CN108048639A - A kind of method for improving graphitizable steel plate stamping and forming performance - Google Patents

A kind of method for improving graphitizable steel plate stamping and forming performance Download PDF

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Publication number
CN108048639A
CN108048639A CN201711315901.XA CN201711315901A CN108048639A CN 108048639 A CN108048639 A CN 108048639A CN 201711315901 A CN201711315901 A CN 201711315901A CN 108048639 A CN108048639 A CN 108048639A
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China
Prior art keywords
steel plate
graphitization
improving
stamping
ferrite
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CN201711315901.XA
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Chinese (zh)
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CN108048639B (en
Inventor
张永军
张鹏程
王九花
于文杰
韩静涛
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University of Science and Technology Beijing USTB
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University of Science and Technology Beijing USTB
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    • CCHEMISTRY; METALLURGY
    • C21METALLURGY OF IRON
    • C21DMODIFYING THE PHYSICAL STRUCTURE OF FERROUS METALS; GENERAL DEVICES FOR HEAT TREATMENT OF FERROUS OR NON-FERROUS METALS OR ALLOYS; MAKING METAL MALLEABLE, e.g. BY DECARBURISATION OR TEMPERING
    • C21D8/00Modifying the physical properties by deformation combined with, or followed by, heat treatment
    • C21D8/02Modifying the physical properties by deformation combined with, or followed by, heat treatment during manufacturing of plates or strips
    • C21D8/04Modifying the physical properties by deformation combined with, or followed by, heat treatment during manufacturing of plates or strips to produce plates or strips for deep-drawing
    • C21D8/0421Modifying the physical properties by deformation combined with, or followed by, heat treatment during manufacturing of plates or strips to produce plates or strips for deep-drawing characterised by the working steps
    • C21D8/0431Warm rolling
    • CCHEMISTRY; METALLURGY
    • C21METALLURGY OF IRON
    • C21DMODIFYING THE PHYSICAL STRUCTURE OF FERROUS METALS; GENERAL DEVICES FOR HEAT TREATMENT OF FERROUS OR NON-FERROUS METALS OR ALLOYS; MAKING METAL MALLEABLE, e.g. BY DECARBURISATION OR TEMPERING
    • C21D8/00Modifying the physical properties by deformation combined with, or followed by, heat treatment
    • C21D8/02Modifying the physical properties by deformation combined with, or followed by, heat treatment during manufacturing of plates or strips
    • C21D8/04Modifying the physical properties by deformation combined with, or followed by, heat treatment during manufacturing of plates or strips to produce plates or strips for deep-drawing
    • C21D8/0447Modifying the physical properties by deformation combined with, or followed by, heat treatment during manufacturing of plates or strips to produce plates or strips for deep-drawing characterised by the heat treatment
    • CCHEMISTRY; METALLURGY
    • C22METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22CALLOYS
    • C22C38/00Ferrous alloys, e.g. steel alloys
    • C22C38/02Ferrous alloys, e.g. steel alloys containing silicon
    • CCHEMISTRY; METALLURGY
    • C22METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22CALLOYS
    • C22C38/00Ferrous alloys, e.g. steel alloys
    • C22C38/04Ferrous alloys, e.g. steel alloys containing manganese
    • CCHEMISTRY; METALLURGY
    • C21METALLURGY OF IRON
    • C21DMODIFYING THE PHYSICAL STRUCTURE OF FERROUS METALS; GENERAL DEVICES FOR HEAT TREATMENT OF FERROUS OR NON-FERROUS METALS OR ALLOYS; MAKING METAL MALLEABLE, e.g. BY DECARBURISATION OR TEMPERING
    • C21D2211/00Microstructure comprising significant phases
    • C21D2211/005Ferrite
    • CCHEMISTRY; METALLURGY
    • C21METALLURGY OF IRON
    • C21DMODIFYING THE PHYSICAL STRUCTURE OF FERROUS METALS; GENERAL DEVICES FOR HEAT TREATMENT OF FERROUS OR NON-FERROUS METALS OR ALLOYS; MAKING METAL MALLEABLE, e.g. BY DECARBURISATION OR TEMPERING
    • C21D2211/00Microstructure comprising significant phases
    • C21D2211/006Graphite

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  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Mechanical Engineering (AREA)
  • Materials Engineering (AREA)
  • Metallurgy (AREA)
  • Organic Chemistry (AREA)
  • Physics & Mathematics (AREA)
  • Thermal Sciences (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Heat Treatment Of Sheet Steel (AREA)
  • Heat Treatment Of Steel (AREA)

Abstract

A kind of method for improving graphitizable steel plate stamping and forming performance, belongs to steel material processing technique field.It is characterized in that using warm deformation technology, the warm deformation of Dynamic Recrystallization of Ferrite is carried out to the graphitization steel plate after graphitization processing, the stamping formabilily of graphitization steel plate is improved by controlling refinement and the homogenization of ferrite dynamic crystal grain.Specific method is that the graphitization steel plate Jing Guo graphitization processing is heated to 550~710 DEG C, and the flat rolling that drafts is 8~15% is carried out after samming, room temperature is air-cooled to after rolling.The graphitization steel plate handled using this method, ferrite crystal grain is fined and uniformly, stamping formabilily is good, yield tensile ratio≤0.56, strain hardening exponent >=0.25, in-plane anisotropy≤0.15.

Description

A kind of method for improving graphitizable steel plate stamping and forming performance
Technical field
The present invention relates to a kind of methods for improving graphitizable steel plate stamping and forming performance, belong to steel material processing technology neck Domain.
Background technology
The preparation flow of graphitization steel plate mainly includes steel-making, pours into a mould, the techniques mistake such as hot rolling or cold rolling, graphitization processing Journey.Wherein, steel plate shows higher stamping formabilily after graphitization processing, has relatively low yield tensile ratio, can soften To the level as mild steel.
Steel plate through graphitization processing, tissue are mainly made of ferrite+graphite.However, due to graphitization processing mistake The time that journey needs is longer, and the ferritic structure often led in steel plate is coarse, and uneven, such tissue characteristic, it is difficult to Make steel plate that there is good stamping formabilily.
Therefore, it is coarse to solve ferrite crystal grain present in existing graphitization processing method, and non-uniform problem, this Invention is proposed using warm deformation technology, and the temperature of Dynamic Recrystallization of Ferrite is carried out to the graphitization steel plate after graphitization processing It rolls, to realize the refinement of ferrite crystal grain, homogenization, good Preparedness Directorate is provided to be subsequently stamping, further to carry Its high stamping formabilily.
The content of the invention
Graphitization steel plate after graphitization processing has higher stamping formabilily.Due to graphitization processing process In to easily cause ferrite crystal grain coarse and uneven.Therefore, in order to solve the problems, such as this, the present invention is based on warm deformations can make iron Ferritic recrystallizes, to make fetrite grain refinement and homogenization, it is proposed that one kind can further improve graphitization steel plate and strike out The method of shape performance.
The present invention is realized by following technical measures:
A kind of method for improving graphitizable steel plate stamping and forming performance, it is characterised in that using warm deformation technology, to graphite Change treated graphitization steel plate carry out Dynamic Recrystallization of Ferrite warm deformation, with realize the refinement of ferrite crystal grain and uniformly Change.Specific method is that the graphitization steel plate Jing Guo graphitization processing is heated to 550~710 DEG C, and drafts is carried out after samming For 8~15% flat rolling, room temperature is air-cooled to after rolling.The graphitization processing, refer to graphitization steel plate be in temperature Isothermal when progress 8~16 is small in the range of 600 DEG C~Ac1, and cool to a heat treatment process of room temperature with the furnace.This method is main It is 0.30~1.20% to C content to be, Si contents are 0.60~1.60%, Mn contents are 0.20~0.50%, P content≤ 0.015%th, S content≤0.015%, remaining content carry out for the graphitization steel plate of Fe.
Beneficial effects of the present invention:
The graphitization steel plate handled using this method, ferrite crystal grain are fined and homogenized, and can be follow-up punching Pressing formation provides good Preparedness Directorate, hence it is evident that improves the stamping formabilily of graphitization steel plate, yield tensile ratio≤0.56, strain Hardenability value >=0.25, in-plane anisotropy≤0.15.
Specific embodiment
After now the embodiment of the present invention is specifically described in.
Technical scheme is described further with reference to embodiments.Embodiment is merely to illustrate the present invention, Rather than limit the present invention in any way.
Embodiment 1
The present embodiment selection C content is 0.86%, Si contents are 0.98%, Mn contents are 0.36%, P content is 0.008%th, the graphitization steel plate for the 2.3mm thickness that S contents are 0.015%, remaining content is Fe, through 680 DEG C, 10 it is small when etc. Temperature, after being furnace-cooled to the graphitization processing of room temperature, tissue is mainly made of ferrite and graphite, but ferrite crystal grain is coarse, and It is uneven.The steel plate is packed into heating furnace at room temperature, comes out of the stove, starts after graphitization steel plate is heated to 630 DEG C of sammings Warm-rolling, drafts 0.3mm, i.e., 13% are carried out on flat roll mill to it;Finishing temperature is not less than 550 DEG C;It is air-cooled to after rolling Room temperature.
Metallographic Analysis and mechanical test are carried out to the graphitization steel plate Jing Guo above-mentioned processing, the results show that its institutional framework In observe ferrite crystal grain it is uniform, radial dimension mostly be in 15~18 μ ms, yield tensile ratio σsbFor 0.52, strain hardening exponentFor 0.28, in-plane anisotropy △ r are 0.13.
Embodiment 2
The present embodiment selection C content is 1.16%, Si contents are 1.38%, Mn contents are 0.42%, P content is 0.009%th, the graphitization steel plate for the 3.3mm thickness that S contents are 0.008%, remaining content is Fe, through 700 DEG C, 12 it is small when isothermal, After being furnace-cooled to the graphitization processing of room temperature, tissue is mainly made of ferrite and graphite, and similary ferrite crystal grain is coarse, and not Uniformly.The steel plate is packed into heating furnace at room temperature, comes out of the stove, starts flat after graphitization steel plate is heated to 660 DEG C of sammings Warm-rolling, drafts 0.3mm, i.e., 9.1% are carried out on roller mill to it;Finishing temperature is not less than 550 DEG C;Room is air-cooled to after rolling Temperature.
Metallographic Analysis and mechanical test are carried out to the graphitization steel plate Jing Guo above-mentioned processing, the results show that its institutional framework In observe ferrite crystal grain it is uniform, radial dimension mostly be in 19~21 μ ms, yield tensile ratio σsbFor 0.55, strain hardening exponentFor 0.26, in-plane anisotropy △ r are 0.15.
By embodiment as it can be seen that before graphitizable steel plate stamping and forming, warm-rolling deformation is carried out to it, it can be ensured that the steel plate has There is a good stamping formabilily, i.e. warm-rolling deformation can be rear stamping to provide good Preparedness Directorate.

Claims (3)

  1. A kind of 1. method for improving graphitizable steel plate stamping and forming performance, it is characterised in that using warm deformation technology, to graphitization Treated graphitization steel plate carry out Dynamic Recrystallization of Ferrite warm deformation, with realize the refinement of ferrite crystal grain and uniformly Change;
    Specific method is that the graphitization steel plate Jing Guo graphitization processing is heated to 550~710 DEG C, and drafts is carried out after samming For 8~15% flat rolling, room temperature is air-cooled to after rolling.
  2. 2. according to a kind of method for improving graphitizable steel plate stamping and forming performance described in claim 1, which is characterized in that described Graphitization processing refers to that graphitization steel plate be isothermal when progress 8~16 is small in the range of 600 DEG C~Ac1 in temperature, and with furnace cooling But to a heat treatment process of room temperature.
  3. 3. according to a kind of method for improving graphitizable steel plate stamping and forming performance described in claim 1, which is characterized in that the stone The main chemical compositions and its mass percentage content of inkization steel plate are:C:0.30~1.20%;Si:0.60~1.60%;Mn: 0.20~0.50%;P≤0.015%;S:≤ 0.015%;Remaining content is Fe.
CN201711315901.XA 2017-12-12 2017-12-12 A method of improving graphitizable steel plate stamping and forming performance Active CN108048639B (en)

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN111189701A (en) * 2020-01-08 2020-05-22 吉林大学 Method for measuring large-strain compression hardening curve of metal hyperbolic sample
CN111471844A (en) * 2020-04-02 2020-07-31 北京科技大学 Treatment method for realizing superplasticity of graphitized steel

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101899555A (en) * 2010-08-04 2010-12-01 武汉钢铁(集团)公司 Production method of graphitized free-machining steel
CN105671441A (en) * 2014-12-09 2016-06-15 Posco公司 Steel material for graphitization and graphite steel with excellent machinability and cold forging characteristic
CN106048179A (en) * 2016-07-15 2016-10-26 北京科技大学 Preparation method of graphitizing hot rolled steel plate
CN106917044A (en) * 2017-03-03 2017-07-04 北京科技大学 A kind of preparation method of the stamping cold rolling high carbon steel sheet of use graphitization

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101899555A (en) * 2010-08-04 2010-12-01 武汉钢铁(集团)公司 Production method of graphitized free-machining steel
CN105671441A (en) * 2014-12-09 2016-06-15 Posco公司 Steel material for graphitization and graphite steel with excellent machinability and cold forging characteristic
CN106048179A (en) * 2016-07-15 2016-10-26 北京科技大学 Preparation method of graphitizing hot rolled steel plate
CN106917044A (en) * 2017-03-03 2017-07-04 北京科技大学 A kind of preparation method of the stamping cold rolling high carbon steel sheet of use graphitization

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
彭大暑: "《金属塑性加工原理》", 30 April 2014 *

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN111189701A (en) * 2020-01-08 2020-05-22 吉林大学 Method for measuring large-strain compression hardening curve of metal hyperbolic sample
CN111471844A (en) * 2020-04-02 2020-07-31 北京科技大学 Treatment method for realizing superplasticity of graphitized steel

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