CN107828583A - A kind of method that cold sterilization produces muddy type Fang County yellow rice wine - Google Patents

A kind of method that cold sterilization produces muddy type Fang County yellow rice wine Download PDF

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Publication number
CN107828583A
CN107828583A CN201711078929.6A CN201711078929A CN107828583A CN 107828583 A CN107828583 A CN 107828583A CN 201711078929 A CN201711078929 A CN 201711078929A CN 107828583 A CN107828583 A CN 107828583A
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rice wine
yellow rice
fang county
concentrate
cold sterilization
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CN201711078929.6A
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Inventor
万端极
卢扬成
朱正军
谢逾群
徐斌
张爱帝
曹敬华
吴正奇
李猷
余攀
刘萱
刘一萱
蒋园园
叶文祥
王慧娟
黄梦萍
蒋心越
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Fangxian Yellow Wine And Fermentation Industry Bureau
Hubei University of Technology
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Fangxian Yellow Wine And Fermentation Industry Bureau
Hubei University of Technology
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Application filed by Fangxian Yellow Wine And Fermentation Industry Bureau, Hubei University of Technology filed Critical Fangxian Yellow Wine And Fermentation Industry Bureau
Priority to CN201711078929.6A priority Critical patent/CN107828583A/en
Publication of CN107828583A publication Critical patent/CN107828583A/en
Pending legal-status Critical Current

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    • CCHEMISTRY; METALLURGY
    • C12BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
    • C12GWINE; PREPARATION THEREOF; ALCOHOLIC BEVERAGES; PREPARATION OF ALCOHOLIC BEVERAGES NOT PROVIDED FOR IN SUBCLASSES C12C OR C12H
    • C12G3/00Preparation of other alcoholic beverages
    • C12G3/02Preparation of other alcoholic beverages by fermentation
    • CCHEMISTRY; METALLURGY
    • C12BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
    • C12HPASTEURISATION, STERILISATION, PRESERVATION, PURIFICATION, CLARIFICATION OR AGEING OF ALCOHOLIC BEVERAGES; METHODS FOR ALTERING THE ALCOHOL CONTENT OF FERMENTED SOLUTIONS OR ALCOHOLIC BEVERAGES
    • C12H1/00Pasteurisation, sterilisation, preservation, purification, clarification, or ageing of alcoholic beverages
    • C12H1/02Pasteurisation, sterilisation, preservation, purification, clarification, or ageing of alcoholic beverages combined with removal of precipitate or added materials, e.g. adsorption material
    • C12H1/06Precipitation by physical means, e.g. by irradiation, vibrations
    • C12H1/063Separation by filtration

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Health & Medical Sciences (AREA)
  • General Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Biochemistry (AREA)
  • Bioinformatics & Cheminformatics (AREA)
  • General Engineering & Computer Science (AREA)
  • Genetics & Genomics (AREA)
  • Wood Science & Technology (AREA)
  • Zoology (AREA)
  • Food Science & Technology (AREA)
  • Toxicology (AREA)
  • Distillation Of Fermentation Liquor, Processing Of Alcohols, Vinegar And Beer (AREA)

Abstract

The present invention relates to a kind of method that cold sterilization produces muddy type Fang County yellow rice wine, following steps are passed sequentially through:Fang County's yellow wine fermentation process is completed according to traditional fermentation technique;Put fermenting mixture into centrifuge separation, obtain zymotic fluid;Zymotic fluid is separated with micro-filtration film device, respectively obtains clear liquid and concentrate;Concentrate is passed sequentially through into colloid mill, homogenizer, instantaneous sterilizing processing;It is then mixed into clear liquid, sterile filling, that is, obtains muddy type Fang County yellow rice wine.This have the advantage that:Final products are in pale yellow cloudy shape, possess the external appearance characteristic of authentic Fang County's yellow rice wine script;Because using colloid mill and homogenization, product is in homogeneous, stable milkiness state and is not easy to be layered;Because using cold sterilization mode, all kinds of compositions in product are undenatured, and its unique aroma and glycol, long mouthfeel and traditional Fang County's yellow rice wine are completely the same;The shelf-life of product is greatly improved, is advantageous to the selling market of a wide range of extension Fang County yellow rice wine.

Description

A kind of method that cold sterilization produces muddy type Fang County yellow rice wine
Technical field
The present invention relates to a kind of processing technique field of yellow rice wine, and muddy type yellow rice wine is produced more particularly to a kind of cold sterilization Method.
Background technology
Yellow rice wine is one of three most ancient wine kinds in the world, and yellow rice wine is mainly brewageed using rice, milled glutinous broomcorn millet as fermenting raw materials, one As alcohol content be 8%vol~20%vol, belong to minuent, high nutrition, the wine kind of health, be especially suitable for current people due to Living standard improve and to the requirement of alcoholic drink quality.
The developing history of yellow rice wine had more than 2500 years, the most well-known with shao-hsing rice wine, knew to the greatest extent all over the world, but deep in motherland Place, there is a kind of " Fang County's yellow rice wine " is also more early than shao-hsing rice wine to occur 400 years, abound with do not wane so far.
Fang County's yellow rice wine is a kind of very high alcoholic strength low beverage of nutritive value, and scientific research result shows, in Fang County's yellow rice wine Containing abundant protein and several amino acids needed by human, the protein in yellow rice wine is degraded by microbial enzyme, easily Be absorbed by the body utilization.Also containing abundant inorganic salts and trace element in Fang County's yellow rice wine, the inorganic salts detected just have 15 As many as kind, including a variety of macroelements such as calcium, magnesium, potassium, phosphorus and iron, copper, zinc, selenium and other trace elements, contain in Fang County's yellow rice wine Selenium is higher than red wine about 12 times, higher than white wine about 20 times, and safely and effectively, the selenium that can effectively help human body supplement to lack Element.
Fang County's yellow rice wine taste is fabulous, sweet and dilitious, one dense glutinous rice fragrance, great temptation.Fang County's yellow rice wine is unique Part is it brewage with extremely strong regionality, i.e., can only use the Chinese yeast of Fang County, the glutinous rice of Fang County, the stream or ground of Fang County Lower water, the precious good merchantable brand of uniqueness could be brewed out.Fang County's yellow rice wine it is warm-natured and, it is vinosity glycol, long, have a kind of special fragrance, It is fresh and sweet tasty, head cannot not be drunk superfluously, beauty treatment of stimulating the menstrual flow, foster spleen helps liver, relaxing tendons and activating collaterals, refreshes oneself, keeps out the cold, improving a poor appetite, body-building, prolonging The effect of year lengthens one's life.
Fang County is the township of yellow rice wine, almost every household can brewing yellow wine, except now several brewing yellow rice wines for slightly having a scale Outside factory, also big and small unnumbered all kinds of tunners.
The main output mode of Fang County's yellow rice wine is still to be produced according to traditional brewage process at present, simple filling rear direct Fermentation Normal juice, i.e. Swim juice are drunk, product is in pale yellow cloudy shape, is not added with water when drinking, mouthfeel glycol, long, is Fang County and week Genuine authentic Fang County's yellow rice wine that the producers and consumers on side are approved.It is original protein in yellow rice wine, amino acid, micro- Secondary element is all retained, and is had high nutritive value, is loved by consumers.But due to not taking inactivation approach, production Product continue to ferment after filling bottle, as environment temperature is higher or storage time is longer, can cause the rotten even bottle explosion of product, goods The frame phase is extremely short, and the usual shelf-life at most also only has several months or six months, and not easy to store and transport, market coverage region is narrow and small, The serious selling market scope for limiting Fang County's yellow rice wine, the mainly producer oneself are drunk or at source can only sold on periphery. If taking integral high-temperature inactivation approach, the active material in Fang County's yellow rice wine can be caused to be denatured again, lost former in Fang County's yellow rice wine Some nutritional ingredients, change its unique taste and flavor.
Also there is the producer to employ some new techniques now, i.e., after the completion of being fermented according to traditional brewage process, clarification Filtering, filling seal up for safekeeping.A sweety scent assails the nostrils behind Kaifeng, limpid such as water, but taste is flat, normally referred to as blue or green wine, there is long quality guarantee period, Convenience in transport, storage, but be difficult to obtain accepting for the deep Fang County yellow rice wine consumer influenceed by traditional concept over a long time.
In order that its traditional genuineness can be kept by obtaining Fang County's yellow rice wine, while can also there are longer Storage period and shelf Phase, to extend Fang County's yellow rice wine selling market on a large scale, wider consumer groups are obtained, the present invention provides a kind of cold sterilization life The method for producing muddy type Fang County yellow rice wine.
The content of the invention
It is an object of the invention to provide a kind of method that cold sterilization produces muddy type Fang County yellow rice wine, made from the inventive method most Finished product is in pale yellow cloudy shape, possesses the external appearance characteristic of authentic Fang County's yellow rice wine script;Because using colloid mill and homogenization, Product is in homogeneous, stable milkiness state and is not easy to be layered;Because using cold sterilization mode, all kinds of compositions in product are unchanged Property, its unique aroma and glycol, long mouthfeel and traditional Fang County's yellow rice wine are completely the same;Guaranteeing the quality for product is greatly improved Phase, be advantageous to the selling market of a wide range of extension Fang County yellow rice wine.
The present invention is realized using following technical scheme:
A kind of method that cold sterilization produces muddy type Fang County yellow rice wine, passes sequentially through following steps:
(1) Fang County's yellow wine fermentation process is completed according to traditional brewage process;
(2) put the fermenting mixture of step (1) into centrifuge separation, obtain zymotic fluid;
(3) the isolated zymotic fluid of centrifuge is separated using micro-filtration film device, respectively obtains clear liquid and concentrate, its Middle clear liquid aseptically preserves, and microfiltration membranes select the inorganic membrane element or organic film for passing through that aperture is 0.05~0.2 micron Element;
(4) concentrate that will be enriched in macromolecular substances passes sequentially through colloid mill and homogenizer is handled, and condition of work is: The gap of colloid mill is adjusted to 0.2~0.5mm, and the pressure of homogenizer is adjusted to 20~30mPa;
(5) concentrate after above-mentioned processing is put the sterilizing of into instantaneous sterilizing equipment, condition of work is:Sterilising temp 125~ 135 DEG C, sterilization time 15~25 seconds;
(6) it is stored in after the concentrate after sterilizing being mixed into film device separation in the clear liquid in gnotobasis, in sterile bar It is filling under part, that is, obtain muddy type Fang County yellow rice wine.
This have the advantage that:It is in pale yellow cloudy shape to finally give product, possesses authentic Fang County's yellow rice wine script External appearance characteristic;Because using colloid mill and homogenization, product is in homogeneous, stable milkiness state and is not easy to be layered;Using cold The mode of sterilization, make all kinds of compositions in yellow rice wine product undenatured, its unique aroma and glycol, long mouthfeel and tradition Fang County's yellow rice wine is completely the same;The advantages of present invention is the most prominent is after being separated by film device, and concentrate is carried out at colloid mill Reason, homogenization, instantaneous sterilizing, clear liquid sterile filling is then mixed into, can inactivate microorganism and not lose its substantially original Nutritional ingredient, stability and the shelf-life of product is greatly improved, under normal good environmental condition the shelf-life can reach 2 ~3 years, it is suitable for the shelf display of long-distance transport and long period, is advantageous to the sale city of a wide range of extension Fang County yellow rice wine .
Embodiment
With reference to embodiment, the present invention will be described in detail:
Embodiment 1:
A kind of method that cold sterilization produces muddy type Fang County yellow rice wine, passes sequentially through following steps:
(1) Fang County's yellow wine fermentation process is completed according to traditional brewage process;
(2) material for taking 100kg to ferment to obtain puts centrifuge separation into, obtains zymotic fluid 58kg;
(3) by the isolated zymotic fluid of the centrifuge micro-filtration being equipped with by aperture for 0.05 micron of inorganic membrane element Film device separates, and respectively obtains clear liquid 50kg and concentrate 8kg, clear liquid is stored in into gnotobasis;
(4) concentrate is subjected to milling treatment of colloid and homogenization successively, the gap of colloid mill is adjusted to 0.2mm, homogeneous The pressure of machine is adjusted to 20mPa;
(5) concentrate after above-mentioned processing is entered into the sterilizing of instantaneous sterilizing equipment, 125 DEG C of sterilising temp, sterilization time 25 seconds Clock;
(6) it is stored in after the concentrate after sterilizing being mixed into film device separation in the clear liquid in gnotobasis, in sterile bar It is filling under part, you can to obtain muddy type Fang County yellow rice wine 58kg.
Embodiment 2:
A kind of method that cold sterilization produces muddy type Fang County yellow rice wine, passes sequentially through following steps realization:
(1) Fang County's yellow wine fermentation process is completed according to traditional brewage process;
(2) material for taking 100kg to ferment to obtain puts centrifuge separation into, obtains zymotic fluid 58kg;
(3) by the isolated zymotic fluid of the centrifuge micro-filtration being equipped with by aperture for 0.2 micron of organic membrane component Film device separates, and respectively obtains clear liquid 48kg and concentrate 10kg, clear liquid is stored in into gnotobasis;
(4) concentrate is subjected to milling treatment of colloid and homogenization successively, the gap of colloid mill is adjusted to 0.5mm, homogeneous The pressure of machine is adjusted to 30mPa;
(5) concentrate after above-mentioned processing is entered into the sterilizing of instantaneous sterilizing equipment, 135 DEG C of sterilising temp, sterilization time 15 seconds Clock;
(6) it is stored in after the concentrate after sterilizing being mixed into film device separation in the clear liquid in gnotobasis, in sterile bar It is filling under part, you can to obtain muddy type Fang County yellow rice wine 58kg.
Embodiment 3:
A kind of method that cold sterilization produces muddy type Fang County yellow rice wine, passes sequentially through following steps realization:
(1) Fang County's yellow wine fermentation process is completed according to traditional brewage process;
(2) material for taking 100kg to ferment to obtain puts centrifuge separation into, obtains zymotic fluid 58kg;
(3) by the isolated zymotic fluid of the centrifuge micro-filtration being equipped with by aperture for 0.1 micron of organic membrane component Film device separates, and respectively obtains clear liquid 49kg and concentrate 9kg, clear liquid is stored in into gnotobasis;
(4) concentrate is subjected to milling treatment of colloid and homogenization successively, the gap of colloid mill is adjusted to 0.3mm, homogeneous The pressure of machine is adjusted to 25mPa;
(5) concentrate after above-mentioned processing is entered into the sterilizing of instantaneous sterilizing equipment, 130 DEG C of sterilising temp, sterilization time 20 seconds Clock;
(6) it is stored in after the concentrate after sterilizing being mixed into film device separation in the clear liquid in gnotobasis, in sterile bar It is filling under part, you can to obtain muddy type Fang County yellow rice wine 58kg.
Above three embodiment outward appearance, mouthfeel and holding time are made into following table
Outward appearance Mouthfeel Holding time
Embodiment 1 In pale yellow cloudy shape It is glycol, long 3 years
Embodiment 2 In pale yellow cloudy shape It is glycol, long 2 years
Embodiment 3 In pale yellow cloudy shape It is glycol, long 2.5 year
The nutritional ingredient of yellow rice wine also retains original protein, amino acid, trace element in three embodiments of the present invention.

Claims (4)

1. a kind of method that cold sterilization produces muddy type Fang County yellow rice wine, it is characterised in that pass sequentially through following steps:
(1) Fang County's yellow wine fermentation process is completed according to traditional brewage process;
(2) put the fermenting mixture of step (1) into centrifuge separation, obtain zymotic fluid;
(3) the isolated zymotic fluid of centrifuge is separated using micro-filtration film device, clear liquid and concentrate is respectively obtained, wherein clearly Liquid aseptically preserves;
(4) concentrate that will be enriched in macromolecular substances passes sequentially through colloid mill and homogenizer is handled;
(5) concentrate after above-mentioned processing is put the sterilizing of into instantaneous sterilizing equipment;
(6) it is stored in after the concentrate after sterilizing being mixed into film device separation in the clear liquid in gnotobasis, aseptically It is filling, that is, obtain muddy type Fang County yellow rice wine.
2. the method that a kind of cold sterilization according to claim 1 produces muddy type Fang County yellow rice wine, it is characterised in that:The step Suddenly microfiltration membranes select inorganic membrane element or the organic membrane component by the way that aperture is 0.05~0.2 micron in (3).
3. the method that a kind of cold sterilization according to claim 1 produces muddy type Fang County yellow rice wine, it is characterised in that:The step Suddenly the gap of colloid mill is adjusted to 0.2~0.5mm in (4), and the pressure of homogenizer is adjusted to 20~30mPa.
4. the method that a kind of cold sterilization according to claim 1 produces muddy type Fang County yellow rice wine, it is characterised in that:The step Suddenly the condition of work of instantaneous sterilizing is in (5):125~135 DEG C of sterilising temp, sterilization time 15~25 seconds.
CN201711078929.6A 2017-11-06 2017-11-06 A kind of method that cold sterilization produces muddy type Fang County yellow rice wine Pending CN107828583A (en)

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CN201711078929.6A CN107828583A (en) 2017-11-06 2017-11-06 A kind of method that cold sterilization produces muddy type Fang County yellow rice wine

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Application Number Priority Date Filing Date Title
CN201711078929.6A CN107828583A (en) 2017-11-06 2017-11-06 A kind of method that cold sterilization produces muddy type Fang County yellow rice wine

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