CN107860602A - Pole piece high vacuum, high temperature moisture content sampler - Google Patents
Pole piece high vacuum, high temperature moisture content sampler Download PDFInfo
- Publication number
- CN107860602A CN107860602A CN201711351428.0A CN201711351428A CN107860602A CN 107860602 A CN107860602 A CN 107860602A CN 201711351428 A CN201711351428 A CN 201711351428A CN 107860602 A CN107860602 A CN 107860602A
- Authority
- CN
- China
- Prior art keywords
- pole piece
- high temperature
- semicircular cylinder
- stainless steel
- moisture content
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 230000006835 compression Effects 0.000 claims abstract description 18
- 238000007906 compression Methods 0.000 claims abstract description 18
- 229910001220 stainless steel Inorganic materials 0.000 claims description 27
- 239000010935 stainless steel Substances 0.000 claims description 27
- 239000004964 aerogel Substances 0.000 claims description 10
- 239000000203 mixture Substances 0.000 claims 2
- 238000001035 drying Methods 0.000 abstract description 19
- 238000010276 construction Methods 0.000 abstract description 2
- 239000000523 sample Substances 0.000 description 18
- 238000001514 detection method Methods 0.000 description 11
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 10
- 238000000034 method Methods 0.000 description 4
- 238000010438 heat treatment Methods 0.000 description 2
- 238000009434 installation Methods 0.000 description 2
- 238000004519 manufacturing process Methods 0.000 description 2
- 238000004458 analytical method Methods 0.000 description 1
- 230000006378 damage Effects 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 238000003780 insertion Methods 0.000 description 1
- 230000037431 insertion Effects 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 230000028161 membrane depolarization Effects 0.000 description 1
- 238000005070 sampling Methods 0.000 description 1
- 239000002699 waste material Substances 0.000 description 1
Classifications
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N1/00—Sampling; Preparing specimens for investigation
- G01N1/02—Devices for withdrawing samples
- G01N1/04—Devices for withdrawing samples in the solid state, e.g. by cutting
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N1/00—Sampling; Preparing specimens for investigation
- G01N1/28—Preparing specimens for investigation including physical details of (bio-)chemical methods covered elsewhere, e.g. G01N33/50, C12Q
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N1/00—Sampling; Preparing specimens for investigation
- G01N1/28—Preparing specimens for investigation including physical details of (bio-)chemical methods covered elsewhere, e.g. G01N33/50, C12Q
- G01N1/44—Sample treatment involving radiation, e.g. heat
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02E—REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
- Y02E60/00—Enabling technologies; Technologies with a potential or indirect contribution to GHG emissions mitigation
- Y02E60/10—Energy storage using batteries
Abstract
The invention provides a kind of pole piece high vacuum, high temperature moisture content sampler, including for storing by the reel of dry pole piece, it is set with successively from the inside to the outside outside the reel for the fixed fixed bed for store pole piece, the placed layer for placing detected pole piece sample, for making pole piece sample that there is the heat conduction layer of thermal environment identical with stored pole piece inside, and makes pole piece sample with the shell of compression with stored pole piece inside equal tension.The present invention is simple in construction, without dry pole piece roll is taken out, i.e., can provide more accurate pole piece and dry data.The present invention is applied to drying for current all pole pieces and detected.
Description
Technical field
The invention belongs to battery pole piece detection field, is related to a kind of battery pole piece moisture content detection sampler, specifically
It is a kind of pole piece high vacuum, high temperature moisture content sampler.
Background technology
Preceding process material of the battery pole piece as battery production, the size of its moisture content directly affect battery quality, therefore,
The pole piece of production needs to carry out removing water process.The technique of the water removal to battery pole piece is at present, by the pole of 120 microns thickness
Piece is rolled into the pole volume between a diameter of 400mm-1200mm, and then pole volume is placed into drying oven and carries out vacuum and heating drying,
To remove the moisture that depolarization is rolled up.Rolled up in pole and carry out drying phase under vacuum, it is necessary to be detected to the interior moisture content of pole volume, but due to
Pole volume be integral type reel structure, thus be accordingly used in detection water content instrument probe can not extend into pole roll up in detected;Together
When, due to strict to pole volume local environment requirement, therefore pole can not be batched out and directly be contacted with air, otherwise can caused
All that has been achieved is spoiled for drying and dehydrating work.In addition, pole scroll is long-pending, quality is larger, pole can not be rolled up and carry out destruction sampling, in summary,
The detection for carrying out water content is rolled up to pole there is presently no good method, and then can not be known by whether dry pole volume meets to want
Ask.
The content of the invention
The technical problem to be solved in the present invention, it is to provide a kind of pole piece high vacuum, high temperature moisture content sampler, to realize not
Pole volume is destroyed, and ensures pole volume local environment and the moisture content of pole volume can be measured.
In order to solve the above technical problems, the technical solution used in the present invention is:
A kind of pole piece high vacuum, high temperature moisture content sampler, it includes:
For storing by the reel of dry pole piece, the reel is set with successively from the inside to the outside outside stores pole piece for fixation
Fixed bed, the placed layer for placing detected pole piece sample, for make pole piece sample have with inside stored pole piece
The heat conduction layer of identical thermal environment, and make pole piece sample that there is the shell of compression with equal tension inside stored pole piece.
As limitation of the invention:The reel is cylindrical shape made of corrugated paper;Fixed bed is high temperature resistant, vacuum-resistant
The first aerogel layer;The placed layer is the pole piece roll that forms of pole piece coiling identical with the pole piece of storage, on the pole piece roll
Offer the rectangular window for placing pole piece sample;The heat conduction layer is high temperature resistant, the second aerogel layer of vacuum-resistant;Institute
It is stainless steel sleeve to state shell of compression.
As limitation of the invention further:First aerogel layer is integrated cylindrical tube shape structure, the second airsetting
The cylindrical tube shape structure that the first aeroge semicircular cylinder and the second aeroge semicircular cylinder that glue-line matches for size are formed, described two
It is detachably connected between individual aeroge semicircular cylinder by the first bindiny mechanism.
As the restriction to the first bindiny mechanism in the present invention:First bindiny mechanism is included located at the first aeroge half
Projection on cylinder, and the groove to match on the second aeroge semicircular cylinder, with projection.
As the restriction to shell of compression in the present invention:The shell of compression be the first stainless steel semicircular cylinder for matching of size with
The cylindrical tube shape structure that second stainless steel semicircular cylinder is formed, can by the second bindiny mechanism between described two stainless steel semicircular cylinders
Dismantling connection.
As the further restriction to the second bindiny mechanism in the present invention:Second bindiny mechanism includes being respectively arranged on the
Engaging lug on one stainless steel semicircular cylinder and the second stainless steel semicircular cylinder stack shell, the engaging lug on the first stainless steel semicircular cylinder
It is connected with the engaging lug on the second stainless steel semicircular cylinder by bolt mechanism.
As a result of above-mentioned technical scheme, compared with prior art, acquired technological progress is the present invention:
(1)Pole piece sample and pole piece to be dried are co-located in same drying oven by the present invention, and by setting fixed bed, heat
Conducting shell, pole piece sample is arranged between fixed bed and heat conduction layer, the environment residing for simulated pole piece sample, and then makes pole piece
Sample is provided with shell of compression with by dry pole piece centre having same dry environment, make pole piece sample with it is to be dried
Pole piece centre there is same pressure, that is, ensure pole piece sample and same ring had by dry pole piece centre
Border condition, the data of pole piece sample are measured closer to by the data of dry pole piece roll with order;
(2)The fixed bed of the present invention uses aeroge with heat conduction layer, because the thermal conductivity of aeroge is pole piece thermal conductivity
1/10th, therefore when pole piece sample is between two layers aerogel layer, its moisture data after removing water is closer to being dried pole
Piece rolls up the data in centre, makes analysis result more accurate;
(3)The heat conduction layer of the present invention and shell of compression are demountable structure, therefore need to only be opened shell of compression and heat conduction layer
It can be taken off pole piece sample and carry out water content detection, without the drying oven of vacuum high-temperature entirely will be taken out with regard to energy by dry pole piece
The detection to pole piece moisture is enough realized, i.e., whether the pole piece that can determine whether to be dried in the drying process reaches requirement, avoid taking
Go out pole piece measure dry it is unqualified after melt down time for toasting again again and waste and the wasting of resources.
In summary, the present invention is simple in construction, without dry pole piece roll is taken out, i.e., can provide more accurate pole
Piece dries data.
The present invention is applied to drying for current all pole pieces and detected.
The present invention is described in further detail below in conjunction with specific embodiment.
Brief description of the drawings
Fig. 1 is the structural representation of the embodiment of the present invention;
Fig. 2 is Fig. 1 front view;
Fig. 3 is the A-A sectional views shown in Fig. 2.
In figure:1st, reel, 2, fixed bed, 3, placed layer, 4, heat conduction layer, the 41, first aeroge semicircular cylinder, 42, second
Aeroge semicircular cylinder, 5, shell of compression, the 51, first stainless steel semicircular cylinder, the 52, second stainless steel semicircular cylinder, 6, rectangular window, 7, even
Lug, 8, bolt, 9, groove, 10, raised, 11, wing nut.
Embodiment
Embodiment pole piece high vacuum, high temperature moisture content sampler
The present embodiment as shown in Figure 1 to Figure 3, including:
Reel 1, the reel 1 are used to store by dry pole piece, be set with successively from the inside to the outside outside the reel 1 fixed bed 2,
Placed layer 3, heat conduction layer 4, and shell of compression 5.Wherein, the fixed bed 2 is used for the fixed pole piece being accommodated on reel 1, and
Placed layer 3 is used to place detected pole piece sample, and heat conduction layer 4 cooperates with fixed bed 2, makes pole piece sample have and institute
Identical thermal environment inside pole piece is stored, shell of compression 5 then makes pole piece sample have and identical tension force inside stored pole piece.I.e.
By the setting of fixed bed 2, heat conduction layer 4 and shell of compression 5, with the loyalty for making pole piece style with drying being most not easy by dry pole piece
Center portion has identical drying condition, makes the data of pole piece style closer to by dry pole piece.
In order to realize above-mentioned purpose, the reel 1 in the present embodiment is cylindrical shape made of corrugated paper, in the present embodiment
The end of reel 1, which is provided with, is used for the present embodiment in the bolt 8 conveniently picked and placeed in drying oven;And fixed bed 2 is high temperature resistant, vacuum-resistant
The first aerogel layer;Placed layer 3 is then and the pole piece roll that is formed by dry pole piece identical pole piece coiling, the pole piece roll
On offer rectangular window 6 for placing pole piece sample;The heat conduction layer 4 is high temperature resistant, the second aeroge of vacuum-resistant
Layer;The shell of compression 5 is stainless steel sleeve.
The first above-mentioned aerogel layer is integrated cylindrical tube shape structure, and first that the second aerogel layer is that size matches
The cylindrical tube shape structure that the aeroge semicircular cylinder 42 of aeroge semicircular cylinder 41 and second is formed, between described two aeroge semicircular cylinders
It is detachably connected by the first bindiny mechanism.First bindiny mechanism includes the projection on the first aeroge semicircular cylinder 41
10, and on the second aeroge semicircular cylinder 42, with the grooves 9 that match of projection 10, in use, by the first aeroge semicircle
Corresponding to the insertion of projection 10 on cylinder 41 in groove 9, to ensure the fixed effect after installation, the present embodiment is as shown in Figure 1, Figure 2
Two projections 10 and two grooves 9, and length of two projections 10 along the first aeroge semicircular cylinder 41 are respectively provided with shown
Direction is set, and two grooves 9 are then set along the length direction of the second aeroge semicircular cylinder 42.
And the shell of compression in the present embodiment is as shown in Figure 2 and Figure 3, for the first stainless steel semicircular cylinder 51 that size matches with
The cylindrical tube shape structure that second stainless steel semicircular cylinder 52 is formed, pass through the second bindiny mechanism between described two stainless steel semicircular cylinders
It is detachably connected.The second bindiny mechanism in the present embodiment includes being respectively arranged on the first stainless steel semicircular cylinder 51 and the second stainless steel
Engaging lug 7 on the stack shell of semicircular cylinder 52, engaging lug and the second stainless steel semicircular cylinder 52 on the first stainless steel semicircular cylinder 51
On engaging lug 7 be connected by bolt mechanism, the bolt mechanism that the present embodiment is formed with wing nut 11 using bolt will be located at
Engaging lug 7 on two stainless steel semicircular cylinders is fixed on together.
The use principle of the present embodiment is:Before use, fixed bed 2, placed layer 3, pole piece style, heat conduction layer 4, pressure
Layer 5 according to set installation order by it is built-in it is outer install, then dry pole piece will be needed to wind reel on 1, then
It is attached to being wound with by 1 set of the reel of dry pole piece in fixed bed 2, finally whole device is placed into drying oven and dried i.e.
Can.It is qualified if necessary to which whether detection is dried by dry pole piece during drying, without whole device is taken out, and
It is directly to disassemble shell of compression 5 and heat conduction layer 4, takes out pole piece style and carry out water content detection(Due to leading for aeroge
Heating rate is 1/10th of pole piece thermal conductivity, therefore in the drying residing for the pole piece style between fixed bed 2 and heat conduction layer 4
Environment is similar to the dry environment for the pole piece middle part being wound on reel 1, therefore the drying result of pole piece style can be straight
It is reversed should be by the drying effect of dry pole piece)If pole piece style water content detection is qualified, prove to be wound on reel 1
Meet to require by dry pole piece, drying can be stopped;If pole piece style water content detection is unqualified, by the present embodiment
Install, continue drying, untill the water content detection of pole piece style is qualified.
Claims (6)
1. a kind of pole piece high vacuum, high temperature moisture content sampler, it is characterised in that:It includes being used to store by dry pole piece
Reel(1), the reel(1)The outer fixed bed being set with successively from the inside to the outside for fixed stored pole piece(2), for putting
Put the placed layer of detected pole piece sample(3), for making pole piece sample that there is identical with stored pole piece inside thermal environment
Heat conduction layer(4), and make pole piece sample that there is the shell of compression with equal tension inside stored pole piece(5).
2. pole piece high vacuum according to claim 1, high temperature moisture content sampler, it is characterised in that:The reel(1)For
Cylindrical shape made of corrugated paper;Fixed bed(2)For high temperature resistant, the first aerogel layer of vacuum-resistant;The placed layer(3)For with receipts
The pole piece roll that the identical pole piece coiling of pole piece received forms, the rectangular window for placing pole piece sample is offered on the pole piece roll
(6);The heat conduction layer(4)For high temperature resistant, the second aerogel layer of vacuum-resistant;The shell of compression(5)For stainless steel sleeve.
3. pole piece high vacuum according to claim 2, high temperature moisture content sampler, it is characterised in that:First airsetting
Glue-line is integrated cylindrical tube shape structure, and the second aerogel layer is the first aeroge semicircular cylinder that size matches(41)With the second gas
Gel semicircular cylinder(42)The cylindrical tube shape structure of composition, it is removable by the first bindiny mechanism between described two aeroge semicircular cylinders
Unload connection.
4. pole piece high vacuum according to claim 3, high temperature moisture content sampler, it is characterised in that:First connection
Mechanism includes being located at the first aeroge semicircular cylinder(41)On projection(10), and located at the second aeroge semicircular cylinder(42)Upper,
With projection(10)The groove to match(9).
5. pole piece high vacuum, high temperature moisture content sampler according to claim 2-4 any one, it is characterised in that:Institute
State shell of compression(5)The the first stainless steel semicircular cylinder to match for size(51)With the second stainless steel semicircular cylinder(52)The cylinder of composition
Tubular structure, it is detachably connected by the second bindiny mechanism between described two stainless steel semicircular cylinders.
6. pole piece high vacuum according to claim 5, high temperature moisture content sampler, it is characterised in that:Second connection
Mechanism includes being respectively arranged on the first stainless steel semicircular cylinder(51)With the second stainless steel semicircular cylinder(52)Engaging lug on stack shell(7),
The first stainless steel semicircular cylinder(51)On engaging lug(7)With the second stainless steel semicircular cylinder(52)On engaging lug(7)Pass through
Bolt mechanism is connected.
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
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CN201711351428.0A CN107860602B (en) | 2017-12-15 | 2017-12-15 | Pole piece high vacuum, high temperature moisture content sampler |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
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CN201711351428.0A CN107860602B (en) | 2017-12-15 | 2017-12-15 | Pole piece high vacuum, high temperature moisture content sampler |
Publications (2)
Publication Number | Publication Date |
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CN107860602A true CN107860602A (en) | 2018-03-30 |
CN107860602B CN107860602B (en) | 2024-03-22 |
Family
ID=61706805
Family Applications (1)
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CN201711351428.0A Active CN107860602B (en) | 2017-12-15 | 2017-12-15 | Pole piece high vacuum, high temperature moisture content sampler |
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