CN107803173A - A kind of high-purity chelating agent preparation facilities - Google Patents

A kind of high-purity chelating agent preparation facilities Download PDF

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Publication number
CN107803173A
CN107803173A CN201710867388.9A CN201710867388A CN107803173A CN 107803173 A CN107803173 A CN 107803173A CN 201710867388 A CN201710867388 A CN 201710867388A CN 107803173 A CN107803173 A CN 107803173A
Authority
CN
China
Prior art keywords
tank body
wall
inwall
bolted
chelating agent
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Withdrawn
Application number
CN201710867388.9A
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Chinese (zh)
Inventor
朱其军
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Funing Gather New Material Co Ltd
Original Assignee
Funing Gather New Material Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Funing Gather New Material Co Ltd filed Critical Funing Gather New Material Co Ltd
Priority to CN201710867388.9A priority Critical patent/CN107803173A/en
Publication of CN107803173A publication Critical patent/CN107803173A/en
Withdrawn legal-status Critical Current

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Classifications

    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/0006Controlling or regulating processes
    • B01J19/0013Controlling the temperature of the process
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/0053Details of the reactor
    • B01J19/0066Stirrers
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/18Stationary reactors having moving elements inside
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049Controlling or regulating processes
    • B01J2219/00051Controlling the temperature
    • B01J2219/00054Controlling or regulating the heat exchange system
    • B01J2219/00056Controlling or regulating the heat exchange system involving measured parameters
    • B01J2219/00058Temperature measurement
    • B01J2219/0006Temperature measurement of the heat exchange medium
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049Controlling or regulating processes
    • B01J2219/00051Controlling the temperature
    • B01J2219/00074Controlling the temperature by indirect heating or cooling employing heat exchange fluids
    • B01J2219/00087Controlling the temperature by indirect heating or cooling employing heat exchange fluids with heat exchange elements outside the reactor
    • B01J2219/00094Jackets
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049Controlling or regulating processes
    • B01J2219/00162Controlling or regulating processes controlling the pressure

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)

Abstract

The invention discloses a kind of high-purity chelating agent preparation facilities, including base, the bottom inwall of the base has been bolted controller, and the top outer wall of base has been bolted tank body, the bottom inwall of the tank body has been bolted temperature sensor, and the top inwall of tank body is welded with inner canister, the bottom of inner canister side outer wall offers discharging opening, and discharging opening inwall is welded with discharge nozzle, the discharge nozzle passes through tank body, and the outer wall that discharge nozzle is located at outside tank body has been bolted pressure charging valve.The present invention is by increasing temperature sensor and controller, so as to quickly raise and reduce the temperature required for production, while improving production efficiency, the quality of production of chelating agent is improved, by increasing buffer stopper, the impulsive force of water can be reduced, improve the efficiency of cooling and the heating of water, by increasing pressure charging valve, so as to quickly discharge the chelating agent in inner canister, the efficiency of production is improved.

Description

A kind of high-purity chelating agent preparation facilities
Technical field
The present invention relates to chelating agent preparing technical field, more particularly to a kind of high-purity chelating agent preparation facilities.
Background technology
Chelating agent also known as complexing agent, it is a kind of water-soluble complex that stabilization can be formed with heavy metal ion generation chelation Thing, chelating agent generate colored material by being reacted with metal ion, in the equipment of existing production chelating agent, due to basic All it is the operation for carrying out next step again by the temperature manually shown according to thermometer, can not often meets high-purity chelating agent Production requirement, and low production efficiency, it quickly can not reduce and raise the temperature required for production.
The content of the invention
The invention aims to solve shortcoming present in prior art, and a kind of high-purity chelating agent system proposed Standby device.
To achieve these goals, present invention employs following technical scheme:
A kind of high-purity chelating agent preparation facilities, including base, the bottom inwall of the base have been bolted controller, And the top outer wall of base has been bolted tank body, the bottom inwall of the tank body has been bolted TEMP Device, and the top inwall of tank body is welded with inner canister, the bottom of inner canister side outer wall offers discharging opening, and discharging opening inwall Discharge nozzle is welded with, the discharge nozzle passes through tank body, and the outer wall that discharge nozzle is located at outside tank body has been bolted supercharging Valve, the top outer wall of the tank body offers charging aperture, and charging aperture inwall is welded with feed pipe, the top outer wall of the tank body Axis line position offers opening, and the inwall that is open is socketed with bearing, and the inwall of the bearing is socketed with rotary shaft, and rotary shaft Side outer wall be welded with paddle, the top outer wall of the tank body, which is located at directly over bearing, has been bolted motor, And the output shaft of motor, with rotating axis connection, the both sides inwall of the tank body is welded with buffer stopper, and the side outer wall of tank body is opened Provided with cold water inlet, cold water inlet inwall is welded with cold water inlet, and the outer wall of the cold water inlet is consolidated by bolt Surely there is a magnetic valve, the side that the top outer wall of the base is located at tank body has been bolted water heater, and water heater goes out Mouthful end is socketed with circulation pipe, and the outer wall of the circulation pipe has been bolted booster pump, and circulation pipe away from water heater one End is socketed on the side outer wall of tank body.
Preferably, the external diameter of the inner canister is less than the external diameter of tank body, and the height of inner canister is less than the height of tank body, inner canister Both sides outer wall is welded with the second buffer stopper to match with buffer stopper.
Preferably, the quantity of the paddle is nine to ten five, and equidistant be welded on of nine to ten five paddles turns On the both sides outer wall of moving axis.
Preferably, the water inlet end of the water heater is socketed with water inlet pipe, and the one end of water inlet pipe away from water heater is socketed in Tank body is close to the bottom of the side outer wall of water heater.
Preferably, the cold water inlet is located at the same side outer wall with discharge nozzle, and cold water inlet is located at discharge nozzle Surface.
Preferably, the model DATA-7311 of the controller, and the output end of temperature sensor passes through signal wire and control Device connection processed, motor and booster pump, water heater, magnetic valve, pressure charging valve are connected with switch, switch and controller phase by wire Connection.
Beneficial effects of the present invention are:In the present invention, by increasing temperature sensor and controller, so as to quickly raise The temperature required with production is reduced, while improving production efficiency, the quality of production of chelating agent is improved, is buffered by increasing Block, the impulsive force of water can be reduced, improve the efficiency of cooling and the heating of water, by increasing pressure charging valve, so as to quickly by inner canister Interior chelating agent discharge, improve the efficiency of production.
Brief description of the drawings
Fig. 1 is a kind of structural front view of high-purity chelating agent preparation facilities proposed by the present invention;
Fig. 2 is a kind of structure top view of high-purity chelating agent preparation facilities proposed by the present invention.
In figure:1 base, 2 water heaters, 3 booster pumps, 4 circulation pipes, 5 tank bodies, 6 feed pipes, 7 motors, 8 bearings, 9 rotary shafts, 10 paddles, 11 magnetic valves, 12 cold water inlets, 13 buffer stoppers, 14 pressure charging valves, 15 discharge nozzles, 16 controllers, 17 TEMPs Device, 18 inner canisters.
Embodiment
Below in conjunction with the accompanying drawing in the embodiment of the present invention, the technical scheme in the embodiment of the present invention is carried out clear, complete Site preparation describes, it is clear that described embodiment is only part of the embodiment of the present invention, rather than whole embodiments.
Reference picture 1-2, a kind of high-purity chelating agent preparation facilities, including base 1, the bottom inwall of base 1 pass through bolt Controller 16 is fixed with, and the top outer wall of base 1 has been bolted tank body 5, the bottom inwall of tank body 5 is consolidated by bolt Surely there is temperature sensor 17, and the top inwall of tank body 5 is welded with inner canister 18, the bottom of the side outer wall of inner canister 18 offers discharging Mouthful, and discharging opening inwall is welded with discharge nozzle 15, discharge nozzle 15 passes through tank body 5, and discharge nozzle 15 is located at the outer wall outside tank body 5 Pressure charging valve 14 has been bolted, the top outer wall of tank body 5 offers charging aperture, and charging aperture inwall is welded with feed pipe 6, The top outer wall axis line position of tank body 5 offers opening, and the inwall that is open is socketed with bearing 8, and the inwall of bearing 8, which is socketed with, to be turned Moving axis 9, and the side outer wall of rotary shaft 9 is welded with paddle 10, the surface that the top outer wall of tank body 5 is located at bearing 8 pass through Bolt is fixed with motor 7, and the output shaft of motor 7 is connected with rotary shaft 9, and the both sides inwall of tank body 5 is welded with buffer stopper 13, and The side outer wall of tank body 5 offers cold water inlet, and cold water inlet inwall is welded with cold water inlet 12, cold water inlet 12 Outer wall be bolted magnetic valve 11, the side that the top outer wall of base 1 is located at tank body 5 has been bolted hot water Device 2, and the port of export of water heater 2 is socketed with circulation pipe 4, the outer wall of circulation pipe 4 has been bolted booster pump 3, and circulates The one end of pipe 4 away from water heater 2 is socketed on the side outer wall of tank body 5.
In the present invention, the external diameter of inner canister 18 is less than the external diameter of tank body 5, and the height of inner canister 18 is less than the height of tank body 5, interior The both sides outer wall of tank 18 is welded with the second buffer stopper to match with buffer stopper 13, and the quantity of paddle 10 is nine to ten five, And on the equidistant both sides outer wall for being welded on rotary shaft 9 of nine to ten five paddles 10, the water inlet end of water heater 2 is socketed with into water Pipe, and the one end of water inlet pipe away from water heater 2 is socketed in tank body 5 close to the bottom of the side outer wall of water heater 2, cold water inlet 12 are located at the same side outer wall with discharge nozzle 15, and cold water inlet 12 is located at the surface of discharge nozzle 15, the model of controller 16 For DATA-7311, and the output end of temperature sensor 17 is connected by signal wire with controller 16, motor 7 and booster pump 3, heat Hydrophone 2, magnetic valve 11, pressure charging valve 14 are connected with switch by wire, and switch is connected with controller 16.
Operation principle:By the way that chelating agent raw material is entered in inner canister 18 from feed pipe 6, then need to pass through according to temperature Water heater 2 heats the water in tank body 5, by the constantly monitoring temperature of temperature sensor 17, then passes through the rotation of motor 7 Rotary shaft 9 and paddle 10 start to rotate the raw material of stirring chelating agent, by pressure charging valve 14 by inner canister 18 after the completion of stirring Chelating agent is discharged by discharge nozzle 15.
The foregoing is only a preferred embodiment of the present invention, but protection scope of the present invention be not limited thereto, Any one skilled in the art the invention discloses technical scope in, technique according to the invention scheme and its Inventive concept is subject to equivalent substitution or change, should all be included within the scope of the present invention.

Claims (6)

1. a kind of high-purity chelating agent preparation facilities, including base(1), it is characterised in that the base(1)Bottom inwall lead to Cross bolt and be fixed with controller(16), and base(1)Top outer wall be bolted tank body(5), the tank body(5)'s Bottom inwall has been bolted temperature sensor(17), and tank body(5)Top inwall be welded with inner canister(18), it is described interior Tank(18)The bottom of side outer wall offers discharging opening, and discharging opening inwall is welded with discharge nozzle(15), the discharge nozzle(15) Through tank body(5), and discharge nozzle(15)Positioned at tank body(5)Outside outer wall has been bolted pressure charging valve(14), the tank Body(5)Top outer wall offer charging aperture, and charging aperture inwall is welded with feed pipe(6), the tank body(5)Top outer wall Axis line position offers opening, and the inwall that is open is socketed with bearing(8), the bearing(8)Inwall be socketed with rotary shaft (9), and rotary shaft(9)Side outer wall be welded with paddle(10), the tank body(5)Top outer wall be located at bearing(8)'s Surface has been bolted motor(7), and motor(7)Output shaft and rotary shaft(9)Connection, the tank body(5)Two Side inwall is welded with buffer stopper(13), and tank body(5)Side outer wall offer cold water inlet, the welding of cold water inlet inwall There is cold water inlet(12), the cold water inlet(12)Outer wall be bolted magnetic valve(11), the base(1) Top outer wall be located at tank body(5)Side be bolted water heater(2), and water heater(2)The port of export be socketed with Circulation pipe(4), the circulation pipe(4)Outer wall be bolted booster pump(3), and circulation pipe(4)Away from water heater(2) One end be socketed in tank body(5)Side outer wall on.
A kind of 2. high-purity chelating agent preparation facilities according to claim 1, it is characterised in that the inner canister(18)It is outer Footpath is less than tank body(5)External diameter, and inner canister(18)Height be less than tank body(5)Height, inner canister(18)The welding of both sides outer walls Have and buffer stopper(13)The second buffer stopper to match.
A kind of 3. high-purity chelating agent preparation facilities according to claim 1, it is characterised in that the paddle(10)'s Quantity is nine to ten five, and nine to ten five paddles(10)It is equidistant to be welded on rotary shaft(9)Both sides outer wall on.
A kind of 4. high-purity chelating agent preparation facilities according to claim 1, it is characterised in that the water heater(2)'s Water inlet end is socketed with water inlet pipe, and water inlet pipe is away from water heater(2)One end be socketed in tank body(5)Close to water heater(2)One The bottom of side outer wall.
A kind of 5. high-purity chelating agent preparation facilities according to claim 1, it is characterised in that the cold water inlet (12)With discharge nozzle(15)Positioned at the same side outer wall, and cold water inlet(12)Positioned at discharge nozzle(15)Surface.
A kind of 6. high-purity chelating agent preparation facilities according to claim 1, it is characterised in that the controller(16)'s Model DATA-7311, and temperature sensor(17)Output end pass through signal wire and controller(16)Connection, motor(7)With Booster pump(3), water heater(2), magnetic valve(11), pressure charging valve(14)Switch, switch and controller are connected with by wire (16)It is connected.
CN201710867388.9A 2017-09-22 2017-09-22 A kind of high-purity chelating agent preparation facilities Withdrawn CN107803173A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201710867388.9A CN107803173A (en) 2017-09-22 2017-09-22 A kind of high-purity chelating agent preparation facilities

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201710867388.9A CN107803173A (en) 2017-09-22 2017-09-22 A kind of high-purity chelating agent preparation facilities

Publications (1)

Publication Number Publication Date
CN107803173A true CN107803173A (en) 2018-03-16

Family

ID=61584492

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201710867388.9A Withdrawn CN107803173A (en) 2017-09-22 2017-09-22 A kind of high-purity chelating agent preparation facilities

Country Status (1)

Country Link
CN (1) CN107803173A (en)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108435028A (en) * 2018-04-23 2018-08-24 长安大学 A kind of use for laboratory modified pitch automation preparation facilities

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108435028A (en) * 2018-04-23 2018-08-24 长安大学 A kind of use for laboratory modified pitch automation preparation facilities

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Application publication date: 20180316