CN107974091A - A kind of noise reduction drainage pavement high viscose glue powder modified asphalt material and preparation method thereof - Google Patents
A kind of noise reduction drainage pavement high viscose glue powder modified asphalt material and preparation method thereof Download PDFInfo
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- CN107974091A CN107974091A CN201710912227.7A CN201710912227A CN107974091A CN 107974091 A CN107974091 A CN 107974091A CN 201710912227 A CN201710912227 A CN 201710912227A CN 107974091 A CN107974091 A CN 107974091A
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L95/00—Compositions of bituminous materials, e.g. asphalt, tar, pitch
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K2201/00—Specific properties of additives
- C08K2201/014—Additives containing two or more different additives of the same subgroup in C08K
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2201/00—Properties
- C08L2201/08—Stabilised against heat, light or radiation or oxydation
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/03—Polymer mixtures characterised by other features containing three or more polymers in a blend
- C08L2205/035—Polymer mixtures characterised by other features containing three or more polymers in a blend containing four or more polymers in a blend
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2207/00—Properties characterising the ingredient of the composition
- C08L2207/04—Thermoplastic elastomer
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2207/00—Properties characterising the ingredient of the composition
- C08L2207/20—Recycled plastic
- C08L2207/24—Recycled plastic recycling of old tyres and caoutchouc and addition of caoutchouc particles
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Abstract
The present invention relates to a kind of noise reduction drainage pavement with high viscose glue powder modified asphalt material, according to the mass fraction, it is prepared by 56 80 parts of matrix pitches, 15 25 parts of waste Crumb rubber, 13 parts of thermoplastic elastomer (TPE), 1.5 6 parts of waste phosphoric acid esters, 15 parts of thermoplastic resin, 15 parts of plasticizer and 0.1 0.3 parts of crosslinking agent.Its preparation method is to be premixed after mixing waste Crumb rubber, thermoplastic elastomer (TPE), waste phosphoric acid ester, asphalt modifier is made;Asphalt modifier is added after matrix pitch is heated, then adds thermoplastic resin, plasticizer continues insulated and stirred, shearing;Crosslinking agent is eventually adding, modified pitch is made.60 DEG C of dynamic viscosities of high viscose glue powder-modified asphalt of the present invention reach more than 60000Pa.s, have excellent high-temperature stability, anti-rut behavior, ageing resistance, are particularly suitable for summer high temperature, humid area and the making of the big area of day and night temperature or drainage road.
Description
Technical field
The invention belongs to road engineering paving material field, and in particular to a kind of noise reduction drainage pavement is modified with high viscose glue powder
Asphalt material and preparation method thereof.
Background technology
In recent years, often there is " light rain ponding, heavy rain waterlogging " in each big city in China, effectively solve Urban Flood Waterlogging and
The problem of water pollution, is extremely urgent.Sponge urban construction at present is to solve rainwater and surface water resources synthesis profit in city development
The problems such as with, municipal drainage flood control and ecological environmental protection, realize the low important channel for influencing exploitation, to solve urban water shortage and
The environmental problems such as waterlogging, realize urban sustainable development, are of great significance.Wherein drainage pavement is that road is built in sponge city
If chief component.
Noise reduction porous asphalt pavement in drainage pavement is a kind of open gradation, the pavement structure of macroporosity, it can be dropped
Low vehicle caused noise in road driving, improve vehicle brake when friction coefficient, shorten braking distance, and due to
Surface layer is in vesicular structure form, can quickly exclude road table rainwater and reduce surface runoff, have good noise reduction, antiskid
Property, suppress water mist function of surface, advantageously accounting for some bituminous pavings of China there are anti-slide performance does not reach requirement, friction coefficient
The problem of low, provide a favorable security for traffic safety, agree with " sponge city " alleviate urban waterlogging, cut down urban runoff load and
Improve the construction new concept of urban ecological environment, paid attention to and promoted in the construction in sponge city.
Drainage pavement has many good qualities, but since structure is special, road surface voidage reaches 18-25% or so, and general
The intensive voidage with asphalt concrete pavement be 3-6%, and the height of voidage depends primarily upon the asphalt adhesive paved the way
Ramming material, so this just proposes requirements at the higher level to the performance of road tar cementitious matter.
The cementitious matter of drainage pavement generally uses high-viscosity modified asphalt, and the polymer of high-content is added in pitch,
High-viscosity modified asphalt is prepared, but most common in polymer used is styrene-butadiene-styrene
(SBS), however, SBS supply falls short of demand in recent years rise in price, and aging easily occurs since molecular backbone structure is unsaturated, it is mixed
The asphalt membrane thickness of conjunction material is thinner, and it is therefore necessary to select the material of cost performance higher.
China's waste tire amount increases year by year, produces substantial amounts of solid waste every year, if waste-tyre rubber-powder used
In modified pitch, the process problem of solid waste can be solved.But in the prior art, what can be added in modified pitch is useless
Rubber mass is considerably less.
The content of the invention
The technical problems to be solved by the invention are to be directed to the deficiencies in the prior art, there is provided a kind of noise reduction drainage pavement is used
High viscose glue powder modified asphalt material and its preparation method.The high viscose glue powder modified asphalt material of the noise reduction drainage pavement of the present invention
Substantial amounts of damaged tire is added in pitch and is modified, adhesiveness, durability and the wear resistence of pitch can be effectively improved, it is possible to increase
Pitch anti-aging property, can solve the problem of environmental pollution that damaged tire is brought, and can also solve SBS volumes in high adhered modification pitch
The problem of larger of high cost and it is easy to aging the problem of, there is economic benefit and environmental benefit.In addition, this high viscose glue powder is modified
60 DEG C of dynamic viscosities of pitch are more than 60000Pas, asphalt, and performance is significantly larger than《Asphalt highway construction technology is advised
Model》(JTJ052-2000) to the technical requirements of drainage pavement.
To achieve the above object, the present invention adopts the following technical scheme that.
A kind of high viscose glue powder modified asphalt material of noise reduction drainage pavement, the modified asphalt material according to the mass fraction,
By 56-80 parts of matrix pitches, 15-25 parts of waste Crumb rubber, 1-3 parts of thermoplastic elastomer (TPE), 1.5-6 parts of waste phosphoric acid esters, 1-5 parts
Thermoplastic resin, 1-5 parts of plasticizer and 0.1-0.3 parts of crosslinking agent be prepared.
As preferable technical solution:
Preferably, the matrix pitch is 70A grades of bi tumenf orr oads.
Preferably, the waste Crumb rubber is useless heavy sevice type rubber powder, useless car tire rubber powder, useless conveyer belt powder or useless sole rubber
One or more in powder;The waste Crumb rubber is by crushing, and after sieving, obtained particle diameter is the waste Crumb rubber of 20-40 mesh.
Preferably, the thermoplastic elastomer is styrene-butadiene-styrene (SBS) or styrene-isoamyl two
One or more in alkene-styrol copolymer (SIS).
Preferably, the waste phosphoric acid ester is derived from unreacted when Tianjin Li Hai petrochemical industry Co., Ltd prepares phosphate flame retardant
Waste material.
Preferably, the thermoplastic resin is that adhesion promoting component is one or both of note olefine resin or rosin resin, more
Preferably rosin resin;The plasticizer is o-phthalic acid dibutyl ester or dibutyl phthalate.
Preferably, the crosslinking agent for Cosan, sulfur donor, cumyl peroxide, di-t-butyl peroxide benzene,
One or more in magnesia, zinc oxide, lead oxide, rush M, TMTD.
A kind of preparation method present invention also offers noise reduction drainage pavement with high viscose glue powder modified asphalt material, including with
Lower step:
(1) waste Crumb rubber, thermoplastic elastomer (TPE), waste phosphoric acid ester are mixed to join high-speed stirring mixer and are premixed,
Asphalt modifier is made;
(2) matrix pitch is melted at a temperature of 120-140 DEG C and is warming up to 170-190 DEG C again, stirring thereto adds
Stirred 5-10 minutes after the asphalt modifier, then add thermoplastic resin, plasticizer continuation insulated and stirred 5-15 minutes,
Then pass through colloid mill shearing, grinding 10-20 minute after, into stirring development tank insulation development 1-3 it is small when, finally using lifted
Crosslinking agent is slowly added to by auger, continues that the high viscose glue powder-modified asphalt of noise reduction drainage pavement is made when insulated and stirred 1-3 is small.
Preferably the rotating speed of high-speed stirring mixer is:1000-1450 revs/min, stirring is done time as 2-15 minutes in advance, high
Speed stirring can raise rubber powder temperature, can use the temperature of control mixing time control rubber powder at 50-60 DEG C or using other
Temperature control method.
Beneficial effect
1st, the present invention makes thermoplastic elastomer (TPE) and useless rubber by thermoplastic elastomer, waste Crumb rubber, waste phosphoric acid ester by premixing
Vulcanized rubber powder absorbs sufficient oil and carries out either shallow activation, and obtained asphalt modifier can have good compatibility with pitch, when
Independent rubber powder particles and styrol copolymer particle can be made to form elastomeric network after being modified with pitch reaction, make to mix
Material after conjunction is homogeneous system, has preferable storage stability, and ensures the high rheology and ageing-resistant performance of material, can
With effectively solve the problems, such as high-viscosity bitumen modifier deliver directly material and matrix pitch blend uniformity and asphalt membrane it is thin;So as into one
High viscose glue powder-modified asphalt made from step promotion has good high-temperature stability, low-temperature cracking-resistance and ageing-resistant performance concurrently.
2nd, present invention adds the high temperature bond performance and high-temperature stability that rosin resin can increase bituminous concrete, increase
Modeling agent can improve the low-temperature cracking-resistance and elastic recovery capability of pitch.
3rd, 60 DEG C of dynamic viscosities of high viscose glue powder-modified asphalt produced by the present invention reach more than 60000Pa.s, and performance is much
It is higher than《Standard specification for construction and acceptance of highway asphalt pavement》(JTJ052-2000) to the technical requirements of drainage pavement.Not only have excellent
High-temperature stability, anti-rut behavior, ageing resistance, also with excellent crack resistance at low-temperature, fatigue resistance, building stones adhesiveness
Thicker asphalt membrane thickness, is particularly suitable for summer high temperature, humid area and the big area of day and night temperature, for heavy traffic road
Or the making of drainage road, effectively prevent pavement track, embrace, fatigue cracking, cold cracking and water enchroachment (invasion) evil etc. common road
Face, which is destroyed, to be occurred, prolonging service life of pavement.
4th, noise reduction drainage pavement of the invention is filled with high viscose glue powder-modified asphalt due to considerably increasing waste Crumb rubber
Amount, makes it have good high-temperature stability, low-temperature cracking-resistance, ageing-resistant performance and low noise road-ability, can not only
Lift Pavement Condition and expensive import high-viscosity modified asphalt can be replaced, greatly reduce thermoplastic elastomer (TPE)
Addition content, reduce cost, be widely used in the making of drainage asphalt pavement.
Embodiment
The invention will be further elucidated with reference to specific embodiments.It is to be understood that these embodiments are merely to illustrate this hair
It is bright rather than limit the scope of the invention.In addition, it should also be understood that, after reading the content taught by the present invention, art technology
Personnel can make various changes or modifications the present invention, and such equivalent forms equally fall within the application the appended claims and limited
Fixed scope.
The embodiment 1-4 being modified according to this product preparation method is contrasted with high adhered modification pitch below, than
Compared with the performance difference of the high adhered modification pitch prepared using high viscose glue powder-modified asphalt prepared by the present invention with the prior art.
The mesostroma of example 1 below -4 pitch is board 70A grades of Zhenghai bi tumenf orr oad
Waste Crumb rubber gives up heavy sevice type rubber powder for 30 mesh in example 1 below -4
Thermoplastic elastomer is styrene-butadiene-styrene (SBS) in example 1 below -4.
Waste phosphoric acid ester is is derived from when Tianjin Li Hai petrochemical industry Co., Ltd prepares phosphate flame retardant not in example 1 below -4
The waste material of reaction.
Thermoplastic resin is rosin resin in example 1 below -4.
Plasticizer is o-phthalic acid dibutyl ester in example 1 below -4.
Crosslinking agent is using S (Cosan), the composition of Vulcanization accelerator TMTD, its quality parts ratio in example 1 below -4
2:1.
The preparation process of example 1 below -4 is as follows:
(1) waste Crumb rubber, thermoplastic elastomer (TPE), waste phosphoric acid ester are proportionally added into high-speed stirring mixer to carry out
Asphalt modifier is made in premix;
(2) matrix pitch is melted at a temperature of 130 DEG C and is warming up to 180 DEG C again, stirring thereto adds asphalt modification
Agent is stirred 5 minutes, then adds thermoplastic resin, plasticizer continues insulated and stirred 10 minutes, then pass through colloid mill shearing,
Grinding 10 minutes, subsequently into stirring development tank insulation development 2 it is small when, finally crosslinking agent is slowly added to using lifting auger,
Continue that the high viscose glue powder-modified asphalt of noise reduction drainage pavement is made when insulated and stirred 2 is small.
Comparative example 1
7%SBS (linear) is weighed by matrix pitch weight ratio to be added in matrix pitch and shear 15min, is then kept the temperature
Stir 2 it is small when, be subsequently agitated for adding 0.3% crosslinking agent, continue insulated and stirred 2 it is small when, high viscous SBS modified pitch is made.
Embodiment 1
A kind of noise reduction drainage pavement is according to mass fraction with high viscose glue powder-modified asphalt, its composition of raw materials:No. 70 matrix
79.8 parts of pitch, 15 parts of waste Crumb rubber, 1 part of thermoplastic elastomer (TPE), 2 parts of waste phosphoric acid ester, 1 part of thermoplastic resin, 1 part of plasticizer,
0.2 part of crosslinking agent.Preparation process is for example above-mentioned.
Embodiment 2
A kind of noise reduction drainage pavement is according to mass fraction with high viscose glue powder-modified asphalt, its composition of raw materials:No. 70 matrix
73.8 parts of pitch, 18 parts of waste Crumb rubber, 2 parts of thermoplastic elastomer (TPE), 3 parts of waste phosphoric acid ester, 2 parts of thermoplastic resin, 1 part of plasticizer,
0.1 part of crosslinking agent.Preparation process is for example above-mentioned.
Embodiment 3
A kind of noise reduction drainage pavement is according to mass fraction with high viscose glue powder-modified asphalt, its composition of raw materials:No. 70 matrix
59.7 parts of pitch, 25 parts of waste Crumb rubber, 2 parts of thermoplastic elastomer (TPE), 6 parts of waste phosphoric acid ester, 4 parts of thermoplastic resin, 3 parts of plasticizer,
0.3 part of crosslinking agent.Preparation process is for example above-mentioned.
Embodiment 4
A kind of noise reduction drainage pavement is according to mass fraction with high viscose glue powder-modified asphalt, its composition of raw materials:No. 70 matrix
67.8 parts of pitch, 20 parts of waste Crumb rubber, 3 parts of thermoplastic elastomer (TPE), 4 parts of waste phosphoric acid ester, 3 parts of thermoplastic resin, 2 parts of plasticizer,
0.2 part of crosslinking agent.Preparation process is for example above-mentioned.
Embodiment 5-11
A kind of noise reduction drainage pavement modified asphalt material described in high viscose glue powder-modified asphalt, according to the mass fraction, by 56-
80 parts of matrix pitches, 15-25 parts of waste Crumb rubber, 1-3 parts of thermoplastic elastomer (TPE), 1.5-6 parts of waste phosphoric acid esters, 1-5 parts of heat
Plastic resin, 1-5 parts of plasticizer and 0.1-0.3 parts of crosslinking agent are prepared.
The corresponding noise reduction drainage pavements of embodiment 5-11 are with the specific raw material composition of high viscose glue powder modified asphalt material such as the institute of table 1
Show:
The corresponding noise reduction drainage pavements of 1 embodiment 5-15 of table are formed with the raw material of high viscose glue powder modified asphalt material
Wherein, waste phosphoric acid ester prepares unreacted during phosphate flame retardant give up to be derived from Tianjin Li Hai petrochemical industry Co., Ltd
Material, is specially triphenyl phosphate.
Noise reduction drainage pavement is as follows with the preparation method of high viscose glue powder modified asphalt material:
(1) waste Crumb rubber, thermoplastic elastomer (TPE), waste phosphoric acid ester are mixed to join high-speed stirring mixer and are premixed,
Asphalt modifier is made;The rotating speed of high-speed stirring mixer is:1000-1450 revs/min, stirring is done time as 2-15 minutes in advance,
The temperature of high-speed stirred time control glue powder is at 50-60 DEG C.
(2) matrix pitch is melted at a temperature of 120-140 DEG C and is warming up to 170-190 DEG C again, stirring thereto adds
Stirred 5-10 minutes after the asphalt modifier, then add thermoplastic resin, plasticizer continuation insulated and stirred 5-15 minutes,
Then pass through colloid mill shearing, grinding 10-20 minute after, into stirring development tank insulation develop 1-3 it is small when, finally by crosslinking agent
It is slowly added to, continues that the high viscose glue powder-modified asphalt of noise reduction drainage pavement is made when insulated and stirred 1-3 is small.
The preparation condition such as table 2 below institute of the high viscose glue powder modified asphalt material of the corresponding noise reduction drainage pavements of embodiment 5-15
Show:
The preparation condition of the high viscose glue powder modified asphalt material of the corresponding noise reduction drainage pavements of 2 embodiment 5-15 of table
2nd, Function detection
Glue the performance comparison of SBS modified pitch with the general height of comparative example 1 with modified pitch prepared by embodiment 1-4 respectively
Such as table 3:
3 modified asphalt technology index of table
Modified asphalt material prepared by embodiment 1-4 respectively with gather materials (building stones) be mixed to prepare the modifications of AC-13 gradings
Asphalt carries out performance comparison, test result such as table 2:
2 asphalt test result of table
It can be seen that from above experimental data using the high viscose glue powder-modified asphalt of the noise reduction drainage pavement of the invention prepared
Dynamic viscosity is big, softening point is high for 60 DEG C of material, has excellent high-temperature stability, anti-rut behavior, ageing resistance.Pitch mixes
Material performance is fully achieved and is higher than《Standard specification for construction and acceptance of highway asphalt pavement》(JTJ052-2000) to the requirement of drainage pavement,
And its loss of dispersing, leakage analysis losing are smaller, there is higher dynamic stability, freeze-thaw split intensity ratio and higher asphalt filmthickness
Degree, the adhesiveness of asphalt and aggregate is more preferable, road surface have high temperature rutting resistance, low temperature anti-cracking ability, service life it is long, into
This low advantage, has high cost performance.
The above, is only presently preferred embodiments of the present invention, not the present invention is imposed any restrictions, it is every according to the present invention
Any simple modification, change and the equivalent structure change that technical spirit makees above example, still fall within skill of the present invention
In the protection domain of art scheme.
Claims (8)
1. a kind of high viscose glue powder modified asphalt material of noise reduction drainage pavement, it is characterized in that:The modified asphalt material presses quality
Number meter, by 56-80 parts of matrix pitches, 15-25 parts of waste Crumb rubber, 1-3 parts of thermoplastic elastomer (TPE), 1.5-6 parts of waste phosphoric acids
Ester, 1-5 parts of thermoplastic resin, 1-5 parts of plasticizer and 0.1-0.3 parts of crosslinking agent is prepared.
A kind of 2. high viscose glue powder modified asphalt material of noise reduction drainage pavement according to claim 1, it is characterised in that institute
It is 70A grades of bi tumenf orr oads to state matrix pitch.
A kind of 3. high viscose glue powder modified asphalt material of noise reduction drainage pavement according to claim 1, it is characterised in that institute
It is the one or more in useless heavy sevice type rubber powder, useless car tire rubber powder, useless conveyer belt powder or useless sole rubber powder to state waste Crumb rubber;
The waste Crumb rubber is by crushing, and after sieving, obtained particle diameter is the waste Crumb rubber of 20-40 mesh.
A kind of 4. high viscose glue powder modified asphalt material of noise reduction drainage pavement according to claim 1, it is characterised in that institute
Thermoplastic elastomer is stated as one in styrene-butadiene-styrene or styrene-isoprene-styrene copolymer
Kind is several.
A kind of 5. high viscose glue powder modified asphalt material of noise reduction drainage pavement according to claim 1, it is characterised in that institute
Thermoplastic resin is stated as one or both of note olefine resin or rosin resin;The plasticizer for o-phthalic acid dibutyl ester or
Dibutyl phthalate.
A kind of 6. high viscose glue powder modified asphalt material of noise reduction drainage pavement according to claim 1, it is characterised in that institute
Crosslinking agent is stated as Cosan, sulfur donor, cumyl peroxide, di-t-butyl peroxide benzene, magnesia, zinc oxide, oxygen
Change the one or more in lead, captax or Vulcanization accelerator TMTD.
7. according to the preparation method of any high viscose glue powder modified asphalt materials of noise reduction drainage pavement of claim 1-6,
It is characterised in that it includes following steps:
(1)Waste Crumb rubber, thermoplastic elastomer (TPE), waste phosphoric acid ester are mixed to join high-speed stirring mixer and are premixed, is made
Asphalt modifier;
(2)Matrix pitch is melted at a temperature of 120-140 DEG C and is warming up to 170-190 DEG C again, thereto described in stirring addition
Stirred 5-10 minutes after asphalt modifier, then add thermoplastic resin, plasticizer continuation insulated and stirred 5-15 minutes, then
After colloid mill is sheared, grinds 10-20 minutes, into stirring development tank insulation development 1-3 it is small when, it is finally that crosslinking agent is slow
Add, continue that the high viscose glue powder-modified asphalt of noise reduction drainage pavement is made when insulated and stirred 1-3 is small.
8. a kind of preparation method of the high viscose glue powder modified asphalt material of noise reduction drainage pavement according to claim 7, its
It is characterized in that, the rotating speed of the high-speed stirring mixer is:1000-1450 revs/min, stirring is done time as 2-15 minutes in advance, high
The temperature of speed stirring time control glue powder is at 50-60 DEG C.
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CN109796777A (en) * | 2018-12-14 | 2019-05-24 | 苏州三品交通建设工程有限公司 | Sponge urban water-through road surface pitch and preparation method thereof |
CN109943085A (en) * | 2019-03-20 | 2019-06-28 | 广西交通科学研究院有限公司 | A kind of composite modified high-viscosity asphalt of noise reduction drainage pavement rubber powder and preparation method |
CN111393787A (en) * | 2020-05-19 | 2020-07-10 | 上海群康沥青科技股份有限公司 | Anti-aging asphalt modifier for permeable pavement and preparation method and application thereof |
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CN117417645A (en) * | 2023-11-28 | 2024-01-19 | 河南金欧特实业集团股份有限公司 | Solid waste rubber powder modified emulsified asphalt for permeable pavement and preparation method and application thereof |
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