019-02-12 | 淄博工陶耐火材料有限公司 | A kind of material and preparation method thereof of high-purity cordierite combination mullite |
| CN110028314A (en) * | 2019-04-08 | 2019-07-19 | 福建省德化县创捷窑具有限公司 | A kind of high thermal shock resistance dichroite-mullite kiln furnitures and preparation method thereof |
| CN112094127A (en) * | 2020-09-25 | 2020-12-18 | 南阳开元高温新材料有限公司 | Manufacturing process of kyanite tailing series sagger |
| CN113072386A (en) * | 2021-03-24 | 2021-07-06 | 福建省德化县创捷窑具有限公司 | Environment-friendly refractory kiln furniture and preparation method thereof |
Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2014073928A (en) * | 2012-10-03 | 2014-04-24 | Asahi Glass Co Ltd | Sintered oxide ceramics and manufacturing method thereof |
| CN103936406A (en) * | 2013-01-22 | 2014-07-23 | 福建省德化县创捷窑具有限公司 | Iolite-mullite deck and preparation method thereof |
| CN105669244A (en) * | 2016-01-27 | 2016-06-15 | 北京创导工业陶瓷有限公司 | Cordierite-mullite kiln furniture material with high thermal shock resistance |
| CN105801098A (en) * | 2016-04-19 | 2016-07-27 | 福建省德化县创捷窑具有限公司 | Economical and environment-friendly cordierite-mullite kiln furniture composite material and manufacturing method thereof |
| CN106518146A (en) * | 2016-11-16 | 2017-03-22 | 福建省德化荣信陶瓷有限公司 | Cordierite ceramic synthesized from ceramic whiteware waste, and preparation method thereof |
-
2017
- 2017-12-26 CN CN201711437792.9A patent/CN108059450B/en active Active
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2014073928A (en) * | 2012-10-03 | 2014-04-24 | Asahi Glass Co Ltd | Sintered oxide ceramics and manufacturing method thereof |
| CN103936406A (en) * | 2013-01-22 | 2014-07-23 | 福建省德化县创捷窑具有限公司 | Iolite-mullite deck and preparation method thereof |
| CN105669244A (en) * | 2016-01-27 | 2016-06-15 | 北京创导工业陶瓷有限公司 | Cordierite-mullite kiln furniture material with high thermal shock resistance |
| CN105801098A (en) * | 2016-04-19 | 2016-07-27 | 福建省德化县创捷窑具有限公司 | Economical and environment-friendly cordierite-mullite kiln furniture composite material and manufacturing method thereof |
| CN106518146A (en) * | 2016-11-16 | 2017-03-22 | 福建省德化荣信陶瓷有限公司 | Cordierite ceramic synthesized from ceramic whiteware waste, and preparation method thereof |
Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109320224A (en) * | 2018-10-26 | 2019-02-12 | 淄博工陶耐火材料有限公司 | A kind of material and preparation method thereof of high-purity cordierite combination mullite |
| CN110028314A (en) * | 2019-04-08 | 2019-07-19 | 福建省德化县创捷窑具有限公司 | A kind of high thermal shock resistance dichroite-mullite kiln furnitures and preparation method thereof |
| CN110028314B (en) * | 2019-04-08 | 2021-05-25 | 福建省德化县创捷窑具有限公司 | High-thermal-shock-stability cordierite-mullite kiln furniture and preparation method thereof |
| CN112094127A (en) * | 2020-09-25 | 2020-12-18 | 南阳开元高温新材料有限公司 | Manufacturing process of kyanite tailing series sagger |
| CN112094127B (en) * | 2020-09-25 | 2023-02-28 | 南阳开元高温新材料有限公司 | Manufacturing process of kyanite tailing series sagger |
| CN113072386A (en) * | 2021-03-24 | 2021-07-06 | 福建省德化县创捷窑具有限公司 | Environment-friendly refractory kiln furniture and preparation method thereof |
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