CN107964277A - A kind of high-adhesion scraping-resistant wipes organosilicon and scrapes inking and preparation method thereof - Google Patents
A kind of high-adhesion scraping-resistant wipes organosilicon and scrapes inking and preparation method thereof Download PDFInfo
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- CN107964277A CN107964277A CN201711363839.1A CN201711363839A CN107964277A CN 107964277 A CN107964277 A CN 107964277A CN 201711363839 A CN201711363839 A CN 201711363839A CN 107964277 A CN107964277 A CN 107964277A
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- Prior art keywords
- inking
- organosilicon
- scrapes
- wipes
- resistant
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Classifications
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D11/00—Inks
- C09D11/02—Printing inks
- C09D11/10—Printing inks based on artificial resins
- C09D11/102—Printing inks based on artificial resins containing macromolecular compounds obtained by reactions other than those only involving unsaturated carbon-to-carbon bonds
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D11/00—Inks
- C09D11/02—Printing inks
- C09D11/03—Printing inks characterised by features other than the chemical nature of the binder
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D11/00—Inks
- C09D11/02—Printing inks
- C09D11/03—Printing inks characterised by features other than the chemical nature of the binder
- C09D11/033—Printing inks characterised by features other than the chemical nature of the binder characterised by the solvent
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D11/00—Inks
- C09D11/02—Printing inks
- C09D11/03—Printing inks characterised by features other than the chemical nature of the binder
- C09D11/037—Printing inks characterised by features other than the chemical nature of the binder characterised by the pigment
Landscapes
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- General Chemical & Material Sciences (AREA)
- Compositions Of Macromolecular Compounds (AREA)
Abstract
The present invention relates to heat cure to scratch printing technical field of ink.Organosilicon, which is wiped, specifically related to a kind of high-adhesion scraping-resistant scrapes inking and preparation method thereof.This kind of high-adhesion scraping-resistant wipes organosilicon and scrapes inking and preparation method thereof; the high-adhesion scraping-resistant wipes organosilicon and scrapes inking by silica gel layer of cloth, heat conductive silica gel spacer layer and release protective layer; release protective layer is taken away in use; the high-adhesion scraping-resistant wipes organosilicon and scrapes performance of the inking with high intensity and high adhesion force; also there is the high characteristic of heat transfer efficiency at the same time; solve the demand of some terminal Code in Hazardous Special Locations, and there are all characteristics of common heat-conducting pad.In addition a kind of this kind of high-adhesion scraping-resistant wipes organosilicon and scrapes the preparation method of inking for simple and practicable, and securely and reliably, design is scientific and reasonable for step, and easily study easy to operate, is worth of widely use.
Description
Technical field
The present invention relates to heat cure to scratch printing technical field of ink.Being wiped specifically related to a kind of high-adhesion scraping-resistant has
Machine silicon scrapes inking and preparation method thereof.
Background technology
Blade coating printing be by coiled base material, by the scraper of definite shape, coat the glue of a layer specific function, coating or
Ink etc., and wound after drying.Organosilicon ink has obtained city since it has good hydrophobicity performance and satiny feel
The generally accreditation of field.Traditional organosilicon ink is only to have certain adhesive force for organic silicon substrate, is difficult to glue for some
The thermoplastic poor adhesive force connect, not rub resistance, seriously limits the use scope of organosilicon ink.
Organosilicon, which is wiped, it is an object of the invention to provide a kind of high-adhesion scraping-resistant scrapes inking and preparation method thereof, the height
Adhesive force scratch-resistant organosilicon scrapes each component component in inking and configures reasonable, strong adhesive force, scratch resistance for thermoplastic matrix
Hinder that performance is good, crocking resistance is excellent, hardening time is short and the characteristics of blade coating effect is good, manufacturing cost is cheap, stability is high,
Especially suitable for being difficult to the elastomeric substrate surface being bonded, have a good application prospect.In addition the high-adhesion scraping-resistant is wiped and had
Machine silicon scrapes the preparation method of inking for simple and practicable, and securely and reliably, design is scientific and reasonable for step, easily study easy to operate, value
It must promote the use of.
The content of the invention
The technical solution adopted by the present invention to solve the technical problems is：A kind of high-adhesion scraping-resistant wipes organosilicon and scrapes oiling
Ink, the high-adhesion scraping-resistant wiping organosilicon are scraped inking and are made of following raw materials by weight：
Polysiloxane 30%-45%
Color stuffing 10%-35%
Dispersant 5%-10%
Diluent 15%-25%
Crosslinking agent 0.2%-1%
Catalyst 0.01%-5%.
The preferable polysiloxane is ethenyl blocking dimethyl silicone polymer, the poly- ethylene methacrylic of epoxy radicals end-blocking
One or more in radical siloxane and tertiary amino block dimethyl silicone polymer；The color stuffing is nano-titanium dioxide, is received
One or more in rice zinc oxide and talcum powder；The dispersant is the polyethylene glycol that molecular weight is 400；The diluent is
By ethyl acetate and the mixture of dimethylbenzene；The crosslinking agent is hydrogen containing siloxane；The catalyst is the isopropyl of chloroplatinic acid
Alcoholic solution or Karst platinum catalyst.
The preferable ethenyl blocking dimethyl silicone polymer blocks dimethyl silicone polymer, its general formula for end-vinyl
Represent as follows：
Wherein, m=50-100, its viscosity is in 2000-20000mPa s.
The preferable epoxy radicals end-blocking Polymethyl methacrylate is the epoxy terminated poly- methyl ethylene silica of end-blocking
Alkane, its general formula represent as follows：
Wherein, m=50-80, n=8-12.
The general formula of the preferable tertiary amino block dimethyl silicone polymer represents as follows：
Wherein, m=30-50.
The general formula of the preferable hydrogen containing siloxane represents as follows：
Wherein, m=28-40, n=20-28, active hydrogen content is between 0.5%-1%.
The particle diameter of the preferable nano-titanium dioxide is 30-300 nanometers, and the nano-titanium dioxide passes through siloxanes
Cladding processing, the nano titanium dioxide crystal form structure is rutile-type；The Particle Size of Nanometer ZnO is 30-300 nanometers；
The talcum powder fineness is 45 microns, and the talcum powder is laminated structure.
A kind of high-adhesion scraping-resistant wipes the preparation method that organosilicon scrapes inking, it is characterised in that its step is：
In terms of following raw materials by weight,
（1）, the polysiloxane of 30%-45% added in blender, the scattered of 5%-10% is then added in whipping process
Continue stirring 30 minutes after the diluent of agent and 15%-25% so that the material in blender uniformly mixes；
（2）, then add the color stuffing of 10%-35%, the crosslinking agent of 0.2%-1% and the catalyst of 0.01%-5% into blender after
Continue stirring 60 minutes so that the material in blender uniformly mixes；
（3）, by step（2）The mixture stirred evenly, with sand mill be ground 2 it is small when, that is, be prepared into high-adhesion scraping-resistant
Wipe organosilicon and scrape inking.
The preferable step（1）With（2）In mixer stir speed (S.S.) be 400-500 rpms.
Organosilicon, which is wiped, it is an object of the invention to provide a kind of high-adhesion scraping-resistant scrapes inking and preparation method thereof, the height
Adhesive force scratch-resistant organosilicon scrapes each component component in inking and configures reasonable, strong adhesive force, scratch resistance for thermoplastic matrix
Hinder that performance is good, crocking resistance is excellent, hardening time is short and the characteristics of blade coating effect is good, manufacturing cost is cheap, stability is high,
Especially suitable for being difficult to the elastomeric substrate surface being bonded, have a good application prospect.In addition the high-adhesion scraping-resistant is wiped and had
Machine silicon scrapes the preparation method of inking for simple and practicable, and securely and reliably, design is scientific and reasonable for step, easily study easy to operate, value
It must promote the use of.
Embodiment
Specific embodiment one：A kind of high-adhesion scraping-resistant wipes organosilicon and scrapes inking, and the high-adhesion scraping-resistant is wiped organic
Silicon is scraped inking and is made of following raw materials by weight：
Polysiloxane 38%
Color stuffing 28%
Dispersant 8%
Diluent 22%
Crosslinking agent 0.5%
Catalyst 3.5%.
The color stuffing is nano-titanium dioxide；The dispersant is the polyethylene glycol that molecular weight is 400；The diluent
It is the mixture by ethyl acetate and dimethylbenzene；The catalyst be chloroplatinic acid aqueous isopropanol, the polysiloxane
It is that end-vinyl blocks dimethyl silicone polymer for ethenyl blocking dimethyl silicone polymer, its general formula represents as follows：
Wherein, m=50-100, its viscosity is in 2000-20000mPa s.
The general formula of the crosslinking agent hydrogen containing siloxane represents as follows：
Wherein, m=28-40, n=20-28, active hydrogen content is between 0.5%-1%.
The particle diameter of the nano-titanium dioxide is 30-300 nanometers, and the nano-titanium dioxide is by siloxanes cladding
Reason, the nano titanium dioxide crystal form structure is rutile-type.
A kind of high-adhesion scraping-resistant wipes the preparation method that organosilicon scrapes inking, it is characterised in that its step is：
In terms of following raw materials by weight,
（1）, 38% polysiloxane added in blender, 8% dispersant and 22% is then added in whipping process
Continue stirring 30 minutes after diluent so that the material in blender uniformly mixes；
（2）, then added into blender 28% color stuffing, continue stirring 60 after 0.5% crosslinking agent and 3.5% catalyst
Minute so that the material in blender uniformly mixes；
（3）, by step（2）The mixture stirred evenly, with sand mill be ground 2 it is small when, that is, be prepared into high-adhesion scraping-resistant
Wipe organosilicon and scrape inking.
The step（1）With（2）In mixer stir speed (S.S.) be 400 rpms.
Specific embodiment two：A kind of high-adhesion scraping-resistant wipes organosilicon and scrapes inking, and the high-adhesion scraping-resistant is wiped organic
Silicon is scraped inking and is made of following raw materials by weight：
Polysiloxane 45%
Color stuffing 22%
Dispersant 6%
Diluent 23%
Crosslinking agent 1%
Catalyst 3%.
The polysiloxane is epoxy radicals end-blocking Polymethyl methacrylate and tertiary amino block poly dimethyl silicon
Oxygen alkane；The color stuffing is nano zine oxide and talcum powder；The dispersant is the polyethylene glycol that molecular weight is 400；It is described dilute
It is the mixture by ethyl acetate and dimethylbenzene to release agent；The crosslinking agent is hydrogen containing siloxane；The catalyst is Karst
Platinum catalyst.
The epoxy radicals end-blocking Polymethyl methacrylate is epoxy terminated end-blocking Polymethyl methacrylate, it is logical
Formula represents as follows：
Wherein, m=50-80, n=8-12.
The general formula of the tertiary amino block dimethyl silicone polymer represents as follows：
Wherein, m=30-50.
The general formula of the hydrogen containing siloxane represents as follows：
Wherein, m=28-40, n=20-28, active hydrogen content is between 0.5%-1%.
The Particle Size of Nanometer ZnO is 30-300 nanometers；The talcum powder fineness is 45 microns, and the talcum powder is piece
Shape structure.
A kind of high-adhesion scraping-resistant wipes the preparation method that organosilicon scrapes inking, it is characterised in that its step is：
In terms of following raw materials by weight,
（1）, 45% polysiloxane added in blender, 6% dispersant and 22% is then added in whipping process
Continue stirring 30 minutes after diluent so that the material in blender uniformly mixes；
（2）, then added into blender 23% color stuffing, continue stirring 60 minutes after 1% crosslinking agent and 3% catalyst,
So that the material in blender uniformly mixes；
（3）, by step（2）The mixture stirred evenly, with sand mill be ground 2 it is small when, that is, be prepared into high-adhesion scraping-resistant
Wipe organosilicon and scrape inking.
The step（1）With（2）In mixer stir speed (S.S.) be 400-500 rpms.
Organosilicon, which is wiped, object of the present invention is to provide a kind of high-adhesion scraping-resistant scrapes inking and preparation method thereof, should
High-adhesion scraping-resistant wipes organosilicon and scrapes in inking that the configuration of each component component is reasonable, strong adhesive force for thermoplastic matrix, resistance to
The characteristics of scratch performance is good, crocking resistance is excellent, hardening time is short and blade coating effect is good, manufacturing cost are cheap, stability
Height, especially suitable for being difficult to the elastomeric substrate surface being bonded, has a good application prospect.In addition the high-adhesion scraping-resistant is wiped
Organosilicon scrapes the preparation method of inking for simple and practicable, and securely and reliably, design is scientific and reasonable for step, easily study easy to operate,
It is worth of widely use.
Obviously, the above embodiments are merely examples for clarifying the description, and the restriction not to embodiment.It is right
For those of ordinary skill in the art, can also make on the basis of the above description it is other it is various forms of change or
Change.There is no necessity and possibility to exhaust all the enbodiments.And the obvious change thus extended out or
Among changing still in the protection domain of the invention.
Claims (9)
1. a kind of high-adhesion scraping-resistant wipes organosilicon and scrapes inking, it is characterised in that：The high-adhesion scraping-resistant is wiped organosilicon and is scraped
Inking is made of following raw materials by weight：
Polysiloxane 30%-45%
Color stuffing 10%-35%
Dispersant 5%-10%
Diluent 15%-25%
Crosslinking agent 0.2%-1%
Catalyst 0.01%-5%.
2. a kind of high-adhesion scraping-resistant according to claim 1 wipes organosilicon and scrapes inking, it is characterised in that：It is described poly-
Organosiloxane is ethenyl blocking dimethyl silicone polymer, epoxy radicals end-blocking Polymethyl methacrylate and tertiary amino block
One or more in dimethyl silicone polymer；The color stuffing is nano-titanium dioxide, in nano zine oxide and talcum powder
It is one or more；The dispersant is the polyethylene glycol that molecular weight is 400；The diluent is by ethyl acetate and dimethylbenzene
Mixture；The crosslinking agent is hydrogen containing siloxane；The catalyst is the aqueous isopropanol or Karst platinum of chloroplatinic acid
Catalyst.
3. a kind of high-adhesion scraping-resistant according to claim 2 wipes organosilicon and scrapes inking, it is characterised in that：The second
Alkenyl end-blocking dimethyl silicone polymer blocks dimethyl silicone polymer for end-vinyl, its general formula represents as follows：
Wherein, m=50-100, its viscosity is in 2000-20000mPa s.
4. a kind of high-adhesion scraping-resistant according to claim 2 wipes organosilicon and scrapes inking, it is characterised in that：The epoxy
Base end-blocking Polymethyl methacrylate is epoxy terminated end-blocking Polymethyl methacrylate, its general formula represents as follows：
Wherein, m=50-80, n=8-12.
5. a kind of high-adhesion scraping-resistant according to claim 2 wipes organosilicon and scrapes inking, it is characterised in that：The uncle
The general formula of amino block dimethyl silicone polymer represents as follows：
Wherein, m=30-50.
6. a kind of high-adhesion scraping-resistant according to claim 2 wipes organosilicon and scrapes inking, it is characterised in that：It is described to contain
The general formula of hydrogen polysiloxanes represents as follows：
Wherein, m=28-40, n=20-28, active hydrogen content is between 0.5%-1%.
7. a kind of high-adhesion scraping-resistant according to claim 2 wipes organosilicon and scrapes inking, it is characterised in that：It is described to receive
The particle diameter of rice titanium dioxide is 30-300 nanometers, and the nano-titanium dioxide is handled by siloxanes cladding, the nano-silica
It is rutile-type to change titanium crystalline structure；The Particle Size of Nanometer ZnO is 30-300 nanometers；The talcum powder fineness is micro- for 45
Rice, the talcum powder is laminated structure.
8. a kind of high-adhesion scraping-resistant according to claim 1 wipes the preparation method that organosilicon scrapes inking, its feature exists
It is in its step：In terms of following raw materials by weight,
（1）, the polysiloxane of 30%-45% added in blender, the scattered of 5%-10% is then added in whipping process
Continue stirring 30 minutes after the diluent of agent and 15%-25% so that the material in blender uniformly mixes；
（2）, then add the color stuffing of 10%-35%, the crosslinking agent of 0.2%-1% and the catalyst of 0.01%-5% into blender after
Continue stirring 60 minutes so that the material in blender uniformly mixes；
（3）, by step（2）The mixture stirred evenly, with sand mill be ground 2 it is small when, that is, be prepared into high-adhesion scraping-resistant
Wipe organosilicon and scrape inking.
9. a kind of high-adhesion scraping-resistant according to claim 8 wipes the preparation method that organosilicon scrapes inking, its feature exists
In：The step（1）With（2）In mixer stir speed (S.S.) be 400-500 rpms.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201711363839.1A CN107964277A (en) | 2017-12-18 | 2017-12-18 | A kind of high-adhesion scraping-resistant wipes organosilicon and scrapes inking and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201711363839.1A CN107964277A (en) | 2017-12-18 | 2017-12-18 | A kind of high-adhesion scraping-resistant wipes organosilicon and scrapes inking and preparation method thereof |
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| CN107964277A true CN107964277A (en) | 2018-04-27 |
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| CN201711363839.1A Pending CN107964277A (en) | 2017-12-18 | 2017-12-18 | A kind of high-adhesion scraping-resistant wipes organosilicon and scrapes inking and preparation method thereof |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108802874A (en) * | 2018-05-22 | 2018-11-13 | 安徽智博新材料科技有限公司 | A kind of coated particle and preparation method thereof, application |
| WO2021102621A1 (en) * | 2019-11-25 | 2021-06-03 | Dow Silicones Corporation | Flame retardant polysiloxane composition |
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| CN1434788A (en) * | 1999-12-23 | 2003-08-06 | Dsm有限公司 | Optical fiber coating compositions |
| CN101962499A (en) * | 2009-07-22 | 2011-02-02 | 东莞市贝特利新材料有限公司 | Silica gel low-temperature laser-etching ink |
| CN102643580A (en) * | 2012-05-22 | 2012-08-22 | 昆山威茂电子科技有限公司 | Silica gel spraying ink formula and manufacturing technique thereof |
| CN104246605A (en) * | 2012-02-08 | 2014-12-24 | 道康宁韩国有限公司 | Curable and patternable inks and method of printing |
| CN106317894A (en) * | 2015-06-30 | 2017-01-11 | 比亚迪股份有限公司 | Organosilicone composition, reflecting coating, preparation method therefor and photovoltaic module comprising reflecting coating |
-
2017
- 2017-12-18 CN CN201711363839.1A patent/CN107964277A/en active Pending
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1434788A (en) * | 1999-12-23 | 2003-08-06 | Dsm有限公司 | Optical fiber coating compositions |
| CN101962499A (en) * | 2009-07-22 | 2011-02-02 | 东莞市贝特利新材料有限公司 | Silica gel low-temperature laser-etching ink |
| CN104246605A (en) * | 2012-02-08 | 2014-12-24 | 道康宁韩国有限公司 | Curable and patternable inks and method of printing |
| CN102643580A (en) * | 2012-05-22 | 2012-08-22 | 昆山威茂电子科技有限公司 | Silica gel spraying ink formula and manufacturing technique thereof |
| CN106317894A (en) * | 2015-06-30 | 2017-01-11 | 比亚迪股份有限公司 | Organosilicone composition, reflecting coating, preparation method therefor and photovoltaic module comprising reflecting coating |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108802874A (en) * | 2018-05-22 | 2018-11-13 | 安徽智博新材料科技有限公司 | A kind of coated particle and preparation method thereof, application |
| WO2021102621A1 (en) * | 2019-11-25 | 2021-06-03 | Dow Silicones Corporation | Flame retardant polysiloxane composition |
| CN114729190A (en) * | 2019-11-25 | 2022-07-08 | 美国陶氏有机硅公司 | Flame retardant polysiloxane compositions |
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Effective date of registration: 20191125 Address after: 215000 room 2, 245 lushijing Road, Kunshan Development Zone, Suzhou City, Jiangsu Province Applicant after: Kunshan Yuling heat transfer technology Co., Ltd Address before: Suzhou City, Jiangsu province 215300, Kunshan Development Zone Six Road No. 245 room 3 Applicant before: KUNSHAN YULING ELECTRONIC TECHNOLOGY CO., LTD. |
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