CN107913549A - Using the bacteriostasis antibiosis ceramic element of nanometer coal charcoal, preparation method - Google Patents

Using the bacteriostasis antibiosis ceramic element of nanometer coal charcoal, preparation method Download PDF

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Publication number
CN107913549A
CN107913549A CN201711256316.7A CN201711256316A CN107913549A CN 107913549 A CN107913549 A CN 107913549A CN 201711256316 A CN201711256316 A CN 201711256316A CN 107913549 A CN107913549 A CN 107913549A
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small
ceramic element
nanometer
coal charcoal
raw material
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CN201711256316.7A
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Chinese (zh)
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不公告发明人
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Chong Mengxia
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Chong Mengxia
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Abstract

The invention discloses a kind of bacteriostasis antibiosis ceramic element using nanometer coal charcoal, preparation method, it is mainly made of glauconite, bryozoatum, bentonite, nanometer coal charcoal, powdered rice hulls, razor clam king's shell powder, limonite, sodium acid carbonate, acrylic emulsion, cane molasses, monkey grass, corn flour, phenolic resin, epoxidized soybean oil, beeswax, antibacterial additive.The ceramic element of the present invention is with glauconite, bryozoatum is primary raw material, and it with the addition of a nanometer coal charcoal, powdered rice hulls, razor clam king's shell powder, the raw materials such as limonite, so that ceramic element has good strainability, the harmful substances such as heavy metal can effectively be adsorbed, and stable chemical performance, water resistance is good, hokutolite in the antibacterial additive of addition, crystal rubble can discharge substantial amounts of anion, good bactericidal bacteriostasis can be played, natural manganese sand, nanometer silver carbon molecular sieve, nano zine oxide cooperates, not only there is good filtering absorption property, also there is good bactericidal property.

Description

Using the bacteriostasis antibiosis ceramic element of nanometer coal charcoal, preparation method
Technical field
The present invention relates to technical field of ceramic material, more specifically a kind of bacteriostasis antibiosis using nanometer coal charcoal is made pottery Porcelain filter core, preparation method.
Background technology
Ceramic element, is mainly used for filtering drinking water, antibacterial and activation process, harmful chlorine residue and suspended pollution Thing, organic chemicals, color and peculiar smell, the drinking water for reaching certain standard for drinking can be filtered out by using the filter core. Both the industries such as water purifier, bottled water and quality classification water supply can be applied to, can also be applied to water quality is supplied with corresponding requirements its Its occasion.The highest ceramic element of filtering accuracy is film-made ceramic element for dual control in the world at present, and average pore size is 0.1 μm.Through Water after the filter element filtering need not boil, you can drink, the standard of national direct drinking water is fully achieved.As people are to health The pursuit of life and the requirement of water quality are higher and higher, and ceramic element will more be widely used in drinking water treatment field.
Present ambient air pollution is extremely serious, and haze weather has brought great harm, air adsorption filtering Material can adsorb the various hazardous particulate matters of air, such as PM2.5, prevent the life into people or working environment, reduce people Suction of the body lung to harmful substances such as particulate matters, improves the quality of life of people, reduces the generation of disease.Existing filtering material Mainly there are ceramic honey comb, filter paper, nanometer coal charcoal, steel wire etc..Existing ceramic filter material raw material, formula, function all compare It is single, it is impossible to meet the requirement that technology continues to develop.
The content of the invention
The purpose of the invention is to make up the deficiencies in the prior art, there is provided a kind of bacteriostasis antibiosis ceramic element and its preparation Method.
The purpose of the present invention is what is be achieved through the following technical solutions：
A kind of bacteriostasis antibiosis ceramic element, is made of the raw material of following parts by weight：Glauconite 60-70, bryozoatum 30-40, swelling Native 12-15, nanometer coal charcoal 8-12, powdered rice hulls 6-8, razor clam king's shell powder 3-5, limonite 4-6, sodium acid carbonate 3-5, propylene yogurt Liquid 1-2, cane molasses 1-2, monkey grass 2-4, corn flour 1-3, phenolic resin 3-5, epoxidized soybean oil 4-6, beeswax 1-2, suppression Bacteria additive 6-7；
The antibacterial additive is made of following raw material：Hokutolite 20-30, crystal rubble 15-18, natural manganese sand 8- 12nd, nanometer silver carbon molecular sieve 3-5, nano zine oxide 1-3, lauryl glucosyl 0.5-1, hydrogen peroxide 35-45；Preparation method For：Hokutolite, crystal rubble, natural manganese sand are calcined at 810-870 DEG C 1-2 it is small when after attrition grinding into powder, then and receive The silver-colored carbon molecular sieve of rice, nano zine oxide are uniformly mixed, add lauryl glucosyl, hydrogen peroxide stirring 1-1.5 it is small when, so Filtering is taken out afterwards；Cleaned 3-4 times with distilled water, drying.
A kind of preparation method of bacteriostasis antibiosis ceramic element, comprises the following steps：
(1) suitable water is added after mixing glauconite, bryozoatum, bentonite, nanometer coal charcoal, powdered rice hulls, limonite, is stirred When immersion 2-3 is small after uniformly, weakly acidic pH is washed till with clear water after filtering, in 80 DEG C~100 DEG C dryings, in 600 DEG C~800 DEG C calcinings When 1-2 is small, cooling crush；
(2) razor clam king's shell powder, acrylic emulsion, corn flour, phenolic resin, beeswax are added after monkey grass is crushed, in 40-50 It is mixed 30-40 minutes at DEG C；
(3) raw material after being crushed in step (1), the raw material in step (2), antibacterial additive and other remaining compositions are mixed Close, vacuum pugging, be sent into mould in, after the demoulding, be sent into 250-270 DEG C of sintering furnace in sinter 1-2 it is small when, then, with 4-6 DEG C/ Minute speed be warming up to 750-800 DEG C of sintering 2-3 it is small when, then, then with 8-10 DEG C/min of speed be warming up to 1150-1250 DEG C When sintering 4-5 is small to obtain the final product.
The advantage of the invention is that：
The ceramic element of the present invention with the addition of nanometer coal charcoal, powdered rice hulls, a razor clam using glauconite, bryozoatum as primary raw material The raw materials such as king's shell powder, limonite so that ceramic element has good strainability, can effectively adsorb the nuisances such as heavy metal Matter, and stable chemical performance, water resistance is good, and hokutolite, crystal rubble can discharge largely in the antibacterial additive of addition Anion, good bactericidal bacteriostasis, natural manganese sand, nanometer silver carbon molecular sieve, nano zine oxide phase interworking can be played Close, not only with good filtering absorption property, it may have good bactericidal property.
Embodiment
Embodiment 1
A kind of bacteriostasis antibiosis ceramic element, is made of the raw material of following weight (kg)：Glauconite 60, bryozoatum 30, bentonite 12, Nanometer coal charcoal 8, powdered rice hulls 6, razor clam king's shell powder 3, limonite 4, sodium acid carbonate 3, acrylic emulsion 1, cane molasses 1, palm Fiber 2, corn flour 1, phenolic resin 3, epoxidized soybean oil 4, beeswax 1, antibacterial additive 6；
The antibacterial additive is made of following weight (kg) raw material：Hokutolite 20, crystal rubble 15, natural manganese sand 8, nanometer Silver-colored carbon molecular sieve 3, nano zine oxide 1, lauryl glucosyl 0.5, hydrogen peroxide 35；Preparation method is：By hokutolite, crystal Rubble, natural manganese sand calcined at 810 DEG C 2 it is small when after attrition grinding into powder, then with nanometer silver carbon molecular sieve, nano zine oxide Be uniformly mixed, add lauryl glucosyl, hydrogen peroxide stirring 1.5 it is small when, then filtering take out；3 are cleaned with distilled water It is secondary, drying.
A kind of preparation method of bacteriostasis antibiosis ceramic element, comprises the following steps：
(1) suitable water is added after mixing glauconite, bryozoatum, bentonite, nanometer coal charcoal, powdered rice hulls, limonite, is stirred When immersion 2 is small after uniformly, weakly acidic pH is washed till with clear water after filtering, in 80 DEG C of dryings, when 600 DEG C of calcinings 1 are small, cooling crush；
(2) razor clam king's shell powder, acrylic emulsion, corn flour, phenolic resin, beeswax are added after monkey grass is crushed, at 40 DEG C It is lower to be mixed 30 minutes；
(3) raw material after being crushed in step (1), the raw material in step (2), antibacterial additive and other remaining compositions are mixed Close, vacuum pugging, be sent into mould, after the demoulding, when sintering 1 is small in 250 DEG C of sintering furnaces of feeding, then, with 4 DEG C/min of speed Be warming up to 750 DEG C sintering 2 it is small when, then, then with 8 DEG C/min of speed be warming up to 1150 DEG C sintering 4 it is small when to obtain the final product.
Embodiment 2
A kind of bacteriostasis antibiosis ceramic element, is made of the raw material of following weight (kg)：Glauconite 65, bryozoatum 35, bentonite 13, Nanometer coal charcoal 10, powdered rice hulls 7, razor clam king's shell powder 4, limonite 5, sodium acid carbonate 4, acrylic emulsion 1, cane molasses 1, palm Fiber 3, corn flour 2, phenolic resin 4, epoxidized soybean oil 5, beeswax 1, antibacterial additive 6；
The antibacterial additive is made of following weight (kg) raw material：Hokutolite 25, crystal rubble 16, natural manganese sand 10, receive The silver-colored carbon molecular sieve 4 of rice, nano zine oxide 2, lauryl glucosyl 0.7, hydrogen peroxide 40；Preparation method is：By hokutolite, water Brilliant rubble, natural manganese sand calcined at 850 DEG C 1.5 it is small when after attrition grinding into powder, then with nanometer silver carbon molecular sieve, nano oxygen Change zinc be uniformly mixed, add lauryl glucosyl, hydrogen peroxide stirring 1.5 it is small when, then filtering take out；It is clear with distilled water 4 times are washed, drying.
A kind of preparation method of bacteriostasis antibiosis ceramic element, comprises the following steps：
(1) suitable water is added after mixing glauconite, bryozoatum, bentonite, nanometer coal charcoal, powdered rice hulls, limonite, is stirred When immersion 2.5 is small after uniformly, weakly acidic pH is washed till with clear water after filtering, in 90 DEG C of dryings, when 700 DEG C of calcinings 1.5 are small, cools down powder It is broken；
(2) razor clam king's shell powder, acrylic emulsion, corn flour, phenolic resin, beeswax are added after monkey grass is crushed, at 45 DEG C It is lower to be mixed 35 minutes；
(3) raw material after being crushed in step (1), the raw material in step (2), antibacterial additive and other remaining compositions are mixed Close, vacuum pugging, be sent into mould, after the demoulding, when sintering 1.5 is small in 260 DEG C of sintering furnaces of feeding, then, with 5 DEG C/minute of clock rates Degree be warming up to 780 DEG C sintering 2.5 it is small when, then, then with 9 DEG C/min of speed be warming up to 1200 DEG C sintering 4.5 it is small when to obtain the final product.
Embodiment 3
A kind of bacteriostasis antibiosis ceramic element, is made of the raw material of following weight (kg)：Glauconite 70, bryozoatum 40, bentonite 15, Nanometer coal charcoal 12, powdered rice hulls 8, razor clam king's shell powder 5, limonite 6, sodium acid carbonate 5, acrylic emulsion 2, cane molasses 2, palm Fiber 4, corn flour 3, phenolic resin 5, epoxidized soybean oil 6, beeswax 2, antibacterial additive 7；
The antibacterial additive is made of following weight (kg) raw material：Hokutolite 30, crystal rubble 18, natural manganese sand 12, receive The silver-colored carbon molecular sieve 5 of rice, nano zine oxide 3, lauryl glucosyl 0.5-1, hydrogen peroxide 45；Preparation method is：By hokutolite, Crystal rubble, natural manganese sand calcined at 870 DEG C 1 it is small when after attrition grinding into powder, then with nanometer silver carbon molecular sieve, nano oxygen Change zinc be uniformly mixed, add lauryl glucosyl, hydrogen peroxide stirring 1 it is small when, then filtering take out；It is clear with distilled water Wash -4 times, drying.
A kind of preparation method of bacteriostasis antibiosis ceramic element, comprises the following steps：
(1) suitable water is added after mixing glauconite, bryozoatum, bentonite, nanometer coal charcoal, powdered rice hulls, limonite, is stirred When immersion 3 is small after uniformly, weakly acidic pH is washed till with clear water after filtering, in 100 DEG C of dryings, when 800 DEG C of calcinings 2 are small, cooling crush；
(2) razor clam king's shell powder, acrylic emulsion, corn flour, phenolic resin, beeswax are added after monkey grass is crushed, at 50 DEG C It is lower to be mixed 40 minutes；
(3) raw material after being crushed in step (1), the raw material in step (2), antibacterial additive and other remaining compositions are mixed Close, vacuum pugging, be sent into mould, after the demoulding, when sintering 2 is small in 270 DEG C of sintering furnaces of feeding, then, with 6 DEG C/min of speed Be warming up to 800 DEG C sintering 3 it is small when, then, then with 10 DEG C/min of speed be warming up to 1250 DEG C sintering 5 it is small when to obtain the final product.
The absorption property testing result of ceramic element made from above-described embodiment 1-3 is as shown in the table：
The absorption property testing result of ceramic element made from 1 embodiment 1-3 of table
。

Claims (2)

  1. A kind of 1. bacteriostasis antibiosis ceramic element, it is characterised in that：Glauconite 70, bryozoatum 40, bentonite 15, nanometer coal charcoal 12nd, powdered rice hulls 8, razor clam king's shell powder 5, limonite 6, sodium acid carbonate 5, acrylic emulsion 2, cane molasses 2, monkey grass 4, corn Powder 3, phenolic resin 5, epoxidized soybean oil 6, beeswax 2, antibacterial additive 7；
    The antibacterial additive is made of following weight (kg) raw material：Hokutolite 30, crystal rubble 18, natural manganese sand 12, receive The silver-colored carbon molecular sieve 5 of rice, nano zine oxide 3, lauryl glucosyl 0.5-1, hydrogen peroxide 45；Preparation method is：By hokutolite, Crystal rubble, natural manganese sand calcined at 870 DEG C 1 it is small when after attrition grinding into powder, then with nanometer silver carbon molecular sieve, nano oxygen Change zinc be uniformly mixed, add lauryl glucosyl, hydrogen peroxide stirring 1 it is small when, then filtering take out；It is clear with distilled water Wash -4 times, drying.
  2. 2. the preparation method of bacteriostasis antibiosis ceramic element according to claim 1, it is characterised in that：Comprise the following steps：
    (1) suitable water is added after mixing glauconite, bryozoatum, bentonite, nanometer coal charcoal, powdered rice hulls, limonite, is stirred When immersion 3 is small after uniformly, weakly acidic pH is washed till with clear water after filtering, in 100 DEG C of dryings, when 800 DEG C of calcinings 2 are small, cooling crush；
    (2) razor clam king's shell powder, acrylic emulsion, corn flour, phenolic resin, beeswax are added after monkey grass is crushed, at 50 DEG C It is lower to be mixed 40 minutes；
    (3) raw material after being crushed in step (1), the raw material in step (2), antibacterial additive and other remaining compositions are mixed Close, vacuum pugging, be sent into mould, after the demoulding, when sintering 2 is small in 270 DEG C of sintering furnaces of feeding, then, with 6 DEG C/min of speed Be warming up to 800 DEG C sintering 3 it is small when, then, then with 10 DEG C/min of speed be warming up to 1250 DEG C sintering 5 it is small when to obtain the final product.
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