CN107961751A - A kind of reaction vessel for shortening the chemical raw material reaction time - Google Patents
A kind of reaction vessel for shortening the chemical raw material reaction time Download PDFInfo
- Publication number
- CN107961751A CN107961751A CN201711258917.1A CN201711258917A CN107961751A CN 107961751 A CN107961751 A CN 107961751A CN 201711258917 A CN201711258917 A CN 201711258917A CN 107961751 A CN107961751 A CN 107961751A
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- China
- Prior art keywords
- reaction vessel
- reaction
- main body
- air inlet
- inlet pipe
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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Links
- 238000006243 chemical reaction Methods 0.000 title claims abstract description 95
- 230000035484 reaction time Effects 0.000 title claims abstract description 15
- 239000013064 chemical raw material Substances 0.000 title claims abstract description 13
- 238000004904 shortening Methods 0.000 title claims abstract description 13
- 230000002687 intercalation Effects 0.000 claims description 6
- 238000009830 intercalation Methods 0.000 claims description 6
- 239000007788 liquid Substances 0.000 abstract description 10
- 230000009286 beneficial effect Effects 0.000 abstract description 5
- 238000009835 boiling Methods 0.000 abstract description 5
- 239000000463 material Substances 0.000 abstract description 3
- 239000002994 raw material Substances 0.000 description 7
- 238000001704 evaporation Methods 0.000 description 3
- 230000008020 evaporation Effects 0.000 description 3
- 239000003814 drug Substances 0.000 description 2
- 238000000034 method Methods 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- 230000009471 action Effects 0.000 description 1
- 238000001816 cooling Methods 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- 229940079593 drug Drugs 0.000 description 1
- 239000000975 dye Substances 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 238000010438 heat treatment Methods 0.000 description 1
- 230000006872 improvement Effects 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 239000000575 pesticide Substances 0.000 description 1
- 230000008569 process Effects 0.000 description 1
- 230000004044 response Effects 0.000 description 1
- 229910001220 stainless steel Inorganic materials 0.000 description 1
- 239000010935 stainless steel Substances 0.000 description 1
- 238000003756 stirring Methods 0.000 description 1
- 238000006467 substitution reaction Methods 0.000 description 1
- 238000009423 ventilation Methods 0.000 description 1
Classifications
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/18—Stationary reactors having moving elements inside
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/0053—Details of the reactor
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/0053—Details of the reactor
- B01J19/0066—Stirrers
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/00049—Controlling or regulating processes
- B01J2219/00051—Controlling the temperature
- B01J2219/00074—Controlling the temperature by indirect heating or cooling employing heat exchange fluids
- B01J2219/00076—Controlling the temperature by indirect heating or cooling employing heat exchange fluids with heat exchange elements inside the reactor
- B01J2219/00081—Tubes
Abstract
The present invention discloses a kind of reaction vessel for shortening the chemical raw material reaction time, including reactor main body, reactor main body is hollow circular cylinder structure, reaction vessel is equipped with reactor main body, vacuum cavity is equipped between reaction vessel and the inner wall of reactor main body, the reaction vessel interior is equipped with serpentine coil, and serpentine coil is circumferentially positioned at the inner wall of reaction vessel；Rotation axis is equipped with reaction vessel, rotation axis is equipped with rotating vane group, and the lower end of rotation axis is connected with driving motor, and driving motor is connected with frequency converter.By setting serpentine coil in reaction vessel in the technical program, circulating in serpentine coil has high-temperature gas, can fully be exchanged heat with the reacting material liquid in reaction vessel, be heated beneficial to liquid charging stock in reaction vessel, improves boiling degree.
Description
Technical field
The present invention relates to chemical drug equipment technical field, and in particular to a kind of reaction for shortening the chemical raw material reaction time is held
Device.
Background technology
Reaction kettle is the container physically or chemically reacted, by the structure design and parameter configuration to container, realizes technique
It is required that heating, evaporation, the mixture function of cooling and low high speed.And reaction kettle be widely used in oil, chemical industry, rubber, pesticide,
Pressure vessel in the technical process such as dyestuff, medicine, food, general material select stainless steel.
Reaction kettle is when as container for evaporation, and when its main liquid evaporated has toughness, reaction time, length, caused industrial life
It is low to produce efficiency.
Based on this, a kind of reaction vessel for shortening the chemical raw material reaction time has been researched and developed.
The content of the invention
The present invention provides a kind of reaction vessel for shortening the chemical raw material reaction time, and the internal structure of reaction kettle is closed
Reason design, makes the reaction in reaction kettle more abundant, shortens reaction time.
The present invention is achieved through the following technical solutions：
A kind of reaction vessel for shortening the chemical raw material reaction time, including reactor main body, reactor main body are hollow circle
Column structure, reactor main body is interior to be equipped with reaction vessel, and vacuum cavity is equipped between reaction vessel and the inner wall of reactor main body,
The reaction vessel interior is equipped with serpentine coil, and serpentine coil is circumferentially positioned at the inner wall of reaction vessel；It is equipped with reaction vessel
Rotation axis, rotation axis are equipped with rotating vane group, and the lower end of rotation axis is connected with driving motor, and driving motor connects with frequency converter
Connect.
Preferably, in order to preferably realize the present invention, there be the first air inlet pipe, the second air inlet in the bottom of the reaction vessel
Pipe, the first air inlet pipe, the second air inlet pipe are inserted into from the bottom of reaction vessel.
Preferably, in order to preferably realize the present invention, the positional distance in the first air inlet pipe intercalation reaction container is anti-
The distance for answering container bottom is 1/3-the 2/3 of reaction vessel height.
Preferably, in order to preferably realize the present invention, the positional distance in the second air inlet pipe intercalation reaction container is anti-
The distance for answering container bottom is 1/5-the 2/5 of reaction vessel height..
Preferably, the rotating vane group is made of multiple rotating vanes, and the number of rotating vane group has multiple, and rotates
The distance between blade group is equal.
Compared with prior art, the present invention have the following advantages and advantages：
(1) the technical program is reacted by setting vacuum cavity between reactor main body and reaction vessel beneficial to reducing
Heat scatters and disappears in container, it is ensured that the reaction temperature in reaction vessel, the boiling degree that raw material reacts in intensified response container.
(2) by setting serpentine coil in reaction vessel in the technical program, circulating in serpentine coil has high-temperature gas, energy
It is enough fully to be exchanged heat with the reacting material liquid in reaction vessel, heat, carry beneficial to liquid charging stock in reaction vessel
High boiling degree.
(3) by setting rotation axis, rotating vane in reaction vessel in the technical program, make in the driving of driving motor
Under, rotating vane rotates at a high speed, is sufficiently stirred reaction raw materials, accelerates mixing.
Brief description of the drawings
Fig. 1 is the structure diagram of the present invention；
Wherein：1-reactor main body, 2-serpentine coil, 3-vacuum cavity, 4-rotating vane group, 5-rotation axis,
6-rotating vane, the 7-the first air inlet pipe, the 8-the second air inlet pipe, 9-driving motor, 10-reaction vessel.
Embodiment
For the object, technical solutions and advantages of the present invention are more clearly understood, with reference to embodiment, the present invention is made
Further to describe in detail, exemplary embodiment of the invention and its explanation are only used for explaining the present invention, are not intended as to this
The restriction of invention.
Embodiment 1：
As shown in Figure 1, a kind of reaction vessel for shortening the chemical raw material reaction time, including reactor main body 1, reaction kettle master
Body 1 is hollow circular cylinder structure, and reaction vessel 10, reaction vessel 10 and the inner wall of reactor main body 1 are equipped with reactor main body 1
Between be equipped with vacuum cavity 3, the reaction vessel 10 is internally provided with serpentine coil 2, and serpentine coil 2 is circumferentially positioned at reaction vessel
10 inner wall；Rotation axis 5 is equipped with reaction vessel 10, rotation axis 5 is equipped with rotating vane group 4, the lower end of rotation axis 5 and driving
Motor 9 connects, and driving motor 9 is connected with frequency converter.
Reactor main body 1 described in the present embodiment is to carry out the Primary containers of raw material reaction, and the container implemented
For reaction vessel 10, and vacuum cavity 3 is set between reaction vessel 10 and reactor main body 1, i.e., reaction vessel 10 is with reacting
Gap is equipped between 1 inner wall of kettle main body, is vacuumized between gap, beneficial to reaction vessel 10 reaction when, can remain compared with
High temperature, promotes the evaporation of liquid reaction raw material in reaction vessel to carry out.、
For some reactions are carried out in a kettle, such as added in main liquid is reacted and react auxiliary liquid, in order to react main liquid with
React and be uniformly mixed between auxiliary liquid, rotation axis 5 is equipped with reaction vessel, drive and is quickly rotated in rotating vane group 4,
And drive 4 rotating power of rotating vane group for driving motor driving, and in rotating vane group 4 rotating vane speed
It can be controlled by frequency converter.
In the present embodiment, the concrete structure such as the driving motor 9, frequency converter, rotating vane, rotation axis 5, reaction vessel 10
It is known to those skilled in the art, no longer it is described in detail.
Embodiment 2：
The present embodiment further limits on the basis of embodiment, and there be the first air inlet pipe the bottom of the reaction vessel 10
7th, the second air inlet pipe 8, the first air inlet pipe 7, the second air inlet pipe 8 are inserted into from the bottom of reaction vessel 10.
The effect of first air inlet pipe 7, the second air inlet pipe 8 is that gas such as air etc. is added into reaction vessel 10, is promoted
The boiling degree of reaction raw materials into reaction vessel 10.Wherein, the first air inlet pipe 7, the second air inlet pipe 8 are communicating tube structure.May be used also
For other air ventilation passages.
Embodiment 3：
The present embodiment and above-described embodiment difference lies in：Position in first air inlet pipe, the 7 intercalation reaction container 10
Distance apart from 10 bottom of reaction vessel is 1/3-the 2/3 of 10 height of reaction vessel.Second air inlet pipe, 8 intercalation reaction holds
The distance of 10 bottom of positional distance reaction vessel in device 10 is 1/5-the 2/5 of 10 height of reaction vessel.
Here by the way that to the first air inlet pipe 7, the position that the second air inlet pipe 8 is installed in reaction vessel 10 is configured, and is led to
Cross the first air inlet pipe 7, the second air inlet pipe 8 is passed through gas, and is passed through gas to diverse location, the gas being passed through can speed up reaction
The boiling degree of reaction raw materials in container 10.The concrete structure shape of reaction vessel 10 described in the present embodiment is hollow circuit cylinder
Body, and positioned at the inside of reactor main body.
Embodiment 4：
The present embodiment and above-described embodiment difference lies in：The rotating vane group 4 is made of multiple rotating vanes 6, rotation
The number of rotating vane piece group 4 has multiple, and the distance between rotating vane group 4 is equal.By setting rotating vane in rotation axis 5
Group 4, rotating vane group 4 is made of multiple rotating vanes, and the rotating vane 6 in rotating vane group 4 is circumferentially positioned at rotation axis 5
Around, it can speed up the stirring action to reaction raw materials in reaction vessel.Rotating vane 6 described in the present embodiment it is specific
Planform can be curvilaminar, or other shapes.
Above-described embodiment, has carried out the purpose of the present invention, technical solution and beneficial effect further
Describe in detail, it should be understood that the foregoing is merely the embodiment of the present invention, be not intended to limit the present invention
Protection domain, within the spirit and principles of the invention, any modification, equivalent substitution, improvement and etc. done, should all include
Within protection scope of the present invention.
Claims (5)
- A kind of 1. reaction vessel for shortening the chemical raw material reaction time, it is characterised in that：Including reactor main body (1), reaction kettle Main body (1) is hollow circular cylinder structure, and reaction vessel (10), reaction vessel (10) and reaction kettle are equipped with reactor main body (1) Vacuum cavity (3) is equipped between the inner wall of main body (1), the reaction vessel (10) is internally provided with serpentine coil (2), serpentine coil (2) it is circumferentially positioned at the inner wall of reaction vessel (10)；Rotation axis (5) is equipped with reaction vessel (10), rotation axis (5) is equipped with rotation Rotating vane piece group (4), the lower end of rotation axis (5) are connected with driving motor (9), and driving motor (9) is connected with frequency converter.
- A kind of 2. reaction vessel for shortening the chemical raw material reaction time according to claim 1, it is characterised in that：It is described anti- The bottom of container (10) is answered to also have the first air inlet pipe (7), the second air inlet pipe (8), the first air inlet pipe (7), the second air inlet pipe (8) are equal It is inserted into from the bottom of reaction vessel (10).
- A kind of 3. reaction vessel for shortening the chemical raw material reaction time according to claim 2, it is characterised in that：Described The distance of positional distance reaction vessel (10) bottom in one air inlet pipe (7) intercalation reaction container (10) is high for reaction vessel (10) 1/3-the 2/3 of degree.
- A kind of 4. reaction vessel for shortening the chemical raw material reaction time according to claim 2, it is characterised in that：Described The distance of positional distance reaction vessel (10) bottom in two air inlet pipe (8) intercalation reaction container (10) is high for reaction vessel (10) 1/5-the 2/5 of degree.
- A kind of 5. reaction vessel for shortening the chemical raw material reaction time according to claim 4, it is characterised in that：The rotation Rotating vane piece group (4) is made of multiple rotating vanes, the number of rotating vane group (4) have it is multiple, and between rotating vane group (4) Apart from equal.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201711258917.1A CN107961751A (en) | 2017-12-01 | 2017-12-01 | A kind of reaction vessel for shortening the chemical raw material reaction time |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201711258917.1A CN107961751A (en) | 2017-12-01 | 2017-12-01 | A kind of reaction vessel for shortening the chemical raw material reaction time |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN107961751A true CN107961751A (en) | 2018-04-27 |
Family
ID=61999295
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201711258917.1A Pending CN107961751A (en) | 2017-12-01 | 2017-12-01 | A kind of reaction vessel for shortening the chemical raw material reaction time |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN107961751A (en) |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN203577784U (en) * | 2013-09-23 | 2014-05-07 | 厦门市隆兴化工机械有限公司 | Jacket reaction kettle |
| CN104415730A (en) * | 2013-08-30 | 2015-03-18 | 天津市朋得利化工有限公司 | Chemical reaction tank |
| CN105498261A (en) * | 2016-01-21 | 2016-04-20 | 宜宾高县钧恒新材料有限公司 | Distillation kettle and operation process thereof |
| CN208115719U (en) * | 2017-12-01 | 2018-11-20 | 成都欧林生物科技股份有限公司 | A kind of reaction kettle with raw material boiling degree in raising reaction vessel |
-
2017
- 2017-12-01 CN CN201711258917.1A patent/CN107961751A/en active Pending
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104415730A (en) * | 2013-08-30 | 2015-03-18 | 天津市朋得利化工有限公司 | Chemical reaction tank |
| CN203577784U (en) * | 2013-09-23 | 2014-05-07 | 厦门市隆兴化工机械有限公司 | Jacket reaction kettle |
| CN105498261A (en) * | 2016-01-21 | 2016-04-20 | 宜宾高县钧恒新材料有限公司 | Distillation kettle and operation process thereof |
| CN208115719U (en) * | 2017-12-01 | 2018-11-20 | 成都欧林生物科技股份有限公司 | A kind of reaction kettle with raw material boiling degree in raising reaction vessel |
Non-Patent Citations (1)
| Title |
|---|
| 贝聿泷等: "《聚酯纤维手册》", 纺织工业出版社 * |
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| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| RJ01 | Rejection of invention patent application after publication |
Application publication date: 20180427 |