CN107860820A - Heat-resisting steel part deterioration appraisal procedure, device and magnetic parameters instrument - Google Patents

Heat-resisting steel part deterioration appraisal procedure, device and magnetic parameters instrument Download PDF

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Publication number
CN107860820A
CN107860820A CN201711318193.5A CN201711318193A CN107860820A CN 107860820 A CN107860820 A CN 107860820A CN 201711318193 A CN201711318193 A CN 201711318193A CN 107860820 A CN107860820 A CN 107860820A
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China
Prior art keywords
heat
steel part
resisting steel
micro
test sample
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CN201711318193.5A
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Chinese (zh)
Inventor
崔崇
张倚雯
袁廷璧
牛晓光
董勇军
肖德铭
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State's Electric Boiler Inspection Of Pressure Vessel Center
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State's Electric Boiler Inspection Of Pressure Vessel Center
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Priority to CN201711318193.5A priority Critical patent/CN107860820A/en
Publication of CN107860820A publication Critical patent/CN107860820A/en
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    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N27/00Investigating or analysing materials by the use of electric, electrochemical, or magnetic means
    • G01N27/72Investigating or analysing materials by the use of electric, electrochemical, or magnetic means by investigating magnetic variables
    • G01N27/82Investigating or analysing materials by the use of electric, electrochemical, or magnetic means by investigating magnetic variables for investigating the presence of flaws
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01RMEASURING ELECTRIC VARIABLES; MEASURING MAGNETIC VARIABLES
    • G01R33/00Arrangements or instruments for measuring magnetic variables
    • G01R33/12Measuring magnetic properties of articles or specimens of solids or fluids
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01RMEASURING ELECTRIC VARIABLES; MEASURING MAGNETIC VARIABLES
    • G01R33/00Arrangements or instruments for measuring magnetic variables
    • G01R33/12Measuring magnetic properties of articles or specimens of solids or fluids
    • G01R33/14Measuring or plotting hysteresis curves

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  • Physics & Mathematics (AREA)
  • General Physics & Mathematics (AREA)
  • Condensed Matter Physics & Semiconductors (AREA)
  • Chemical & Material Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • Electrochemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Analytical Chemistry (AREA)
  • Biochemistry (AREA)
  • General Health & Medical Sciences (AREA)
  • Immunology (AREA)
  • Pathology (AREA)
  • Investigating Or Analyzing Materials By The Use Of Magnetic Means (AREA)

Abstract

The invention discloses a kind of heat-resisting steel part deterioration appraisal procedure, device and magnetic parameters instrument, heat-resisting steel part deteriorates appraisal procedure, including step:A, the database for characterizing magnetic parameter and degradation level matching relationship is obtained;B, the micro-test sample of heat-resisting steel part is obtained;C, the micro-test sample is detected using magnetic parameters instrument, obtains the magnetic parameter of micro-test sample;D, reference database, obtains the degradation level matched with the magnetic parameter of the micro-test sample, finally draws the degradation level of the heat-resisting steel part.Heat-resisting steel part deterioration appraisal procedure can efficiently solve the problem of existing heat-resisting steel part deterioration appraisal procedure cost is high, evaluation cycle is long, the workpiece recovery difficulty after destructive sampling is larger.

Description

Heat-resisting steel part deterioration appraisal procedure, device and magnetic parameters instrument
Technical field
It is bad more specifically to a kind of heat-resisting steel part the present invention relates to heat resisting steel component capabilities detection technique field Change appraisal procedure, device and magnetic parameters instrument.
Background technology
High temperature, the workpiece of high pressure operating mode are born largely using heat-resisting steel material making, such as power plant, the high temperature in chemical plant Pressure piping, pipe fitting, valve etc..As active time extends, the heat-resisting gradual aging of steel part, its main performance degradation mechanism Including high-temerature creep, heat fatigue and creep-fatigue interaction.
At present, generally use disruptive method (such as pipe cutting, overall cutting) samples to heat-resisting steel workpiece, and passes through length When high-temerature creep experiment (test period thousands of arrive tens thousand of hours), the means such as short time high temperature tension test are to its performance degradation situation Assessed.
Other in addition to conduit component bear high temperature, the part of high pressure is generally not allowed destructive sampling, and there is no at present Effective performance degradation appraisal procedure, such as:Header, valve body, cylinder body etc..
Although workpiece is tested or than clothes by above-mentioned deterioration performance estimating method under approximate military service working condition Accelerated test is carried out under conditions of labour condition is more harsh, confidence level is higher.But experimentation cost is high, evaluation cycle is long, destroys Property sampling after workpiece recover difficulty it is larger, the parts such as header, valve body are not suitable in addition to pipeline.
The content of the invention
In view of this, first purpose of the invention is to provide a kind of heat-resisting steel part deterioration appraisal procedure, and this is heat-resisting Steel part deterioration appraisal procedure can efficiently solve existing heat-resisting steel part deterioration appraisal procedure cost height, evaluation cycle mistake Workpiece after long, destructive sampling recovers the problem of difficulty is larger.Second object of the present invention is to provide a kind of heat resisting steel portion Part deteriorates apparatus for evaluating and magnetic parameters instrument.
In order to reach above-mentioned first purpose, the present invention provides following technical scheme:
A kind of heat-resisting steel part deterioration appraisal procedure, including step:
A, the database for characterizing magnetic parameter and degradation level matching relationship is obtained;
B, the micro-test sample of heat-resisting steel part is obtained;
C, the micro-test sample is detected using magnetic parameters instrument, obtains the magnetic parameter of micro-test sample;
D, reference database, obtains the degradation level matched with the magnetic parameter of the micro-test sample, finally draws described The degradation level of heat-resisting steel part.
Preferably, in above-mentioned heat-resisting steel part deterioration appraisal procedure, the step a is specifically included:
A1, acquisition are respectively at multigroup heat-resisting steel part sample of multiple degradation levels, pass through magnetic parameters instrument Respectively obtain the magnetic parameter of multigroup heat-resisting steel part sample;
A2, magnetic parameter and the matching incidence relation of degradation level are established, and establish database.
Preferably, in above-mentioned heat-resisting steel part deterioration appraisal procedure, the step c is specially:
The micro-test sample is divided into multiple sheet samples, multiple sheet samples examined using magnetic parameters instrument Survey, obtain the magnetic parameter of multiple sheet samples.
Preferably, in above-mentioned heat-resisting steel part deterioration appraisal procedure, the micro-test sample is cylindric, and its external diameter is 20- 100mm, thickness axially is >=2mm.
Preferably, in above-mentioned heat-resisting steel part deterioration appraisal procedure, the cylindric micro-test sample is by along described heat-resisting Steel part wall thickness direction samples to obtain.
Preferably, in above-mentioned heat-resisting steel part deterioration appraisal procedure, the step c is specially:
The micro-test sample is divided into multiple sheet samples axially along, using magnetic parameters instrument to multiple sheets Sample is detected, and obtains the magnetic parameter of multiple sheet samples.
Preferably, in above-mentioned heat-resisting steel part deterioration appraisal procedure, the magnetic parameter is magnetic coercive force, remanence The tangent slope of intensity, hysteresis curve envelope size or hysteresis curve.
A kind of heat-resisting steel part deterioration apparatus for evaluating, including:
Part is sampled, for obtaining micro-test sample from heat-resisting steel part;
Magnetic parameters instrument, for obtaining the magnetic parameter of micro-test sample, the magnetic parameters instrument includes probe and set Two electrodes being placed on the probe, described two electrodes farthest away from the distance between point of other side be 25-45mm;
Storage device, for storing the data of the magnetic parameter with degradation level matching relationship that characterize the micro-test sample Storehouse.
A kind of magnetic parameters instrument, for obtaining the magnetic parameter of micro-test sample, the magnetic parameters instrument includes probe With two electrodes being arranged on the probe, described two electrodes farthest away from the distance between point of other side be 25-45mm.
In heat-resisting steel part deterioration appraisal procedure provided by the invention, obtain characterize magnetic parameter and degradation level first The database of matching relationship, i.e., the degradation level matched with magnetic parameter can be found by database.Then obtain heat-resisting The micro-test sample of steel part, micro-test sample take can't heat-resisting steel part damage, taking can be by resistance to after micro-test sample Hot steel part carries out repairing and allows it to be continuing with.Then micro-test sample is detected using magnetic parameters instrument, obtained The magnetic parameter of micro-test sample.Finally, reference database, the degradation level matched with the magnetic parameter of micro-test sample is obtained, most The degradation level of heat-resisting steel part is drawn eventually.In this way, when carrying out heat-resisting steel part deterioration assessment, micro-test sample only need to be obtained, is passed through Detection to micro-test sample obtains the magnetic parameter of micro-test sample, and reference database draws what is matched with the magnetic parameter of micro-test sample Degradation level.Use heat-resisting steel part deterioration appraisal procedure provided by the invention, it is not necessary to heat-resisting steel part is cut again The destructions such as pipe, overall cutting sample, and can draw the degradation level of heat-resisting steel part, and heat-resisting steel part recovers after obtaining micro-test sample Difficulty is small, substantially reduces sample cost.Moreover, assessment cycle is short, method provided by the invention is equally applicable to header, valve body etc. Part.
In order to reach above-mentioned second purpose, present invention also offers a kind of heat-resisting steel part deterioration apparatus for evaluating and magnetic Parameter measurement instrument.Heat-resisting the steel part deterioration apparatus for evaluating and magnetic parameters instrument should also have corresponding technique effect, herein Repeat no more.
Brief description of the drawings
In order to illustrate more clearly about the embodiment of the present invention or technical scheme of the prior art, below will be to embodiment or existing There is the required accompanying drawing used in technology description to be briefly described, it should be apparent that, drawings in the following description are only this Some embodiments of invention, for those of ordinary skill in the art, on the premise of not paying creative work, can be with Other accompanying drawings are obtained according to these accompanying drawings.
Fig. 1 is the flow chart that heat-resisting steel part provided in an embodiment of the present invention deteriorates appraisal procedure;
Fig. 2 is the schematic diagram that heat-resisting steel part provided in an embodiment of the present invention takes micro-test sample;
Fig. 3 is the structural representation of micro-test sample provided in an embodiment of the present invention;
Fig. 4 is the structural representation of multiple sheet samples provided in an embodiment of the present invention;
Fig. 5 is the structural representation of the probe of magnetic parameters instrument provided in an embodiment of the present invention.
In Fig. 2-5:
The heat-resisting steel parts of 1-, 2- micro-test samples, 2a- sheet samples, 3- probes, 4- electrodes.
Embodiment
First purpose of the present invention is that providing a kind of heat-resisting steel part deteriorates appraisal procedure, heat-resisting steel part deterioration It is long, destructive that appraisal procedure can efficiently solve existing heat-resisting steel part deterioration appraisal procedure cost height, evaluation cycle Workpiece after sampling recovers the problem of difficulty is larger.Second object of the present invention is to provide a kind of heat-resisting steel part deterioration and assessed Device and magnetic parameters instrument.
Below in conjunction with the accompanying drawing in the embodiment of the present invention, the technical scheme in the embodiment of the present invention is carried out clear, complete Site preparation describes, it is clear that described embodiment is only part of the embodiment of the present invention, rather than whole embodiments.It is based on Embodiment in the present invention, those of ordinary skill in the art are obtained every other under the premise of creative work is not made Embodiment, belong to the scope of protection of the invention.
Referring to Fig. 1, Fig. 1 is the flow chart that heat-resisting steel part provided in an embodiment of the present invention deteriorates appraisal procedure, it is wrapped Include step:
S1, obtain the database for characterizing magnetic parameter and degradation level matching relationship.
Multiple magnetic parameters and the degradation level matched with multiple magnetic parameters are stored with database.Pass through Reference database can be derived that degradation level corresponding to each magnetic parameter.
S2, the micro-test sample 2 for obtaining heat-resisting steel part 1.
The size of wherein micro-test sample 2 is smaller, after obtaining micro-test sample 2 on heat-resisting steel part 1, by heat-resisting steel part 1 repairing can be continuing with heat resisting steel part 1, i.e., it can't be caused after micro-test sample 2 being taken on heat-resisting steel part 1 The destruction of irreparability.Specifically, Mechanical Method can be used to obtain micro-test sample 2, or micro-test sample is obtained using magnetic sleeve drill tools 2, herein and it is not especially limited.
S3, using magnetic parameters instrument micro-test sample 2 is detected, obtain the magnetic parameter of micro-test sample 2.
The micro-test sample 2 obtained in step S2 is detected using magnetic parameters instrument in the step, finally gives step The magnetic parameter of the micro-test sample 2 obtained in S2.
S4, reference database, obtain the degradation level matched with the magnetic parameter of micro-test sample 2, finally draw described resistance to The degradation level of hot steel part 1.
I.e. according to the magnetic parameter of the micro-test sample 2 obtained in step S3, reference database, draw with being obtained in step S3 Micro-test sample 2 magnetic parameter matching degradation level, then be the degradation level of heat-resisting steel part 1.
In this way, when carrying out the heat-resisting deterioration of steel part 1 assessment, micro-test sample 2 only need to be obtained, passes through detecting to micro-test sample 2 To the magnetic parameter of micro-test sample 2, reference database draws the degradation level matched with the magnetic parameter of micro-test sample 2. Appraisal procedure is deteriorated using heat-resisting steel part 1 provided by the invention, it is not necessary to pipe cutting, overall cutting are carried out to heat-resisting steel part 1 again Sampling Deng destruction, the degradation level of heat-resisting steel part 1 can be drawn, the heat-resisting recovery of steel part 1 difficulty is small after obtaining micro-test sample 2, Substantially reduce sample cost.Moreover, assessment cycle is short, method provided by the invention is equally applicable to the parts such as header, valve body.
In above-mentioned heat-resisting steel part deterioration appraisal procedure, the step S1 is specifically included:
S11, acquisition are respectively at multigroup heat-resisting steel part sample of multiple degradation levels, are distinguished by magnetic parameters instrument Obtain the magnetic parameter of multigroup heat-resisting steel part sample;
S12, magnetic parameter and the matching incidence relation of degradation level are established, and establish database.
In the step, multiple magnetic parameter scopes can be specifically set, each magnetic parameter scope has the bad of matching Change grade.When the magnetic parameter of micro-test sample 2 is in the range of a certain magnetic parameter, then micro-test sample 2 is in magnetic parameter The degradation level of commensurate in scope.
Wherein it is possible to when implementing long to new heat-resisting steel part 1 high-temerature creep experiment or heat fatigue simulated test draw it is more Multigroup heat-resisting steel part sample of individual degradation level.
In another embodiment, step S3 is specially:Micro-test sample 2 is divided into multiple sheet sample 2a, surveyed using magnetic parameter Amount instrument detects to multiple sheet sample 2a, obtains multiple sheet sample 2a magnetic parameter.
It can so realize and magnetic parameter detection is carried out to the heat-resisting different parts of steel part 1, to realize to heat-resisting steel part 1 not Deterioration assessment is carried out with position, draws the magnetic parameter of the heat-resisting different parts of steel part 1.
Preferably, micro-test sample 2 can be cylindric, and its external diameter is 20mm-100mm, thickness >=2mm axially. Further, cylindric micro-test sample 2 can sample to obtain by the direction along the heat-resisting wall thickness of steel part 1.Certainly, micro-test sample 2 It can also be other shapes, be not limited thereto.
Can be specially in step S3:Micro-test sample 2 is divided into multiple sheet sample 2a axially along, surveyed using magnetic parameter Amount instrument detects to multiple sheet sample 2a, obtains multiple sheet sample 2a magnetic parameter.
When being layered to micro-test sample 2, multiple sheet sample 2a can be divided into along the axial direction of cylindric micro-test sample 2, And then realize that the deterioration to different depth position of the heat-resisting steel part 1 along wall thickness direction is assessed.
Preferably, above-mentioned magnetic parameter can be magnetic coercive force, remanence strength, hysteresis curve envelope size and magnetic One or more in the tangent slope of hysteresis curves, are not limited thereto.
Appraisal procedure is deteriorated based on the heat-resisting steel part provided in above-described embodiment, present invention also offers a kind of heat resisting steel Part deteriorates apparatus for evaluating, and the heat-resisting steel part deterioration apparatus for evaluating includes sampling part, magnetic parameters instrument and storage device.
Wherein, sample part to be used to obtain micro-test sample 2 from heat-resisting steel part 1, it can be that magnetic sleeve bores specifically to sample part. Magnetic parameters instrument is used for the magnetic parameter for obtaining micro-test sample 2, and magnetic parameters instrument includes probe 3 and is arranged on probe 3 Two electrodes 4, two electrodes 4 are 25-45mm farthest away from the distance between point of other side, can so ensure that magnetic parameter is surveyed Amount instrument adapts to a variety of micro-test samples 2.Two electrodes 4 can be specially two magnetic poles, i.e. S poles and N poles.Storage device is used to store The magnetic parameter of micro-test sample 2 and the database of degradation level matching relationship are characterized, storage device can be specially chip, USB flash disk Or paper document.
The embodiment of the present invention additionally provides a kind of magnetic parameters instrument, and it is used for the magnetic parameter for obtaining micro-test sample 2, weight Point is, magnetic parameters instrument includes probe 3 and two electrodes 4 being arranged on the probe 3, two electrodes 4 farthest away from The distance between point of other side is 25-45mm.Micro-test sample 2 is examined in this way, the size between positive pole and negative pole disclosure satisfy that The requirement of survey.Two electrodes 4 can be specially two magnetic poles, i.e. S poles and N poles.
Each embodiment is described by the way of progressive in this specification, what each embodiment stressed be and other The difference of embodiment, between each embodiment identical similar portion mutually referring to.
The foregoing description of the disclosed embodiments, professional and technical personnel in the field are enable to realize or using the present invention. A variety of modifications to these embodiments will be apparent for those skilled in the art, as defined herein General Principle can be realized in other embodiments without departing from the spirit or scope of the present invention.Therefore, it is of the invention The embodiments shown herein is not intended to be limited to, and is to fit to and principles disclosed herein and features of novelty phase one The most wide scope caused.

Claims (9)

1. a kind of heat-resisting steel part deterioration appraisal procedure, it is characterised in that including step:
A, the database for characterizing magnetic parameter and degradation level matching relationship is obtained;
B, the micro-test sample (2) of heat-resisting steel part is obtained;
C, the micro-test sample (2) is detected using magnetic parameters instrument, obtains the magnetic parameter of micro-test sample (2);
D, reference database, the degradation level matched with the magnetic parameter of the micro-test sample (2) is obtained, finally drawn described resistance to The degradation level of hot steel part.
2. heat-resisting steel part deterioration appraisal procedure according to claim 1, it is characterised in that the step a is specifically included:
A1, acquisition are respectively at multigroup heat-resisting steel part sample of multiple degradation levels, are distinguished by magnetic parameters instrument Obtain the magnetic parameter of multigroup heat-resisting steel part sample;
A2, magnetic parameter and the matching incidence relation of degradation level are established, and establish database.
3. heat-resisting steel part deterioration appraisal procedure according to claim 1, it is characterised in that the step c is specially:
The micro-test sample (2) is divided into multiple sheet samples (2a), using magnetic parameters instrument to multiple sheet samples (2a) is detected, and obtains multiple sheet samples (2a) magnetic parameter.
4. heat-resisting steel part deterioration appraisal procedure according to claim 1, it is characterised in that the micro-test sample (2) is circle Column, and its external diameter is 20-100mm, thickness axially is >=2mm.
5. heat-resisting steel part deterioration appraisal procedure according to claim 4, it is characterised in that the cylindric micro-test sample (2) by sampling to obtain along the heat resisting steel part wall thickness direction.
6. heat-resisting steel part deterioration appraisal procedure according to claim 4, it is characterised in that the step c is specially:
The micro-test sample (2) is divided into multiple sheet samples (2a) axially along, using magnetic parameters instrument to multiple described Sheet sample (2a) is detected, and obtains multiple sheet samples (2a) magnetic parameter.
7. heat-resisting steel part deterioration appraisal procedure according to claim 1, it is characterised in that the magnetic parameter is magnetic Coercivity, remanence strength, the tangent slope of hysteresis curve envelope size or hysteresis curve.
A kind of 8. heat-resisting steel part deterioration apparatus for evaluating, it is characterised in that including:
Part is sampled, for obtaining micro-test sample (2) from heat-resisting steel part;
Magnetic parameters instrument, for obtaining the magnetic parameter of micro-test sample (2), the magnetic parameters instrument include probe (3) and Two electrodes (4) being arranged on the probe (3), described two electrodes (4) are farthest away from the distance between point of other side 25-45mm;
Storage device, for storing the database of the magnetic parameter with degradation level matching relationship that characterize the micro-test sample (2).
9. a kind of magnetic parameters instrument, it is characterised in that for obtaining the magnetic parameter of micro-test sample (2), the magnetic parameter is surveyed Amount instrument includes probe (3) and is arranged at two electrodes (4) popped one's head on (3), described two electrodes (4) farthest away from other side The distance between point be 25-45mm.
CN201711318193.5A 2017-12-12 2017-12-12 Heat-resisting steel part deterioration appraisal procedure, device and magnetic parameters instrument Pending CN107860820A (en)

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CN108791880A (en) * 2018-05-04 2018-11-13 国电锅炉压力容器检验中心 A kind of pressure vessel inspection unmanned plane
CN113189199A (en) * 2021-03-30 2021-07-30 国能锅炉压力容器检验有限公司 Nonlinear ultrasonic detection grading evaluation method for heat-resistant steel part performance degradation

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CN113189199A (en) * 2021-03-30 2021-07-30 国能锅炉压力容器检验有限公司 Nonlinear ultrasonic detection grading evaluation method for heat-resistant steel part performance degradation

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