CN107778410A - A kind of sealed damp-proof medicine bottle water-absorbing resin - Google Patents
A kind of sealed damp-proof medicine bottle water-absorbing resin Download PDFInfo
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- CN107778410A CN107778410A CN201710865445.XA CN201710865445A CN107778410A CN 107778410 A CN107778410 A CN 107778410A CN 201710865445 A CN201710865445 A CN 201710865445A CN 107778410 A CN107778410 A CN 107778410A
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- Prior art keywords
- sweet potato
- water
- potato powder
- bottle
- absorbing resin
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
- C08F251/00—Macromolecular compounds obtained by polymerising monomers on to polysaccharides or derivatives thereof
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B65—CONVEYING; PACKING; STORING; HANDLING THIN OR FILAMENTARY MATERIAL
- B65D—CONTAINERS FOR STORAGE OR TRANSPORT OF ARTICLES OR MATERIALS, e.g. BAGS, BARRELS, BOTTLES, BOXES, CANS, CARTONS, CRATES, DRUMS, JARS, TANKS, HOPPERS, FORWARDING CONTAINERS; ACCESSORIES, CLOSURES, OR FITTINGS THEREFOR; PACKAGING ELEMENTS; PACKAGES
- B65D39/00—Closures arranged within necks or pouring openings or in discharge apertures, e.g. stoppers
- B65D39/04—Cup-shaped plugs or like hollow flanged members
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B65—CONVEYING; PACKING; STORING; HANDLING THIN OR FILAMENTARY MATERIAL
- B65D—CONTAINERS FOR STORAGE OR TRANSPORT OF ARTICLES OR MATERIALS, e.g. BAGS, BARRELS, BOTTLES, BOXES, CANS, CARTONS, CRATES, DRUMS, JARS, TANKS, HOPPERS, FORWARDING CONTAINERS; ACCESSORIES, CLOSURES, OR FITTINGS THEREFOR; PACKAGING ELEMENTS; PACKAGES
- B65D53/00—Sealing or packing elements; Sealings formed by liquid or plastics material
- B65D53/02—Collars or rings
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B65—CONVEYING; PACKING; STORING; HANDLING THIN OR FILAMENTARY MATERIAL
- B65D—CONTAINERS FOR STORAGE OR TRANSPORT OF ARTICLES OR MATERIALS, e.g. BAGS, BARRELS, BOTTLES, BOXES, CANS, CARTONS, CRATES, DRUMS, JARS, TANKS, HOPPERS, FORWARDING CONTAINERS; ACCESSORIES, CLOSURES, OR FITTINGS THEREFOR; PACKAGING ELEMENTS; PACKAGES
- B65D81/00—Containers, packaging elements, or packages, for contents presenting particular transport or storage problems, or adapted to be used for non-packaging purposes after removal of contents
- B65D81/24—Adaptations for preventing deterioration or decay of contents; Applications to the container or packaging material of food preservatives, fungicides, pesticides or animal repellants
- B65D81/26—Adaptations for preventing deterioration or decay of contents; Applications to the container or packaging material of food preservatives, fungicides, pesticides or animal repellants with provision for draining away, or absorbing, or removing by ventilation, fluids, e.g. exuded by contents; Applications of corrosion inhibitors or desiccators
- B65D81/264—Adaptations for preventing deterioration or decay of contents; Applications to the container or packaging material of food preservatives, fungicides, pesticides or animal repellants with provision for draining away, or absorbing, or removing by ventilation, fluids, e.g. exuded by contents; Applications of corrosion inhibitors or desiccators for absorbing liquids
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- Engineering & Computer Science (AREA)
- Mechanical Engineering (AREA)
- Chemical & Material Sciences (AREA)
- Health & Medical Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Organic Chemistry (AREA)
- Food Science & Technology (AREA)
- Medical Preparation Storing Or Oral Administration Devices (AREA)
- Solid-Sorbent Or Filter-Aiding Compositions (AREA)
- Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
Abstract
The invention discloses a kind of sealed damp-proof medicine bottle water-absorbing resin, the preparation method of described Water-absorbing high polymer are as follows：Step 1：Sweet potato is removed the peel, dry, crush, ground, sweet potato powder is made, and is washed with akaline liquid under conditions of normal pressure, 100 DEG C 120 DEG C, wash time is 120 150min, the specific time is adjusted according to different sweet potato surface naturies, filters, dries after washing.Step 2：Surface activation process is carried out to the sweet potato powder after step 1 with activator, activator is well mixed with sweet potato powder, at ambient pressure, the sweet potato powder after 50 100 DEG C of reactions, 68 hours obtained activation modifications.Step 3：By the uniformly mixing of the sweet potato powder after step 1, ethylacrylic acid, 100 200 parts of water, 0.1 2 parts of lauroyl peroxide, reacted 15 hours at 50 100 DEG C of normal pressure, products therefrom is dried, Water-absorbing high polymer is made.
Description
Technical field
The present invention relates to field of medical products, is specifically a kind of medicine bottle.
Background technology
In daily life, the easily moisture absorption medicament such as bottled solid-state, powder state reagent, medicine, microbiology dehydrated medium exists
Different degrees of deliquescence, caking or oxidation deterioration etc. are tended to occur after unpacking and can not be continuing with.Cause very big waste.It is existing
In some technologies, mainly sealed using three kinds of modes；The first uses and drier is placed in bottle, or sets and put in bottle cap
The hothouse of desiccant bag is put, by the suction-operated of drier, removes the moisture in medicine bottle, but this mode needs additionally to add
Add drier, although this mode drying effect is good, the drier additionally placed adds cost of drugs, also occupies medicine
Limited space in bottle, and whole Transporting weight is added, thus it is unfavorable for the reduction of production and transportation cost；Be for second
Bottleneck is sealed with aluminium film, and is needed to open aluminium film when in use and could be taken out material, with opening for aluminium film, is again sealed off effect
And can not ensure, aluminium film sealing adds a procedure, increases workload；It is exactly to use bottle stopper side that the third is the most frequently used
Formula, by being to fill in bottleneck to be sealed by bottle stopper, but sealing bottle cork is not easily taken out, it is necessary to by instrument.
The content of the invention
It is an object of the invention to：For above-mentioned problem, there is provided a kind of biological medicine bottle, there is excellent sealing
Property, and then the performance with excellent moistureproof anti-metamorphic.
The technical solution adopted by the present invention is as follows：
The invention discloses a kind of sealed damp-proof medicine bottle, including bottle and bottle stopper, micro air pump is provided with described bottle stopper, it is miniature
Air pump is connected by the first tracheae, and micro air pump is connected by the second tracheae with bottle, described micro air pump connection battery and
Switch positioned at bottle stopper surface.
As an improvement, described battery is battery, the charge port positioned at surface is connected with battery.
As an improvement, being additionally provided with microprocessor in described bottle stopper, microprocessor is between switch and air pump, with micro- place
Reason is also associated with the detector positioned at bottle space and bottle stopper contact surface；
When medicine is not needed, by bottle stopper on bottle, switch is opened, microprocessor control micro air pump first is taken out
Gas operates, until the air pressure that detector detects is after particular value, microprocessor control micro air pump is automatically stopped pumping work
Make.
As an improvement, being provided with annular groove in described bottle stopper, water-absorbing resin ring is provided with described groove, with annular tree
Fat groove is communicated with the 3rd tracheae, and the 3rd described tracheae connects with micro air pump.
As an improvement, the side that described water-absorbing resin ring is located at bottle is provided with elastic membrane.
As an improvement, described water-absorbing resin ring is made up of Water-absorbing high polymer, described Water-absorbing high polymer
Preparation method is as follows：
Step 1：Sweet potato is removed the peel, dry, crush, ground, is made sweet potato powder, and with akaline liquid normal pressure, 100 DEG C -120
Washed under conditions of DEG C, wash time 120-150min, the specific time is adjusted according to different sweet potato surface naturies
It is whole, filter, dry after washing.
Step 2：Surface activation process is carried out to the sweet potato powder after step 1 with activator, by activator and sweet potato powder
Well mixed, at ambient pressure, the sweet potato powder after activation modification is made in 50-100 DEG C of reaction 6-8 hour.
Step 3：By the sweet potato powder after step 1, ethylacrylic acid, water 100-200 parts, lauroyl peroxide 0.1-2 parts
Uniformly mixing, 1-5 hours are reacted at 50-100 DEG C of normal pressure, products therefrom is dried, Water-absorbing high polymer is made.
Preferably, described akaline liquid is sodium hydroxide liquid, potassium hydroxide, one kind of saleratus solution.
Preferably, the activator is alkenyl triethoxysilane, vinyl trichlorosilane, two (dimethylamino) methyl
Vinyl silanes, dimethylvinylmethoxysiiane, dimethyl vinyl chlorosilane, diphenylacetylene Ethoxysilane,
(4- ethenylphenyls) trimethoxy silane, the tert-butyl peroxide silane of vinyl three, vinyl three ('beta '-methoxy ethyoxyl)
Silane, vinyltrimethoxy silane, sodium alkyl sulfate, DTAC, ethoxylated dodecyl alcohol, ten
One kind of dialkyl group glycine betaine.
Preferably, the sweet potato powder after the step 1 refers to average grain diameter in the mesh powder of 40 mesh -120.
In summary, by adopting the above-described technical solution, the beneficial effects of the invention are as follows：
Sealed damp-proof medicine bottle disclosed by the invention has excellent sealing, can prevent medicine from making moist, and ensures the property of medicine of medicine；
In improvement project, present invention employs the mode of battery so that air-tight bottle can repeatedly charging uses for a long time；
The present invention carries out water suction sealing by water-absorbing resin ring, and on the one hand in the presence of air pump pressure, water-absorbing resin ring is pressed
To inner side, the micro gap blocked between bottleneck and bottle stopper, moisture that on the other hand can be in water-absorbing resin gap, dual
In the presence of, moisture will not be entered in bottle.
Brief description of the drawings
Fig. 1 is the structural representation of the present invention；
The structural representation of Fig. 2 water-absorbing resin ring；
Fig. 3 is Fig. 1 A-A1 sectional view；
Marked in figure：1- micro air pumps, the tracheaes of 101- first, the tracheaes of 102- second, 2- microprocessors, 201- switches, 202- inspections
Survey device, 3- batteries, 301- charge ports, the tracheaes of 401- the 3rd, 402- water-absorbing resin rings.
Embodiment
Below in conjunction with the accompanying drawings, the present invention is described in detail.
In order to make the purpose , technical scheme and advantage of the present invention be clearer, it is right below in conjunction with drawings and Examples
The present invention is further elaborated.It should be appreciated that the specific embodiments described herein are merely illustrative of the present invention, and
It is not used in the restriction present invention.
Specific embodiment 1：As shown in Figure 1-2, the invention discloses a kind of sealed damp-proof medicine bottle, including bottle and bottle stopper,
Micro air pump 1 is provided with described bottle stopper, micro air pump 1 is connected by the first tracheae 101, and micro air pump 1 passes through the second tracheae
102 connect with bottle, described micro air pump connection battery 301 and the switch 201 positioned at bottle stopper surface.
Described battery 3 is battery, and the charge port 301 positioned at surface is connected with battery.
Microprocessor 2 is additionally provided with described bottle stopper, microprocessor 2 is between switch 201 and air pump 1, with microprocessor
It is also associated with the detector 202 positioned at bottle space and bottle stopper contact surface；
When medicine is not needed, by bottle stopper on bottle, switch 201 is opened, microprocessor control micro air pump first enters
Row air suction process, until the air pressure that detector detects is taken out for after particular value, microprocessor control micro air pump is automatically stopped
Gas works.
Annular groove is provided with described bottle stopper, water-absorbing resin ring is provided with described groove, is connected with annular resin storage tank
There is the 3rd tracheae 401, the 3rd described tracheae 401 connects with micro air pump.
The side that described water-absorbing resin ring is located at bottle is provided with elastic membrane.
Described water-absorbing resin ring 402 is made up of Water-absorbing high polymer, the preparation side of described Water-absorbing high polymer
Method is as follows：
Step 1：Sweet potato is removed the peel, dry, crush, ground, sweet potato powder is made, and with akaline liquid in normal pressure, 100 DEG C of bar
Washed under part, wash time 120min, the specific time is adjusted according to different sweet potato surface naturies, mistake after washing
Filter, dry so that average grain diameter is 40 mesh.
Step 2：Surface activation process is carried out to the sweet potato powder after step 1 with activator, by activator and sweet potato powder
It is well mixed, at ambient pressure, the sweet potato powder after 50 DEG C of reactions, 6 hours obtained activation modifications.
Step 3：Sweet potato powder after step 1, ethylacrylic acid, 100 parts of water, 0.1 part of lauroyl peroxide is uniformly mixed
Close, reacted 1 hour at 50 DEG C of normal pressure, products therefrom is dried, Water-absorbing high polymer is made.
Described akaline liquid is sodium hydroxide liquid.
The activator is alkenyl triethoxysilane.
Specific embodiment 2：As shown in Figure 1-2, the invention discloses a kind of sealed damp-proof medicine bottle, including bottle and bottle stopper,
Micro air pump 1 is provided with described bottle stopper, micro air pump 1 is connected by the first tracheae 101, and micro air pump 1 passes through the second tracheae
102 connect with bottle, described micro air pump connection battery 301 and the switch 201 positioned at bottle stopper surface.
Described battery 3 is battery, and the charge port 301 positioned at surface is connected with battery.
Microprocessor 2 is additionally provided with described bottle stopper, microprocessor 2 is between switch 201 and air pump 1, with microprocessor
It is also associated with the detector 202 positioned at bottle space and bottle stopper contact surface；
When medicine is not needed, by bottle stopper on bottle, switch 201 is opened, microprocessor control micro air pump first enters
Row air suction process, until the air pressure that detector detects is taken out for after particular value, microprocessor control micro air pump is automatically stopped
Gas works.
Annular groove is provided with described bottle stopper, water-absorbing resin ring is provided with described groove, is connected with annular resin storage tank
There is the 3rd tracheae 401, the 3rd described tracheae 401 connects with micro air pump.
The side that described water-absorbing resin ring is located at bottle is provided with elastic membrane.
Described water-absorbing resin ring 402 is made up of Water-absorbing high polymer, the preparation side of described Water-absorbing high polymer
Method is as follows：
Step 1：Sweet potato is removed the peel, dry, crush, ground, sweet potato powder is made, and with akaline liquid in normal pressure, 120 DEG C of bar
Washed under part, wash time 150min, the specific time is adjusted according to different sweet potato surface naturies, mistake after washing
Filter, dry so that average grain diameter is in 120 mesh.
Step 2：Surface activation process is carried out to the sweet potato powder after step 1 with activator, by activator and sweet potato powder
It is well mixed, at ambient pressure, the sweet potato powder after 100 DEG C of reactions, 8 hours obtained activation modifications.
Step 3：Sweet potato powder after step 1, ethylacrylic acid, 200 parts of water, 2 parts of lauroyl peroxide are uniformly mixed,
Reacted 5 hours at 100 DEG C of normal pressure, products therefrom is dried, Water-absorbing high polymer is made.
Described akaline liquid is potassium hydroxide.
The activator is vinyl trichlorosilane.
Specific embodiment 3：As shown in Figure 1-2, the invention discloses a kind of sealed damp-proof medicine bottle, including bottle and bottle stopper,
Micro air pump 1 is provided with described bottle stopper, micro air pump 1 is connected by the first tracheae 101, and micro air pump 1 passes through the second tracheae
102 connect with bottle, described micro air pump connection battery 301 and the switch 201 positioned at bottle stopper surface.
Described battery 3 is battery, and the charge port 301 positioned at surface is connected with battery.
Microprocessor 2 is additionally provided with described bottle stopper, microprocessor 2 is between switch 201 and air pump 1, with microprocessor
It is also associated with the detector 202 positioned at bottle space and bottle stopper contact surface；
When medicine is not needed, by bottle stopper on bottle, switch 201 is opened, microprocessor control micro air pump first enters
Row air suction process, until the air pressure that detector detects is taken out for after particular value, microprocessor control micro air pump is automatically stopped
Gas works.
Annular groove is provided with described bottle stopper, water-absorbing resin ring is provided with described groove, is connected with annular resin storage tank
There is the 3rd tracheae 401, the 3rd described tracheae 401 connects with micro air pump.
The side that described water-absorbing resin ring is located at bottle is provided with elastic membrane.
Described water-absorbing resin ring 402 is made up of Water-absorbing high polymer, the preparation side of described Water-absorbing high polymer
Method is as follows：
Step 1：Sweet potato is removed the peel, dry, crush, ground, sweet potato powder is made, and with akaline liquid in normal pressure, 110 DEG C of bar
Washed under part, wash time 140min, the specific time is adjusted according to different sweet potato surface naturies, mistake after washing
Filter, dry so that average grain diameter is in 100 mesh.
Step 2：Surface activation process is carried out to the sweet potato powder after step 1 with activator, by activator and sweet potato powder
It is well mixed, at ambient pressure, the sweet potato powder after 80 DEG C of reactions, 7 hours obtained activation modifications.
Step 3：Sweet potato powder after step 1, ethylacrylic acid, 120 parts of water, 1 part of lauroyl peroxide are uniformly mixed,
Reacted 4 hours at 80 DEG C of normal pressure, products therefrom is dried, Water-absorbing high polymer is made.
Described akaline liquid is potassium hydroxide.
The activator is dimethylvinylmethoxysiiane.
Specific embodiment 4：As shown in Figure 1-2, the invention discloses a kind of sealed damp-proof medicine bottle, including bottle and bottle stopper,
Micro air pump 1 is provided with described bottle stopper, micro air pump 1 is connected by the first tracheae 101, and micro air pump 1 passes through the second tracheae
102 connect with bottle, described micro air pump connection battery 301 and the switch 201 positioned at bottle stopper surface.
Described battery 3 is battery, and the charge port 301 positioned at surface is connected with battery.
Microprocessor 2 is additionally provided with described bottle stopper, microprocessor 2 is between switch 201 and air pump 1, with microprocessor
It is also associated with the detector 202 positioned at bottle space and bottle stopper contact surface；
When medicine is not needed, by bottle stopper on bottle, switch 201 is opened, microprocessor control micro air pump first enters
Row air suction process, until the air pressure that detector detects is taken out for after particular value, microprocessor control micro air pump is automatically stopped
Gas works.
Annular groove is provided with described bottle stopper, water-absorbing resin ring is provided with described groove, is connected with annular resin storage tank
There is the 3rd tracheae 401, the 3rd described tracheae 401 connects with micro air pump.
The side that described water-absorbing resin ring is located at bottle is provided with elastic membrane.
Described water-absorbing resin ring 402 is made up of Water-absorbing high polymer, the preparation side of described Water-absorbing high polymer
Method is as follows：
Step 1：Sweet potato is removed the peel, dry, crush, ground, sweet potato powder is made, and with akaline liquid in normal pressure, 100 DEG C of bar
Washed under part, wash time 150min, the specific time is adjusted according to different sweet potato surface naturies, mistake after washing
Filter, dry so that average grain diameter is in 40 mesh.
Step 2：Surface activation process is carried out to the sweet potato powder after step 1 with activator, by activator and sweet potato powder
It is well mixed, at ambient pressure, the sweet potato powder after 100 DEG C of reactions, 6 hours obtained activation modifications.
Step 3：Sweet potato powder after step 1, ethylacrylic acid, 200 parts of water, 0.1 part of lauroyl peroxide is uniformly mixed
Close, reacted 1 hour at 100 DEG C of normal pressure, products therefrom is dried, Water-absorbing high polymer is made.
Described akaline liquid is potassium hydroxide, concentration 2mol/L.
The activator is the tert-butyl peroxide silane of vinyl three.
Specific embodiment 5：As shown in Figure 1-2, the invention discloses a kind of sealed damp-proof medicine bottle, including bottle and bottle stopper,
Micro air pump 1 is provided with described bottle stopper, micro air pump 1 is connected by the first tracheae 101, and micro air pump 1 passes through the second tracheae
102 connect with bottle, described micro air pump connection battery 301 and the switch 201 positioned at bottle stopper surface.
Described battery 3 is battery, and the charge port 301 positioned at surface is connected with battery.
Microprocessor 2 is additionally provided with described bottle stopper, microprocessor 2 is between switch 201 and air pump 1, with microprocessor
It is also associated with the detector 202 positioned at bottle space and bottle stopper contact surface；
When medicine is not needed, by bottle stopper on bottle, switch 201 is opened, microprocessor control micro air pump first enters
Row air suction process, until the air pressure that detector detects is taken out for after particular value, microprocessor control micro air pump is automatically stopped
Gas works.
Annular groove is provided with described bottle stopper, water-absorbing resin ring is provided with described groove, is connected with annular resin storage tank
There is the 3rd tracheae 401, the 3rd described tracheae 401 connects with micro air pump.
The side that described water-absorbing resin ring is located at bottle is provided with elastic membrane.
Described water-absorbing resin ring 402 is made up of Water-absorbing high polymer, the preparation side of described Water-absorbing high polymer
Method is as follows：
Step 1：Sweet potato is removed the peel, dry, crush, ground, sweet potato powder is made, and with akaline liquid in normal pressure, 100 DEG C of bar
Washed under part, wash time 150min, the specific time is adjusted according to different sweet potato surface naturies, mistake after washing
Filter, dry so that average grain diameter is in 40 mesh.
Step 2：Surface activation process is carried out to the sweet potato powder after step 1 with activator, by activator and sweet potato powder
It is well mixed, at ambient pressure, the sweet potato powder after 100 DEG C of reactions, 6 hours obtained activation modifications.
Step 3：Sweet potato powder after step 1, ethylacrylic acid, 200 parts of water, 2 parts of lauroyl peroxide are uniformly mixed,
Reacted 1 hour at 50 DEG C of normal pressure, products therefrom is dried, Water-absorbing high polymer is made.
Described akaline liquid is saleratus solution, concentration 1mol/L
The activator is alkenyl triethoxysilane.
Specific embodiment 1：As shown in Figure 1-2, the invention discloses a kind of sealed damp-proof medicine bottle, including bottle and bottle stopper,
Micro air pump 1 is provided with described bottle stopper, micro air pump 1 is connected by the first tracheae 101, and micro air pump 1 passes through the second tracheae
102 connect with bottle, described micro air pump connection battery 301 and the switch 201 positioned at bottle stopper surface.
Described battery 3 is battery, and the charge port 301 positioned at surface is connected with battery.
Microprocessor 2 is additionally provided with described bottle stopper, microprocessor 2 is between switch 201 and air pump 1, with microprocessor
It is also associated with the detector 202 positioned at bottle space and bottle stopper contact surface；
When medicine is not needed, by bottle stopper on bottle, switch 201 is opened, microprocessor control micro air pump first enters
Row air suction process, until the air pressure that detector detects is taken out for after particular value, microprocessor control micro air pump is automatically stopped
Gas works.
Annular groove is provided with described bottle stopper, water-absorbing resin ring is provided with described groove, is connected with annular resin storage tank
There is the 3rd tracheae 401, the 3rd described tracheae 401 connects with micro air pump.
The side that described water-absorbing resin ring is located at bottle is provided with elastic membrane.
Described water-absorbing resin ring 402 is made up of Water-absorbing high polymer, the preparation side of described Water-absorbing high polymer
Method is as follows：
Step 1：Sweet potato is removed the peel, dry, crush, ground, is made sweet potato powder, and with akaline liquid normal pressure, 100 DEG C -120
Washed under conditions of DEG C, wash time 120-150min, the specific time is adjusted according to different sweet potato surface naturies
It is whole, filter, dry after washing so that average grain diameter is in the mesh of 40 mesh -120.
Step 2：Surface activation process is carried out to the sweet potato powder after step 1 with activator, by activator and sweet potato powder
Well mixed, at ambient pressure, the sweet potato powder after activation modification is made in 50-100 DEG C of reaction 6-8 hour.
Step 3：By the sweet potato powder after step 1, ethylacrylic acid, water 100-200 parts, lauroyl peroxide 0.1-2 parts
Uniformly mixing, 1-5 hours are reacted at 50-100 DEG C of normal pressure, products therefrom is dried, Water-absorbing high polymer is made.
Described akaline liquid is sodium hydroxide liquid, potassium hydroxide, one kind of saleratus solution.
The activator is alkenyl triethoxysilane, vinyl trichlorosilane, two (dimethylamino) methyl ethylene silicon
Alkane, dimethylvinylmethoxysiiane, dimethyl vinyl chlorosilane, diphenylacetylene Ethoxysilane, (4- ethene
Base phenyl) trimethoxy silane, the tert-butyl peroxide silane of vinyl three, vinyl three ('beta '-methoxy ethyoxyl) silane, second
Alkenyl trimethoxy silane, sodium alkyl sulfate, DTAC, ethoxylated dodecyl alcohol, dodecyl
One kind of glycine betaine.
The foregoing is merely illustrative of the preferred embodiments of the present invention, is not intended to limit the invention, all essences in the present invention
All any modification, equivalent and improvement made within refreshing and principle etc., should be included in the scope of the protection.
Claims (4)
1. a kind of sealed damp-proof medicine bottle water-absorbing resin, it is characterised in that the preparation method of described Water-absorbing high polymer is such as
Under：
Step 1：Sweet potato is removed the peel, dry, crush, ground, is made sweet potato powder, and with akaline liquid normal pressure, 100 DEG C -120
Washed under conditions of DEG C, wash time 120-150min, the specific time is adjusted according to different sweet potato surface naturies
It is whole, filter, dry after washing;
Step 2：Surface activation process is carried out to the sweet potato powder after step 1 with activator, activator is mixed with sweet potato powder
Uniformly, at ambient pressure, the sweet potato powder after activation modification is made in 50-100 DEG C of reaction 6-8 hour;
Step 3：Sweet potato powder after step 1, ethylacrylic acid, water 100-200 parts, lauroyl peroxide 0.1-2 parts is uniform
Mixing, 1-5 hours are reacted at 50-100 DEG C of normal pressure, products therefrom is dried, Water-absorbing high polymer is made.
2. sealed damp-proof medicine bottle water-absorbing resin according to claim 1, it is characterised in that described akaline liquid is hydrogen
Sodium oxide molybdena liquid, potassium hydroxide, one kind of saleratus solution.
3. sealed damp-proof medicine bottle water-absorbing resin according to claim 1, it is characterised in that the activator is alkenyl three
Ethoxysilane, vinyl trichlorosilane, two (dimethylamino) ethylene methacrylic base silanes, dimethylvinylmethoxysiiane,
Dimethyl vinyl chlorosilane, diphenylacetylene Ethoxysilane, (4- ethenylphenyls) trimethoxy silane, vinyl three
Tert-butyl peroxide silane, vinyl three ('beta '-methoxy ethyoxyl) silane, vinyltrimethoxy silane, fatty alcohol sulphuric acid
Sodium, DTAC, ethoxylated dodecyl alcohol, one kind of empgen BB.
4. sealed damp-proof medicine bottle water-absorbing resin according to claim 3, it is characterised in that the sweet potato after the step 1
Powder refers to average grain diameter in the mesh powder of 40 mesh -120.
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710865445.XA CN107778410A (en) | 2016-09-20 | 2016-09-20 | A kind of sealed damp-proof medicine bottle water-absorbing resin |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610834064.0A CN106428954B (en) | 2016-09-20 | 2016-09-20 | A kind of sealed damp-proof medicine bottle |
| CN201710865445.XA CN107778410A (en) | 2016-09-20 | 2016-09-20 | A kind of sealed damp-proof medicine bottle water-absorbing resin |
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| CN201710865445.XA Withdrawn CN107778410A (en) | 2016-09-20 | 2016-09-20 | A kind of sealed damp-proof medicine bottle water-absorbing resin |
| CN201610834064.0A Active CN106428954B (en) | 2016-09-20 | 2016-09-20 | A kind of sealed damp-proof medicine bottle |
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| CN103910896A (en) * | 2014-04-08 | 2014-07-09 | 万华化学集团股份有限公司 | Preparation method of macromolecular water-absorbent resin with low reverse osmosis |
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE3139998C2 (en) * | 1981-10-08 | 1983-12-01 | Wolfgang 4156 Willich Berrens | Fresh keeping device for bread and the like. Food |
| CN1053201C (en) * | 1996-07-25 | 2000-06-07 | 化学工业部北京化工研究院 | Wate-absorption resin and preparing method thereof |
| CN2931353Y (en) * | 2006-07-12 | 2007-08-08 | 太平洋科技制造有限公司 | Full-automatic fresh-keeping damp-proof vacuum container |
| CN202107211U (en) * | 2011-06-17 | 2012-01-11 | 宁波泰尔斯电子实业有限公司 | Vacuum preservation integrated machine |
| CN202321186U (en) * | 2011-11-25 | 2012-07-11 | 程辉 | Vacuum box |
| CN104443728A (en) * | 2014-11-18 | 2015-03-25 | 曹东 | Vacuum dampproof preservation box |
| CN104910284B (en) * | 2015-06-26 | 2019-08-09 | 江南大学 | A kind of double bond containing modified starch, preparation method and application |
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2016
- 2016-09-20 CN CN201710865160.6A patent/CN107674152A/en not_active Withdrawn
- 2016-09-20 CN CN201710865445.XA patent/CN107778410A/en not_active Withdrawn
- 2016-09-20 CN CN201610834064.0A patent/CN106428954B/en active Active
Patent Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103910896A (en) * | 2014-04-08 | 2014-07-09 | 万华化学集团股份有限公司 | Preparation method of macromolecular water-absorbent resin with low reverse osmosis |
Also Published As
| Publication number | Publication date |
|---|---|
| CN106428954A (en) | 2017-02-22 |
| CN106428954B (en) | 2018-05-11 |
| CN107674152A (en) | 2018-02-09 |
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