CN108018125A - Light chlorimation directly agitates hot -70 method of method production chlorination gutter oil of air cooling - Google Patents
Light chlorimation directly agitates hot -70 method of method production chlorination gutter oil of air cooling Download PDFInfo
- Publication number
- CN108018125A CN108018125A CN201710416312.4A CN201710416312A CN108018125A CN 108018125 A CN108018125 A CN 108018125A CN 201710416312 A CN201710416312 A CN 201710416312A CN 108018125 A CN108018125 A CN 108018125A
- Authority
- CN
- China
- Prior art keywords
- chlorine
- production
- kettle
- gutter oil
- agitation device
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11C—FATTY ACIDS FROM FATS, OILS OR WAXES; CANDLES; FATS, OILS OR FATTY ACIDS BY CHEMICAL MODIFICATION OF FATS, OILS, OR FATTY ACIDS OBTAINED THEREFROM
- C11C3/00—Fats, oils, or fatty acids by chemical modification of fats, oils, or fatty acids obtained therefrom
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- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
- C10G73/00—Recovery or refining of mineral waxes, e.g. montan wax
- C10G73/38—Chemical modification of petroleum
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B13/00—Recovery of fats, fatty oils or fatty acids from waste materials
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B3/00—Refining fats or fatty oils
- C11B3/001—Refining fats or fatty oils by a combination of two or more of the means hereafter
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B3/00—Refining fats or fatty oils
- C11B3/008—Refining fats or fatty oils by filtration, e.g. including ultra filtration, dialysis
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B3/00—Refining fats or fatty oils
- C11B3/10—Refining fats or fatty oils by adsorption
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02W—CLIMATE CHANGE MITIGATION TECHNOLOGIES RELATED TO WASTEWATER TREATMENT OR WASTE MANAGEMENT
- Y02W30/00—Technologies for solid waste management
- Y02W30/50—Reuse, recycling or recovery technologies
- Y02W30/74—Recovery of fats, fatty oils, fatty acids or other fatty substances, e.g. lanolin or waxes
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- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Chemistry (AREA)
- Wood Science & Technology (AREA)
- Microbiology (AREA)
- General Chemical & Material Sciences (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Physical Or Chemical Processes And Apparatus (AREA)
Abstract
Title of the present invention is that Light chlorimation directly agitates hot 70 method of method production chlorination gutter oil of air cooling, belong to chlorinated paraffin technical field, in order to improve 70 speed of production of chlorinated paraffin, the upper light source of installation in kettle is adopted the technical scheme that based on former 87106851.6 patents are improved with it, chlorine source chlorine is directly placed into agitation device through heat exchanger, heat exchangers in series between cyclic part and agitation device, gutter oil is boiled, layering removes impurity, debris, moisture content, after 150 DEG C or so of heating, with activated decoloration, pass through press filtration again, again salt reduction degree is washed through superheated water, after being layered water again, reacted in input kettle, production operation such as traditional thermal chlorination Bubbling method production chlorinated paraffin.A kind of faster production method is provided.
Description
(1) technical field:The present invention relates to a kind of method for producing chlorination gutter oil -70, belongs to production chlorinated paraffin technology
Field.
(2) background technology:" equipment for preparation of paraffin chloride by forced circulating blast method " (former patent No.:87106851.6) its
Technical solution is:Chlorine is sent into the hydrogen chloride gas extraction in reaction kettle space, chlorine and reaction generation, through jet pump and reservoir
Groove, is only absorbed by the water, and remaining chlorine drum is pressed into agitation device, such continuous fast reaction.But for producing chlorinated paraffin speed also not
Enough ideals, especially produce high chlorinated paraffin product, and to the reaction later stage, speed eases up.
(3) content of the invention:The task of the present invention is based on a kind of improvement to former 87106851.6 patents of invention, there is provided
A kind of method of the gutter oil of production chlorination faster -70, adopts the technical scheme that and installs upper light source in kettle additional, supplied by chlorine source
Chlorine is passed directly into agitation device through heat exchanger, and material in reactor is agitated.Exported in device agitation device and cyclic part
Between heat exchangers in series, be passed through agitation device after the reacting gas for entering agitation device is first heated or cooled down, it is ensured that optimal
Reaction temperature.Gutter oil is boiled, layering removes impurity, debris, moisture content, after 150 DEG C or so of heating, is taken off with atlapulgite
Color, then by press filtration, then salt reduction degree is washed through superheated water, then after being layered water, put into kettle and react, production operation such as tradition heat
Chlorination Bubbling method produces chlorinated paraffin.
(4) embodiment:A set of " equipment for preparation of paraffin chloride by forced circulating blast method ", uses 500 liters of reactions
Kettle, its reaction kettle is interior to install upper 1000 watts of mercury lamps additional, its chlorine source chlorine is passed directly into the agitation device in kettle through heat exchanger.Use heat-transfer surface
2.5 rice2Heat exchanger be connected between agitation device and cyclic part outlet, gutter oil is boiled, layering removes impurity, miscellaneous
Thing, moisture content, after 150 DEG C or so of heating, with activated decoloration, then by press filtration, then through superheated water washing salt reduction degree, then are layered
After removing water, put into kettle and react, production operation such as traditional thermal chlorination Bubbling method production chlorinated paraffin.
Present invention operation and " equipment for preparation of paraffin chloride by forced circulating blast method " are same.Material temperature is low, heat exchanger heating, on the contrary
Cooling.
Claims (1)
1. a kind of Light chlorimation directly agitates hot -70 method of method production chlorination gutter oil of air cooling, including chlorine and hydrogen chloride gas
Extraction, hydrogen chloride gas are only absorbed by the water in jet pump and hopper, and remaining chlorine drum is pressed into agitation device, so continuous, its feature
It is:Light source chlorination is housed, chlorine source chlorine is directly placed into agitation device in kettle through heat exchanger, and agitation device exports it with cyclic part in kettle
Between heat exchangers in series, reacting gas is heated or cooled, gutter oil is boiled, layering remove impurity, debris, moisture content, add
After 150 DEG C or so of heat, with activated decoloration, then by press filtration, then through superheated water salt reduction degree is washed, then after being layered water, throw
Enter in kettle and react, production operation such as traditional thermal chlorination Bubbling method production chlorinated paraffin.
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN201710416312.4A CN108018125A (en) | 2017-05-16 | 2017-05-16 | Light chlorimation directly agitates hot -70 method of method production chlorination gutter oil of air cooling |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN201710416312.4A CN108018125A (en) | 2017-05-16 | 2017-05-16 | Light chlorimation directly agitates hot -70 method of method production chlorination gutter oil of air cooling |
Publications (1)
Publication Number | Publication Date |
---|---|
CN108018125A true CN108018125A (en) | 2018-05-11 |
Family
ID=62079223
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CN201710416312.4A Withdrawn CN108018125A (en) | 2017-05-16 | 2017-05-16 | Light chlorimation directly agitates hot -70 method of method production chlorination gutter oil of air cooling |
Country Status (1)
Country | Link |
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CN (1) | CN108018125A (en) |
Citations (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN87106851A (en) * | 1987-10-06 | 1988-07-27 | 林群祥 | Equipment for preparation of paraffin chloride by forced circulating blast method |
CN106010645A (en) * | 2016-05-04 | 2016-10-12 | 林群祥 | Method for producing chlorinated paraffin-70 in light chlorination direct propelling gas cold-heat mode |
CN106350216A (en) * | 2016-08-25 | 2017-01-25 | 林群祥 | Chlorinated waste edible oil |
-
2017
- 2017-05-16 CN CN201710416312.4A patent/CN108018125A/en not_active Withdrawn
Patent Citations (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN87106851A (en) * | 1987-10-06 | 1988-07-27 | 林群祥 | Equipment for preparation of paraffin chloride by forced circulating blast method |
CN106010645A (en) * | 2016-05-04 | 2016-10-12 | 林群祥 | Method for producing chlorinated paraffin-70 in light chlorination direct propelling gas cold-heat mode |
CN106350216A (en) * | 2016-08-25 | 2017-01-25 | 林群祥 | Chlorinated waste edible oil |
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WW01 | Invention patent application withdrawn after publication | ||
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Application publication date: 20180511 |