CN107867866A - A kind of manufacture method of Cutting free nickel zinc magnetic core semi-finished product - Google Patents

A kind of manufacture method of Cutting free nickel zinc magnetic core semi-finished product Download PDF

Info

Publication number
CN107867866A
CN107867866A CN201711119332.1A CN201711119332A CN107867866A CN 107867866 A CN107867866 A CN 107867866A CN 201711119332 A CN201711119332 A CN 201711119332A CN 107867866 A CN107867866 A CN 107867866A
Authority
CN
China
Prior art keywords
finished product
magnetic core
parts
manufacture method
nickel zinc
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201711119332.1A
Other languages
Chinese (zh)
Inventor
陈诗煌
甘智豪
温礼栋
倪春林
周家容
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
ZHONGSHAN DONGCHEN MAGNETIC ELECTRONIC PRODUCT CO Ltd
Original Assignee
ZHONGSHAN DONGCHEN MAGNETIC ELECTRONIC PRODUCT CO Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by ZHONGSHAN DONGCHEN MAGNETIC ELECTRONIC PRODUCT CO Ltd filed Critical ZHONGSHAN DONGCHEN MAGNETIC ELECTRONIC PRODUCT CO Ltd
Priority to CN201711119332.1A priority Critical patent/CN107867866A/en
Publication of CN107867866A publication Critical patent/CN107867866A/en
Pending legal-status Critical Current

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B35/00Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
    • C04B35/622Forming processes; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
    • C04B35/626Preparing or treating the powders individually or as batches ; preparing or treating macroscopic reinforcing agents for ceramic products, e.g. fibres; mechanical aspects section B
    • C04B35/62605Treating the starting powders individually or as mixtures
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B35/00Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
    • C04B35/01Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on oxide ceramics
    • C04B35/26Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on oxide ceramics based on ferrites
    • C04B35/265Compositions containing one or more ferrites of the group comprising manganese or zinc and one or more ferrites of the group comprising nickel, copper or cobalt
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2235/00Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/02Composition of constituents of the starting material or of secondary phases of the final product
    • C04B2235/30Constituents and secondary phases not being of a fibrous nature
    • C04B2235/32Metal oxides, mixed metal oxides, or oxide-forming salts thereof, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
    • C04B2235/3231Refractory metal oxides, their mixed metal oxides, or oxide-forming salts thereof
    • C04B2235/3244Zirconium oxides, zirconates, hafnium oxides, hafnates, or oxide-forming salts thereof
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2235/00Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/02Composition of constituents of the starting material or of secondary phases of the final product
    • C04B2235/30Constituents and secondary phases not being of a fibrous nature
    • C04B2235/32Metal oxides, mixed metal oxides, or oxide-forming salts thereof, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
    • C04B2235/327Iron group oxides, their mixed metal oxides, or oxide-forming salts thereof
    • C04B2235/3279Nickel oxides, nickalates, or oxide-forming salts thereof
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2235/00Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/02Composition of constituents of the starting material or of secondary phases of the final product
    • C04B2235/30Constituents and secondary phases not being of a fibrous nature
    • C04B2235/32Metal oxides, mixed metal oxides, or oxide-forming salts thereof, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
    • C04B2235/3281Copper oxides, cuprates or oxide-forming salts thereof, e.g. CuO or Cu2O
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2235/00Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/02Composition of constituents of the starting material or of secondary phases of the final product
    • C04B2235/30Constituents and secondary phases not being of a fibrous nature
    • C04B2235/32Metal oxides, mixed metal oxides, or oxide-forming salts thereof, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
    • C04B2235/3284Zinc oxides, zincates, cadmium oxides, cadmiates, mercury oxides, mercurates or oxide forming salts thereof
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2235/00Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/02Composition of constituents of the starting material or of secondary phases of the final product
    • C04B2235/30Constituents and secondary phases not being of a fibrous nature
    • C04B2235/32Metal oxides, mixed metal oxides, or oxide-forming salts thereof, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
    • C04B2235/3298Bismuth oxides, bismuthates or oxide forming salts thereof, e.g. zinc bismuthate
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2235/00Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/02Composition of constituents of the starting material or of secondary phases of the final product
    • C04B2235/30Constituents and secondary phases not being of a fibrous nature
    • C04B2235/34Non-metal oxides, non-metal mixed oxides, or salts thereof that form the non-metal oxides upon heating, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
    • C04B2235/3418Silicon oxide, silicic acids or oxide forming salts thereof, e.g. silica sol, fused silica, silica fume, cristobalite, quartz or flint
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2235/00Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/60Aspects relating to the preparation, properties or mechanical treatment of green bodies or pre-forms
    • C04B2235/602Making the green bodies or pre-forms by moulding

Landscapes

  • Engineering & Computer Science (AREA)
  • Chemical & Material Sciences (AREA)
  • Ceramic Engineering (AREA)
  • Manufacturing & Machinery (AREA)
  • Materials Engineering (AREA)
  • Structural Engineering (AREA)
  • Organic Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Powder Metallurgy (AREA)
  • Soft Magnetic Materials (AREA)

Abstract

The invention discloses a kind of manufacture method of Cutting free nickel zinc magnetic core semi-finished product, its step includes:Raw material is mixed into vibration and pelletizing, is transferred to pre-burning in rotary kiln, configuration polyvinyl alcohol glue, by first two steps product mixed aid in the lump extra-fine grinding, mist projection granulating, compressing, nickel zinc magnetic core semi-finished product intensity obtained by this method is higher, flexibility is good, less brittle, homogeneous, convenient follow-up cutting, rupture, breakage are not susceptible to during cutting, otch is neat, can substantially reduce the scrappage of production process, production cost is advantageously reduced, improves production efficiency.

Description

A kind of manufacture method of Cutting free nickel zinc magnetic core semi-finished product
Technical field
The present invention relates to a kind of nickel zinc magnetic core, particularly a kind of manufacture method of Cutting free nickel zinc magnetic core semi-finished product.
Background technology
Nickel zinc magnetic core semi-finished product are made step and are:Mix vibrations, pre-burning, mist projection granulating, shaping compacting, square cutting.It is existing Have that the nickel zinc magnetic core semi-finished product hardness in technology is larger, show fragility, and quality is uneven, density and mechanical property performance everywhere Differ, the defects of causing to occur in follow-up working angles rupture, damaged, otch incompleteness, these defects not only influenceed outward appearance but also Electromagnetic performance is influenceed, thus the semi-finished product for these defects occur will be scrapped, and increase production cost, reduce production efficiency.
The content of the invention
For overcome the deficiencies in the prior art, the present invention provides a kind of manufacture method of Cutting free nickel zinc magnetic core semi-finished product.
The technical solution adopted for the present invention to solve the technical problems is:
A kind of manufacture method of Cutting free nickel zinc magnetic core semi-finished product, comprises the following steps:
A, dispensing and mixing vibration:By mass fraction by raw material di-iron trioxide 65%-70%, zinc oxide 15%-19%, cupric oxide 3%-5%, nickel protoxide 10%-15%, bismuth oxide 0.1%-0.3%, tungsten oxide 0.05%-0.1%, zirconium oxide 0.005%-0.01%, two Silica 0.05-0.1%, which is uniformly poured into ball mill hopper, carries out mixing vibration 60 minutes, is then transferred in pelletizer and is made Ball operation, pelletizing material is obtained, the sphere diameter requirement of the pelletizing material is between 1-8mm;
B, pre-burning:The pelletizing material that step A is obtained, which is even added to from hopper in rotary kiln, carries out pre-burning, in rotary kiln Four regions, temperature rotates boiler tube 30-50 minutes between 820-860 DEG C, with 3-5r/min rotating speed, then is carried out with ball mill Ball milling 50 minutes, obtain pre-burning vibration material;
C, glue is boiled:92 parts of pure water are warming up to 50-55 DEG C by weight, 8 parts of granule of polyvinyl alcohol stirrings is then added and is warming up to 95 DEG C, continue stopping heating after heating while stirring 5 hours and continue to stir, filter, gathered after temperature is dropped to below 45 DEG C Vinyl alcohol glue, be sealed with glue bucket it is standby, wherein, the granule of polyvinyl alcohol includes two kinds of models, specially described poly- BP-17 mass fractions account for 30%-70% in vinyl alcohol particle, and BP-05 accounts for 30%-70%;
D, extra-fine grinding:The described vibration material 58-65 parts for by weight obtaining pure water 20-25 parts and step B add vertical sand Grinding machine is ground 20 minutes, then toward adding dispersant 0.2-0.5 parts, defoamer 0.1-0.35 parts, sintering in the vertical grinding machine Described polyvinyl alcohol glue 16-20 parts that auxiliary agent 0.6-1.8 parts and step C are obtained, grinding are pumped into horizontal sand mill after 60 minutes Extra-fine grinding 60 minutes is carried out, obtains slurry;
E, mist projection granulating:The slurry that step D is obtained carries out spray granulation granulation, and spray condition is set as being sprayed into 300 ± 20 DEG C of temperature of mouth, 110 ± 10 DEG C of spray outlet temperature, feeding frequency are 10-13Hz, rejection tablet frequency setting 60Hz, are sprayed Particulate material out needs to carry out humidification process, it is desirable to apparent density 1.25-1.45g/cm3, water content≤0.4% obtains Pellet warehouse entry is standby;
F, shaping compacting:The particulate material that step E is obtained presses institute by particular manufacturing craft on powder former Need the semi-finished product of shape and size.
The temperature in four regions described in rotary kiln is specially 860 DEG C, 845 DEG C, 845 DEG C, 820 DEG C in step B.
Granule of polyvinyl alcohol described in step C is made up of BP-17 40% and BP-05 60%.
Sintering aid described in step D by following mass fraction material composition:Cupric oxide 62%-94%, bismuth oxide 6%- 38%。
The requirement of slurry average grain diameter D50 described in step D is below 0.5 μm.
The beneficial effects of the invention are as follows:It is higher with nickel zinc magnetic core semi-finished product intensity made from manufacture method of the present invention, it is soft Property good, less brittle, homogeneous, convenient follow-up cutting, rupture, damaged is not susceptible to during cutting, otch is neat, can substantially reduce The scrappage of production process, production cost is advantageously reduced, improve production efficiency.
Embodiment
A kind of manufacture method of Cutting free nickel zinc magnetic core semi-finished product, comprises the following steps:
A, dispensing and mixing vibration:By mass fraction by raw material di-iron trioxide 65%-70%, zinc oxide 15%-19%, cupric oxide 3%-5%, nickel protoxide 10%-15% and auxiliary material bismuth oxide 0.1%-0.3%, tungsten oxide 0.05%-0.1%, zirconium oxide 0.005%- 0.01%th, silica 0.05-0.1%, which is uniformly poured into ball mill hopper, carries out mixing vibration 60 minutes, mixes various raw materials It is uniform and levigate, progress pelletizing operation in pelletizer is then transferred to, obtains pelletizing material, the sphere diameter requirement of the pelletizing material is in 1- Between 8mm.
B, pre-burning:The pelletizing material that step A is obtained, which is even added to from hopper in rotary kiln, carries out pre-burning, makes to mix Condensation material reduces shrinkage factor in follow-up sintering step, to prevent Product Variant.Four regions in rotary kiln, temperature is in 820-860 Between DEG C, specifically it is set as 860 DEG C, 845 DEG C, 845 DEG C, 820 DEG C, is rotated boiler tube 30-50 minutes with 3-5r/min rotating speed, then Ball milling is carried out with ball mill 50 minutes, obtains pre-burning vibration material.
C, glue is boiled:92 parts of pure water are warming up to 50-55 DEG C by weight, 8 parts of granule of polyvinyl alcohol stirrings is then added and rises Temperature continues stopping heating after heating while stirring 5 hours and continues to stir, filter, obtain after temperature is dropped to below 45 DEG C to 95 DEG C To polyvinyl alcohol glue, it is sealed with glue bucket standby.Wherein, the granule of polyvinyl alcohol includes two kinds of models, specially institute State BP-17 mass fractions in granule of polyvinyl alcohol and account for 30%-70%, BP-05 accounts for 30%-70%.It is highly preferred that the polyvinyl alcohol Grain is made up of BP-17 40% and BP-05 60%.
D, extra-fine grinding:The described vibration material 58-65 parts for by weight obtaining pure water 20-25 parts and step B add vertical Formula sand mill is ground 20 minutes, then toward add in the vertical grinding machine dispersant 0.2-0.5 parts, defoamer 0.1-0.35 parts, Described polyvinyl alcohol glue 16-20 parts that sintering aid 0.6-1.8 parts and step C are obtained, grinding are pumped into Horizontal sand after 60 minutes Grinding machine carries out extra-fine grinding 60 minutes, obtains slurry.It is required that slurry average grain diameter D50 is less than 0.5 micron.The sintering aid tool Body by following mass fraction material composition:Cupric oxide 62%-94%, bismuth oxide 6%-38%.The defoamer uses ND44 DEfoamer, the dispersant use ROHM AND HAAS 731D.
E, mist projection granulating:The slurry that step D is obtained carries out spray granulation granulation, material is had necessarily Mobility is to be molded.Spray condition is set as 300 ± 20 DEG C of inlet temperature of spraying, 110 ± 10 DEG C of spray outlet temperature, feeding Frequency is 10-13Hz, rejection tablet frequency setting 60Hz, and the powder for spraying out needs to carry out humidification process, it is desirable to which apparent density is 1.25-1.45g/cm3, water content≤0.4%, it is standby to obtain particulate material warehouse entry.
F, shaping compacting:By the particulate material that step E is obtained by particular manufacturing craft on powder former it is compressing The semi-finished product of shape and size needed for going out.
Higher with nickel zinc magnetic core semi-finished product intensity made from manufacture method of the present invention, flexibility is good, less brittle, and quality is equal It is even, convenient follow-up cutting, rupture, damaged is not susceptible to during cutting, otch is neat, can substantially reduce the scrappage of production process. Scrappage is more than 1.5% in subsequently cutting step for the nickel zinc magnetic core semi-finished product of art methods manufacture, by the inventive method The nickel zinc magnetic core of manufacture subsequently cutting step in scrappage only below 0.2%.The method of the present invention, which advantageously reduces, to be produced into This, improves production efficiency.

Claims (5)

1. a kind of manufacture method of Cutting free nickel zinc magnetic core semi-finished product, it is characterised in that comprise the following steps:
A, dispensing and mixing vibration:By mass fraction by raw material di-iron trioxide 65%-70%, zinc oxide 15%-19%, cupric oxide 3%-5%, nickel protoxide 10%-15%, bismuth oxide 0.1%-0.3%, tungsten oxide 0.05%-0.1%, zirconium oxide 0.005%-0.01%, two Silica 0.05-0.1%, which is uniformly poured into ball mill hopper, carries out mixing vibration 60 minutes, is then transferred in pelletizer and is made Ball operation, pelletizing material is obtained, the sphere diameter requirement of the pelletizing material is between 1-8mm;
B, pre-burning:The pelletizing material that step A is obtained, which is even added to from hopper in rotary kiln, carries out pre-burning, in rotary kiln Four regions, temperature rotates boiler tube 30-50 minutes between 820-860 DEG C, with 3-5r/min rotating speed, then is carried out with ball mill Ball milling 50 minutes, obtain pre-burning vibration material;
C, glue is boiled:92 parts of pure water are warming up to 50-55 DEG C by weight, 8 parts of granule of polyvinyl alcohol stirrings is then added and is warming up to 95 DEG C, continue stopping heating after heating while stirring 5 hours and continue to stir, filter, gathered after temperature is dropped to below 45 DEG C Vinyl alcohol glue, be sealed with glue bucket it is standby, wherein, the granule of polyvinyl alcohol includes two kinds of models, specially described poly- BP-17 mass fractions account for 30%-70% in vinyl alcohol particle, and BP-05 accounts for 30%-70%;
D, extra-fine grinding:The described vibration material 58-65 parts for by weight obtaining pure water 20-25 parts and step B add vertical sand Grinding machine is ground 20 minutes, then toward adding dispersant 0.2-0.5 parts, defoamer 0.1-0.35 parts, sintering in the vertical grinding machine Described polyvinyl alcohol glue 16-20 parts that auxiliary agent 0.6-1.8 parts and step C are obtained, grinding are pumped into horizontal sand mill after 60 minutes Extra-fine grinding 60 minutes is carried out, obtains slurry;
E, mist projection granulating:The slurry that step D is obtained carries out spray granulation granulation, and spray condition is set as being sprayed into 300 ± 20 DEG C of temperature of mouth, 110 ± 10 DEG C of spray outlet temperature, feeding frequency are 10-13Hz, rejection tablet frequency setting 60Hz, are sprayed Powder out needs to carry out humidification process, it is desirable to apparent density 1.25-1.45g/cm3, water content≤0.4%, obtain particle Expect that warehouse entry is standby;
F, shaping compacting:The particulate material that step E is obtained presses institute by particular manufacturing craft on powder former Need the semi-finished product of shape and size.
2. the manufacture method of Cutting free nickel zinc magnetic core semi-finished product according to claim 1, it is characterised in that turned round in step B The temperature in four regions described in kiln is specially 860 DEG C, 845 DEG C, 845 DEG C, 820 DEG C.
3. the manufacture method of Cutting free nickel zinc magnetic core semi-finished product according to claim 1, it is characterised in that described in step C Granule of polyvinyl alcohol is made up of BP-17 40% and BP-05 60%.
4. the manufacture method of Cutting free nickel zinc magnetic core semi-finished product according to claim 1, it is characterised in that described in step D Sintering aid by following mass fraction material composition:Cupric oxide 62%-94%, bismuth oxide 6%-38%.
5. the manufacture method of high pendulum folding intensity nickel zinc soft magnetic core according to claim 1, it is characterised in that institute in step D Slurry average grain diameter D50 requirements are stated below 0.5 μm.
CN201711119332.1A 2017-11-14 2017-11-14 A kind of manufacture method of Cutting free nickel zinc magnetic core semi-finished product Pending CN107867866A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201711119332.1A CN107867866A (en) 2017-11-14 2017-11-14 A kind of manufacture method of Cutting free nickel zinc magnetic core semi-finished product

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201711119332.1A CN107867866A (en) 2017-11-14 2017-11-14 A kind of manufacture method of Cutting free nickel zinc magnetic core semi-finished product

Publications (1)

Publication Number Publication Date
CN107867866A true CN107867866A (en) 2018-04-03

Family

ID=61753928

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201711119332.1A Pending CN107867866A (en) 2017-11-14 2017-11-14 A kind of manufacture method of Cutting free nickel zinc magnetic core semi-finished product

Country Status (1)

Country Link
CN (1) CN107867866A (en)

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN111508699A (en) * 2020-04-21 2020-08-07 东莞市南祥磁电科技有限公司 Method for reprocessing magnetic core powder after compression molding
CN114653939A (en) * 2022-03-01 2022-06-24 山东汇嘉磁电科技有限公司 Production and processing method of U-shaped magnetic powder core

Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US5055322A (en) * 1989-11-02 1991-10-08 Nippon Zeon Co., Ltd. Method of producing magnetic recording media
CN107098692A (en) * 2017-06-07 2017-08-29 沅陵辰州磁电高科有限公司 A kind of preparation method of high intensity nickel zinc soft magnetic core

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US5055322A (en) * 1989-11-02 1991-10-08 Nippon Zeon Co., Ltd. Method of producing magnetic recording media
CN107098692A (en) * 2017-06-07 2017-08-29 沅陵辰州磁电高科有限公司 A kind of preparation method of high intensity nickel zinc soft magnetic core

Non-Patent Citations (2)

* Cited by examiner, † Cited by third party
Title
夏德贵等: "《软磁铁氧体制造原理与技术》", 31 December 2010 *
张美云等: "《加工纸与特种纸》", 31 January 2010 *

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN111508699A (en) * 2020-04-21 2020-08-07 东莞市南祥磁电科技有限公司 Method for reprocessing magnetic core powder after compression molding
CN111508699B (en) * 2020-04-21 2022-06-10 东莞市南祥磁电科技有限公司 Method for reprocessing magnetic core powder after compression molding
CN114653939A (en) * 2022-03-01 2022-06-24 山东汇嘉磁电科技有限公司 Production and processing method of U-shaped magnetic powder core

Similar Documents

Publication Publication Date Title
CN102583973B (en) Soft chemical preparation method of hollow glass microspheres, prepared hollow glass microspheres and application thereof
CN104150883B (en) A kind of preparation method of aluminum oxide pelletizing
CN105563363B (en) A kind of method that centrifugal drying granulating technique prepares vitrified bond accumulation abrasive material
CN101786160B (en) Special molybdenum powder used for automatic forming and preparation method thereof
CN103495693A (en) High-temperature-resisting easy collapse molding sand and preparation method thereof
CN104607102B (en) A manufacturing method of a high-strength small-size mill ball
CN107867866A (en) A kind of manufacture method of Cutting free nickel zinc magnetic core semi-finished product
CN103752213A (en) Device suitable for humidifying and granulating dry powder
CN107892563A (en) A kind of manufacture method of high pendulum folding intensity nickel zinc soft magnetic core
CN105859258A (en) Ceramic grinding ball for cement ball mill, and preparation method thereof
CN104876595B (en) Bitter earth nano powder prepares the method and apparatus of zirconium oxide metering nozzle
CN104129977B (en) A kind of preparation method of hot pressurized water valve block special aluminium oxide pelletizing
CN104858021B (en) The surface treatment method of quartz sand
CN104629683B (en) Preparation method of high-strength parent nucleus for centrifugal shaping of ceramic grinding ball
CN106216699A (en) A kind of 3D prints and uses metal dust preparation technology
CN102225837B (en) Manufacture method of spray-free fused quartz crucible used for polycrystalline silicon cast ingots
CN102219360B (en) Method for manufacturing polycrystalline silicon ingot casting fused quartz crucible without spraying
CN105541305A (en) Preparation method of silicon controlled rectifier product with inner diameter of 180mm
CN203976886U (en) A kind ofly can produce the palletizing device with inside and outside double-layer structure pellet
CN107887151A (en) A kind of discarded magnetic core reconstruction method
CN105859261A (en) Ceramic grinding section for cement ball mill, and preparation method thereof
CN104475652A (en) Anti-shakeout molding sand and preparation method thereof
CN204185405U (en) Hot melt granular chemical fertilizer coating machine
CN103521682A (en) Molding sand used for special casting mould surface and preparation method thereof
CN107034407B (en) A kind of production method of hard alloy

Legal Events

Date Code Title Description
PB01 Publication
PB01 Publication
SE01 Entry into force of request for substantive examination
SE01 Entry into force of request for substantive examination
RJ01 Rejection of invention patent application after publication
RJ01 Rejection of invention patent application after publication

Application publication date: 20180403