CN107917996A - A kind of finished product rice multifunctional detecting device and its application method - Google Patents
A kind of finished product rice multifunctional detecting device and its application method Download PDFInfo
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- CN107917996A CN107917996A CN201710976515.9A CN201710976515A CN107917996A CN 107917996 A CN107917996 A CN 107917996A CN 201710976515 A CN201710976515 A CN 201710976515A CN 107917996 A CN107917996 A CN 107917996A
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- chamber
- sensing chamber
- process chamber
- finished product
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- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N33/00—Investigating or analysing materials by specific methods not covered by groups G01N1/00 - G01N31/00
- G01N33/02—Food
- G01N33/10—Starch-containing substances, e.g. dough
Abstract
The invention belongs to finished product rice health detection technique field, more particularly to a kind of finished product rice multifunctional detecting device and its application method, function includes aflatoxin detection, heavy-metal residual detection and Detecting Pesticide, its structure includes sensing chamber, and sensing chamber includes sensing chamber one, multistep sensing chamber and single step sensing chamber.The present invention has the following advantages compared with prior art:It is detected in the present invention after being handled accordingly respectively finished product rice of device science, multistep sensing chamber and single step sensing chamber can operate at the same time, substantially increase the work efficiency of detection, wherein to the detection relative error control of finished product rice heavy-metal residual within 3%, to the control of Detecting Pesticide relative error within 1%, to aflatoxin detection relative error control within 1.4%, whole device can realize the monitoring of hygiene requirement of finished product rice, practicality is high, can promote the use of.
Description
Technical field
The invention belongs to finished product rice health detection technique field, and in particular to a kind of finished product rice multifunctional detecting device
And its application method.
Background technology
China is eating rice production country maximum in the world at present, account for the yield in the whole world 35%, while has been ranked among
The rice exports state ranks of medicine, rice are the Chinese medicine commodity of agricultural products in China international trade, are main agricultural exports, rice
Inlet and outlet particularly outlet is the important form that China participates in international cooperation with competition, but rice and dependent merchandise outlet in recent years
The barrier of green trade is often bumped against, in order to reach in the world to the maximum residue limit standard of rice product, it is existing to become us
In urgent problem, but existing detection method is relatively cumbersome, it is necessary to more multidisciplinary realize, slow down China significantly
To the speed of rice product quality testing, therefore, it is necessary to for rice product health examination criteria, study a kind of convenient detection
Device.
The content of the invention
The purpose of the present invention is for existing issue, there is provided a kind of finished product rice multifunctional detecting device and its user
Method.
The present invention is achieved by the following technical solutions:A kind of finished product rice multifunctional detecting device, its function include
Aflatoxin detection, heavy-metal residual detection and Detecting Pesticide, its structure include sensing chamber, bag are equipped with above sensing chamber
The pretreatment chamber of sloped sidewall is included, feed pipe and water inlet pipe one are equipped with above pretreatment chamber;Detected for cylinder sensing chamber bottom
Room one, one bottom centre position of sensing chamber set groove equipped with card, and sieve is in bottom surface of the sensing chamber one in addition to card sets groove, sieve bottom
Portion is equipped with multiple telescopic baffles, and multiple telescopic baffle splicing gained are overall and sieve shape is just as telescopic baffle is by being installed on inspection
Survey the telescopic device control of room side wall;The sensing chamber one corresponds to upper center position and is equipped with driving device one, driving device one
Interior to be equipped with arrangements for speed regulation, one lower section connection rotating shaft one of driving device, one periphery of shaft is equipped with paddle one, and the lower section of paddle one is
It is even to be equipped with multiple protrusions, wherein driving device one can drive shaft one move up and down;
Sensing chamber's one side wall installation heavy metal detector, heavy metal detector side connection display device;
The lower section of sensing chamber is divided into multistep sensing chamber and single step sensing chamber by demarcation strip;
Wherein multistep sensing chamber includes process chamber one, centrifugal chamber and part flow arrangement one, and wherein process chamber one is by tipping tube one and inspection
Survey room one to connect, one upper end of process chamber connection feed pipe two, process chamber one is connected and installed in sensing chamber's side wall by spring one, handles
Vibrator one is installed in one bottom of room, and process chamber one side wall upper end is equipped with negative pressure straw one, the connection centrifugation of one other end of negative pressure straw
Room, centrifugal chamber upper end connection feed pipe three, centrifugal chamber is interior to be equipped with the shaft two driven by driving device two, is equipped with around shaft two
Paddle two, centrifugal chamber sidewall upper are equipped with negative pressure straw two, and negative pressure straw two connects part flow arrangement one, one lower end of part flow arrangement
Equipped with diversion pipe one, diversion pipe is once correspondingly provided with detection box one;
Wherein single step sensing chamber includes process chamber two and part flow arrangement two, and wherein process chamber two is connected by tipping tube two and sensing chamber one
Logical, two upper end of process chamber connection feed pipe four, process chamber two is connected and installed in sensing chamber's side wall, two bottom of process chamber by spring two
Vibrator two is installed, two sidewall upper of process chamber is equipped with negative pressure straw three, and three other end of negative pressure straw connection part flow arrangement two, divides
Two lower end of stream device is equipped with diversion pipe two, and detection box two is correspondingly provided with diversion pipe two.
Wherein, the sensing chamber one is detected for heavy-metal residual, and multistep sensing chamber is used for Detecting Pesticide, single step inspection
Room is surveyed to detect for aflatoxin.
Wherein, the feed pipe one is passed through raw material as the finished product rice after crushing, and powder particle diameter is 20-80 mesh.
A kind of application method of finished product rice multifunctional detecting device, including herein below:
(1)By rice crushed material and water by weight 1:3 add, and add completion one shaft one of rear drive equipment and are moved downwardly to turn
Axis one is located at card and sets in groove, and after the stirring 2 minutes of 600-800 revs/min of rotating speed, heavy metal detector draws part suspension
It is detected;
(2)Rotation axis one is again turned on, with the above-mentioned suspension of 20-40 revs/min of stirring of rotating speed, telescopic device is by telescopic baffle
Withdraw, suspension uniformly enters tipping tube one and tipping tube two by the sieve of bottom;
(3)Weigh to entering the suspension in process chamber one, add the second containing 0.1% acetic acid equivalent to its weight 50%
Nitrile, opens vibrator one, and the vibration frequency of vibrator one is 60Hz, after shaking 1 minute, continuously adds anhydrous with acetonitrile equivalent
Magnesium sulfate and the sodium acetate equivalent to its weight 25%, vibrator one work on after ten minutes, close vibrator one, stand
When 1.5-2 is small;
(4)Start negative pressure straw one, draw the upper solution of gross weight 6-8% in process chamber one at this time, start negative pressure straw one
Before, added in centrifugal chamber equivalent to the PSA of its weight 5%, 15% anhydrous magnesium sulfate and 5% C18;Upper solution has added
Into rear startup driving device two, stirred 5 minutes for 3000-3600 revs/min with rotating speed, when standing 6-8 is small;
(5)Start negative pressure straw two, draw the upper solution two of gross weight 6-8% in centrifugal chamber at this time, upper solution two-way is undue
Stream device one shunts, then is imported by diversion pipe one in corresponding detection box one, detects in box one and holds corresponding Test paper;
(6)To weighing into the suspended of process chamber two, the first that the mass concentration for adding 5-6 times equivalent to its weight is 50%
Alcohol solution, opens vibrator two, and the vibration frequency of vibrator two is 80-100Hz, after shaking 3 minutes, when standing 3-4 is small;
(7)Start negative pressure straw three, draw the upper solution of gross weight 15-18% in process chamber two at this time, upper solution two passes through
Part flow arrangement two shunts, then is imported by diversion pipe two in corresponding detection box two, detects in box two and holds corresponding Test paper.
The wherein setting of spring one and spring two, contributes to material in process chamber one and process chamber two uniformly to mix.
The present invention has the following advantages compared with prior art:Device science carries out phase respectively to finished product rice in the present invention
It is detected after the processing answered, multistep sensing chamber and single step sensing chamber can operate at the same time, substantially increase the work effect of detection
Rate, wherein to the detection relative error control of finished product rice heavy-metal residual within 3%, to Detecting Pesticide relative error control
System is within 1%, and to aflatoxin detection relative error control within 1.4%, whole device can realize defending for finished product rice
Raw detection requirement, practicality is high, can promote the use of.
Brief description of the drawings
Fig. 1 is the structure diagram of the present invention.
Embodiment
The present invention is further described below in conjunction with the accompanying drawings.
As shown in fig. 1, a kind of finished product rice multifunctional detecting device, its function include aflatoxin detection, a huge sum of money
Belong to residue detection and Detecting Pesticide, its structure includes sensing chamber 1, and the top of sensing chamber 1 is equipped with the pre- place for including sloped sidewall
Room 2 is managed, the top of pretreatment chamber 2 is equipped with feed pipe 3 and water inlet pipe 1;2 bottom of sensing chamber is cylindrical sensing chamber 1, is detected
One 29 bottom centre position of room sets groove 26 equipped with card, and sieve is in bottom surface of the sensing chamber 1 in addition to card sets groove 26, sieve bottom
Portion is equipped with multiple telescopic baffles 41, and the multiple splicing of telescopic baffle 41 gained are overall and sieve shape is just as telescopic baffle 41 is by pacifying
Telescopic device control 4 loaded on 1 side wall of sensing chamber;The sensing chamber 1 corresponds to upper center position and is equipped with driving device one
22, driving device 1 is interior to be equipped with arrangements for speed regulation(Do not marked in figure), one 22 lower section connection rotating shaft 1 of driving device, shaft one
23 peripheries are equipped with paddle 1, and the lower section of paddle 1 is uniformly provided with multiple protrusions, and protrusion can be semi-circular projection or square herein
Shape is raised, contributes to raw material to be stirred evenly with water, wherein driving device 1 can drive shaft 1 move up and down;
Sensing chamber's one 29 side wall installation heavy metal detector 27,27 side of heavy metal detector connection display device 28;
The lower section of sensing chamber 1 is divided into multistep sensing chamber 5 and single step sensing chamber 6 by demarcation strip;
Wherein multistep sensing chamber 5 includes process chamber 1, centrifugal chamber 52 and part flow arrangement 1, and wherein process chamber 1 is by tilting
Pipe 1 is connected with sensing chamber 1, and one 51 upper end of process chamber connection feed pipe 2 512, process chamber 1 is connected by spring 1
Connect and be installed on 1 side wall of sensing chamber, one 51 bottom of process chamber installing vibrator 1, one 51 sidewall upper of process chamber is equipped with negative pressure
Suction pipe 1, one 514 other end of negative pressure straw connection centrifugal chamber 52,52 upper end of centrifugal chamber connection feed pipe 3 521, centrifugal chamber
The shaft 2 524 driven by driving device 2 523 is equipped with 52, paddle 2 525, centrifugal chamber 52 are equipped with around shaft 2 524
Sidewall upper is equipped with negative pressure straw 2 522, and negative pressure straw 2 522 connects part flow arrangement 1, and one 53 lower end of part flow arrangement is equipped with
Diversion pipe 1, detection box 1 is correspondingly provided with diversion pipe 1;
Wherein single step sensing chamber 6 includes process chamber 2 61 and part flow arrangement 2 62, wherein process chamber 2 61 by tipping tube 2 613 with
Sensing chamber 1 connects, and 2 61 upper end of process chamber connection feed pipe 4 612, process chamber 2 61 is connected and installed in by spring 2 611
1 side wall of sensing chamber, 2 61 bottom of process chamber installing vibrator 2 614,2 61 sidewall upper of process chamber are equipped with negative pressure straw three
615,3 615 other end of negative pressure straw connection part flow arrangement 2 62,2 62 lower end of part flow arrangement is equipped with diversion pipe 2 621, water conservancy diversion
Detection box 2 622 is correspondingly provided with pipe 2 621.
Wherein, the sensing chamber 1 is detected for heavy-metal residual, and multistep sensing chamber 5 is used for Detecting Pesticide, single
Sensing chamber 6 is walked to detect for aflatoxin.
Wherein, the feed pipe 1 is passed through raw material as the finished product rice after crushing, and powder particle diameter is 20-80 mesh.
A kind of application method of finished product rice multifunctional detecting device, including herein below:
(1)By rice crushed material and water by weight 1:3 add, and add completion one 22 shaft 1 of rear drive equipment and move downward
It is located at card to shaft 1 to set in groove 26, after the stirring 2 minutes of 600-800 revs/min of rotating speed, heavy metal detector 27 is drawn
Part suspension is detected;
(2)Rotation axis 1 is again turned on, with the above-mentioned suspension of 20-40 revs/min of stirring of rotating speed, telescopic device 4 will be flexible
Baffle 41 is withdrawn, and suspension uniformly enters tipping tube 1 and tipping tube 2 613 by the sieve of bottom;
(3)Weigh to entering the suspension in process chamber 1, add the second containing 0.1% acetic acid equivalent to its weight 50%
Nitrile, opens vibrator 1, and the vibration frequency of vibrator 1 is 60Hz, after shaking 1 minute, continuously adds and acetonitrile equivalent
Anhydrous magnesium sulfate and the sodium acetate equivalent to its weight 25%, vibrator 1 work on after ten minutes, close vibrator
One 515, when standing 1.5-2 is small;
(4)Start negative pressure straw 1, draw the upper solution of gross weight 6-8% in process chamber 1 at this time, start negative pressure
Before suction pipe 1, added in centrifugal chamber 52 equivalent to the PSA of its weight 5%, 15% anhydrous magnesium sulfate and 5% C18;Upper strata
Solution starts driving device 2 523 after the completion of adding, and is stirred 5 minutes for 3000-3600 revs/min with rotating speed, when standing 6-8 is small;
(5)Start negative pressure straw 2 522, draw the upper solution two of gross weight 6-8% in centrifugal chamber 52 at this time, upper solution two
Shunted by part flow arrangement 1, then imported by diversion pipe 1 in corresponding detection box 1, detected and held in box 1
Corresponding Test paper;
(6)To weighing into the suspended of process chamber 2 61, the mass concentration for adding 5-6 times equivalent to its weight is 50%
Methanol aqueous solution, opens vibrator 2 614, and the vibration frequency of vibrator 2 614 is 80-100Hz, after shaking 3 minutes, stands 3-
4 it is small when;
(7)Start negative pressure straw 3 615, draw the upper solution of gross weight 15-18% in process chamber 2 61 at this time, upper solution
Two-way crosses the shunting of part flow arrangement 2 62, then is imported by diversion pipe 2 621 in corresponding detection box 2 622, is contained in detection box 2 622
Put corresponding Test paper.
It is opposite to Detecting Pesticide to miss wherein to the detection relative error control of finished product rice heavy-metal residual within 3%
Difference control is within 1%, and to aflatoxin detection relative error control within 1.4%, whole device can realize finished product rice
The monitoring of hygiene requirement.
Specifically, application method is only preferred embodiment in the present invention, by the chemical substance for adding other parts by weight
Respective substance is effectively extracted, it is also possible to device in the present invention;, also can be by adjusting adding to other crops or food inspection room
Charging uses.
The foregoing is merely illustrative of the preferred embodiments of the present invention, is not intended to limit the invention, all essences in the present invention
All any modification, equivalent and improvement made within refreshing and principle etc., should all be included in the protection scope of the present invention.
Claims (4)
1. a kind of finished product rice multifunctional detecting device, it is characterised in that its function is residual including aflatoxin detection, heavy metal
Detection and Detecting Pesticide are stayed, its structure includes sensing chamber, is equipped with the pretreatment chamber for including sloped sidewall above sensing chamber, in advance
Feed pipe and water inlet pipe one are equipped with above process chamber;Sensing chamber bottom is cylindrical sensing chamber one, one bottom centre of sensing chamber position
Card is installed and has set groove, as sieve, screen bottom is equipped with multiple telescopic baffles, multiple for bottom surface of the sensing chamber one in addition to card sets groove
Telescopic baffle splicing gained is overall and sieve shape is just as telescopic baffle is controlled by the telescopic device for being installed on sensing chamber's side wall;
The sensing chamber one corresponds to upper center position and is equipped with driving device one, and arrangements for speed regulation, driving device are equipped with driving device one
One lower section connection rotating shaft one, one periphery of shaft are equipped with paddle one, and the lower section of paddle one is uniformly provided with multiple protrusions, wherein driving
Device one can drive shaft one move up and down;
Sensing chamber's one side wall installation heavy metal detector, heavy metal detector side connection display device;
The lower section of sensing chamber is divided into multistep sensing chamber and single step sensing chamber by demarcation strip;
Wherein multistep sensing chamber includes process chamber one, centrifugal chamber and part flow arrangement one, and wherein process chamber one is by tipping tube one and inspection
Survey room one to connect, one upper end of process chamber connection feed pipe two, process chamber one is connected and installed in sensing chamber's side wall by spring one, handles
Vibrator one is installed in one bottom of room, and process chamber one side wall upper end is equipped with negative pressure straw one, the connection centrifugation of one other end of negative pressure straw
Room, centrifugal chamber upper end connection feed pipe three, centrifugal chamber is interior to be equipped with the shaft two driven by driving device two, is equipped with around shaft two
Paddle two, centrifugal chamber sidewall upper are equipped with negative pressure straw two, and negative pressure straw two connects part flow arrangement one, one lower end of part flow arrangement
Equipped with diversion pipe one, diversion pipe is once correspondingly provided with detection box one;
Wherein single step sensing chamber includes process chamber two and part flow arrangement two, and wherein process chamber two is connected by tipping tube two and sensing chamber one
Logical, two upper end of process chamber connection feed pipe four, process chamber two is connected and installed in sensing chamber's side wall, two bottom of process chamber by spring two
Vibrator two is installed, two sidewall upper of process chamber is equipped with negative pressure straw three, and three other end of negative pressure straw connection part flow arrangement two, divides
Two lower end of stream device is equipped with diversion pipe two, and detection box two is correspondingly provided with diversion pipe two.
2. a kind of finished product rice multifunctional detecting device as claimed in claim 1, it is characterised in that the sensing chamber one is used for weight
Metal residual detects, and multistep sensing chamber is used for Detecting Pesticide, and single step sensing chamber is detected for aflatoxin.
3. a kind of finished product rice multifunctional detecting device as claimed in claim 2, it is characterised in that the feed pipe one is passed through
Raw material is the finished product rice after crushing, and powder particle diameter is 20-80 mesh.
4. a kind of application method of finished product rice multifunctional detecting device as claimed in claim 3, it is characterised in that including following
Content:
(1)By rice crushed material and water by weight 1:3 add, and add completion one shaft one of rear drive equipment and are moved downwardly to turn
Axis one is located at card and sets in groove, and after the stirring 2 minutes of 600-800 revs/min of rotating speed, heavy metal detector draws part suspension
It is detected;
(2)Rotation axis one is again turned on, with the above-mentioned suspension of 20-40 revs/min of stirring of rotating speed, telescopic device is by telescopic baffle
Withdraw, suspension uniformly enters tipping tube one and tipping tube two by the sieve of bottom;
(3)Weigh to entering the suspension in process chamber one, add the second containing 0.1% acetic acid equivalent to its weight 50%
Nitrile, opens vibrator one, and the vibration frequency of vibrator one is 60Hz, after shaking 1 minute, continuously adds anhydrous with acetonitrile equivalent
Magnesium sulfate and the sodium acetate equivalent to its weight 25%, vibrator one work on after ten minutes, close vibrator one, stand
When 1.5-2 is small;
(4)Start negative pressure straw one, draw the upper solution of gross weight 6-8% in process chamber one at this time, start negative pressure straw one
Before, added in centrifugal chamber equivalent to the PSA of its weight 5%, 15% anhydrous magnesium sulfate and 5% C18;Upper solution has added
Into rear startup driving device two, stirred 5 minutes for 3000-3600 revs/min with rotating speed, when standing 6-8 is small;
(5)Start negative pressure straw two, draw the upper solution two of gross weight 6-8% in centrifugal chamber at this time, upper solution two-way is undue
Stream device one shunts, then is imported by diversion pipe one in corresponding detection box one, detects in box one and holds corresponding Test paper;
(6)To weighing into the suspended of process chamber two, the first that the mass concentration for adding 5-6 times equivalent to its weight is 50%
Alcohol solution, opens vibrator two, and the vibration frequency of vibrator two is 80-100Hz, after shaking 3 minutes, when standing 3-4 is small;
(7)Start negative pressure straw three, draw the upper solution of gross weight 15-18% in process chamber two at this time, upper solution two passes through
Part flow arrangement two shunts, then is imported by diversion pipe two in corresponding detection box two, detects in box two and holds corresponding Test paper.
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CN201710976515.9A CN107917996A (en) | 2017-10-19 | 2017-10-19 | A kind of finished product rice multifunctional detecting device and its application method |
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CN201710976515.9A CN107917996A (en) | 2017-10-19 | 2017-10-19 | A kind of finished product rice multifunctional detecting device and its application method |
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Cited By (2)
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CN108613854A (en) * | 2018-05-09 | 2018-10-02 | 深圳市中科智诚科技有限公司 | A kind of agricultural products quality detection apparatus that detection result is good |
CN111855355A (en) * | 2020-07-29 | 2020-10-30 | 江西省农业科学院农产品质量安全与标准研究所 | Detection apparatus for pesticide residue in livestock and poultry breeding feed |
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Application publication date: 20180417 |
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