CN107824155A - A kind of zeolite molecular sieve dynamic, static dual-purpose crystallization device - Google Patents
A kind of zeolite molecular sieve dynamic, static dual-purpose crystallization device Download PDFInfo
- Publication number
- CN107824155A CN107824155A CN201711290936.2A CN201711290936A CN107824155A CN 107824155 A CN107824155 A CN 107824155A CN 201711290936 A CN201711290936 A CN 201711290936A CN 107824155 A CN107824155 A CN 107824155A
- Authority
- CN
- China
- Prior art keywords
- permanent magnet
- reactor
- electrical heating
- reaction vessel
- molecular sieve
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/28—Moving reactors, e.g. rotary drums
- B01J19/285—Shaking or vibrating reactors; reactions under the influence of low-frequency vibrations or pulsations
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/0006—Controlling or regulating processes
- B01J19/0013—Controlling the temperature of the process
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/0053—Details of the reactor
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/24—Stationary reactors without moving elements inside
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B39/00—Compounds having molecular sieve and base-exchange properties, e.g. crystalline zeolites; Their preparation; After-treatment, e.g. ion-exchange or dealumination
- C01B39/02—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof; Direct preparation thereof; Preparation thereof starting from a reaction mixture containing a crystalline zeolite of another type, or from preformed reactants; After-treatment thereof
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/00049—Controlling or regulating processes
- B01J2219/00051—Controlling the temperature
- B01J2219/00132—Controlling the temperature using electric heating or cooling elements
- B01J2219/00135—Electric resistance heaters
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Life Sciences & Earth Sciences (AREA)
- General Life Sciences & Earth Sciences (AREA)
- Geology (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Inorganic Chemistry (AREA)
- Silicates, Zeolites, And Molecular Sieves (AREA)
- Physical Or Chemical Processes And Apparatus (AREA)
Abstract
The present invention relates to equipment of chemical industry technical field, specially a kind of zeolite molecular sieve dynamic, static dual-purpose crystallization device, including electrical heating sleeve；Electric heating cover is provided with electrical heating sleeve, synthesis reaction vessel is provided with electric heating cover, synthesis reaction vessel upper and lower ends are respectively arranged with reactor end cap and reactor base, one side permanent magnet is fixedly installed above reactor end cap, two-sided permanent magnet is provided with above one side permanent magnet, two-sided permanent magnet is arranged on one group of magnet trip shaft, magnet trip shaft one end is fixedly connected through electrical heating sleeve with one group of turn drive motor main shaft, back-moving spring is provided with below reactor base, the back-moving spring other end is fixedly connected with reactor base；The present invention ensures that device can realize dynamic, static two kinds of reactivenesses by setting one side permanent magnet and one group of two-sided permanent magnet driven by motor to drive the motion of reactor and stopping above synthesis reaction vessel.
Description
Technical field
The present invention relates to equipment of chemical industry technical field, more particularly to a kind of zeolite molecular sieve dynamic, static dual-purpose crystalline substance
Change reactor.
Background technology
Zeolite molecular sieve is the hydrate of crystalline alumino metal salt, is unique absorption with shape selective, catalysis
Material, not only can be by selective catalysis to reduce the generation of byproduct, improve the utilization rate of reaction raw materials, and can pass through
The means such as structural adjustment, loaded modified form the function catalysis material needed for production, thus it is more and more it is studied use it is all
Multi-field, use is also more and more extensive.At present, the synthesis mode of zeolite molecular sieve is mainly divided to two classes, be static monitor respectively with
Dynamic synthesizes.Correspondingly, the device of static monitor is mainly reactor and baking oven, by synthesis materials such as silicon source, silicon source, templates
It is added in synthesis reactor, then will be placed into reactor in baking oven.Whole synthetic reaction process remains static；It is dynamic
State synthetic method is mainly that the synthesis reactor with heater is furnished with agitating device again.Generally used in both of which experiment
Method, different synthesis modes, also have an impact to zeolite molecular sieve product, during routine experimentation, if investigated static and dynamic
Influence of the state synthetic method to zeolite molecular sieve, often to prepare two sets of synthesizers, add equipment cost, it is more complicated.
The content of the invention
Instant invention overcomes above-mentioned the deficiencies in the prior art, there is provided a kind of zeolite molecular sieve dynamic, static dual-purpose crystallization
Reactor.The present invention by set above synthesis reaction vessel one side permanent magnet and one group by motor drive it is two-sided forever
Magnet drives the motion of reactor and stopping, ensureing that device can realize dynamic, static two kinds of reactivenesses.
Technical scheme：
A kind of zeolite molecular sieve dynamic, static dual-purpose crystallization device, including electrical heating sleeve, socket cover, electric heating cover,
Synthesis reaction vessel；The electrical heating sleeve is arranged in the reactor base, and electrical heating is provided with the electrical heating sleeve
Cover, be machined with chute in the electric heating cover, the synthesis reaction vessel, the synthesis reaction vessel are movably set with the chute
Top is provided with reactor end cap, and reactor base is provided with below the synthesis reaction vessel, and the reactor end cap top is solid
Surely one side permanent magnet is provided with, is provided with two-sided permanent magnet above the one side permanent magnet, the two-sided permanent magnet is arranged on one
On group magnet trip shaft, described magnet trip shaft one end is fixed through the electrical heating sleeve with one group of turn drive motor main shaft
Connection, the reactor base lower section are provided with back-moving spring, and the back-moving spring other end is fixed with the reactor base
Connection, the electrical heating sleeve upper end is provided with electric heating cover cover.
Further, the turn drive motor is arranged on the electric machine support, and the electric machine support adds with the electricity
Hot jacket drum outer wall is fixedly connected.
Further, the one side permanent magnet is N poles permanent magnetic iron bar.
Further, the two-sided permanent magnet is the two-sided different poles permanent magnet bars of N/S.
The present invention has the advantages that relative to prior art：
The present invention drives the two-sided different poles permanent magnet bars of N/S to rotate by turn drive motor, is repelled by homopolarity, heteropole
The attracting N poles permanent magnet covered with reactor interacts, and driving synthesis reaction vessel moves up and down in chute, realizes zeolite
Molecular sieve dynamic synthesizes；When experiment needs static monitor, do not start motor, you can realize static reaction；Electrical heating sleeve can
Realize that building-up process temperature is precisely controlled；Furthermore it is possible to by controlling turn drive motor rotating speed to control mixing rate；Crystallization is closed
Cheng Houke opens heating mantle cover, realizes charging, takes out the cleaning of synthetic product and reactor；
Strong applicability of the present invention, simple in construction, easily operated, device volume is small, saves space；
The up and down motion of the synthesis reaction vessel of the present invention, can be well mixed reaction raw materials, and up and down motion amplitude is little,
The condition that mitigation required for just meeting zeolite molecular sieve growth mixes, is advantageous to the growth of molecular sieve；
Synthesis reaction vessel of the present invention improves sealing, ensure that the pressure in kettle, have boiling concurrently without built-in agitating device
Stone molecular sieve dynamic, static dual-purpose reactor, provide easily experiment condition for zeolite molecular sieve compound experiment, meet respectively not
Requirement of experiment with the case of.
Brief description of the drawings
Fig. 1 is the structural representation of the present invention；
Fig. 2 is the top view of the synthesis reaction vessel of the present invention.
1- electrical heating sleeve in figure；2- electric heating cover covers；3- electric heating covers；4- synthesis reaction vessels；41- reactors end
Lid；42- reactor bases；5- reactor bases；6- chutes；7- one side permanent magnets；The two-sided permanent magnets of 8-；9- magnet trip shafts；
10- turn drive motors；11- back-moving springs；12- electric machine supports.
Embodiment
Below with reference to accompanying drawing, the present invention is described in detail.
Show with reference to Fig. 1-Fig. 2, a kind of zeolite molecular sieve dynamic, static dual-purpose crystallization device, bag disclosed in the present embodiment
Include electrical heating sleeve 1, electric heating cover cover 2, electric heating cover 3, synthesis reaction vessel 4；The electrical heating sleeve 1 is arranged on described anti-
Answer on device base 5, electric heating cover 3 is provided with the electrical heating sleeve 1, chute 6 is machined with the electric heating cover 3, it is described
The synthesis reaction vessel 4 is movably set with chute 6, the top of synthesis reaction vessel 4 is provided with reactor end cap 41, the conjunction
The lower section of reactor 4 is provided with reactor base 42, the top of reactor end cap 41 is fixedly installed one side permanent magnet 7, institute
State the top of one side permanent magnet 7 and be provided with two-sided permanent magnet 8, the two-sided permanent magnet 8 is arranged on one group of magnet trip shaft 9, institute
State the one end of magnet trip shaft 9 to be fixedly connected with one group of main shaft of turn drive motor 10 through the electrical heating sleeve 1, the reaction
The lower section of bottom seat 4 is provided with back-moving spring 11, and the other end of back-moving spring 11 is fixedly connected with the reactor base 5, institute
State the upper end of electrical heating sleeve 1 and be provided with electric heating cover cover 2.
Specifically, the turn drive motor 10 is arranged on the electric machine support 12, the electric machine support 12 with it is described
The outer wall of electrical heating sleeve 1 is fixedly connected.
More specifically, the one side permanent magnet 7 is N poles permanent magnetic iron bar；The two-sided permanent magnet 8 is the two-sided heteropoles of N/S
Permanent magnetic iron bar.
More specifically, temperature sensor, the input of temperature sensor and one group of PLC are provided with synthesis reaction vessel
End electrical connection, the PLC are arranged in control panel, and some groups of control buttons, institute are provided with the control panel
Input of the control button also with the PLC is stated to electrically connect, the output end of the PLC also with the electrical heating
Set and turn drive motor electrical connection.
The present invention drives the two-sided different poles permanent magnet bars of N/S to rotate by turn drive motor, is repelled by homopolarity, heteropole
It is attracting to have covered the permanent magnet interaction of N poles with reactor, drive synthesis reactor to move up and down, realize that zeolite molecular sieve dynamic is closed
Into；When experiment needs static monitor, do not start motor, pulling down the two-sided different poles permanent magnet bar electrical heating sleeves of N/S can realize
Building-up process temperature is precisely controlled；In addition, mixing rate can be controlled by motor speed；Heating mantle can be opened after crystallization synthesis
Cover, charging is realized, take out the cleaning of synthetic product and reactor.
Above example is the exemplary illustration to this patent, does not limit its protection domain, people in the art
Member can also be changed to its part, as long as no the Spirit Essence beyond this patent, all in the protection domain of this patent.
Claims (4)
1. a kind of zeolite molecular sieve dynamic, static dual-purpose crystallization device, it is characterised in that：Add including electrical heating sleeve (1), electricity
Hot jacket cover (2), electric heating cover (3), synthesis reaction vessel (4)；The electrical heating sleeve (1) is arranged on the reactor base
(5) on, electric heating cover (3) is provided with the electrical heating sleeve (1), chute (6), institute are machined with the electric heating cover (3)
State and the synthesis reaction vessel (4) is movably set with chute (6), reactor end cap is provided with above the synthesis reaction vessel (4)
(41) reactor base (42), is provided with below the synthesis reaction vessel (4), is fixedly installed above the reactor end cap (41)
There is one side permanent magnet (7), be provided with two-sided permanent magnet (8) above the one side permanent magnet (7), the two-sided permanent magnet (8) sets
Put on one group of magnet trip shaft (9), described magnet trip shaft (9) one end passes through the electrical heating sleeve (1) and one group of upset
Motor (10) main shaft is fixedly connected, and back-moving spring (11), the back-moving spring are provided with below the reactor base (4)
(11) other end is fixedly connected with the reactor base (5), and electrical heating sleeve (1) upper end is provided with electric heating cover cover
(2)。
2. a kind of zeolite molecular sieve dynamic according to claim 1, static dual-purpose crystallization device, it is characterised in that institute
State turn drive motor (10) to be arranged on the electric machine support (12), the electric machine support (12) and the electrical heating sleeve
(1) outer wall is fixedly connected.
3. a kind of zeolite molecular sieve dynamic according to claim 2, static dual-purpose crystallization device, it is characterised in that institute
It is N poles permanent magnetic iron bar to state one side permanent magnet (7).
4. a kind of zeolite molecular sieve dynamic according to claim 3, static dual-purpose crystallization device, it is characterised in that institute
It is the two-sided different poles permanent magnet bars of N/S to state two-sided permanent magnet (8).
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201711290936.2A CN107824155A (en) | 2017-12-07 | 2017-12-07 | A kind of zeolite molecular sieve dynamic, static dual-purpose crystallization device |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201711290936.2A CN107824155A (en) | 2017-12-07 | 2017-12-07 | A kind of zeolite molecular sieve dynamic, static dual-purpose crystallization device |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN107824155A true CN107824155A (en) | 2018-03-23 |
Family
ID=61642450
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201711290936.2A Pending CN107824155A (en) | 2017-12-07 | 2017-12-07 | A kind of zeolite molecular sieve dynamic, static dual-purpose crystallization device |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN107824155A (en) |
Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPH0596564U (en) * | 1992-05-27 | 1993-12-27 | 株式会社千代田製作所 | Adapter for magnetic coupling of culture device |
| CN203226699U (en) * | 2013-03-21 | 2013-10-09 | 九阳股份有限公司 | Intelligent thermos |
| CN203400666U (en) * | 2013-07-29 | 2014-01-22 | 宁波慧通新能源科技有限公司 | Planetary type stirring machine |
| CN106378082A (en) * | 2016-11-18 | 2017-02-08 | 黑龙江省能源环境研究院 | Molecular sieve dynamic synthesis device |
| CN207576428U (en) * | 2017-12-07 | 2018-07-06 | 黑龙江省能源环境研究院 | A kind of zeolite molecular sieve dynamic, static dual-purpose crystallization device |
-
2017
- 2017-12-07 CN CN201711290936.2A patent/CN107824155A/en active Pending
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPH0596564U (en) * | 1992-05-27 | 1993-12-27 | 株式会社千代田製作所 | Adapter for magnetic coupling of culture device |
| CN203226699U (en) * | 2013-03-21 | 2013-10-09 | 九阳股份有限公司 | Intelligent thermos |
| CN203400666U (en) * | 2013-07-29 | 2014-01-22 | 宁波慧通新能源科技有限公司 | Planetary type stirring machine |
| CN106378082A (en) * | 2016-11-18 | 2017-02-08 | 黑龙江省能源环境研究院 | Molecular sieve dynamic synthesis device |
| CN207576428U (en) * | 2017-12-07 | 2018-07-06 | 黑龙江省能源环境研究院 | A kind of zeolite molecular sieve dynamic, static dual-purpose crystallization device |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN110035680A (en) | Diet beverages regulation machine comprising a magnetic couplings group | |
| CN204600200U (en) | A kind of mixed stirring device | |
| CN201987367U (en) | Blender | |
| CN207576428U (en) | A kind of zeolite molecular sieve dynamic, static dual-purpose crystallization device | |
| CN108324146A (en) | Multi-function foodstuff machine | |
| CN107551876A (en) | A kind of Full-automatic heating for Cosmetic Manufacture stirs intelligent emulsifier unit | |
| CN206253137U (en) | A kind of super absorbent resin produces isothermal reaction equipment | |
| CN104162460A (en) | Electromagnetic stirring type ultrasonic water bath device | |
| CN107824155A (en) | A kind of zeolite molecular sieve dynamic, static dual-purpose crystallization device | |
| CN102160760B (en) | Stirrer | |
| CN208286891U (en) | Cooking apparatus | |
| CN106378082B (en) | A kind of molecular sieve dynamic synthesizer | |
| CN206721212U (en) | A kind of drum-type anaerobic fermentation tank | |
| CN207590475U (en) | Cooking apparatus | |
| CN204503085U (en) | A kind of use for laboratory magnetic agitation reactor device | |
| CN102008934B (en) | Non-contact reaction kettle | |
| CN207493628U (en) | A kind of compound ketoconazole ointment production constant temperature blender with magnetic force | |
| CN207805615U (en) | A kind of magnetic agitation hydrothermal synthesis device | |
| CN207805602U (en) | A kind of Modified starch heating reaction unit | |
| CN201920550U (en) | Stirring device for brewing milk powder | |
| CN206823793U (en) | A kind of desk-top liftable pyroreaction kettle of controllable temperature thermometric | |
| CN206103770U (en) | Diatom mud agitated vessel that can stir automatically | |
| CN207722687U (en) | A kind of dry powder paint mixing machine | |
| CN104874340B (en) | Vertical stirring reaction kettle | |
| CN207187570U (en) | A kind of nickel minerals is mixed machine |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination |