CN107858590B - A kind of 42CrMo4 wind driven generator principal shaft control method - Google Patents

A kind of 42CrMo4 wind driven generator principal shaft control method Download PDF

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CN107858590B
CN107858590B CN201710975697.8A CN201710975697A CN107858590B CN 107858590 B CN107858590 B CN 107858590B CN 201710975697 A CN201710975697 A CN 201710975697A CN 107858590 B CN107858590 B CN 107858590B
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42crmo4
driven generator
wind driven
control method
principal shaft
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CN107858590A (en
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傅排先
孙宸
刘宏伟
胡小强
王培�
刘航航
李殿中
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Changzhou Lin Hong Special Steel Co Ltd
Institute of Metal Research of CAS
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Changzhou Linhong Special Steel Co ltd
Institute of Metal Research of CAS
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    • CCHEMISTRY; METALLURGY
    • C22METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22CALLOYS
    • C22C38/00Ferrous alloys, e.g. steel alloys
    • C22C38/02Ferrous alloys, e.g. steel alloys containing silicon
    • CCHEMISTRY; METALLURGY
    • C21METALLURGY OF IRON
    • C21DMODIFYING THE PHYSICAL STRUCTURE OF FERROUS METALS; GENERAL DEVICES FOR HEAT TREATMENT OF FERROUS OR NON-FERROUS METALS OR ALLOYS; MAKING METAL MALLEABLE, e.g. BY DECARBURISATION OR TEMPERING
    • C21D1/00General methods or devices for heat treatment, e.g. annealing, hardening, quenching or tempering
    • C21D1/18Hardening; Quenching with or without subsequent tempering
    • CCHEMISTRY; METALLURGY
    • C21METALLURGY OF IRON
    • C21DMODIFYING THE PHYSICAL STRUCTURE OF FERROUS METALS; GENERAL DEVICES FOR HEAT TREATMENT OF FERROUS OR NON-FERROUS METALS OR ALLOYS; MAKING METAL MALLEABLE, e.g. BY DECARBURISATION OR TEMPERING
    • C21D1/00General methods or devices for heat treatment, e.g. annealing, hardening, quenching or tempering
    • C21D1/26Methods of annealing
    • CCHEMISTRY; METALLURGY
    • C21METALLURGY OF IRON
    • C21DMODIFYING THE PHYSICAL STRUCTURE OF FERROUS METALS; GENERAL DEVICES FOR HEAT TREATMENT OF FERROUS OR NON-FERROUS METALS OR ALLOYS; MAKING METAL MALLEABLE, e.g. BY DECARBURISATION OR TEMPERING
    • C21D1/00General methods or devices for heat treatment, e.g. annealing, hardening, quenching or tempering
    • C21D1/26Methods of annealing
    • C21D1/28Normalising
    • CCHEMISTRY; METALLURGY
    • C21METALLURGY OF IRON
    • C21DMODIFYING THE PHYSICAL STRUCTURE OF FERROUS METALS; GENERAL DEVICES FOR HEAT TREATMENT OF FERROUS OR NON-FERROUS METALS OR ALLOYS; MAKING METAL MALLEABLE, e.g. BY DECARBURISATION OR TEMPERING
    • C21D8/00Modifying the physical properties by deformation combined with, or followed by, heat treatment
    • C21D8/06Modifying the physical properties by deformation combined with, or followed by, heat treatment during manufacturing of rods or wires
    • C21D8/065Modifying the physical properties by deformation combined with, or followed by, heat treatment during manufacturing of rods or wires of ferrous alloys
    • CCHEMISTRY; METALLURGY
    • C21METALLURGY OF IRON
    • C21DMODIFYING THE PHYSICAL STRUCTURE OF FERROUS METALS; GENERAL DEVICES FOR HEAT TREATMENT OF FERROUS OR NON-FERROUS METALS OR ALLOYS; MAKING METAL MALLEABLE, e.g. BY DECARBURISATION OR TEMPERING
    • C21D9/00Heat treatment, e.g. annealing, hardening, quenching or tempering, adapted for particular articles; Furnaces therefor
    • C21D9/28Heat treatment, e.g. annealing, hardening, quenching or tempering, adapted for particular articles; Furnaces therefor for plain shafts
    • CCHEMISTRY; METALLURGY
    • C22METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22CALLOYS
    • C22C38/00Ferrous alloys, e.g. steel alloys
    • C22C38/005Ferrous alloys, e.g. steel alloys containing rare earths, i.e. Sc, Y, Lanthanides
    • CCHEMISTRY; METALLURGY
    • C22METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22CALLOYS
    • C22C38/00Ferrous alloys, e.g. steel alloys
    • C22C38/04Ferrous alloys, e.g. steel alloys containing manganese
    • CCHEMISTRY; METALLURGY
    • C22METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22CALLOYS
    • C22C38/00Ferrous alloys, e.g. steel alloys
    • C22C38/06Ferrous alloys, e.g. steel alloys containing aluminium
    • CCHEMISTRY; METALLURGY
    • C22METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22CALLOYS
    • C22C38/00Ferrous alloys, e.g. steel alloys
    • C22C38/18Ferrous alloys, e.g. steel alloys containing chromium
    • C22C38/20Ferrous alloys, e.g. steel alloys containing chromium with copper
    • CCHEMISTRY; METALLURGY
    • C22METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22CALLOYS
    • C22C38/00Ferrous alloys, e.g. steel alloys
    • C22C38/18Ferrous alloys, e.g. steel alloys containing chromium
    • C22C38/22Ferrous alloys, e.g. steel alloys containing chromium with molybdenum or tungsten
    • CCHEMISTRY; METALLURGY
    • C22METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22CALLOYS
    • C22C38/00Ferrous alloys, e.g. steel alloys
    • C22C38/18Ferrous alloys, e.g. steel alloys containing chromium
    • C22C38/24Ferrous alloys, e.g. steel alloys containing chromium with vanadium
    • CCHEMISTRY; METALLURGY
    • C22METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22CALLOYS
    • C22C38/00Ferrous alloys, e.g. steel alloys
    • C22C38/18Ferrous alloys, e.g. steel alloys containing chromium
    • C22C38/40Ferrous alloys, e.g. steel alloys containing chromium with nickel
    • C22C38/42Ferrous alloys, e.g. steel alloys containing chromium with nickel with copper
    • CCHEMISTRY; METALLURGY
    • C22METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22CALLOYS
    • C22C38/00Ferrous alloys, e.g. steel alloys
    • C22C38/18Ferrous alloys, e.g. steel alloys containing chromium
    • C22C38/40Ferrous alloys, e.g. steel alloys containing chromium with nickel
    • C22C38/44Ferrous alloys, e.g. steel alloys containing chromium with nickel with molybdenum or tungsten
    • CCHEMISTRY; METALLURGY
    • C22METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22CALLOYS
    • C22C38/00Ferrous alloys, e.g. steel alloys
    • C22C38/18Ferrous alloys, e.g. steel alloys containing chromium
    • C22C38/40Ferrous alloys, e.g. steel alloys containing chromium with nickel
    • C22C38/46Ferrous alloys, e.g. steel alloys containing chromium with nickel with vanadium

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Abstract

The present invention relates to material composition design and Field of Heat-treatment, more particularly to a kind of high-performance 42CrMo4 wind driven generator principal shaft control method.By weight percentage, the chemical composition ranges of 42CrMo4 wind driven generator principal shaft are as follows: C:0.39~0.42%;Si:0.20~0.30%;Mn:0.70~0.80%;Cr:1.10~1.20%;Mo:0.25~0.30%;Cu :≤0.10%;Al :≤0.05%;P :≤0.012%;S :≤0.008%, surplus Fe.The present invention is added by microalloy, the processing of molten steel sublimate and forging, heat-treated sturcture control, the 42CrMo4 blower fan main shaft of manufacture is finally set to obtain good tough matching degree, performance reaches at subcutaneous 185mm: yield strength (Re) >=525MPa, tensile strength (Rm) >=680MPa, elongation (A) >=16%, -30 DEG C of ballistic work (AKv) >=27J.

Description

A kind of 42CrMo4 wind driven generator principal shaft control method
Technical field
The present invention relates to material composition design and Field of Heat-treatment, send out more particularly to a kind of high-performance 42CrMo4 wind-force Electric machine main shaft control method.
Background technique
Wind driven generator principal shaft is the key components and parts for connecting blade and generator, and working environment is complicated, is needed good Obdurability matching.In recent years, blower was also increased accordingly in enlarged development trend, the specification of main shaft, and organizational controls difficulty increases Add, along with mechanical performance index requires higher and higher, performance requirement at subcutaneous 185mm are as follows: yield strength >=525MPa, tension Intensity >=680Mpa, -30 DEG C of Impact energy Ak v >=27J, existing manufacturing process can not meet technical requirements.
Summary of the invention
The purpose of the present invention is to provide a kind of high-performance 42CrMo4 wind driven generator principal shaft control methods, make 42CrMo4 Blower fan main shaft can have good tough matching degree, be wanted with meeting use of the Wind turbines in low temperature complex work environment It asks.
The technical scheme is that
A kind of 42CrMo4 wind driven generator principal shaft control method, which is characterized in that under basic 42CrMo4 member condition Carry out microalloy adjustment;In original smelting pouring technology: electric furnace+LF+VD+ carries out low being mingled with control under conditions of molding;Using Forging+annealing+normalizing guarantees that grain size is greater than 7 grades;Guarantee that matrix meets product using alternately water quenching+tempering process Can: yield strength Re >=525MPa, tensile strength Rm >=680MPa, elongation A >=16%, -30 DEG C of ballistic work AKv >=27J.
The 42CrMo4 wind driven generator principal shaft control method, 42CrMo4 wind driven generator principal shaft material composition and its Weight percentage is C:0.39~0.42%;Si:0.20~0.30%;Mn:0.70~0.80%;Cr:1.10~ 1.20%;Mo:0.25~0.30%;Cu :≤0.10%;Al :≤0.05%;P :≤0.012%;S :≤0.008%, surplus is Fe。
The 42CrMo4 wind driven generator principal shaft control method, the 42CrMo4 wind driven generator principal shaft material of optimization at In point, microalloy element Ni:0.35~0.60% is added;V:0.1~0.3%;RE≤0.025%;Wherein, guarantee Ni+V > 0.55%.
The 42CrMo4 wind driven generator principal shaft control method, in original smelting pouring technology: electric furnace+LF+VD+ mould Carried out under conditions of casting it is low be mingled with control, in conjunction with slag steel balance control and pass through after LF refining add rare earth treatment realize; Selected refining slag system is aluminium oxide >=20wt%, silica≤12wt%, and rare earth adding quantity≤0.025wt% presss from both sides A, C Sundries Type Control≤0.5 grade, by Control and Inclusion Removal≤1 grade B, D.
The 42CrMo4 wind driven generator principal shaft control method guarantees that grain size is greater than 7 using forging+annealing+normalizing Grade, in which: upset ratio is greater than 5, keeps the temperature 20~25 hours at 800~900 DEG C after main shaft is forged, then carries out pearlite and moves back Fire keeps the temperature 20~30 hours at 700~750 DEG C, improves even grain size, eliminates mixed crystal;Later, at using double normalizing Reason, 800~900 DEG C of double normalizing temperature, soaking time 20~25 hours.
The 42CrMo4 wind driven generator principal shaft control method guarantees matrix group using alternately water quenching+tempering process It knits and meets properties of product, in which: in quenching technical, 840~890 DEG C of hardening heat, soaking time 20~25 hours, using friendship For water quenching mode, and the entire hardening process cooling rate of main shaft is controlled using contact whole process real-time cooling speed control method System;In tempering process, 645~665 DEG C of tempering temperature, soaking time 25~30 hours.
The 42CrMo4 wind driven generator principal shaft control method, in quenching technical, 42CrMo4 wind driven generator principal Axis enters coolant-temperature gage control at 840~900 DEG C.
The each Design of Chemical Composition thought and synergistic effect of high-performance 42CrMo4 wind driven generator principal shaft material of the present invention It is: is deployed by constituent contents such as C, Cr, Mn, Ni, Mo, understands the relationship between constituent content and material harden ability, intensity;It is logical The allotment of the constituent contents such as C, Ni, V is crossed, the relationship between element and toughness of material is understood;Pass through the allotment of microelement V and rare earth Have the function that refine crystal grain, the control of deoxidation is realized by the control of Si, Al content.
The heat treatment mechanism of high-performance 42CrMo4 wind driven generator principal shaft material of the present invention is: utilizing the lamella of pearlite Structure provides forming core point for austenite grain, improves number of nuclei, refines even grained.
The invention has the advantages and beneficial effects that:
1, the present invention develops a kind of high property by spindle material optimizing components and choosing special thermal treatment technique study Energy 42CrMo4 blower fan main shaft material, can satisfy requirement of the Wind turbines in low temperature complex work environment.Its performance is enough Meet: yield strength >=525MPa, tensile strength >=680MPa, elongation percentage >=16%, -30 DEG C of ballistic work (AKv) >=27J.
2, the steel grade of the invention performance after pearlite annealing, modifier treatment is stablized, and can be used in great key components and parts On.
3, heat treatment method of the present invention can be widely applied to the heat treatment of 42CrMo4 wind driven generator principal shaft product.
Specific embodiment
In the specific implementation process, the smelting process of high-performance 42CrMo4 wind driven generator principal shaft material of the present invention, in original Have carried out under the conditions of smelting pouring technology (electric furnace+LF+VD+ molding) it is low be mingled with control, mainly in combination with slag steel balance control and It is realized by adding rare earth treatment after LF refining.Selected refining slag system be aluminium oxide >=20%, silica≤12%, Rare earth adding quantity≤0.025%, effect can be effectively by A, C field trash Type Control≤0.5 grade, by B, D Control and Inclusion Removal ≤ 1 grade;
In the following, by embodiment, invention is further described in detail.
Embodiment 1
In the present embodiment, the cast steel ingredient of high-strength high-toughness and low-temperature military service cast steel material is as follows:
Element Content (wt%)
C 0.41
Si 0.25
Mn 0.73
P 0.01
S 0.001
Ni 0.53
Cr 1.12
Mo 0.26
V 0.2
Al 0.017
Cu 0.04
RE 0.016
Fe Surplus
Heat treatment uses following steps: being kept the temperature after 1. main shaft is forged at 860 DEG C, soaking time is thick by 1h/25mm Selected, later in 730 DEG C of progress pearlite annealings, soaking time is selected by 1h/25mm thickness.2. then main shaft carries out twice just Fire processing, normalizing temperature is 860 DEG C, and soaking time is selected by 1h/25mm thickness, is then come out of the stove air-cooled to 300 DEG C or less.3. so Main shaft is quenched afterwards, using alternately water quenching mode, and using contact whole process real-time cooling speed control method to master The entire hardening process cooling rate of axis is controlled, and it is 850 DEG C that main shaft, which enters coolant-temperature gage, and soaking time presses 1h/25mm.4. tempering temperature is selected 650 DEG C are selected as, soaking time presses 1h/25mm, comes out of the stove after tempering and is air-cooled to room temperature.
After heat treatment, material property is as follows:
Yield strength (Re) is 661MPa, and tensile strength (Rm) is 822MPa, and elongation (A) is 19%, -30 DEG C of ballistic works It (AKv) is 33J.
Embodiment 2
In the present embodiment, the cast steel ingredient of high-strength high-toughness and low-temperature military service cast steel material is as follows:
Element Content (wt%)
C 0.41
Si 0.27
Mn 0.79
P 0.011
S 0.006
Ni 0.46
Cr 1.10
Mo 0.27
V 0.25
Al 0.01
Cu 0.08
RE 0.011
Fe Surplus
Heat treatment uses following steps: being kept the temperature after 1. main shaft is forged at 860 DEG C, soaking time is thick by 1h/25mm Selected, later in 750 DEG C of progress pearlite annealings, soaking time is selected by 1h/25mm thickness.2. then main shaft carries out twice just Fire processing, normalizing temperature is 880 DEG C, and soaking time is selected by 1h/25mm thickness, is then come out of the stove air-cooled to 300 DEG C or less.3. so Main shaft is quenched afterwards, using alternately water quenching mode, and using contact whole process real-time cooling speed control method to master The entire hardening process cooling rate of axis is controlled, and it is 869 DEG C that main shaft, which enters coolant-temperature gage, and soaking time presses 1h/25mm.4. tempering temperature is selected 660 DEG C are selected as, soaking time presses 1h/25mm, comes out of the stove after tempering and is air-cooled to room temperature.
After heat treatment, material property is as follows:
Yield strength (Re) is 689MPa, and tensile strength (Rm) is 860MPa, and elongation (A) is 18%, -30 DEG C of ballistic works It (AKv) is 30J.
Embodiment 3
In the present embodiment, the cast steel ingredient of high-strength high-toughness and low-temperature military service cast steel material is as follows:
Element Content (wt%)
C 0.42
Si 0.22
Mn 0.75
P 0.008
S 0.003
Ni 0.57
Cr 1.13
Mo 0.25
V 0.18
Al 0.022
Cu 0.10
RE 0.020
Fe Surplus
Heat treatment uses following steps: being kept the temperature after 1. main shaft is forged at 860 DEG C, soaking time is thick by 1h/25mm Selected, later in 710 DEG C of progress pearlite annealings, soaking time is selected by 1h/25mm thickness.2. then main shaft carries out twice just Fire processing, normalizing temperature is 890 DEG C, and soaking time is selected by 1h/25mm thickness, is then come out of the stove air-cooled to 300 DEG C or less.3. so Main shaft is quenched afterwards, using alternately water quenching mode, and using contact whole process real-time cooling speed control method to master The entire hardening process cooling rate of axis is controlled, and it is 876 DEG C that main shaft, which enters coolant-temperature gage, and soaking time presses 1h/25mm.4. tempering temperature is selected 645 DEG C are selected as, soaking time presses 1h/25mm, comes out of the stove after tempering and is air-cooled to room temperature.
After heat treatment, material property is as follows:
Yield strength (Re) is 641MPa, and tensile strength (Rm) is 828MPa, and elongation (A) is 19%, -30 DEG C of ballistic works It (AKv) is 31J.
Embodiment the result shows that, the 42CrMo4 wind driven generator principal shaft material involved in the present invention arrived after heat treatment, can To reach technical requirements, requirement of the Wind turbines in low temperature complex work environment can satisfy.

Claims (6)

1. a kind of 42CrMo4 wind driven generator principal shaft control method, which is characterized in that under basic 42CrMo4 member condition into The adjustment of row microalloy;In original smelting pouring technology: electric furnace+LF+VD+ carries out low being mingled with control under conditions of molding;Using forging Make+anneal+normalizing guarantee grain size be greater than 7 grades;Guarantee that matrix meets product using alternately water quenching+tempering process Can: yield strength Re >=525MPa, tensile strength Rm >=680MPa, elongation A >=16%, -30 DEG C of ballistic work AKv >=27J;
It is described to guarantee that grain size is greater than 7 grades using forging+annealing+normalizing, in which: upset ratio is greater than 5, after main shaft is forged 800~900 DEG C keep the temperature 20~25 hours, then carry out pearlite annealing, keep the temperature 20~30 hours at 700~750 DEG C, improve Even grain size eliminates mixed crystal;Later, it is handled using double normalizing, 800~900 DEG C of double normalizing temperature, soaking time 20~25 hours.
2. 42CrMo4 wind driven generator principal shaft control method according to claim 1, which is characterized in that 42CrMo4 wind Power generator spindle material ingredient and its weight percentage are C:0.39~0.42%;Si:0.20~0.30%;Mn:0.70~ 0.80%;Cr:1.10~1.20%;Mo:0.25~0.30%;Cu:≤0.10%;Al:≤0.05%; P:≤0.012%;S:≤ 0.008%, surplus Fe.
3. 42CrMo4 wind driven generator principal shaft control method according to claim 1, which is characterized in that 42CrMo4 wind Power generator spindle material ingredient and its weight percentage are C:0.39~0.42%;Si:0.20~0.30%;Mn:0.70~ 0.80%;Cr:1.10~1.20%;Mo:0.25~0.30%;Cu:≤0.10%;Al:≤0.05%; P:≤0.012%;S:≤ 0.008%, add microalloy element Ni:0.35~0.60%;V:0.1~0.3%;RE≤0.025%;Surplus is Fe, wherein is guaranteed Ni+V > 0.55%.
4. 42CrMo4 wind driven generator principal shaft control method according to claim 1, which is characterized in that in original smelting Refining pouring technology: carried out under conditions of electric furnace+LF+VD+ molding it is low be mingled with control, balance control in conjunction with slag steel and by smart in LF Addition rare earth treatment is realized after refining;Selected refining slag system is aluminium oxide >=20wt%, silica≤12wt%, and rare earth is added Amount≤0.025wt%, by A, C field trash Type Control≤0.5 grade, by Control and Inclusion Removal≤1 grade B, D.
5. 42CrMo4 wind driven generator principal shaft control method according to claim 1, which is characterized in that using alternating Water quenching+tempering process guarantees that matrix meets properties of product, in which: in quenching technical, 840~890 DEG C of hardening heat, Soaking time 20~25 hours, using alternately water quenching mode, and using contact whole process real-time cooling speed control method to master The entire hardening process cooling rate of axis is controlled;In tempering process, 645~665 DEG C of tempering temperature, soaking time 25~30 is small When.
6. 42CrMo4 wind driven generator principal shaft control method according to claim 5, which is characterized in that in quenching technical In, 42CrMo4 wind driven generator principal shaft enters coolant-temperature gage control at 840~900 DEG C.
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CN109536691B (en) * 2018-11-21 2020-12-29 东北大学无锡研究院 Preparation method of low-temperature impact resistant CrMo alloy steel forged circle
CN109536833A (en) * 2018-12-05 2019-03-29 南阳汉冶特钢有限公司 A kind of high duty alloy tool steel 42CrMo4 hardened and tempered steel plate and its production method
CN110157867B (en) * 2019-04-29 2020-09-18 中国科学院金属研究所 Control method for white abnormal structure in large-size CrMo steel member
CN110396648B (en) * 2019-06-29 2021-04-09 江阴兴澄特种钢铁有限公司 Super-thick alloy die steel plate produced by continuous casting billet and manufacturing method thereof
CN111299481B (en) * 2019-11-19 2021-12-07 湖北坚丰科技股份有限公司 Closed forging and pressing forming process for gear shaft of new energy automobile engine
CN111809112A (en) * 2020-06-19 2020-10-23 张家港海锅新能源装备股份有限公司 Production method of S42Cr1S forging for piston rod of marine diesel engine

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Publication number Priority date Publication date Assignee Title
CN106435405A (en) * 2015-08-06 2017-02-22 江苏金源锻造股份有限公司 42CrMo4 wind power main shaft after-forging heat treatment method of low-wind-speed wind turbine generator
CN106702099A (en) * 2017-01-18 2017-05-24 抚顺特殊钢股份有限公司 Large-size 42 CrMo4 hardened and tempered steel manufacturing process for wind power gearbox outer main shaft

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106435405A (en) * 2015-08-06 2017-02-22 江苏金源锻造股份有限公司 42CrMo4 wind power main shaft after-forging heat treatment method of low-wind-speed wind turbine generator
CN106702099A (en) * 2017-01-18 2017-05-24 抚顺特殊钢股份有限公司 Large-size 42 CrMo4 hardened and tempered steel manufacturing process for wind power gearbox outer main shaft

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