CN107899525A - A kind of open type enamel concentration kettle - Google Patents
A kind of open type enamel concentration kettle Download PDFInfo
- Publication number
- CN107899525A CN107899525A CN201711188036.7A CN201711188036A CN107899525A CN 107899525 A CN107899525 A CN 107899525A CN 201711188036 A CN201711188036 A CN 201711188036A CN 107899525 A CN107899525 A CN 107899525A
- Authority
- CN
- China
- Prior art keywords
- titanium
- open type
- concentration kettle
- heat exchange
- type enamel
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 210000003298 dental enamel Anatomy 0.000 title claims abstract description 24
- RTAQQCXQSZGOHL-UHFFFAOYSA-N Titanium Chemical compound [Ti] RTAQQCXQSZGOHL-UHFFFAOYSA-N 0.000 claims abstract description 33
- 239000010936 titanium Substances 0.000 claims abstract description 33
- 229910052719 titanium Inorganic materials 0.000 claims abstract description 33
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 5
- 238000000034 method Methods 0.000 claims description 4
- 241000233855 Orchidaceae Species 0.000 claims 1
- 238000005260 corrosion Methods 0.000 abstract description 6
- 230000007797 corrosion Effects 0.000 abstract description 6
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 6
- IAZDPXIOMUYVGZ-UHFFFAOYSA-N Dimethylsulphoxide Chemical compound CS(C)=O IAZDPXIOMUYVGZ-UHFFFAOYSA-N 0.000 description 4
- 239000011521 glass Substances 0.000 description 4
- 238000010438 heat treatment Methods 0.000 description 4
- HHVIBTZHLRERCL-UHFFFAOYSA-N sulfonyldimethane Chemical compound CS(C)(=O)=O HHVIBTZHLRERCL-UHFFFAOYSA-N 0.000 description 4
- 229910000975 Carbon steel Inorganic materials 0.000 description 3
- 239000010962 carbon steel Substances 0.000 description 3
- 239000012452 mother liquor Substances 0.000 description 3
- 235000012239 silicon dioxide Nutrition 0.000 description 3
- 239000000377 silicon dioxide Substances 0.000 description 3
- MHAJPDPJQMAIIY-UHFFFAOYSA-N Hydrogen peroxide Chemical compound OO MHAJPDPJQMAIIY-UHFFFAOYSA-N 0.000 description 2
- 229910052751 metal Inorganic materials 0.000 description 2
- 239000002184 metal Substances 0.000 description 2
- 229910000831 Steel Inorganic materials 0.000 description 1
- 239000002131 composite material Substances 0.000 description 1
- 239000003814 drug Substances 0.000 description 1
- 230000003628 erosive effect Effects 0.000 description 1
- 238000009776 industrial production Methods 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 239000003921 oil Substances 0.000 description 1
- 239000000575 pesticide Substances 0.000 description 1
- 238000004064 recycling Methods 0.000 description 1
- 238000005245 sintering Methods 0.000 description 1
- 239000010959 steel Substances 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/02—Apparatus characterised by being constructed of material selected for its chemically-resistant properties
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/00049—Controlling or regulating processes
- B01J2219/00051—Controlling the temperature
- B01J2219/00074—Controlling the temperature by indirect heating or cooling employing heat exchange fluids
- B01J2219/00087—Controlling the temperature by indirect heating or cooling employing heat exchange fluids with heat exchange elements outside the reactor
- B01J2219/00092—Tubes
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/00049—Controlling or regulating processes
- B01J2219/00051—Controlling the temperature
- B01J2219/00074—Controlling the temperature by indirect heating or cooling employing heat exchange fluids
- B01J2219/00105—Controlling the temperature by indirect heating or cooling employing heat exchange fluids part or all of the reactants being heated or cooled outside the reactor while recycling
- B01J2219/00108—Controlling the temperature by indirect heating or cooling employing heat exchange fluids part or all of the reactants being heated or cooled outside the reactor while recycling involving reactant vapours
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/02—Apparatus characterised by their chemically-resistant properties
- B01J2219/0204—Apparatus characterised by their chemically-resistant properties comprising coatings on the surfaces in direct contact with the reactive components
- B01J2219/0213—Apparatus characterised by their chemically-resistant properties comprising coatings on the surfaces in direct contact with the reactive components of enamel
Abstract
This practicality newly discloses a kind of open type enamel concentration kettle, including big lid and autoclave body, it is characterised in that：The titanium heat exchange coil that vertical cylinder and one of two ends all with flange are arranged in the vertical cylinder is additionally provided with, the vertical cylinder and titanium heat exchange coil are fixed between the big lid and autoclave body by flange.The present invention will not destroy existing concentration kettle structure since big cover in open type enamel concentration kettle fixes titanium heat exchange disk between autoclave body with flange, while titanium tube is corrosion-resistant, therefore can efficiently use the steam heat that reaction kettle comes out.
Description
Technical field
The present invention relates to a kind of enamel concentration kettle, more particularly to a kind of open type enamel concentration kettle.
Background technology
Enamel still is by the glass containing high silicon dioxide, serves as a contrast the inner surface in steel vessel, through high temperature sintering securely
Adherence has the stability of glass and the two-fold advantage of metal strength in becoming composite product on metal surface, is a kind of
Excellent corrosion resistant apparatus, has been widely used in the industry such as chemical industry, oil, medicine, pesticide, food.Industrial is usually profit
With dimethyl sulfoxide (DMSO) and hydrogen peroxide reaction generation dimethyl sulfone, the concentration Fu Zhuo of the recycling mother liquor used is open type enamel still, by
Be lined with the glass containing high silicon dioxide in open type enamel still inner surface, mostly an only carbon steel heat exchange jacket, the chuck intolerant to
Corrosion.When open type enamel concentration kettle carries out mother liquor concentrations, since the steam zone that reaction kettle comes out is corrosive, being cannot be direct
For chuck heating, if the higher steam of temperature that utilize reaction kettle to come out, only increases in open type enamel concentration kettle
Add new heat-exchange system, may so destroy the structure of existing open type enamel concentration kettle, influence its safety coefficient.
The content of the invention
It is an object of the invention to provide one kind not to destroy existing concentration kettle structure, with regard to can efficiently use reaction kettle come out
The open type enamel concentration kettle of steam heat.
The present invention uses following technical scheme：A kind of open type enamel concentration kettle, including big lid and autoclave body, it is characterised in that：
The titanium heat exchange coil that vertical cylinder and one of two ends all with flange are arranged in the vertical cylinder is additionally provided with, it is described
Vertical cylinder and titanium heat exchange coil are fixed between the big lid and autoclave body by flange.
Titanium heat exchange coil of the present invention includes two sections of horizontally disposed titanium manifold and the above-mentioned two Duan Tai manifold of connection uses
Spring coil pipe, wherein top titanium manifold is steam inlet tube, lower section titanium manifold is steam and condensed water outlet pipe.
Spring coil pipe of the present invention is 3 or more than 3, to be arranged concentrically.
The coil pipe of spring coil pipe of the present invention is fixed on stent with anchor ear.
Steam all bands that the reaction kettle of industrial production dimethyl sulfone comes out are corrosive, and carry substantial amounts of thermal energy.By
The glass containing high silicon dioxide is lined with existing open type enamel still inner surface, is mostly provided only with a carbon steel heat exchange jacket, together
When chuck be not corrosion resistant.When carrying out mother liquor concentrations with open type enamel concentration kettle, existing technique can only all utilize original
Carbon steel heat exchange jacket heating, reaction kettle come out steam be cannot be directly used to chuck heating, not so can corrode chuck.And
The present invention fixes a titanium heat exchange coil between big lid and autoclave body with flange, and existing open type enamel concentration kettle is not carried out
Destroy, add a new heat-exchange system, while titanium tube is corrosion-resistant, the steam that reaction kettle comes out will not produce titanium tube rotten
Erosion, therefore the higher steam of the temperature of reaction kettle out can be utilized.And it is that flange connects between titanium heat exchange coil and big lid and autoclave body
Connect, install and remove and is all very convenient.
The present invention, will not due to fixing a titanium heat exchange coil with flange between the big lid and autoclave body of open type enamel concentration kettle
Existing concentration kettle structure is destroyed, while titanium tube is corrosion-resistant, therefore the steam heat that reaction kettle comes out can be efficiently used.
Brief description of the drawings
Fig. 1 is the structure chart of the present invention；
Fig. 2 is the structure chart of titanium heat exchange disk of the present invention；
Fig. 3 is the plane structure chart of titanium heat exchange disk of the present invention；
In figure, 1 is to cover greatly, and 2 be autoclave body, and 3 be vertical cylinder, and 4 be anchor ear, and 5 be steam and condensed water outlet pipe, and 6 be stent, and 7 are
Steam inlet tube, 8 be spring titanium dish pipe.
Embodiment
The invention will be further described with concrete mode below in conjunction with the accompanying drawings：
From fig. 1, it can be seen that the present invention is a kind of open type enamel concentration kettle, including big lid and autoclave body, it is additionally provided with two ends and all carries
The vertical cylinder of flange and a titanium heat exchange coil being arranged in the vertical cylinder, the vertical cylinder and titanium heat exchange coil
It is fixed on by flange between the big lid and autoclave body, wherein titanium heat exchange disk includes two sections of horizontally disposed titanium manifold and connection
Above-mentioned two Duan Tai manifold is with spring coil pipe, wherein top titanium manifold is steam inlet tube, lower section titanium manifold is steam and condensed water
Outlet pipe, spring coil pipe is 3 or more than 3, to be arranged concentrically.
The coil pipe of the spring coil pipe of the present invention is fixed on stent with anchor ear.
Application method：The open type enamel that the top titanium manifold of the titanium heat exchange coil of the present invention is connected to previous technique reacts
The steam that kettle comes out.Lead to steam with original mode of heating i.e. chuck again when not reacted to heat, until concentration is completed.
Embodiment of the present invention is only the description carried out to the preferred embodiment of the present invention, not to the present invention
Spirit and scope are defined, and on the premise of design philosophy of the present invention is not departed from, engineers and technicians are to this hair in this area
The all variations and modifications that bright technical solution is made, should all fall into protection scope of the present invention, the claimed skill of the present invention
Art content, has all been recorded in detail in the claims.
Claims (4)
1. a kind of open type enamel concentration kettle, including big lid and autoclave body, it is characterised in that：It is additionally provided with two ends and all carries flange
Vertical cylinder and a titanium heat exchange coil being arranged in the vertical cylinder, the vertical cylinder and titanium heat exchange coil pass through method
Orchid is fixed between the big lid and autoclave body.
2. open type enamel concentration kettle according to claim 1, it is characterised in that：The titanium heat exchange coil includes two sections of water
Titanium manifold and connection above-mentioned two Duan Tai manifold the spring coil pipe of flat setting, wherein top titanium manifold is steam inlet tube, lower section
Titanium manifold is steam and condensed water outlet pipe.
3. open type enamel concentration kettle according to claim 2, it is characterised in that：The spring coil pipe for 3 or 3 with
On, to be arranged concentrically.
4. open type enamel concentration kettle according to claim 2, it is characterised in that：The coil pipe anchor ear of the spring coil pipe
It is fixed on stent.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201711188036.7A CN107899525A (en) | 2017-11-24 | 2017-11-24 | A kind of open type enamel concentration kettle |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201711188036.7A CN107899525A (en) | 2017-11-24 | 2017-11-24 | A kind of open type enamel concentration kettle |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN107899525A true CN107899525A (en) | 2018-04-13 |
Family
ID=61847516
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201711188036.7A Pending CN107899525A (en) | 2017-11-24 | 2017-11-24 | A kind of open type enamel concentration kettle |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN107899525A (en) |
Citations (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101966997A (en) * | 2010-10-29 | 2011-02-09 | 江苏瑞普膜技术有限公司 | Process and device for producing pyrotechnite from sodium sulfate decahydrate |
| CN103145153A (en) * | 2013-04-11 | 2013-06-12 | 南风化工集团股份有限公司 | Application of MVR (Mechanical Vapor Recompression) crystallization evaporator to industrialized production of anhydrous sodium sulphate |
| CN203030269U (en) * | 2013-01-25 | 2013-07-03 | 湖北泰盛化工有限公司 | Stainless steel rectification reaction kettle |
| CN103598980A (en) * | 2013-07-29 | 2014-02-26 | 江中药业股份有限公司 | Traditional Chinese medicine extraction and concentration device |
| CN203695046U (en) * | 2013-11-20 | 2014-07-09 | 北京华腾大搪设备有限公司 | Enamel pot |
| CN206019422U (en) * | 2016-08-31 | 2017-03-15 | 四川省玉鑫药业有限公司 | A kind of concentration kettle chiller |
| CN207546486U (en) * | 2017-11-24 | 2018-06-29 | 岳阳湘茂医药化工有限公司 | A kind of open type enamel concentration kettle |
-
2017
- 2017-11-24 CN CN201711188036.7A patent/CN107899525A/en active Pending
Patent Citations (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101966997A (en) * | 2010-10-29 | 2011-02-09 | 江苏瑞普膜技术有限公司 | Process and device for producing pyrotechnite from sodium sulfate decahydrate |
| CN203030269U (en) * | 2013-01-25 | 2013-07-03 | 湖北泰盛化工有限公司 | Stainless steel rectification reaction kettle |
| CN103145153A (en) * | 2013-04-11 | 2013-06-12 | 南风化工集团股份有限公司 | Application of MVR (Mechanical Vapor Recompression) crystallization evaporator to industrialized production of anhydrous sodium sulphate |
| CN103598980A (en) * | 2013-07-29 | 2014-02-26 | 江中药业股份有限公司 | Traditional Chinese medicine extraction and concentration device |
| CN203695046U (en) * | 2013-11-20 | 2014-07-09 | 北京华腾大搪设备有限公司 | Enamel pot |
| CN206019422U (en) * | 2016-08-31 | 2017-03-15 | 四川省玉鑫药业有限公司 | A kind of concentration kettle chiller |
| CN207546486U (en) * | 2017-11-24 | 2018-06-29 | 岳阳湘茂医药化工有限公司 | A kind of open type enamel concentration kettle |
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| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| WD01 | Invention patent application deemed withdrawn after publication | ||
| WD01 | Invention patent application deemed withdrawn after publication |
Application publication date: 20180413 |