CN107779795A - The double_stage guide heat riser and method of a kind of aluminium alloy thick plate - Google Patents

The double_stage guide heat riser and method of a kind of aluminium alloy thick plate Download PDF

Info

Publication number
CN107779795A
CN107779795A CN201610775544.4A CN201610775544A CN107779795A CN 107779795 A CN107779795 A CN 107779795A CN 201610775544 A CN201610775544 A CN 201610775544A CN 107779795 A CN107779795 A CN 107779795A
Authority
CN
China
Prior art keywords
temperature
burner hearth
slab
solid solubility
aluminium alloy
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201610775544.4A
Other languages
Chinese (zh)
Inventor
邓运来
范世通
龙涛
张研
黄心悦
欧世声
徐进军
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Central South University
Original Assignee
Central South University
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Central South University filed Critical Central South University
Priority to CN201610775544.4A priority Critical patent/CN107779795A/en
Publication of CN107779795A publication Critical patent/CN107779795A/en
Pending legal-status Critical Current

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C22METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22FCHANGING THE PHYSICAL STRUCTURE OF NON-FERROUS METALS AND NON-FERROUS ALLOYS
    • C22F1/00Changing the physical structure of non-ferrous metals or alloys by heat treatment or by hot or cold working
    • C22F1/04Changing the physical structure of non-ferrous metals or alloys by heat treatment or by hot or cold working of aluminium or alloys based thereon
    • CCHEMISTRY; METALLURGY
    • C21METALLURGY OF IRON
    • C21DMODIFYING THE PHYSICAL STRUCTURE OF FERROUS METALS; GENERAL DEVICES FOR HEAT TREATMENT OF FERROUS OR NON-FERROUS METALS OR ALLOYS; MAKING METAL MALLEABLE, e.g. BY DECARBURISATION OR TEMPERING
    • C21D9/00Heat treatment, e.g. annealing, hardening, quenching or tempering, adapted for particular articles; Furnaces therefor
    • C21D9/0056Furnaces through which the charge is moved in a horizontal straight path
    • CCHEMISTRY; METALLURGY
    • C21METALLURGY OF IRON
    • C21DMODIFYING THE PHYSICAL STRUCTURE OF FERROUS METALS; GENERAL DEVICES FOR HEAT TREATMENT OF FERROUS OR NON-FERROUS METALS OR ALLOYS; MAKING METAL MALLEABLE, e.g. BY DECARBURISATION OR TEMPERING
    • C21D9/00Heat treatment, e.g. annealing, hardening, quenching or tempering, adapted for particular articles; Furnaces therefor
    • C21D9/0081Heat treatment, e.g. annealing, hardening, quenching or tempering, adapted for particular articles; Furnaces therefor for slabs; for billets

Landscapes

  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Physics & Mathematics (AREA)
  • Thermal Sciences (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Mechanical Engineering (AREA)
  • Materials Engineering (AREA)
  • Metallurgy (AREA)
  • Organic Chemistry (AREA)
  • Heat Treatments In General, Especially Conveying And Cooling (AREA)

Abstract

The invention discloses the double_stage guide heat riser and method of a kind of aluminium alloy thick plate, solution heat device is roller-hearth solution furnace, is divided into medium temperature solid solution burner hearth and high temperature solid solution burner hearth.First medium temperature solid solution burner hearth is heated to being far above first order solid solubility temperature, high temperature solid solution burner hearth is heated to be far above second level solid solubility temperature;Then aluminium alloy thick plate is put into medium temperature solid solution burner hearth, until slab temperature is warming up to first order solid solubility temperature, then fire box temperature is quickly down to the insulation of first order solid solubility temperature;Slab finally is transferred into high temperature solid solution burner hearth to continue to heat up, when slab temperature is warming up to two level solid solubility temperature, fire box temperature is reduced to the insulation of two level solid solubility temperature.Aluminium alloy thick plate temperature fast and efficiently can be heated to solid solubility temperature by the present invention, reduce heat treatment time, improve production efficiency, while can avoid the performance loss caused by long-time heating.The process is easy to operate, cost-effective, has actual industrial production application value.

Description

The double_stage guide heat riser and method of a kind of aluminium alloy thick plate
Technical field
The present invention relates to a kind of heat treatment method of aluminium alloy thick plate, belongs to nonferrous materials and its hot-working field.
Background technology
Aluminium alloy thick plate is because it is in the comprehensive advantage of manufacturing cost, structure loss of weight and formability etc., in aviation, boat My god, be widely used in the important lightweight overall structure such as navigation and communications and transportation.Industrial aluminium alloy plate is generally dissolved Can enhanced type aluminium alloy, it is necessary to by being dissolved, quenching, the solid solution craft such as timeliness obtain high intensity, high tenacity and decay resistance. For aluminium alloy thick plate, double_stage guide solid solution system can separate out Al in advance in the solid solution stage3Zr particles, it can effectively suppress to tie again Crystalline substance, to improve its mechanical property.Existing double_stage guide temperature-rising method does not consider the heating hesitation of big slab typically, directly will Furnace gas temperature is warming up to target solid solubility temperature, and now, aluminium alloy thick plate temperature will be far below target solid solubility temperature, is unable to reach double The effect of level solid solution.And this programming rate is excessively slow, to reach solid solubility temperature, it is necessary to can significantly extend the heating-up time, reduce Production efficiency.Meanwhile long-time heat preservation may cause grain structure to grow up at high temperature, material property is reduced.
Structural member manufactured by high-performance aluminium alloy slab is the important light weight such as Aeronautics and Astronautics, navigation and communications and transportation Change integrally-built key position, its performance and uniformity govern such component load-bearing ability and safety of being on active service.With current The development of such aluminium alloy structure tends to big specification integration and high combination property, the solid solution work to large-size aluminum alloy slab Skill proposes new challenge.Double_stage guide method can effectively improve the mechanical property of aluminium alloy thick plate.Therefore, a kind of essence of invention Really this solid solution system effectively can be applied to industrial production by the double_stage guide method of being rapidly heated of control aluminium alloy thick plate temperature, Be of great practical significance.
The content of the invention
A kind of the fast of accurate control aluminium alloy thick plate temperature is provided it is an object of the invention to overcome prior art deficiency Fast temperature-rising method.
The purpose of the present invention is realized by the following method:The double_stage guide heat riser and method of a kind of aluminium alloy thick plate, Characterized in that, solution heat device is roller-hearth solution furnace, it is divided into two parts of medium temperature solid solution burner hearth and high temperature solid solution burner hearth, Medium temperature solid solution burner hearth is heated to first higher than the first order solid solubility temperature 20-300 °C, high temperature solid solution burner hearth is heated to than the Two level solid solubility temperature is high 20-200 °C;Then aluminium alloy thick plate is put into medium temperature solid solution burner hearth, until slab temperature is warming up to the One-level solid solubility temperature, then fire box temperature is quickly down to the insulation of first order solid solubility temperature;Slab is finally transferred to high temperature solid solution Burner hearth continues to heat up, and when slab temperature is warming up to two level solid solubility temperature, fire box temperature is reduced to the insulation of two level solid solubility temperature; Slab reaches the time of the first order and second level solid solubility temperature by formula:It is determined that in formula,T f For furnace gas temperature,T 0 For slab initial temperature,TFor solid solubility temperature,AIt is 9.8 × 10 for constant value-6-1.0×10-3,t Reach the time of solid solubility temperature for slab.
Methods described, the thickness of described aluminium alloy thick plate is 4-650mm.
Methods described, the heat-treatment temperature range of described aluminium alloy thick plate is 300-550 DEG C.
The present invention has considered below in technological design:In slab temperature-rise period, furnace gas and slab remain very The big temperature difference, it is ensured that slab is all the time in the state that is rapidly heated;Slab directly can accurately be calculated using formula and reach solid solution The time of temperature, fast cooling now is carried out to furnace gas, can effectively place slab burning;Slab is dissolved in burner hearth at two OK, it can remain that fire box temperature is in same temperature section, the thermal loss of burner hearth heating and cooling can be reduced, while greatly improve Production efficiency.
The invention has the advantages that:1. furnace gas temperature is far above solid solubility temperature, the programming rate of slab can be effectively improved.It is 2. thick When plate is warming up to target solid solubility temperature soon, still there is the temperature difference in furnace gas and slab, and plate temperature can be made to be quickly ramped up to target temperature.3. stove In the gas fast cooling stage, furnace gas temperature can be made to be reduced to solid solubility temperature, slab burning can be prevented.4. because the heating-up time significantly subtracts Few, material grains caused by the heating-up time can be prevented long are grown up, and can effectively improve component performance.5. double_stage guide processing exists Carried out in two burner hearths, heating and cooling time and thermal loss can be reduced, greatly improved production capacity and production efficiency, reduce cost. 6. the process is easy to operate, there is actual industrial production application value.
Brief description of the drawings
Fig. 1 is the furnace gas of Processing Example 1 of the present invention and the temperature-rise period of slab.Fig. 2 is not using present invention processing pair The furnace gas of ratio 1 and the temperature-rise period of slab.Fig. 3 is the furnace gas of Processing Example 2 of the present invention and the temperature-rise period of slab.Fig. 4 It is not using the furnace gas of present invention processing comparative example 2 and the temperature-rise period of slab.Fig. 5 is present invention process schematic diagram.
Embodiment
The present invention is intended to further illustrate with reference to embodiments, is not intended to limit the present invention.
Embodiment
Aluminium alloy thick plate material is 7085 aluminium alloys, and size is:3000×1200×180mm.Slab is placed in two Double_stage guide processing (300 DEG C/30min+480 DEG C/30min) is carried out in the roller hearth type heating furnace of individual burner hearth:TakeABe worth for 2.2 × 10-4, calculated according to formula, be first dissolved in the medium temperature that furnace gas temperature is 450 DEG C in burner hearth and be incubated 70min, then fast cooling is to 300 DEG C, it is incubated 30min;Then fast transfer to the high-temperature burner hearth that furnace gas temperature is 570 DEG C is incubated 46min, then fast cooling is to 480 DEG C, it is incubated 30min.The temperature-rise period of furnace gas and slab, is shown in Fig. 3.
Comparative example 1
Aluminium alloy thick plate material is 7085 aluminium alloys, and size is:3000×1200×180mm.Slab is placed in an only stove Double_stage guide processing (300 DEG C/30min+480 DEG C/30min) is carried out in the roller hearth type heating furnace of thorax:Furnace gas is first warming up to 452 DEG C, then fast cooling is to 300 DEG C, is incubated 30min;570 DEG C are warming up to, then fast cooling is incubated 30min to 480 DEG C.Furnace gas and The temperature-rise period of slab, is shown in Fig. 2.
Comparative example 2
Aluminium alloy thick plate material is 7085 aluminium alloys, and size is:3000×1200×180mm.Slab is placed in an only stove Double_stage guide processing (300 DEG C/30min+480 DEG C/30min) is carried out in the roller hearth type heating furnace of thorax:Furnace gas is first warming up to 300 DEG C, it is incubated 30min;480 DEG C are warming up to again, are incubated 30min.The temperature-rise period of furnace gas and slab, is shown in Fig. 3.

Claims (3)

1. the double_stage guide heat riser and method of a kind of aluminium alloy thick plate, it is characterised in that solution heat device is roller-bottom type Solid solution furnace, it is divided into two parts of medium temperature solid solution burner hearth and high temperature solid solution burner hearth, medium temperature solid solution burner hearth is heated to than first first Level solid solubility temperature is high 20-300 °C, and high temperature solid solution burner hearth is heated to higher than the second level solid solubility temperature 20-200 °C;Then will Aluminium alloy thick plate is put into medium temperature solid solution burner hearth, until slab temperature is warming up to first order solid solubility temperature, then fire box temperature is quick It is down to the insulation of first order solid solubility temperature;Slab finally is transferred into high temperature solid solution burner hearth to continue to heat up, when slab temperature is warming up to During two level solid solubility temperature, fire box temperature is reduced to the insulation of two level solid solubility temperature;Slab reaches the first order and second level solid solution temperature The time of degree is by formula:It is determined that in formula,T f For furnace gas temperature,T 0 For slab initial temperature,T For solid solubility temperature,AIt is 9.8 × 10 for constant value-6-1.0×10-3,tReach the time of solid solubility temperature for slab.
2. according to the method for claim 1, it is characterised in that the thickness of the aluminium alloy thick plate is 4-650mm.
3. according to the method for claim 1, it is characterised in that the solid solubility temperature scope of the aluminium alloy thick plate is 300- 550℃。
CN201610775544.4A 2016-08-31 2016-08-31 The double_stage guide heat riser and method of a kind of aluminium alloy thick plate Pending CN107779795A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201610775544.4A CN107779795A (en) 2016-08-31 2016-08-31 The double_stage guide heat riser and method of a kind of aluminium alloy thick plate

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201610775544.4A CN107779795A (en) 2016-08-31 2016-08-31 The double_stage guide heat riser and method of a kind of aluminium alloy thick plate

Publications (1)

Publication Number Publication Date
CN107779795A true CN107779795A (en) 2018-03-09

Family

ID=61450253

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201610775544.4A Pending CN107779795A (en) 2016-08-31 2016-08-31 The double_stage guide heat riser and method of a kind of aluminium alloy thick plate

Country Status (1)

Country Link
CN (1) CN107779795A (en)

Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1600466A (en) * 2004-10-14 2005-03-30 北京科技大学 Method for preparing block of nano aluminum alloy in ultrahigh strength
CN102936708A (en) * 2012-11-23 2013-02-20 江苏常铝铝业股份有限公司 Aluminum alloy material temperature difference proportion annealing technique

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1600466A (en) * 2004-10-14 2005-03-30 北京科技大学 Method for preparing block of nano aluminum alloy in ultrahigh strength
CN102936708A (en) * 2012-11-23 2013-02-20 江苏常铝铝业股份有限公司 Aluminum alloy material temperature difference proportion annealing technique

Similar Documents

Publication Publication Date Title
CN103695659B (en) A kind of method improving nickel base superalloy purity
CN104630722B (en) A kind of method preparing ORC at tantalum alloy material surface
CN104745867A (en) High-temperature-resistant titanium alloy plate
CN104313298B (en) A kind of cold charge heating means of Continuous Casting Bloom of Bearing Steel
CN102517529A (en) Vacuum heat treatment process of cold rolled titanium strip coil for plate heat exchanger
CN103480657A (en) Roller preheating and heat-insulation system
CN107779795A (en) The double_stage guide heat riser and method of a kind of aluminium alloy thick plate
CN101269383A (en) Hot working method for smelting molybdenum rhenium alloy casting ingot by suspending
CN107937841A (en) A kind of aluminium alloy single-stage is dissolved the method that is rapidly heated
CN104099542B (en) The heat treatment method of aluminium alloy heavy forging
CN105441838B (en) Improve the heat treatment method of 2 ××× T3 plate fatigue crack growth rates
CN105583251A (en) Forging method for large-size Inconel690 alloy bar
CN105483602B (en) A kind of heating means for reducing heavy rail decarburized layer
CN107663617A (en) A kind of aluminium alloy double_stage guide is rapidly heated method with stove
CN107586998A (en) A kind of high temperature resistant titanium alloy plate and its method for annealing
CN102095310B (en) Dual-chamber dual-temperature pipe type atmosphere comprehensive resistance furnace and using method thereof
CN103882195A (en) Heat treatment technique for normalizing and tempering ZG275-485H steel
CN103882196A (en) Heat treatment technique for normalizing and tempering ZG35Mn steel
CN110872661A (en) High-temperature-resistant titanium alloy plate and preparation method thereof
CN204203806U (en) The cascade temperature control system of a kind of horse not heat-treatment furnace
CN107746912A (en) Metalwork anti-deformation Technology for Heating Processing
CN204795658U (en) Hot plate of vapourizing furnace
CN102041362B (en) Isothermal spheroidizing annealing furnace for bearing steels
JP5526648B2 (en) Metal slab heating method
CN203824325U (en) Energy-saving heating furnace for heat treatment of cast balls

Legal Events

Date Code Title Description
PB01 Publication
PB01 Publication
SE01 Entry into force of request for substantive examination
SE01 Entry into force of request for substantive examination
RJ01 Rejection of invention patent application after publication

Application publication date: 20180309

RJ01 Rejection of invention patent application after publication