CN107874070A - A kind of beet red pigment emulsifying process - Google Patents
A kind of beet red pigment emulsifying process Download PDFInfo
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- CN107874070A CN107874070A CN201711092553.4A CN201711092553A CN107874070A CN 107874070 A CN107874070 A CN 107874070A CN 201711092553 A CN201711092553 A CN 201711092553A CN 107874070 A CN107874070 A CN 107874070A
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- red pigment
- oil
- beet red
- emulsifying
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- 235000016068 Berberis vulgaris Nutrition 0.000 title claims abstract description 65
- 241000335053 Beta vulgaris Species 0.000 title claims abstract description 65
- 239000001054 red pigment Substances 0.000 title claims abstract description 63
- 238000000034 method Methods 0.000 title claims abstract description 26
- 230000008569 process Effects 0.000 title claims abstract description 26
- 230000001804 emulsifying effect Effects 0.000 title claims abstract description 23
- 239000000203 mixture Substances 0.000 claims abstract description 44
- 239000000843 powder Substances 0.000 claims abstract description 31
- 238000004945 emulsification Methods 0.000 claims abstract description 26
- 239000003995 emulsifying agent Substances 0.000 claims abstract description 26
- 239000007788 liquid Substances 0.000 claims abstract description 18
- 239000006185 dispersion Substances 0.000 claims abstract description 13
- 239000003921 oil Substances 0.000 claims description 60
- 235000019198 oils Nutrition 0.000 claims description 60
- 238000000498 ball milling Methods 0.000 claims description 20
- 239000004519 grease Substances 0.000 claims description 16
- 238000002844 melting Methods 0.000 claims description 14
- 230000008018 melting Effects 0.000 claims description 14
- 239000000463 material Substances 0.000 claims description 12
- 238000002156 mixing Methods 0.000 claims description 10
- KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid group Chemical group C(CC(O)(C(=O)O)CC(=O)O)(=O)O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 claims description 9
- 239000003094 microcapsule Substances 0.000 claims description 9
- 239000002245 particle Substances 0.000 claims description 8
- 235000019484 Rapeseed oil Nutrition 0.000 claims description 7
- 239000003549 soybean oil Substances 0.000 claims description 7
- 235000012424 soybean oil Nutrition 0.000 claims description 7
- 239000000498 cooling water Substances 0.000 claims description 6
- 239000000839 emulsion Substances 0.000 claims description 6
- 238000003701 mechanical milling Methods 0.000 claims description 6
- 239000002994 raw material Substances 0.000 claims description 6
- 235000019486 Sunflower oil Nutrition 0.000 claims description 5
- -1 sucrose ester Chemical class 0.000 claims description 5
- 239000002600 sunflower oil Substances 0.000 claims description 5
- 229930006000 Sucrose Natural products 0.000 claims description 4
- 230000008859 change Effects 0.000 claims description 4
- 239000005720 sucrose Substances 0.000 claims description 4
- 229910052845 zircon Inorganic materials 0.000 claims description 4
- GFQYVLUOOAAOGM-UHFFFAOYSA-N zirconium(iv) silicate Chemical compound [Zr+4].[O-][Si]([O-])([O-])[O-] GFQYVLUOOAAOGM-UHFFFAOYSA-N 0.000 claims description 4
- JLPULHDHAOZNQI-ZTIMHPMXSA-N 1-hexadecanoyl-2-(9Z,12Z-octadecadienoyl)-sn-glycero-3-phosphocholine Chemical compound CCCCCCCCCCCCCCCC(=O)OC[C@H](COP([O-])(=O)OCC[N+](C)(C)C)OC(=O)CCCCCCC\C=C/C\C=C/CCCCC JLPULHDHAOZNQI-ZTIMHPMXSA-N 0.000 claims description 3
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims description 3
- 229910000831 Steel Inorganic materials 0.000 claims description 3
- 239000011324 bead Substances 0.000 claims description 3
- 229940083466 soybean lecithin Drugs 0.000 claims description 3
- 239000010959 steel Substances 0.000 claims description 3
- 125000005456 glyceride group Chemical group 0.000 claims description 2
- 239000004375 Dextrin Substances 0.000 claims 1
- 229920001353 Dextrin Polymers 0.000 claims 1
- 240000000528 Ricinus communis Species 0.000 claims 1
- 235000004443 Ricinus communis Nutrition 0.000 claims 1
- 210000000481 breast Anatomy 0.000 claims 1
- 235000019425 dextrin Nutrition 0.000 claims 1
- 235000020238 sunflower seed Nutrition 0.000 claims 1
- 235000013305 food Nutrition 0.000 abstract description 11
- 239000000049 pigment Substances 0.000 abstract description 9
- 238000000227 grinding Methods 0.000 abstract description 5
- 238000004519 manufacturing process Methods 0.000 abstract description 3
- 230000008021 deposition Effects 0.000 abstract description 2
- 238000009826 distribution Methods 0.000 abstract description 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 5
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 4
- 230000004888 barrier function Effects 0.000 description 4
- 239000003086 colorant Substances 0.000 description 4
- 230000005496 eutectics Effects 0.000 description 4
- 235000002864 food coloring agent Nutrition 0.000 description 4
- 229910052760 oxygen Inorganic materials 0.000 description 4
- 239000001301 oxygen Substances 0.000 description 4
- 238000003860 storage Methods 0.000 description 4
- 229920000858 Cyclodextrin Polymers 0.000 description 3
- HFHDHCJBZVLPGP-UHFFFAOYSA-N schardinger α-dextrin Chemical compound O1C(C(C2O)O)C(CO)OC2OC(C(C2O)O)C(CO)OC2OC(C(C2O)O)C(CO)OC2OC(C(O)C2O)C(CO)OC2OC(C(C2O)O)C(CO)OC2OC2C(O)C(O)C1OC2CO HFHDHCJBZVLPGP-UHFFFAOYSA-N 0.000 description 3
- 241000871189 Chenopodiaceae Species 0.000 description 2
- 241000196324 Embryophyta Species 0.000 description 2
- 201000010099 disease Diseases 0.000 description 2
- 208000037265 diseases, disorders, signs and symptoms Diseases 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 235000019601 food appearance Nutrition 0.000 description 2
- 241000219317 Amaranthaceae Species 0.000 description 1
- 235000021537 Beetroot Nutrition 0.000 description 1
- 241001474374 Blennius Species 0.000 description 1
- 235000010254 Jasminum officinale Nutrition 0.000 description 1
- 240000005385 Jasminum sambac Species 0.000 description 1
- 241001465754 Metazoa Species 0.000 description 1
- 230000002776 aggregation Effects 0.000 description 1
- 238000004220 aggregation Methods 0.000 description 1
- 230000003712 anti-aging effect Effects 0.000 description 1
- 230000001093 anti-cancer Effects 0.000 description 1
- 239000003963 antioxidant agent Substances 0.000 description 1
- 230000003078 antioxidant effect Effects 0.000 description 1
- 235000006708 antioxidants Nutrition 0.000 description 1
- 235000013361 beverage Nutrition 0.000 description 1
- 239000012620 biological material Substances 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 239000008280 blood Substances 0.000 description 1
- 210000004369 blood Anatomy 0.000 description 1
- 235000012970 cakes Nutrition 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- 238000004040 coloring Methods 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 235000009508 confectionery Nutrition 0.000 description 1
- 235000014113 dietary fatty acids Nutrition 0.000 description 1
- 239000000975 dye Substances 0.000 description 1
- 229930195729 fatty acid Natural products 0.000 description 1
- 239000000194 fatty acid Substances 0.000 description 1
- 239000002778 food additive Substances 0.000 description 1
- 235000013373 food additive Nutrition 0.000 description 1
- 235000015243 ice cream Nutrition 0.000 description 1
- 230000006872 improvement Effects 0.000 description 1
- 150000002632 lipids Chemical class 0.000 description 1
- 230000003908 liver function Effects 0.000 description 1
- 239000002932 luster Substances 0.000 description 1
- 231100000252 nontoxic Toxicity 0.000 description 1
- 230000003000 nontoxic effect Effects 0.000 description 1
- 235000010958 polyglycerol polyricinoleate Nutrition 0.000 description 1
- 239000003996 polyglycerol polyricinoleate Substances 0.000 description 1
- 230000001603 reducing effect Effects 0.000 description 1
- 238000003756 stirring Methods 0.000 description 1
- 238000006467 substitution reaction Methods 0.000 description 1
- 238000003786 synthesis reaction Methods 0.000 description 1
- 235000019222 white chocolate Nutrition 0.000 description 1
- 235000014101 wine Nutrition 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L5/00—Preparation or treatment of foods or foodstuffs, in general; Food or foodstuffs obtained thereby; Materials therefor
- A23L5/40—Colouring or decolouring of foods
- A23L5/42—Addition of dyes or pigments, e.g. in combination with optical brighteners
- A23L5/43—Addition of dyes or pigments, e.g. in combination with optical brighteners using naturally occurring organic dyes or pigments, their artificial duplicates or their derivatives
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L29/00—Foods or foodstuffs containing additives; Preparation or treatment thereof
- A23L29/03—Organic compounds
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L29/00—Foods or foodstuffs containing additives; Preparation or treatment thereof
- A23L29/03—Organic compounds
- A23L29/035—Organic compounds containing oxygen as heteroatom
- A23L29/04—Fatty acids or derivatives
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L29/00—Foods or foodstuffs containing additives; Preparation or treatment thereof
- A23L29/10—Foods or foodstuffs containing additives; Preparation or treatment thereof containing emulsifiers
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23P—SHAPING OR WORKING OF FOODSTUFFS, NOT FULLY COVERED BY A SINGLE OTHER SUBCLASS
- A23P10/00—Shaping or working of foodstuffs characterised by the products
- A23P10/30—Encapsulation of particles, e.g. foodstuff additives
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09B—ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
- C09B67/00—Influencing the physical, e.g. the dyeing or printing properties of dyestuffs without chemical reactions, e.g. by treating with solvents grinding or grinding assistants, coating of pigments or dyes; Process features in the making of dyestuff preparations; Dyestuff preparations of a special physical nature, e.g. tablets, films
- C09B67/0001—Post-treatment of organic pigments or dyes
- C09B67/0014—Influencing the physical properties by treatment with a liquid, e.g. solvents
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09B—ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
- C09B67/00—Influencing the physical, e.g. the dyeing or printing properties of dyestuffs without chemical reactions, e.g. by treating with solvents grinding or grinding assistants, coating of pigments or dyes; Process features in the making of dyestuff preparations; Dyestuff preparations of a special physical nature, e.g. tablets, films
- C09B67/006—Preparation of organic pigments
- C09B67/0069—Non aqueous dispersions of pigments containing only a solvent and a dispersing agent
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2002/00—Food compositions, function of food ingredients or processes for food or foodstuffs
Abstract
The invention discloses a kind of beet red pigment emulsifying process, it includes grinding in beet red pigment powder and oil phase dispersion liquid, prepare oil mixture and by the oil mixture and the step of emulsifying agent vacuum emulsification, water-soluble beet red pigment with oil phase dispersion liquid through together grinding and after emulsification treatment, it is dispersed among oil-based system, so as to be used in oil phase, for improving the exterior quality of the higher food of oil content, prevent pigment deposition in the high food of oil content, the uneven situation of distribution of color, expand the application of beet red pigment, emulsifying process is simple, equipment investment is few, production cost is low.
Description
Technical field
The invention belongs to food additives production technical field, is related to a kind of beet red pigment handling process, specifically
It is related to a kind of beet red pigment emulsifying process.
Background technology
With economic development and the improvement of people's living standards, nowadays requirement of the people to food is not solely restricted to inside
Quality, while the also more and more higher of the requirement to food appearance quality, and the color and luster of food occupies phase in food appearance quality
Work as consequence, therefore the research to food color has been increasingly becoming study hotspot.
Food color includes synthetic dyestuff and natural pigment, natural pigment with it is safe, some are with preventing and treating disease
The health-care effect of disease, containing required nutriment, tone is natural, can imitate the advantages of natural colored, from animals and plants and micro-
Safe natural pigment is extracted in biomaterial as food color and receives much concern and payes attention to.
In numerous natural food Agents, beet red pigment is widely used a kind of edible natural pigment in the world,
It is present in the various plants such as Amaranthaceae, Chenopodiaceae, seaweed jasmine section, is extracted more from the root tuber of Chenopodiaceae red beet, beet red pigment
Colorability is strong, nontoxic, safe, and also having improves liver function, anti-oxidant, anticancer, anti-aging, reducing blood lipid, protect eyes, promotion
The effect digested and assimilated, be one of preferable natural red colouring matter of substitution synthesis haematochrome, be widely used in beverage, ice cream, wine,
Candy, cake mounting flower, the processing of tank first-class product.
But beet red pigment is easily soluble in water, can not be dissolved in grease, easily there is pigment in the high food of oil content
Aggregation, disperse the problem of uneven, so as to limit its application in the high food of oil content (such as white chocolate).
The content of the invention
Therefore, the technical problems to be solved by the invention are that traditional beet red pigment does not dissolve in grease, in floorboard with high oil content
Easily assemble in food, make the scattered inequality of food colour, the outward appearance of food is have impact on, so as to propose that one kind turns into beet red pigment
The beet red pigment emulsifying process of oily soluble/dispersible pigment.
In order to solve the above technical problems, the technical scheme is that：
The present invention provides a kind of beet red pigment emulsifying process, and it comprises the following steps：
S1, it is ground after beet red pigment powder is mixed with oil phase dispersion liquid, obtains oil mixture, the beet
Haematochrome powder accounts for the 5~30% of the oil mixture gross mass；
S2, emulsifying agent is added into the oil mixture, and carry out vacuum emulsification, the addition of the emulsifying agent is oil
The 5-20% of phase mixture.
Preferably, also include using in the beet red pigment powder before mixing with oil phase dispersion liquid in the step S1
The step of microencapsulation material processing.
Preferably, in the step S1, the grinding carries out ball milling, the grinding-material of the ball mill using ball mill
For steel ball, zircon pearl or agate bead, the rotating speed of the ball mill is 5-3000r/min.
It is preferably, cold to ball mill progress using cooling water of the temperature not higher than 30 DEG C in the process of lapping
But, the mixture actual temperature of beet red pigment and oil phase dispersion liquid is not higher than 30 DEG C in mechanical milling process, and the oil phase after ball milling mixes
Compound particle diameter is not more than 5 μm.
Preferably, in the step S2, in the step S2, the vacuum emulsification is carried out in vacuum emulsification tank, institute
The mixing speed for stating emulsion tank is 5-1000r/min, and vacuum is -0.2-0Mpa, emulsification times 10-30min.
Preferably, the oil phase dispersion liquid is low melting point grease, the emulsifying agent is lipophilic emulsifier.
Preferably, the oil phase dispersion liquid is sunflower oil, rapeseed oil or soybean oil；The emulsifying agent is citric acid fat
Fatty acid glyceride, sucrose ester, soybean lecithin or polyglycerol polyricinoleate.
Preferably, the emulsifying agent is made using sunflower oil, rapeseed oil or soybean oil as raw material.
Preferably, the color value of the beet red pigment is 4E-200E.
Preferably, the wall material of the microcapsules is cyclodextrin.
The above-mentioned technical proposal of the present invention has advantages below compared with prior art：
Beet red pigment emulsifying process of the present invention, it includes grinding beet red pigment powder with oil phase dispersion liquid
Grind, prepare oil mixture and the step of by the oil mixture and emulsifying agent vacuum emulsification, water-soluble beet red pigment warp
Together ground with oil phase dispersion liquid and after emulsification treatment, oil-based system is dispersed among, so as to be used in oil phase, for improving
The exterior quality of the higher food of oil content, it is therefore prevented that the uneven situation of pigment deposition, distribution of color in the high food of oil content,
The application of beet red pigment is expanded, emulsifying process is simple, and equipment investment is few, and production cost is low.
Embodiment
In order that present disclosure is more likely to be clearly understood, below according to specific embodiment of the invention to this hair
It is bright to be described in further detail.
Embodiment 1
The present embodiment provides a kind of emulsifying process of beet red pigment, and it comprises the following steps：
S1, ball milling is carried out in ball mill after beet red pigment powder is mixed with low melting point grease, obtain oil phase mixing
Thing, in the present embodiment, the beet red pigment powder accounts for the 10% of the oil mixture quality.Eutectic described in the present embodiment
It is sunflower oil to select grease, and the beet red pigment powder can be the pigmented powder that commercially available color value is 4E-200E.
The ball mill is using steel ball as grinding-material, and the rotating speed of the ball mill is 700r/min during ball milling, ball milling
It is not more than 5 μm to the oil mixture particle diameter；It need to ensure that beet red pigment powder is in lower temperature during ball milling, therefore to ball
Grinding machine is passed through cooling water of the temperature not higher than 30 DEG C and ball mill is cooled down, and makes beet red pigment and low melting point in mechanical milling process
The mixed liquor actual temperature of grease is not higher than 30 DEG C, and after ball milling, the particle diameter of oil mixture is directly detected using screw-thread micrometer,
Obtain satisfactory oil mixture.
S2, add lipophile and low melting point emulsifying agent, the addition of the emulsifying agent into the oil mixture and account for oil
The 10% of phase mixture quality, and obtained mixture is placed in vacuum emulsification tank and carries out vacuum emulsification, institute in the present embodiment
It is to be using citric acid fatty glyceride made from sunflower oil as raw material, the mixing speed of the emulsion tank to state emulsifying agent
5r/min, vacuum is -0.05MPa, emulsification times 20min, after the completion of emulsification, by obtained colorant dispersing liquid in barrier
It is packaged in the container well (block water, hinder oxygen, lucifuge), sealed storage uses.
Embodiment 2
The present embodiment provides a kind of emulsifying process of beet red pigment, and it comprises the following steps：
S1, microcapsules are handled after beet red pigment powder mixed with low melting point grease after ball is carried out in ball mill
Mill, the wall material of the microcapsules is that (processing is together to stir microcapsules and pigment powder to cyclodextrin, or can use city
Sell the beet red pigment powder of microcapsules processing), obtain oil mixture, in the present embodiment, the beet red pigment powder accounts for
The 30% of the oil mixture quality.Low melting point grease described in the present embodiment is rapeseed oil, the beet red pigment powder
It can be the pigmented powder that commercially available color value is 4E-200E.
The ball mill is using zircon pearl as grinding-material, and the rotating speed of the ball mill is 100r/min during ball milling, ball
The oil mixture particle diameter is milled to no more than 5 μm；It need to ensure that beet red pigment powder is in lower temperature during ball milling, therefore to
Ball mill is passed through cooling water of the temperature not higher than 30 DEG C and ball mill is cooled down, and makes beet red pigment and eutectic in mechanical milling process
The mixed liquor actual temperature for selecting grease is not higher than 30 DEG C, and after ball milling, the grain of oil mixture is directly detected using screw-thread micrometer
Footpath, obtain satisfactory oil mixture.
S2, add lipophile and low melting point emulsifying agent, the addition of the emulsifying agent into the oil mixture and account for oil
The 20% of phase mixture quality, and obtained mixture is placed in vacuum emulsification tank and carries out vacuum emulsification, institute in the present embodiment
It is using sucrose ester made from rapeseed oil as raw material to state emulsifying agent, and the mixing speed of the emulsion tank is 850r/min, vacuum
For -0.1MPa, emulsification times 30min, after the completion of emulsification, obtained colorant dispersing liquid (is blocked water, hindered in excellent in barrier property
Oxygen, lucifuge) container in be packaged, sealed storage use.
Embodiment 3
The present embodiment provides a kind of emulsifying process of beet red pigment, and it comprises the following steps：
S1, carried out after the beet red pigment powder after the processing of commercially available microcapsules is mixed with low melting point grease in ball mill
Ball milling, the wall material of the microcapsules is cyclodextrin, obtains oil mixture, and in the present embodiment, the beet red pigment powder accounts for
The 5% of the oil mixture quality.Low melting point grease described in the present embodiment is soybean oil, and the beet red pigment powder can
Think the pigmented powder that commercially available color value is 4E-200E.
The ball mill is using agate bead as grinding-material, and the rotating speed of the ball mill is 2000r/min during ball milling, ball
The oil mixture particle diameter is milled to no more than 5 μm；It need to ensure that beet red pigment powder is in lower temperature during ball milling, therefore to
Ball mill is passed through cooling water of the temperature not higher than 30 DEG C and ball mill is cooled down, and makes beet red pigment and eutectic in mechanical milling process
The mixed liquor actual temperature for selecting grease is not higher than 30 DEG C, and after ball milling, the grain of oil mixture is directly detected using screw-thread micrometer
Footpath, obtain satisfactory oil mixture.
S2, add lipophile and low melting point emulsifying agent, the addition of the emulsifying agent into the oil mixture and account for oil
The 7% of phase mixture quality, and obtained mixture is placed in vacuum emulsification tank and carries out vacuum emulsification, described in the present embodiment
Emulsifying agent is using soybean lecithin made from soybean oil as raw material, and the mixing speed of the emulsion tank is 300r/min, vacuum
For -0.02MPa, emulsification times 10min, after the completion of emulsification, obtained colorant dispersing liquid (is blocked water, hindered in excellent in barrier property
Oxygen, lucifuge) container in be packaged, sealed storage use.
Embodiment 4
The present embodiment provides a kind of emulsifying process of beet red pigment, and it comprises the following steps：
S1, carried out after the beet red pigment powder after the processing of commercially available microcapsules is mixed with low melting point grease in ball mill
Ball milling, obtains oil mixture, and in the present embodiment, the beet red pigment powder accounts for the 15% of the oil mixture quality.
Low melting point grease described in the present embodiment is soybean oil, and the beet red pigment powder can be that commercially available color value is 4E-200E
Pigmented powder.
The ball mill is using zircon pearl as grinding-material, and the rotating speed of the ball mill is 2500r/min during ball milling, ball
The oil mixture particle diameter is milled to no more than 5 μm；It need to ensure that beet red pigment powder is in lower temperature during ball milling, therefore to
Ball mill is passed through cooling water of the temperature not higher than 30 DEG C and ball mill is cooled down, and makes beet red pigment and eutectic in mechanical milling process
The mixed liquor actual temperature for selecting grease is not higher than 30 DEG C, and after ball milling, beet red pigment powder is directly detected using screw-thread micrometer
Particle diameter, obtain satisfactory oil mixture.
S2, add lipophile and low melting point emulsifying agent, the addition of the emulsifying agent into the oil mixture and account for oil
The 18% of phase mixture quality, and obtained mixture is placed in vacuum emulsification tank and carries out vacuum emulsification, institute in the present embodiment
It is using rapeseed oil oil as sucrose ester made from raw material to state emulsifying agent, and the mixing speed of the emulsion tank is 150r/min, vacuum
Spend for -0.15MPa, emulsification times 25min, after the completion of emulsification, by obtained colorant dispersing liquid excellent in barrier property (block water,
Resistance oxygen, lucifuge) container in be packaged, sealed storage use.
Obviously, above-described embodiment is only intended to clearly illustrate example, and is not the restriction to embodiment.It is right
For those of ordinary skill in the art, can also make on the basis of the above description it is other it is various forms of change or
Change.There is no necessity and possibility to exhaust all the enbodiments.And the obvious change thus extended out or
Among changing still in the protection domain of the invention.
Claims (10)
1. a kind of beet red pigment emulsifying process, it is characterised in that comprise the following steps：
S1, it is ground after beet red pigment powder is mixed with oil phase dispersion liquid, obtains oil mixture, the beet is red
Plain powder accounts for the 5~30% of the oil mixture gross mass；
S2, emulsifying agent is added into the oil mixture for be ground to predetermined size, and carry out vacuum emulsification, the emulsifying agent adds
Dosage is the 5-20% of oil mixture.
2. beet red pigment emulsifying process according to claim 1, it is characterised in that disperse in the step S1 with oil phase
The step of also including handling the beet red pigment powder with microencapsulation material before liquid mixing.
3. beet red pigment emulsifying process according to claim 1 or 2, it is characterised in that described to grind in the step S1
Mill carries out ball milling using ball mill, and the grinding-material of the ball mill is steel ball, zircon pearl or agate bead, and the ball mill turns
Speed is 5-3000r/min.
4. beet red pigment emulsifying process according to claim 3, it is characterised in that temperature is used in the process of lapping
Cooling water not higher than 30 DEG C cools down to the ball mill, the mixing of beet red pigment and oil phase dispersion liquid in mechanical milling process
Thing actual temperature is not higher than 30 DEG C, and the oil mixture particle diameter after ball milling is not more than 5 μm.
5. beet red pigment emulsifying process according to claim 4, it is characterised in that in the step S2, the vacuum
It is emulsified in vacuum emulsification tank and carries out, the mixing speed of the emulsion tank is 5-1000r/min, and vacuum is -0.2-0Mpa, breast
The change time is 10-30min.
6. beet red pigment emulsifying process according to claim 5, it is characterised in that the oil phase dispersion liquid is low melting point
Grease, the emulsifying agent are lipophilic emulsifier.
7. beet red pigment emulsifying process according to claim 6, it is characterised in that the oil phase dispersion liquid is sunflower seeds
Oil, rapeseed oil or soybean oil；The emulsifying agent is citric acid fatty glyceride, sucrose ester, soybean lecithin or polyglycereol castor-oil plant
Alcohol ester.
8. beet red pigment emulsifying process according to claim 7, it is characterised in that the emulsifying agent with sunflower oil,
Rapeseed oil or soybean oil are made for raw material.
9. beet red pigment emulsifying process according to claim 8, it is characterised in that the color value of the beet red pigment is
4E-200E。
10. beet red pigment emulsifying process according to claim 9, it is characterised in that the wall material of the microcapsules is ring
Dextrin.
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