CN107815337A - A kind of preparation method of Digit Control Machine Tool special lube - Google Patents

A kind of preparation method of Digit Control Machine Tool special lube Download PDF

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Publication number
CN107815337A
CN107815337A CN201710937518.1A CN201710937518A CN107815337A CN 107815337 A CN107815337 A CN 107815337A CN 201710937518 A CN201710937518 A CN 201710937518A CN 107815337 A CN107815337 A CN 107815337A
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CN
China
Prior art keywords
oil
parts
mixing
lube
prepared
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Withdrawn
Application number
CN201710937518.1A
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Chinese (zh)
Inventor
朱嬴华
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Zhenjiang Yan Nc Equipment Co Ltd
Original Assignee
Zhenjiang Yan Nc Equipment Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Zhenjiang Yan Nc Equipment Co Ltd filed Critical Zhenjiang Yan Nc Equipment Co Ltd
Priority to CN201710937518.1A priority Critical patent/CN107815337A/en
Publication of CN107815337A publication Critical patent/CN107815337A/en
Withdrawn legal-status Critical Current

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Classifications

    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M169/00—Lubricating compositions characterised by containing as components a mixture of at least two types of ingredient selected from base-materials, thickeners or additives, covered by the preceding groups, each of these compounds being essential
    • C10M169/04—Mixtures of base-materials and additives
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2203/00—Organic non-macromolecular hydrocarbon compounds and hydrocarbon fractions as ingredients in lubricant compositions
    • C10M2203/10—Petroleum or coal fractions, e.g. tars, solvents, bitumen
    • C10M2203/1006—Petroleum or coal fractions, e.g. tars, solvents, bitumen used as base material
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2205/00—Organic macromolecular hydrocarbon compounds or fractions, whether or not modified by oxidation as ingredients in lubricant compositions
    • C10M2205/02—Organic macromolecular hydrocarbon compounds or fractions, whether or not modified by oxidation as ingredients in lubricant compositions containing acyclic monomers
    • C10M2205/0206—Organic macromolecular hydrocarbon compounds or fractions, whether or not modified by oxidation as ingredients in lubricant compositions containing acyclic monomers used as base material
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2207/00—Organic non-macromolecular hydrocarbon compounds containing hydrogen, carbon and oxygen as ingredients in lubricant compositions
    • C10M2207/28—Esters
    • C10M2207/287—Partial esters
    • C10M2207/289—Partial esters containing free hydroxy groups
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2215/00—Organic non-macromolecular compounds containing nitrogen as ingredients in lubricant compositions
    • C10M2215/02—Amines, e.g. polyalkylene polyamines; Quaternary amines
    • C10M2215/06—Amines, e.g. polyalkylene polyamines; Quaternary amines having amino groups bound to carbon atoms of six-membered aromatic rings
    • C10M2215/064—Di- and triaryl amines
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2219/00—Organic non-macromolecular compounds containing sulfur, selenium or tellurium as ingredients in lubricant compositions
    • C10M2219/06—Thio-acids; Thiocyanates; Derivatives thereof
    • C10M2219/062—Thio-acids; Thiocyanates; Derivatives thereof having carbon-to-sulfur double bonds
    • C10M2219/066—Thiocarbamic type compounds
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2223/00—Organic non-macromolecular compounds containing phosphorus as ingredients in lubricant compositions
    • C10M2223/02—Organic non-macromolecular compounds containing phosphorus as ingredients in lubricant compositions having no phosphorus-to-carbon bonds
    • C10M2223/04—Phosphate esters
    • C10M2223/041—Triaryl phosphates
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2223/00—Organic non-macromolecular compounds containing phosphorus as ingredients in lubricant compositions
    • C10M2223/02—Organic non-macromolecular compounds containing phosphorus as ingredients in lubricant compositions having no phosphorus-to-carbon bonds
    • C10M2223/04—Phosphate esters
    • C10M2223/045—Metal containing thio derivatives
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
    • C10N2030/00—Specified physical or chemical properties which is improved by the additive characterising the lubricating composition, e.g. multifunctional additives
    • C10N2030/06—Oiliness; Film-strength; Anti-wear; Resistance to extreme pressure

Landscapes

  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Organic Chemistry (AREA)
  • Lubricants (AREA)

Abstract

A kind of preparation method of Digit Control Machine Tool special lube of the present invention, step are as follows:(1) base oil is prepared, poly- a alkene PAO base oils and oil base oil mix；（2）Prepare lube oil additive,（3）Lubricating oil is prepared, 75 95 parts of base oil, 30 40 parts of lube oil additive are mixed, incorporation time is 2 3H, and mixing can obtain finished product after terminating；Above number is mass fraction.Prepared using multistep mixing method, pass through the addition of the lube oil additive of special formulation component so that the lubricating oil has very strong self-lubricating property, and can be good at reducing friction, ensures lubricant effect, preparation technology of the present invention is simple, workable.

Description

A kind of preparation method of Digit Control Machine Tool special lube
Technical field
The present invention is more particularly directed to a kind of preparation method of Digit Control Machine Tool special lube.
Background technology
Fretting wear is the phenomenon of generally existing in friction process, according to statistics, a performance in the world more than 1/3rd The loss in source carrys out self-friction, and therefore, economic loss caused by reducing friction and wear is significant.And it is drop to lubricate Low friction, the effective technology for reducing or avoiding abrasion.
The content of the invention
The present invention proposes a kind of preparation method of Digit Control Machine Tool special lube regarding to the issue above.
Specific technical scheme is as follows：
A kind of preparation method of Digit Control Machine Tool special lube, it is characterised in that step is as follows:
(1) base oil is prepared, poly- a alkene PAO base oils and oil base oil mix, mixing quality ratio is poly- a Alkene PAO base oils：Oil base oil=5:Base oil is completed to obtain in 1, incorporation time 2-3H, mixing；
（2）Lube oil additive is prepared, by β-positive octadecanol ester 10-40 parts of (3,5- di-tert-butyl-hydroxy phenyl) propionic acid, Alkyl diphenylamine 20-30 parts, β-different monooctyl ester 10-20 parts of (3,5- di-tert-butyl-hydroxy phenyl) propionic acid are mixed, mixing Time 1-2h, mixing add methylene-bis--alkyl dithiocarbamate 10-30 parts, two (2- ethylhexyls) two after terminating D2EHDTPA molybdenum 10-15 parts, triphenyl phosphate 3-5 parts continue to mix, and incorporation time is 1.5-3H, is moistened after the completion of mixing Oil additive, above number are mass fraction；
（3）Lubricating oil is prepared, base oil 75-95 parts, lube oil additive 30-40 parts are mixed, incorporation time 2-3H, Mixing can obtain finished product after terminating；Above number is mass fraction.
A kind of preparation method of Digit Control Machine Tool special lube, it is characterised in that two (the 2- ethylhexyls) two is thio The mass ratio of molybdenum phosphate and the triphenyl phosphate is 3:1.
Beneficial effects of the present invention are：Prepared using multistep mixing method, added by the lubricating oil of special formulation component Add the addition of agent so that the lubricating oil has very strong self-lubricating property, and can be good at reducing friction, ensures lubrication effect Fruit, preparation technology of the present invention is simple, workable.
Embodiment
To make technical scheme become apparent from clearly, below the present invention is described further, it is any to this The scheme that the technical characteristic progress equivalencing of inventive technique scheme and conventional reasoning are drawn each falls within the scope of the present invention.
Embodiment 1
A kind of preparation method of Digit Control Machine Tool special lube, it is characterised in that step is as follows:
(1) base oil is prepared, poly- a alkene PAO base oils and oil base oil mix, mixing quality ratio is poly- a Alkene PAO base oils：Oil base oil=5:Base oil is completed to obtain in 1, incorporation time 2H, mixing；
（2）Lube oil additive is prepared, by β-positive 10 parts of octadecanol ester of (3,5- di-tert-butyl-hydroxy phenyl) propionic acid, alkane 20 parts of base diphenylamines, β-different 10 parts of monooctyl ester of (3,5- di-tert-butyl-hydroxy phenyl) propionic acid are mixed, incorporation time 1h, are mixed Conjunction adds methylene-bis- -10 parts of alkyl dithiocarbamate, two (2- ethylhexyls) molybdenum dithiophosphates 10 after terminating Part, 3 parts of triphenyl phosphate continues to mix, and incorporation time 1.5H obtains lube oil additive after the completion of mixing, above number is equal For mass fraction；
（3）Lubricating oil is prepared, 75 parts of base oil, 30 parts of lube oil additive are mixed, incorporation time 2H, mixing terminates After can obtain finished product；Above number is mass fraction.
Embodiment 2
A kind of preparation method of Digit Control Machine Tool special lube, it is characterised in that step is as follows:
(1) base oil is prepared, poly- a alkene PAO base oils and oil base oil mix, mixing quality ratio is poly- a Alkene PAO base oils：Oil base oil=5:Base oil is completed to obtain in 1, incorporation time 3H, mixing；
（2）Lube oil additive is prepared, by β-positive 40 parts of octadecanol ester of (3,5- di-tert-butyl-hydroxy phenyl) propionic acid, alkane 30 parts of base diphenylamines, β-different 20 parts of monooctyl ester of (3,5- di-tert-butyl-hydroxy phenyl) propionic acid are mixed, incorporation time 2h, are mixed Conjunction adds methylene-bis- -30 parts of alkyl dithiocarbamate, two (2- ethylhexyls) molybdenum dithiophosphate 10- after terminating 15 parts, 5 parts of triphenyl phosphate continues to mix, incorporation time 3H, and lube oil additive is obtained after the completion of mixing, and above number is equal For mass fraction；
（3）Lubricating oil is prepared, 95 parts of base oil, 40 parts of lube oil additive are mixed, incorporation time 3H, mixing terminates After can obtain finished product；Above number is mass fraction.
Beneficial effects of the present invention are：Prepared using multistep mixing method, added by the lubricating oil of special formulation component Add the addition of agent so that the lubricating oil has very strong self-lubricating property, and can be good at reducing friction, ensures lubrication effect Fruit, preparation technology of the present invention is simple, workable.

Claims (2)

1. a kind of preparation method of Digit Control Machine Tool special lube, it is characterised in that step is as follows:
(1) base oil is prepared, poly- a alkene PAO base oils and oil base oil mix, mixing quality ratio is poly- a Alkene PAO base oils：Oil base oil=5:Base oil is completed to obtain in 1, incorporation time 2-3H, mixing；
（2）Lube oil additive is prepared, by β-positive octadecanol ester 10-40 parts of (3,5- di-tert-butyl-hydroxy phenyl) propionic acid, Alkyl diphenylamine 20-30 parts, β-different monooctyl ester 10-20 parts of (3,5- di-tert-butyl-hydroxy phenyl) propionic acid are mixed, mixing Time 1-2h, mixing add methylene-bis--alkyl dithiocarbamate 10-30 parts, two (2- ethylhexyls) two after terminating D2EHDTPA molybdenum 10-15 parts, triphenyl phosphate 3-5 parts continue to mix, and incorporation time is 1.5-3H, is moistened after the completion of mixing Oil additive, above number are mass fraction；
（3）Lubricating oil is prepared, base oil 75-95 parts, lube oil additive 30-40 parts are mixed, incorporation time 2-3H, Mixing can obtain finished product after terminating；Above number is mass fraction.
2. a kind of preparation method of Digit Control Machine Tool special lube as claimed in claim 1, it is characterized in that, two (the 2- second Base hexyl) mass ratio of molybdenum dithiophosphate and the triphenyl phosphate is 3:1.
CN201710937518.1A 2017-09-30 2017-09-30 A kind of preparation method of Digit Control Machine Tool special lube Withdrawn CN107815337A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201710937518.1A CN107815337A (en) 2017-09-30 2017-09-30 A kind of preparation method of Digit Control Machine Tool special lube

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201710937518.1A CN107815337A (en) 2017-09-30 2017-09-30 A kind of preparation method of Digit Control Machine Tool special lube

Publications (1)

Publication Number Publication Date
CN107815337A true CN107815337A (en) 2018-03-20

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Family Applications (1)

Application Number Title Priority Date Filing Date
CN201710937518.1A Withdrawn CN107815337A (en) 2017-09-30 2017-09-30 A kind of preparation method of Digit Control Machine Tool special lube

Country Status (1)

Country Link
CN (1) CN107815337A (en)

Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105602653A (en) * 2016-02-05 2016-05-25 锦州康泰润滑油添加剂股份有限公司 Lubricant additive with antioxidant, antiwear and rustproof functions as well as preparation method and application thereof
CN105733787A (en) * 2016-04-21 2016-07-06 东莞太平洋博高润滑油有限公司 Anti-pitting self-repairing gear grease

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105602653A (en) * 2016-02-05 2016-05-25 锦州康泰润滑油添加剂股份有限公司 Lubricant additive with antioxidant, antiwear and rustproof functions as well as preparation method and application thereof
CN105733787A (en) * 2016-04-21 2016-07-06 东莞太平洋博高润滑油有限公司 Anti-pitting self-repairing gear grease

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Application publication date: 20180320

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