CN107961318A - The concocting method of stir-baked RHIZOMA POLYGONATI with yellow rice wine - Google Patents
The concocting method of stir-baked RHIZOMA POLYGONATI with yellow rice wine Download PDFInfo
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- CN107961318A CN107961318A CN201711397385.XA CN201711397385A CN107961318A CN 107961318 A CN107961318 A CN 107961318A CN 201711397385 A CN201711397385 A CN 201711397385A CN 107961318 A CN107961318 A CN 107961318A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
- A61K36/18—Magnoliophyta (angiosperms)
- A61K36/88—Liliopsida (monocotyledons)
- A61K36/896—Liliaceae (Lily family), e.g. daylily, plantain lily, Hyacinth or narcissus
- A61K36/8969—Polygonatum (Solomon's seal)
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2236/00—Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
- A61K2236/10—Preparation or pretreatment of starting material
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2236/00—Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
- A61K2236/10—Preparation or pretreatment of starting material
- A61K2236/17—Preparation or pretreatment of starting material involving drying, e.g. sun-drying or wilting
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Abstract
The invention discloses a kind of concocting method of stir-baked RHIZOMA POLYGONATI with yellow rice wine, yellow rice wine is added into dry sealwort medicinal material, sealwort medicinal material is fully absorbed yellow rice wine, then after 0 36h of vexed profit, the sealwort medicinal material for absorbing yellow rice wine is steamed, taken out after steaming 7 13h, and piece is cut into, then dry at 60 90 DEG C, drying to water content is down to 8 11%, by dried sealwort pulverizing medicinal materials to 40 mesh sieves are crossed, stir-baked RHIZOMA POLYGONATI with yellow rice wine is obtained.Provide clear and definite steaming time, vexed profit time and drying temperature, the stir-baked RHIZOMA POLYGONATI with yellow rice wine stable quality obtained according to parameter production, meet medicinal material requirement, improve the quality of steamed sealwort decoction piece, also it is the chemical composition change that have studied in sealwort concocting process at the same time, disclose the principle in concocting process, there is provided more theoretical foundations.
Description
Technical field
The present invention relates to Chinese medicine processing technique field, is specially a kind of concocting method of stir-baked RHIZOMA POLYGONATI with yellow rice wine.
Background technology
Sealwort has long medicinal history in China, and sealwort health product can stimulate throat, meanwhile, after processing its tonifying Qi support
The cloudy, effect of invigorating the spleen moistening lung is strengthened, so there are the custom processed to sealwort in the successive dynasties, concocting method is with cooking process
Based on, mainly there is the methods of single steaming, steaming, nine steam nine exposures, add auxiliary material to steam again.2015 editions《Chinese Pharmacopoeia》Sealwort and wine are recorded
Two kinds of processed products of sealwort, but rule regulation has only been done, can only in actual production without the specific technological parameter of science
Processed by the experience of worker, it is difficult to ensure the quality of medicine materical crude slice after processing.
2015 editions《Chinese Pharmacopoeia》Two kinds of processed products of sealwort and stir-baked RHIZOMA POLYGONATI with yellow rice wine have been recorded, but have only done rule regulation,
There is no the specific technological parameter of science, the experience of worker can only be leaned in actual production to process, it is difficult to ensure medicine materical crude slice after processing
Quality.
The content of the invention
In view of the deficiencies of the prior art, the present invention provides a kind of concocting method of stir-baked RHIZOMA POLYGONATI with yellow rice wine, it specify that stir-baked RHIZOMA POLYGONATI with yellow rice wine
The technological parameter of processing, the stir-baked RHIZOMA POLYGONATI with yellow rice wine stable quality obtained according to parameter production, meets medicinal material requirement.
In order to achieve the above object, the present invention is achieved by the following technical programs：The concocting method of stir-baked RHIZOMA POLYGONATI with yellow rice wine, to drying
Yellow rice wine is added in sealwort medicinal material, sealwort medicinal material is fully absorbed yellow rice wine, then after vexed profit 0-36h, the sealwort of yellow rice wine will be absorbed
Medicinal material is steamed, and is taken out after steaming 7-13h, and is cut into piece, then dry at 60-90 DEG C, dry to water content drop
To 8-11%, by dried sealwort pulverizing medicinal materials to 40 mesh sieves are crossed, stir-baked RHIZOMA POLYGONATI with yellow rice wine is obtained.
The mass ratio of dry sealwort medicinal material and yellow rice wine is 100：15-30.
Beneficial effect
The present invention provides a kind of Special constant temperature sink.Possesses following beneficial effect：Provide clear and definite steaming time, vexed
Moisten time and drying temperature, the stir-baked RHIZOMA POLYGONATI with yellow rice wine stable quality obtained according to parameter production, meets medicinal material requirement, improves steamed Huang
The quality of smart medicine materical crude slice, while be also the chemical composition change that have studied in sealwort concocting process, the principle in concocting process is disclosed,
Provide more theoretical foundations.
Embodiment
The embodiment of the present invention：The concocting method of stir-baked RHIZOMA POLYGONATI with yellow rice wine
1 experiment material and instrument
1.1 experiment crude drug sources
This problem medicinal material sample is planted company by Guizhou Province great Yu king and is provided, and for December, Huang is spent more in lifes in 3 years of harvesting
Essence, HUANGJING ZANYU CAPSULE David's-harp (Polygonatum Cyrtonema Hua) is accredited as through Guizhou University professor Xiong Xinyuan.
1.2 experiment reagent
Absolute ethyl alcohol A.R, Chongqing Chuan Dong Chemical Co., Ltd.s chemical reagent factory
Concentrated sulfuric acid A.R, Chongqing Chuan Dong Chemical Co., Ltd.s chemical reagent factory
Anthrone A.R, Tianjin Kermel Chemical Reagent Co., Ltd.
Glucose Chinese food drug assay research institute
Make by oneself in distilled water laboratory
Yellow rice wine 12.0%vol, Zhejiang Yue Jing Shaoxing rice wines Co., Ltd
1.3 laboratory apparatus
Current chart level instruments and meters Co., Ltd on FA2004 assay balances
0027391 enviromental protection instrument factory of Jintan City of digital display thermostat water bath Jiangsu Province
Give positive experimental instruments and equipment limited in SHZ-95B type multiplex vavuum pump of circulating water type Shanghai
Medical Equipment Plant of GZX-9146MBE digital display air dry ovens Shanghai Boxun Industrial Co., Ltd.
HY-0413 type medicinal herb grinder Huan Ya Tianyuans Mechanical Technology Inc.
UV-1801 type ultraviolet specrophotometers Beijing Rayleigh Analytical Instrument Co., Ltd
Vernier caliper Shanghai Measuring and Cutting Tools Plant
HR83 moisture analysers Mettler Toledo Inc.
2 experimental methods and result
The concocting method of stir-baked RHIZOMA POLYGONATI with yellow rice wine, adds 20g yellow rice wine into dry 100g sealwort medicinal materials, makes sealwort medicinal material that yellow rice wine is complete
Absorb, then after vexed profit 0-36h, the sealwort medicinal material for absorbing yellow rice wine is steamed, is taken out after steaming 7-13h, and be cut into
Piece, is then dried at 60-90 DEG C, and 8-11% is down in drying to water content, by dried sealwort pulverizing medicinal materials to 40 mesh excessively
Sieve, obtains stir-baked RHIZOMA POLYGONATI with yellow rice wine.
2.1 stir-baked RHIZOMA POLYGONATI with yellow rice wine processing procedure single factor explorations
2.1.1 the investigation of stir-baked RHIZOMA POLYGONATI with yellow rice wine vexed profit time
(1) processing of different vexed profit time samples
The drying sealwort medicinal material 100g after Habitat producing is chosen, is put into tool plug wide-mouth bottle, is weighed 20g yellow rice wine and pour into wide-mouth
In bottle, plug is covered, wide-mouth bottle is shaken in rotation, and after sealwort is exhausted yellow rice wine, respectively after vexed profit 0,12,24,36h, sample is put
Enter and steamed in suitable steamer, take out sample after steaming 7h, record the appearance mouthfeel of sample, cut sheet, be put into 70 DEG C of oven dryings, extremely
Sample moisture content is down to about 10%, stops drying, takes out sample, it is spare to crushed 40 mesh sieves with pulverizer.
(2) the appearance mouth feel score of different vexed profit time samples
Stir-baked RHIZOMA POLYGONATI with yellow rice wine medicine materical crude slice using it is inside and outside moisten, color it is black, it is sweet, without bitter taste and without numb feeling in the tongue as top grade.So taste with sample
Profit situation (30%), color (30%) and mouthfeel (40%) etc. carry out comprehensive grading to sample, and standards of grading are shown in Table 4-1.
Table 4-1 sample appearance mouth feel score standards
Using moist situation, color and the mouthfeel of sample as index, scored respectively each sample by 5 people, full marks 100
Point, the appearance mouth feel score for sample is finally averaged, the results are shown in Table 4-2.
Table 4-2 sample appearance mouth feel score results
(3) polyoses content, alcohol leaching thing and the soaking object assay of different vexed profit time samples
The sample obtained by 2.1.1 is taken, according to polysaccharide, alcohol leaching thing and the soaking object content of the method measurement each sample of chapter 2.
It the results are shown in Table 4-3.
Polysaccharide, alcohol leaching thing and the soaking object content of table 4-3 samples
(4) selection of vexed profit time
Appearance mouth feel score, polyoses content, alcohol leaching thing content and the soaking object content of comprehensive sample, calculate the person in servitude of each sample
Category degree, formula：Comprehensive grading=appearance mouthfeel degree of membership × 30%+ polysaccharide degree of membership × 30%+ soaking objects degree of membership ×
20%+ alcohol leaching thing degree of membership × 20%, calculates the comprehensive grading of each sample, the results are shown in Table 4-4.
The comprehensive grading of the different vexed profit time samples of table 4-4
From table 4-4, the appearance mouth feel score of vexed 0h samples is up to 81 points, the appearance mouth feel score of vexed 24h samples
It is minimum, it is 76 points.The polyoses content highest of vexed 12h samples, is 6.79%, the polyoses content of vexed 24h samples is minimum, is
6.13%；The alcohol leaching thing content highest of vexed 0h samples, is 84.77%, the alcohol leaching thing content of vexed 24h samples is minimum, is
78.79%；The soaking object content highest of vexed 0h samples, is 83.74%, the soaking object content of vexed 24h samples is minimum, is
78.35%.The comprehensive grading highest of sample when the vexed profit time is 0h, is 0.90；The comprehensive grading of vexed profit 24h samples is minimum, is
0。
2.1.2 the investigation of stir-baked RHIZOMA POLYGONATI with yellow rice wine steaming time
(1) processing of different steaming time samples
The drying sealwort medicinal material 100g after Habitat producing is chosen, is put into tool plug wide-mouth bottle, is weighed 20g yellow rice wine and pour into wide-mouth
In bottle, plug is covered, wide-mouth bottle is shaken in rotation, sealwort is exhausted yellow rice wine, after vexed profit 12h, sample is put into suitable steamer and is steamed
System, steam 7 respectively, 9,11, take out sample after 13h, after the appearance mouthfeel for recording sample, cut sheet, be put into 70 DEG C of oven dryings,
Sample moisture content is down to about 10%, stops drying, takes out sample, it is spare to crushed 40 mesh sieves with pulverizer.
(2) the appearance mouth feel score of different steaming time samples
Score according to 2.1 sample appearance mouth feel score method the sample of different steaming times, gained appraisal result
It is shown in Table 4-5.
The appearance mouth feel score of table 4-5 samples
(3) measure of the polysaccharide of different steaming time samples, alcohol leaching thing and soaking object content
The sample of different steaming times is taken, is contained according to polysaccharide, alcohol leaching thing and the soaking object of the method measurement each sample of chapter 2
Amount.It the results are shown in Table 4-6.
Polysaccharide, alcohol leaching thing and the soaking object content of table 4-6 samples
(3) selection of stir-baked RHIZOMA POLYGONATI with yellow rice wine steaming time
Appearance mouth feel score, polyoses content, alcohol leaching thing content and the soaking object content of comprehensive sample, calculate the person in servitude of each sample
Category degree, formula：Comprehensive grading=appearance mouthfeel degree of membership × 30%+ polysaccharide degree of membership × 30%+ soaking objects degree of membership ×
20%+ alcohol leaching thing degree of membership × 20%, calculates the comprehensive grading of each sample, the results are shown in Table 4-7.
The comprehensive grading of table 4-7 difference steaming time samples
From table 4-7, the appearance mouth feel score for steaming 13h samples is up to 80 points, steams the appearance mouthfeel of 7h samples
Score minimum, be 73 points；The polyoses content highest of 7h samples is steamed, is 6.97%, it is minimum to steam the polyoses content of 13h samples,
For 5.39%；The alcohol leaching thing content highest of 9h samples is steamed, is 84.76%, it is minimum to steam the alcohol leaching thing content of 7h samples, is
82.07%；The soaking object content highest of 9h samples is steamed, is 85.68%, it is minimum to steam the soaking object content of 7h samples, is
81.36%.Appearance mouth feel score increases with the increase of steaming time, and polyoses content is continuous with the increase of steaming time
Reduction, alcohol leaching thing content and soaking object content are then the trend in reduction after first increasing.The synthesis of sample when steaming time is 11h
Score highest, is 0.74；It is minimum to steam the comprehensive grading of 7h samples, is 0.30.
2.1.3 the investigation of stir-baked RHIZOMA POLYGONATI with yellow rice wine drying temperature
(1) processing of different dry Temperature samples
The drying sealwort medicinal material 100g after Habitat producing is chosen, is put into tool plug wide-mouth bottle, is weighed 20g yellow rice wine and pour into wide-mouth
In bottle, plug is covered, wide-mouth bottle is shaken in rotation, sealwort is exhausted yellow rice wine, after vexed profit 12h, sample is put into suitable steamer and is steamed
Make, take out sample after 7h, cut sheet, be respectively put into 60,70,80,90 DEG C of oven dryings, about 10% is down to sample moisture content,
Drying time is recorded, stops drying, it is spare to crushed 40 mesh sieves with pulverizer.
(2) polysaccharide, alcohol leaching thing and the soaking object content of different dry Temperature samples
The sample of different drying temperatures is taken, is contained according to polysaccharide, alcohol leaching thing and the soaking object of the method measurement each sample of chapter 2
Amount, formula：Comprehensive grading=polysaccharide degree of membership × 35%+ soaking objects degree of membership × 25%+ alcohol leaching thing degree of membership × 25%+
Time degree of membership × 15%, calculates the comprehensive grading of each sample, the results are shown in Table and be shown in Table 4-8.
The comprehensive grading of the different dry Temperature samples of table 4-8
From table 4-8, when drying temperature is 70 DEG C, polysaccharide, alcohol leaching thing and the soaking object content of sample reach maximum；
With the rising of drying temperature, drastically reduced the time required to dry, but the polysaccharide of sample, alcohol leaching thing and soaking object content are also anxious
Reduce sharply few.When drying temperature reaches more than 90 DEG C, the indices of sample have obvious reduction；Drying temperature is done at 60 DEG C
The dry time is longer, and polyoses content, alcohol leaching thing and soaking object content have declined.By the COMPREHENSIVE CALCULATING to each sample index,
The composite score highest of the David's-harp sample of 70 DEG C of oven dryings is obtained, is the David's-harp sample of 0.90,90 DEG C of oven dryings
The composite score of product is minimum, is 0.15.With the rising of drying temperature, the composite score of each sample is in first to rise becoming of declining afterwards
Gesture.
The orthogonal test of 2.2 stir-baked RHIZOMA POLYGONATI with yellow rice wine
According to single factor exploration as a result, using vexed profit time, steaming time and drying temperature as investigation factor, three are respectively taken
Level design is tested, and factor level table is shown in Table 4-9.
Table 4-9 factor level tables
Tested with the factor level table of table 4-9, appearance mouth feel score, polyoses content, the alcohol leaching of measurement gained sample
Thing and soaking object content, calculate the degree of membership of each sample, formula：Comprehensive grading=appearance mouthfeel degree of membership × 30%+ is more
Sugared degree of membership × 30%+ soaking objects degree of membership × 20%+ alcohol leaching thing degree of membership × 20%, calculates the comprehensive grading of each sample, knot
Fruit is shown in Table 4-10, analysis in table 4-11 directly perceived, and variance analysis is shown in Table 4-12.
The comprehensive grading of table 4-10 samples
The analysis directly perceived of table 4-11 orthogonal experiments
Table 4-12 orthogonal experiments variance analyses
From table 4-11 and table 4-12, influence of 3 kinds of factors to sample comprehensive grading is followed successively by C ＞ A ＞ from big to small
B, it is maximum to show that drying temperature influences the comprehensive grading of stir-baked RHIZOMA POLYGONATI with yellow rice wine medicine materical crude slice, secondly the vexed profit time, the influence of steaming time is most
It is small.Optimal stir-baked RHIZOMA POLYGONATI with yellow rice wine processing technology is A2B3C1, be it is vexed profit the time for 6 it is small when, steaming time for 12 it is small when after, 65 DEG C of dryings.
Although an embodiment of the present invention has been shown and described, for the ordinary skill in the art, can be with
Understanding without departing from the principles and spirit of the present invention can carry out these embodiments a variety of changes, modification, replace
And modification, the scope of the present invention is defined by the appended.
Claims (2)
- A kind of 1. concocting method of stir-baked RHIZOMA POLYGONATI with yellow rice wine, it is characterised in that：Yellow rice wine is added into dry sealwort medicinal material, makes sealwort medicinal material by Huang Wine fully absorbs, then after vexed profit 0-36h, the sealwort medicinal material for absorbing yellow rice wine is steamed, is taken out after steaming 7-13h, and will It is cut into slices, and then dry at 60-90 DEG C, 8-11% is down in drying to water content, by dried sealwort pulverizing medicinal materials extremely 40 mesh sieves are crossed, obtain stir-baked RHIZOMA POLYGONATI with yellow rice wine.
- It is 2. according to claim 1, it is characterised in that：The mass ratio of dry sealwort medicinal material and yellow rice wine is 100：15-30.
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Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110898160A (en) * | 2019-10-25 | 2020-03-24 | 桂东县兴民药材种植专业合作社 | Processing method of rhizoma polygonati |
| CN111773312A (en) * | 2020-07-22 | 2020-10-16 | 西藏天虹科技股份有限责任公司 | Fine processing method of sealwort particles |
| CN113616729A (en) * | 2021-07-24 | 2021-11-09 | 吉林化工学院 | Optimized processing technology of polygonatum sibiricum with wine |
| CN114748572A (en) * | 2022-03-19 | 2022-07-15 | 南京中医药大学 | Immunity-enhancing polygonatum sibiricum decoction pieces as well as processing method and application thereof |
| CN115814021A (en) * | 2022-12-01 | 2023-03-21 | 陕西中医药大学 | Rhizoma polygonati total flavone extract and extraction method and application thereof |
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2017
- 2017-12-21 CN CN201711397385.XA patent/CN107961318A/en active Pending
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110898160A (en) * | 2019-10-25 | 2020-03-24 | 桂东县兴民药材种植专业合作社 | Processing method of rhizoma polygonati |
| CN111773312A (en) * | 2020-07-22 | 2020-10-16 | 西藏天虹科技股份有限责任公司 | Fine processing method of sealwort particles |
| CN113616729A (en) * | 2021-07-24 | 2021-11-09 | 吉林化工学院 | Optimized processing technology of polygonatum sibiricum with wine |
| CN114748572A (en) * | 2022-03-19 | 2022-07-15 | 南京中医药大学 | Immunity-enhancing polygonatum sibiricum decoction pieces as well as processing method and application thereof |
| CN115814021A (en) * | 2022-12-01 | 2023-03-21 | 陕西中医药大学 | Rhizoma polygonati total flavone extract and extraction method and application thereof |
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