CN107814483A - One kind energy-conservation fire resistance hollow glass and its manufacture method - Google Patents
One kind energy-conservation fire resistance hollow glass and its manufacture method Download PDFInfo
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- CN107814483A CN107814483A CN201711258600.8A CN201711258600A CN107814483A CN 107814483 A CN107814483 A CN 107814483A CN 201711258600 A CN201711258600 A CN 201711258600A CN 107814483 A CN107814483 A CN 107814483A
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- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C3/00—Glass compositions
- C03C3/04—Glass compositions containing silica
- C03C3/076—Glass compositions containing silica with 40% to 90% silica, by weight
- C03C3/102—Glass compositions containing silica with 40% to 90% silica, by weight containing lead
- C03C3/108—Glass compositions containing silica with 40% to 90% silica, by weight containing lead containing boron
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- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03B—MANUFACTURE, SHAPING, OR SUPPLEMENTARY PROCESSES
- C03B25/00—Annealing glass products
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- Materials Engineering (AREA)
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Abstract
The invention discloses one kind energy-conservation fire resistance hollow glass and its manufacture method, the double glazing, including the glass body for making its middle part be in sealing cavity structure is bonded by binding agent, the glass body includes according to the raw material of parts by weight：45 85 parts of silica, 3 25 parts of lead oxide, 1 20 parts of sodium oxide molybdena, 1 35 parts of barium monoxide, 0.01 8 parts of diboron trioxide, 0.01 8 parts of titanium dioxide, 0.01 8 parts of zirconium dioxide, 1 20 parts of magnesia, 1 12 parts of calcium oxide, 1 20 parts of bichromate, 1 18 parts of iron oxide.Raw material is mixed, is heated to 90 150 DEG C, and be incubated 4 15h；1,600 1800 DEG C are warming up to again, and is incubated 2 10h at such a temperature, make its shaping, then annealed, cooling；Being bonded by binding agent makes its middle part be produced in the glass body of sealing cavity structure.Double glazing produced by the present invention has excellent fire resistance, and sound insulating and absorbing works well；Preparation technology is simple, easy to operate, and production cost is low, and prospect of the application is good, suitable for industrialized production.
Description
Technical field
The present invention relates to glass technology field, is specifically a kind of energy-conservation fire resistance hollow glass and its manufacture method.
Background technology
Double glazing is a kind of good heat-insulated, sound insulation, novel building material that is beautiful and applicable and can reducing building deadweight
Material.Double glazing is made up of two layers or multi-layer planar glass.The high-strength high-air-tightness compound binding agent of surrounding, by two panels or more
Sheet glass and sealing strip, glass bar are Nian Jie, sealing.Centre is filled with dry gas, and inframe is filled with drier, to ensure between sheet glass
The aridity of air.The original sheet glass of various different performances can be selected as requested, as colorless transparent float glass are embossed glass
Glass, antisolar glass, heat-reflecting glass, wire glass, safety glass etc. and frame（Aluminium chassis or glass bar etc.）, through cementing, weldering
Connect or welding and be made.High-performance hollow glass is different from general ordinary insulating glass, except enclosing drying among layer glass
Outside air, particulate metal film of last layer good in thermal property also in outside glass intermediate air layer side, is applied.It can end by
The sun is mapped to the suitable energy of interior, plays bigger effect of heat insulation.But existing double glazing fire resisting effect is poor, technique
Complexity, cost are high.
The content of the invention
It is an object of the invention to provide one kind energy-conservation fire resistance hollow glass and its manufacture method, to solve above-mentioned background skill
The problem of being proposed in art.
To achieve the above object, the present invention provides following technical scheme：
One kind energy-conservation fire resistance hollow glass, including the glass body for making its middle part be in sealing cavity structure is bonded by binding agent,
The glass body includes according to the raw material of parts by weight：Silica 45-85 parts, lead oxide 3-25 parts, sodium oxide molybdena 1-20 parts, oxygen
Change barium 1-35 parts, diboron trioxide 0.01-8 parts, titanium dioxide 0.01-8 parts, zirconium dioxide 0.01-8 parts, magnesia 1-20 parts,
Calcium oxide 1-12 parts, bichromate 1-20 parts, iron oxide 1-18 parts.
As the further scheme of the present invention：The glass body includes according to the raw material of parts by weight：Silica 48-82
Part, lead oxide 4-22 parts, sodium oxide molybdena 2-18 parts, barium monoxide 2-32 parts, diboron trioxide 0.1-6 parts, titanium dioxide 0.01-6 parts,
Zirconium dioxide 0.01-6 parts, magnesia 2-10 parts, calcium oxide 2-8 parts, bichromate 2-18 parts, iron oxide 2-15 parts.
As the further scheme of the present invention：The glass body includes according to the raw material of parts by weight：Silica 50-80
Part, lead oxide 5-20 parts, sodium oxide molybdena 3-15 parts, barium monoxide 5-30 parts, diboron trioxide 0.2-5 parts, titanium dioxide 0.01-5 parts,
Zirconium dioxide 0.01-5 parts, magnesia 3-8 parts, calcium oxide 3-6 parts, bichromate 5-15 parts, iron oxide 5-12 parts.
A kind of manufacture method for saving fire resistance hollow glass, comprises the following steps：
1）Weigh silica, lead oxide, sodium oxide molybdena, barium monoxide, diboron trioxide, titanium dioxide, two respectively according to parts by weight
Zirconium oxide, magnesia, calcium oxide, bichromate, iron oxide；
2）By silica, lead oxide, sodium oxide molybdena, barium monoxide, diboron trioxide, titanium dioxide, zirconium dioxide, bichromate,
Magnesia, calcium oxide, iron oxide are mixed evenly, and are heated to 90-150 DEG C, and be incubated 4-15h at such a temperature；It is made mixed
Close material；
3）Compound is warming up to 1600-1800 DEG C, and is incubated 2-10h at such a temperature, makes its shaping, then annealed, cooling；
Being bonded by binding agent makes its middle part be produced in the glass body of sealing cavity structure.
As the further scheme of the present invention：Step 2）In, 100-130 DEG C is heated to, and be incubated 5- at such a temperature
12h。
As the further scheme of the present invention：Step 3）In, annealing temperature is 600-680 DEG C, time 40-90min.
Compared with prior art, the beneficial effects of the invention are as follows：
Double glazing produced by the present invention has excellent fire resistance, and sound insulating and absorbing works well；Preparation technology is simple, easily behaviour
Make, production cost is low, energy-conserving and environment-protective, and prospect of the application is good, suitable for industrialized production.
Embodiment
Below in conjunction with the embodiment of the present invention, the technical scheme in the embodiment of the present invention is clearly and completely described,
Obviously, described embodiment is only part of the embodiment of the present invention, rather than whole embodiments.Based in the present invention
Embodiment, the every other embodiment that those of ordinary skill in the art are obtained under the premise of creative work is not made, all
Belong to the scope of protection of the invention.
Embodiment 1
In the embodiment of the present invention, one kind energy-conservation fire resistance hollow glass, including being bonded by binding agent makes its middle part be in sealing cavity
The glass body of structure, the glass body include according to the raw material of parts by weight：45 parts of silica, 3 parts of lead oxide, sodium oxide molybdena
1 part, 1 part of barium monoxide, 0.01 part of diboron trioxide, 0.01 part of titanium dioxide, 0.01 part of zirconium dioxide, 1 part of magnesia, calcium oxide
1 part, 1 part of bichromate, 1 part of iron oxide.
A kind of manufacture method for saving fire resistance hollow glass, comprises the following steps：
1）Weigh silica, lead oxide, sodium oxide molybdena, barium monoxide, diboron trioxide, titanium dioxide, two respectively according to parts by weight
Zirconium oxide, magnesia, calcium oxide, bichromate, iron oxide.
2）By silica, lead oxide, sodium oxide molybdena, barium monoxide, diboron trioxide, titanium dioxide, zirconium dioxide, dichromic acid
Salt, magnesia, calcium oxide, iron oxide are mixed evenly, and are heated to 90 DEG C, and be incubated 4h at such a temperature；Compound is made.
3）Compound is warming up to 1600 DEG C, and is incubated 2h at such a temperature, makes its shaping；Annealed again, cooling, passes through
Binding agent, which bonds, makes its middle part produce double glazing in the glass body of sealing cavity structure, and annealing temperature is 600 DEG C, and the time is
40min。
Embodiment 2
In the embodiment of the present invention, one kind energy-conservation fire resistance hollow glass, including being bonded by binding agent makes its middle part be in sealing cavity
The glass body of structure, the glass body include according to the raw material of parts by weight：85 parts of silica, 25 parts of lead oxide, oxidation
20 parts of sodium, 35 parts of barium monoxide, 8 parts of diboron trioxide, 8 parts of titanium dioxide, 8 parts of zirconium dioxide, 20 parts of magnesia, calcium oxide 12
Part, 20 parts of bichromate, 18 parts of iron oxide.
A kind of manufacture method for saving fire resistance hollow glass, comprises the following steps：
1）Weigh silica, lead oxide, sodium oxide molybdena, barium monoxide, diboron trioxide, titanium dioxide, two respectively according to parts by weight
Zirconium oxide, magnesia, calcium oxide, bichromate, iron oxide.
2）By silica, lead oxide, sodium oxide molybdena, barium monoxide, diboron trioxide, titanium dioxide, zirconium dioxide, dichromic acid
Salt, magnesia, calcium oxide, iron oxide are mixed evenly, and are heated to 150 DEG C, and be incubated 15h at such a temperature；Mixing is made
Material.
3）Compound is warming up to 1800 DEG C, and is incubated 10h at such a temperature, makes its shaping, then annealed, cooling, leads to
Crossing binding agent and bonding makes its middle part produce double glazing in the glass body of sealing cavity structure, and annealing temperature is 680 DEG C, the time
For 90min.
Embodiment 3
In the embodiment of the present invention, one kind energy-conservation fire resistance hollow glass, including being bonded by binding agent makes its middle part be in sealing cavity
The glass body of structure, the glass body include according to the raw material of parts by weight：48 parts of silica, 4 parts of lead oxide, sodium oxide molybdena
2 parts, 2 parts of barium monoxide, 0.1 part of diboron trioxide, 0.01 part of titanium dioxide, 0.01 part of zirconium dioxide, 2 parts of magnesia, calcium oxide 2
Part, 2 parts of bichromate, 2 parts of iron oxide.
A kind of manufacture method for saving fire resistance hollow glass, comprises the following steps：
1）Weigh silica, lead oxide, sodium oxide molybdena, barium monoxide, diboron trioxide, titanium dioxide, two respectively according to parts by weight
Zirconium oxide, magnesia, calcium oxide, bichromate, iron oxide.
2）By silica, lead oxide, sodium oxide molybdena, barium monoxide, diboron trioxide, titanium dioxide, zirconium dioxide, dichromic acid
Salt, magnesia, calcium oxide, iron oxide are mixed evenly, and are heated to 100 DEG C, and be incubated 5h at such a temperature；Mixing is made
Material.
3）Compound is warming up to 1650 DEG C, and is incubated 4h at such a temperature, makes its shaping, then annealed, cooling, passes through
Binding agent, which bonds, makes its middle part produce double glazing in the glass body of sealing cavity structure, and annealing temperature is 620 DEG C, and the time is
50min。
Embodiment 4
In the embodiment of the present invention, one kind energy-conservation fire resistance hollow glass, including being bonded by binding agent makes its middle part be in sealing cavity
The glass body of structure, the glass body include according to the raw material of parts by weight：82 parts of silica, 22 parts of lead oxide, oxidation
18 parts of sodium, 32 parts of barium monoxide, 6 parts of diboron trioxide, 6 parts of titanium dioxide, 6 parts of zirconium dioxide, 10 parts of magnesia, 8 parts of calcium oxide,
18 parts of bichromate, 15 parts of iron oxide.
A kind of manufacture method for saving fire resistance hollow glass, comprises the following steps：
1）Weigh silica, lead oxide, sodium oxide molybdena, barium monoxide, diboron trioxide, titanium dioxide, two respectively according to parts by weight
Zirconium oxide, magnesia, calcium oxide, bichromate, iron oxide.
2）By silica, lead oxide, sodium oxide molybdena, barium monoxide, diboron trioxide, titanium dioxide, zirconium dioxide, dichromic acid
Salt, magnesia, calcium oxide, iron oxide are mixed evenly, and are heated to 130 DEG C, and be incubated 12h at such a temperature；Mixing is made
Material.
3）Compound is warming up to 1750 DEG C, and is incubated 8h at such a temperature, makes its shaping, then annealed, cooling, passes through
Binding agent, which bonds, makes its middle part produce double glazing in the glass body of sealing cavity structure, and annealing temperature is 660 DEG C, and the time is
70min。
Embodiment 5
In the embodiment of the present invention, one kind energy-conservation fire resistance hollow glass, including being bonded by binding agent makes its middle part be in sealing cavity
The glass body of structure, the glass body include according to the raw material of parts by weight：50 parts of silica, 5 parts of lead oxide, sodium oxide molybdena
3 parts, 5 parts of barium monoxide, 0.2 part of diboron trioxide, 0.01 part of titanium dioxide, 0.01 part of zirconium dioxide, 3 parts of magnesia, calcium oxide 3
Part, 5 parts of bichromate, 5 parts of iron oxide.
A kind of manufacture method for saving fire resistance hollow glass, comprises the following steps：
1）Weigh silica, lead oxide, sodium oxide molybdena, barium monoxide, diboron trioxide, titanium dioxide, two respectively according to parts by weight
Zirconium oxide, magnesia, calcium oxide, bichromate, iron oxide.
2）By silica, lead oxide, sodium oxide molybdena, barium monoxide, diboron trioxide, titanium dioxide, zirconium dioxide, dichromic acid
Salt, magnesia, calcium oxide, iron oxide are mixed evenly, and are heated to 110 DEG C, and be incubated 7h at such a temperature；Mixing is made
Material.
3）Compound is warming up to 1700 DEG C, and is incubated 6h at such a temperature, makes its shaping, then annealed, cooling, passes through
Binding agent, which bonds, makes its middle part produce double glazing in the glass body of sealing cavity structure, and annealing temperature is 640 DEG C, and the time is
60min。
Embodiment 6
In the embodiment of the present invention, one kind energy-conservation fire resistance hollow glass, including being bonded by binding agent makes its middle part be in sealing cavity
The glass body of structure, the glass body include according to the raw material of parts by weight：80 parts of silica, 20 parts of lead oxide, oxidation
15 parts of sodium, 30 parts of barium monoxide, 5 parts of diboron trioxide, 5 parts of titanium dioxide, 5 parts of zirconium dioxide, 8 parts of magnesia, 6 parts of calcium oxide,
15 parts of bichromate, 12 parts of iron oxide.
A kind of manufacture method for saving fire resistance hollow glass, comprises the following steps：
1）Weigh silica, lead oxide, sodium oxide molybdena, barium monoxide, diboron trioxide, titanium dioxide, two respectively according to parts by weight
Zirconium oxide, magnesia, calcium oxide, bichromate, iron oxide.
2）By silica, lead oxide, sodium oxide molybdena, barium monoxide, diboron trioxide, titanium dioxide, zirconium dioxide, dichromic acid
Salt, magnesia, calcium oxide, iron oxide are mixed evenly, and are heated to 120 DEG C, and be incubated 8h at such a temperature；Mixing is made
Material.
3）Compound is warming up to 1700 DEG C, and is incubated 5h at such a temperature, makes its shaping, then annealed, cooling, passes through
Binding agent, which bonds, makes its middle part produce double glazing in the glass body of sealing cavity structure, and annealing temperature is 640 DEG C, and the time is
70min。
It is obvious to a person skilled in the art that the invention is not restricted to the details of above-mentioned one exemplary embodiment, Er Qie
In the case of without departing substantially from spirit or essential attributes of the invention, the present invention can be realized in other specific forms.Therefore, no matter
From the point of view of which point, embodiment all should be regarded as exemplary, and be nonrestrictive, the scope of the present invention is by appended power
Profit requires rather than described above limits, it is intended that all in the implication and scope of the equivalency of claim by falling
Change is included in the present invention.
Moreover, it will be appreciated that although the present specification is described in terms of embodiments, not each embodiment is only wrapped
Containing an independent technical scheme, this narrating mode of specification is only that those skilled in the art should for clarity
Using specification as an entirety, the technical solutions in the various embodiments may also be suitably combined, forms those skilled in the art
It is appreciated that other embodiment.
Claims (6)
1. one kind energy-conservation fire resistance hollow glass, including the glass sheet for making its middle part be in sealing cavity structure is bonded by binding agent
Body, it is characterised in that the glass body includes according to the raw material of parts by weight：Silica 45-85 parts, lead oxide 3-25 parts,
Sodium oxide molybdena 1-20 parts, barium monoxide 1-35 parts, diboron trioxide 0.01-8 parts, titanium dioxide 0.01-8 parts, zirconium dioxide 0.01-8
Part, magnesia 1-20 parts, calcium oxide 1-12 parts, bichromate 1-20 parts, iron oxide 1-18 parts.
2. energy-conservation fire resistance hollow glass according to claim 1, it is characterised in that the glass body is according to parts by weight
Raw material includes：Silica 48-82 parts, lead oxide 4-22 parts, sodium oxide molybdena 2-18 parts, barium monoxide 2-32 parts, diboron trioxide
0.1-6 parts, titanium dioxide 0.01-6 parts, zirconium dioxide 0.01-6 parts, magnesia 2-10 parts, calcium oxide 2-8 parts, bichromate 2-
18 parts, iron oxide 2-15 parts.
3. energy-conservation fire resistance hollow glass according to claim 1, it is characterised in that the glass body is according to parts by weight
Raw material includes：Silica 50-80 parts, lead oxide 5-20 parts, sodium oxide molybdena 3-15 parts, barium monoxide 5-30 parts, diboron trioxide
0.2-5 parts, titanium dioxide 0.01-5 parts, zirconium dioxide 0.01-5 parts, magnesia 3-8 parts, calcium oxide 3-6 parts, bichromate 5-
15 parts, iron oxide 5-12 parts.
4. it is a kind of as described in claim 1-3 is any energy-conservation fire resistance hollow glass manufacture method, it is characterised in that including with
Lower step：
1）Weigh silica, lead oxide, sodium oxide molybdena, barium monoxide, diboron trioxide, titanium dioxide, two respectively according to parts by weight
Zirconium oxide, magnesia, calcium oxide, bichromate, iron oxide；
2）By silica, lead oxide, sodium oxide molybdena, barium monoxide, diboron trioxide, titanium dioxide, zirconium dioxide, bichromate,
Magnesia, calcium oxide, iron oxide are mixed evenly, and are heated to 90-150 DEG C, and be incubated 4-15h at such a temperature；It is made mixed
Close material；
3）Compound is warming up to 1600-1800 DEG C, and is incubated 2-10h at such a temperature, makes its shaping, is bonded by binding agent
Make the glass body that its middle part is in sealing cavity structure；It is annealed again, cool down and produce.
5. the manufacture method of energy-conservation fire resistance hollow glass according to claim 4, it is characterised in that step 2）In, heating
To 100-130 DEG C, and 5-12h is incubated at such a temperature.
6. the manufacture method of energy-conservation fire resistance hollow glass according to claim 4, it is characterised in that step 3）In, annealing
Temperature is 600-680 DEG C, time 40-90min.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201711258600.8A CN107814483A (en) | 2017-12-04 | 2017-12-04 | One kind energy-conservation fire resistance hollow glass and its manufacture method |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201711258600.8A CN107814483A (en) | 2017-12-04 | 2017-12-04 | One kind energy-conservation fire resistance hollow glass and its manufacture method |
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| Publication Number | Publication Date |
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| CN107814483A true CN107814483A (en) | 2018-03-20 |
Family
ID=61605648
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| Application Number | Title | Priority Date | Filing Date |
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| CN201711258600.8A Pending CN107814483A (en) | 2017-12-04 | 2017-12-04 | One kind energy-conservation fire resistance hollow glass and its manufacture method |
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110386760A (en) * | 2019-08-15 | 2019-10-29 | 徐宝辰 | Glass rock powder and preparation method thereof |
| CN112299711A (en) * | 2020-11-06 | 2021-02-02 | 苏州市亿林玻璃加工制造有限公司 | Energy-saving and environment-friendly hollow glass and preparation method thereof |
| CN114262154A (en) * | 2021-12-10 | 2022-04-01 | 江苏神盾新材料科技有限公司 | Special radiation-proof glass for nuclear power station and preparation process thereof |
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|---|---|---|---|---|
| CN1275118A (en) * | 1998-09-04 | 2000-11-29 | 日本电气硝子株式会社 | CRT bulb glass containing PBO and Fe2O3 |
| CN1545719A (en) * | 2001-08-23 | 2004-11-10 | 日本电气硝子株式会社 | Funnel glass for cathode-ray tube |
| CN101781089A (en) * | 2010-01-27 | 2010-07-21 | 彩虹集团电子股份有限公司 | Cone glass for tricolour picture tube and preparation method thereof |
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2017
- 2017-12-04 CN CN201711258600.8A patent/CN107814483A/en active Pending
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1275118A (en) * | 1998-09-04 | 2000-11-29 | 日本电气硝子株式会社 | CRT bulb glass containing PBO and Fe2O3 |
| CN1545719A (en) * | 2001-08-23 | 2004-11-10 | 日本电气硝子株式会社 | Funnel glass for cathode-ray tube |
| CN101781089A (en) * | 2010-01-27 | 2010-07-21 | 彩虹集团电子股份有限公司 | Cone glass for tricolour picture tube and preparation method thereof |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110386760A (en) * | 2019-08-15 | 2019-10-29 | 徐宝辰 | Glass rock powder and preparation method thereof |
| CN112299711A (en) * | 2020-11-06 | 2021-02-02 | 苏州市亿林玻璃加工制造有限公司 | Energy-saving and environment-friendly hollow glass and preparation method thereof |
| CN114262154A (en) * | 2021-12-10 | 2022-04-01 | 江苏神盾新材料科技有限公司 | Special radiation-proof glass for nuclear power station and preparation process thereof |
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Application publication date: 20180320 |