CN107790076A - Industrial chemicals production reaction vessel - Google Patents

Industrial chemicals production reaction vessel Download PDF

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Publication number
CN107790076A
CN107790076A CN201610763727.4A CN201610763727A CN107790076A CN 107790076 A CN107790076 A CN 107790076A CN 201610763727 A CN201610763727 A CN 201610763727A CN 107790076 A CN107790076 A CN 107790076A
Authority
CN
China
Prior art keywords
housing
industrial chemicals
reaction vessel
upper cover
chemicals production
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201610763727.4A
Other languages
Chinese (zh)
Inventor
陈小勇
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Jiangsu Jihua Chemical Co Ltd
Original Assignee
Jiangsu Jihua Chemical Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Jiangsu Jihua Chemical Co Ltd filed Critical Jiangsu Jihua Chemical Co Ltd
Priority to CN201610763727.4A priority Critical patent/CN107790076A/en
Publication of CN107790076A publication Critical patent/CN107790076A/en
Pending legal-status Critical Current

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Classifications

    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/0006Controlling or regulating processes
    • B01J19/002Avoiding undesirable reactions or side-effects, e.g. avoiding explosions, or improving the yield by suppressing side-reactions
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D46/00Filters or filtering processes specially modified for separating dispersed particles from gases or vapours
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D53/00Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/0053Details of the reactor
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/0053Details of the reactor
    • B01J19/006Baffles
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00761Details of the reactor
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00761Details of the reactor
    • B01J2219/00763Baffles
    • B01J2219/00765Baffles attached to the reactor wall
    • B01J2219/0077Baffles attached to the reactor wall inclined
    • B01J2219/00774Baffles attached to the reactor wall inclined in the form of cones

Landscapes

  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Analytical Chemistry (AREA)
  • General Chemical & Material Sciences (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Physical Or Chemical Processes And Apparatus (AREA)

Abstract

The present invention relates to industrial chemicals production reaction vessel, including:Housing, upper cover and low head;The enclosure interior is provided with conical plate, and the conical plate upper end is connected with gas collection pipe, and the gas collection pipe is connected after overhanging housing with pneumatic filter, and the pneumatic filter is fixedly connected with housing;The upper cover top is provided with reaction-ure inlet, and the upper cover upper end is additionally provided with liquid level observing mouth;The low head bottom is provided with reactant exit, and the reactant exit upper end is provided with stop valve;The present invention can be good at pernicious gas caused by absorbing reaction by setting conical plate inside apparatus casing;By setting pneumatic filter, discharged after filtration treatment can be carried out to pernicious gas well, there is good environmental-protection function;By setting liquid level observing mouth, the control of enclosure interior reaction solution height can be conveniently carried out, prevents solution from flooding conical plate, influences reaction process;Structure of the present invention is relatively simple, and practicality is higher, is adapted to promote the use of.

Description

Industrial chemicals production reaction vessel
Technical field
The present invention relates to field of chemical equipment, specifically industrial chemicals production reaction vessel.
Background technology
Reactor is the equipment for realizing course of reaction, is widely used in the industrial departments such as chemical industry, oil refining, metallurgy, light industry.Change Reaction engineering is learned using the course of reaction carried out in industrial reactor as research object, reactor number is established with mathematical model method Model is learned, influence and reactor dynamic characteristic and reactor parameter of the research reactor transmittance process to chemical reaction are sensitive Property, to realize the Reliable Design of industrial reactor and operational control.For realize single liquid phase course of reaction and liquid liquid, gas-liquid, The heterogeneous reaction process such as liquid is solid, gas-liquid-solid.Being set up in device has stirring(Mechanical agitation, airflow stirring etc.)Device.Ratio of height to diameter compared with When big, multiple impellers leaf can be used.When material need to be heated or cooled during the course of the reaction, chuck can be set at reactor wall, Or heat-transfer surface is set in device, it can also be exchanged heat by outer circulation;Existing reaction vessel is raw during medium reacts Tend not to be handled well during into unnecessary pernicious gas, some enterprises are directly by pernicious gas caused by reaction to sky Discharge, seriously pollutes air.
Based on above reason, it is necessary to which a kind of industrial chemicals production is devised with reaction vessel, by apparatus casing Inside sets conical plate, while promoting reaction fully to carry out, can be good at pernicious gas caused by absorbing reaction;Pass through Pneumatic filter is set, is being discharged after filtration treatment can be carried out to pernicious gas well, there is good environmental-protection function;Pass through Liquid level observing mouth is set, the control of enclosure interior reaction solution height can be conveniently carried out, prevent solution from flooding conical plate, influence Reaction process;That is industrial chemicals production reaction vessel.
The content of the invention
In order to solve technical problem existing for above-mentioned existing chemical reaction container, the invention provides industrial chemicals production to use Reaction vessel.
The technical solution adopted for the present invention to solve the technical problems is:
Industrial chemicals production reaction vessel, including:Housing, upper cover and low head, the upper cover and housing, low head and Housing is welded to connect by automatic welding;The enclosure interior is provided with conical plate, and the conical plate is fixed by gusset In enclosure interior, the conical plate upper end is connected with gas collection pipe, and the gas collection pipe is overhang after housing and pneumatic filter Connection, the pneumatic filter are fixedly connected with housing;The pneumatic filter upper end is provided with gas outlet;The upper cover top End is provided with the first reaction-ure inlet, and the first reaction-ure inlet side is provided with the second reaction-ure inlet, the upper cover Upper end is additionally provided with liquid level observing mouth;The low head bottom is provided with reactant exit, the reactant exit upper end installation There is stop valve, the housing lower end is fixedly installed supporting leg, and the supporting leg lower end is fixedly installed backing plate.
As the preferred scheme of the present invention, when being welded between the housing and upper cover, low head, docking port unfitness of butt joint is small In 5mm, ensure good molding effect, prevent stress corrosion;The housing and upper cover, low head by automatic welding weld into Row welding, has good weld integrity.
As the preferred scheme of the present invention, the pneumatic filter is built-in with detection of poison gas and cleaning system, pernicious gas By carrying out putting idle discharge again after detecting system detection is qualified after cleaning system.
As the preferred scheme of the present invention, the conical plate opening is 150 ° of subtended angles, is had by calculating 150 ° of opening angles There is good liquid separation ability, also allow for carrying out the collection of gas well.
As the preferred scheme of the present invention, the gas outlet is arranged to 90 ° of elbow structures, convenient to carry out with discharge duct pair Connect gas transmission.
As the preferred scheme of the present invention, the supporting leg is made up of I-steel, has good non-deformability.
As the preferred scheme of the present invention, the liquid level observing mouth is coated toughened glass with filter, is had resistance to well Corrosive nature, corrosion of long-term use of enclosure interior gas to filter is prevented, reduce filter service life.
As the present invention preferred scheme, first reaction-ure inlet and the second reaction-ure inlet be arranged on it is same enter It on mouth pipeline, can be reacted when entering enclosure interior at the beginning of reactant, then be shunted by conical plate, can fully improve reactant Contact area.
The beneficial effects of the invention are as follows:Industrial chemicals production reaction vessel, by setting taper inside apparatus casing Plate, while promoting to react fully progress, it can be good at pernicious gas caused by absorbing reaction;By setting gas filtration Device, discharged after filtration treatment can be carried out to pernicious gas well, there is good environmental-protection function;By setting liquid level observing Mouthful, the control of enclosure interior reaction solution height can be conveniently carried out, prevents solution from flooding conical plate, influences reaction process;This Inventive structure is relatively simple, and practicality is higher, is adapted to promote the use of.
Brief description of the drawings
The present invention is further described with reference to the accompanying drawings and examples.
Fig. 1 is the structural representation of the present invention.
In figure:1st, housing, 2, upper cover, 3, low head, 4, pneumatic filter, 5, conical plate, 6, gusset, 7, discharge Road, 8, gas outlet, the 9, first reaction-ure inlet, the 10, second reaction-ure inlet, 11, reactant exit, 12, stop valve, 13, branch Leg, 14, backing plate, 15, liquid level observing mouth.
Embodiment
In order to make the purpose , technical scheme and advantage of the present invention be clearer, it is right below in conjunction with drawings and Examples The present invention is further elaborated.It should be appreciated that the specific embodiments described herein are merely illustrative of the present invention, and It is not used in the restriction present invention.
As shown in figure 1, industrial chemicals production reaction vessel of the present invention, including:Housing 1, upper cover 2 and lower envelope First 3, the upper cover 2 and housing 1, low head 3 and housing 1 are welded to connect by automatic welding;Set inside the housing 1 Conical plate 5 is equipped with, the conical plate 5 is fixed on inside housing 1 by gusset 6, and the upper end of conical plate 5 is connected with gas collection pipe 7, the gas collection pipe 7 is connected after overhanging housing 1 with pneumatic filter 4, and the pneumatic filter 4 is fixedly connected with housing 1; The upper end of pneumatic filter 4 is provided with gas outlet 8;The top of upper cover 2 is provided with the first reaction-ure inlet 9, and described The side of one reaction-ure inlet 9 is provided with the second reaction-ure inlet 10, and the upper end of upper cover 2 is additionally provided with liquid level observing mouth 15; The bottom of low head 3 is provided with reactant exit 11, and the upper end of reactant exit 11 is provided with stop valve 12, the housing 1 lower end is fixedly installed supporting leg 13, and the lower end of supporting leg 13 is fixedly installed backing plate 14.
When being welded between the housing 1 and upper cover 2, low head 3, docking port unfitness of butt joint is less than 5mm, ensure well into Type effect, prevents stress corrosion;The housing 1 and upper cover 2, low head 3 are welded by automatic welding, are had fine Weld integrity.
The pneumatic filter 4 is built-in with detection of poison gas and cleaning system, pernicious gas by after cleaning system through detection Carry out putting idle discharge again after system detectio is qualified.
The opening of conical plate 5 is 150 ° of subtended angles, has good liquid separation ability by calculating 150 ° of opening angles, also just In the collection for carrying out gas well.
The gas outlet 8 is arranged to 90 ° of elbow structures, convenient to carry out docking gas transmission with discharge duct.
The supporting leg 13 is made up of I-steel, has good non-deformability.
The liquid level observing mouth 15 is coated toughened glass with filter, has good decay resistance, prevents from making for a long time With corrosion of the internal gas of housing 1 to filter, filter service life is reduced.
The reaction-ure inlet 10 of first reaction-ure inlet 9 and second is arranged on same inlet pipeline, in reactant It can be reacted when just entering 1 inside of housing, then be shunted by conical plate 5, can fully improve the contact area of reactant.
General principle, principal character and the advantages of the present invention of the present invention has been shown and described above.The technology of the industry Personnel are it should be appreciated that the present invention is not limited to the above embodiments, and the simply explanation described in above-described embodiment and specification is originally The principle of invention, without departing from the spirit and scope of the present invention, various changes and modifications of the present invention are possible, these changes Change and improvement all fall within the protetion scope of the claimed invention.The claimed scope of the invention by appended claims and its Equivalent thereof.

Claims (8)

1. industrial chemicals production reaction vessel, it is characterised in that:Including housing(1), upper cover(2)And low head(3), it is described Upper cover (2) and housing (1), low head (3) and housing (1) are welded to connect by automatic welding;The housing (1) is internal Conical plate (5) is provided with, the conical plate (5) is fixed on housing (1) inside by gusset (6), and conical plate (5) upper end connects Gas collection pipe (7) is connected to, the gas collection pipe (7) overhangs housing (1) and connected afterwards with pneumatic filter (4), the gas mistake Filter (4) is fixedly connected with housing (1);Pneumatic filter (4) upper end is provided with gas outlet (8);Upper cover (2) top End is provided with the first reaction-ure inlet (9), and the first reaction-ure inlet (9) side is provided with the second reaction-ure inlet (10), Upper cover (2) upper end is additionally provided with liquid level observing mouth (15);Low head (3) bottom is provided with reactant exit (11), reactant exit (11) upper end is provided with stop valve (12), the housing(1)Lower end is fixedly installed supporting leg (13), the supporting leg(13)Lower end is fixedly installed backing plate(14).
2. industrial chemicals production reaction vessel according to claim 1, it is characterised in that:The housing(1)With upper envelope Head(2), low head(3)Between when welding, docking port unfitness of butt joint is less than 5mm;The housing(1)And upper cover(2), low head (3)Welded by automatic welding.
3. industrial chemicals production reaction vessel according to claim 1, it is characterised in that:The pneumatic filter(4) It is built-in with detection of poison gas and cleaning system.
4. industrial chemicals production reaction vessel according to claim 1, it is characterised in that:The conical plate(5)Opening For 150 ° of subtended angles.
5. industrial chemicals production reaction vessel according to claim 1, it is characterised in that:The gas outlet(8)Set For 90 ° of elbow structures.
6. industrial chemicals production reaction vessel according to claim 1, it is characterised in that:The supporting leg(13)For I-shaped Steel is made.
7. industrial chemicals production reaction vessel according to claim 1, it is characterised in that:The liquid level observing mouth(15) It is coated toughened glass with filter.
8. industrial chemicals production reaction vessel according to claim 1, it is characterised in that:First reaction-ure inlet (9)With the second reaction-ure inlet(10)It is arranged on same inlet pipeline.
CN201610763727.4A 2016-08-30 2016-08-30 Industrial chemicals production reaction vessel Pending CN107790076A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201610763727.4A CN107790076A (en) 2016-08-30 2016-08-30 Industrial chemicals production reaction vessel

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201610763727.4A CN107790076A (en) 2016-08-30 2016-08-30 Industrial chemicals production reaction vessel

Publications (1)

Publication Number Publication Date
CN107790076A true CN107790076A (en) 2018-03-13

Family

ID=61528187

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201610763727.4A Pending CN107790076A (en) 2016-08-30 2016-08-30 Industrial chemicals production reaction vessel

Country Status (1)

Country Link
CN (1) CN107790076A (en)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109499215A (en) * 2018-12-29 2019-03-22 上海华林工业气体有限公司 A kind of chemical plant facility or power plants equipment gas safety environment protection emission device

Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN204973880U (en) * 2015-07-29 2016-01-20 天津琛琛科技有限公司 Novel living beings reactor
CN105561881A (en) * 2016-03-10 2016-05-11 黄斌 Efficient reaction kettle with vibration absorption device

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN204973880U (en) * 2015-07-29 2016-01-20 天津琛琛科技有限公司 Novel living beings reactor
CN105561881A (en) * 2016-03-10 2016-05-11 黄斌 Efficient reaction kettle with vibration absorption device

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109499215A (en) * 2018-12-29 2019-03-22 上海华林工业气体有限公司 A kind of chemical plant facility or power plants equipment gas safety environment protection emission device

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Application publication date: 20180313

WD01 Invention patent application deemed withdrawn after publication