CN107774887A - A kind of Antistatic resin sand preparation technology - Google Patents

A kind of Antistatic resin sand preparation technology Download PDF

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Publication number
CN107774887A
CN107774887A CN201610729008.0A CN201610729008A CN107774887A CN 107774887 A CN107774887 A CN 107774887A CN 201610729008 A CN201610729008 A CN 201610729008A CN 107774887 A CN107774887 A CN 107774887A
Authority
CN
China
Prior art keywords
parts
lauxite
antistatic
grain
resin sand
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201610729008.0A
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Chinese (zh)
Inventor
李玉敏
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Qingdao Tiandi Casting Co Ltd
Original Assignee
Qingdao Tiandi Casting Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Qingdao Tiandi Casting Co Ltd filed Critical Qingdao Tiandi Casting Co Ltd
Priority to CN201610729008.0A priority Critical patent/CN107774887A/en
Publication of CN107774887A publication Critical patent/CN107774887A/en
Pending legal-status Critical Current

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Classifications

    • BPERFORMING OPERATIONS; TRANSPORTING
    • B22CASTING; POWDER METALLURGY
    • B22CFOUNDRY MOULDING
    • B22C1/00Compositions of refractory mould or core materials; Grain structures thereof; Chemical or physical features in the formation or manufacture of moulds
    • B22C1/16Compositions of refractory mould or core materials; Grain structures thereof; Chemical or physical features in the formation or manufacture of moulds characterised by the use of binding agents; Mixtures of binding agents
    • B22C1/20Compositions of refractory mould or core materials; Grain structures thereof; Chemical or physical features in the formation or manufacture of moulds characterised by the use of binding agents; Mixtures of binding agents of organic agents
    • B22C1/22Compositions of refractory mould or core materials; Grain structures thereof; Chemical or physical features in the formation or manufacture of moulds characterised by the use of binding agents; Mixtures of binding agents of organic agents of resins or rosins
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08GMACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G12/00Condensation polymers of aldehydes or ketones with only compounds containing hydrogen attached to nitrogen
    • C08G12/02Condensation polymers of aldehydes or ketones with only compounds containing hydrogen attached to nitrogen of aldehydes
    • C08G12/04Condensation polymers of aldehydes or ketones with only compounds containing hydrogen attached to nitrogen of aldehydes with acyclic or carbocyclic compounds
    • C08G12/10Condensation polymers of aldehydes or ketones with only compounds containing hydrogen attached to nitrogen of aldehydes with acyclic or carbocyclic compounds with acyclic compounds having the moiety X=C(—N<)2 in which X is O, S or —N
    • C08G12/12Ureas; Thioureas

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  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Health & Medical Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Organic Chemistry (AREA)
  • Materials Engineering (AREA)
  • Mechanical Engineering (AREA)
  • Processes Of Treating Macromolecular Substances (AREA)
  • Processing And Handling Of Plastics And Other Materials For Molding In General (AREA)

Abstract

The invention discloses a kind of Antistatic resin sand preparation technology, including synthesis Lauxite, kneading process, drying process, pulverizing process, ball milling and sieve powder, granulating working procedure and whole grain process, mixing, packaging and other steps.Anlistatig resin sand provided by the present invention and preparation method thereof, there is antistatic effect, and reached the requirements of airframe surface treatment, particularly need not spray antistatic liquid to resin sand in use.

Description

A kind of Antistatic resin sand preparation technology
Technical field
The invention belongs to casting technology field, and in particular to a kind of Antistatic resin sand preparation technology.
Background technology
Airframe surface is due to its particularity, it is necessary to there is the function of antistatic, and the method generally used in the world is Antistatic liquid is sprayed in resin sand, causes sand surface that there is antistatic effect, reaching body surface has anlistatig work( Energy;But a trouble is also brought, i.e., need to repeat to spray antistatic liquid when resin sand is reused, not only each use will increase Add material and cost of labor, and to increase readiness time.
The content of the invention
In order to overcome above mentioned problem existing for prior art, it is an object of the present invention to provide a kind of antistatic tree Fat sand preparation technology, there is antistatic effect in the resin sand that can make finally to be processed into, and reached at airframe surface The requirements of reason, particularly antistatic liquid need not be sprayed to resin sand in use.
A kind of Antistatic resin sand preparation technology provided by the invention, comprises the following steps:
1) Lauxite is synthesized:Prepare urea 250-290 parts, formaldehyde 470-530 by the weight proportion of recipe requirements
Part, methenamine 17-28 parts.First disposably put into formaldehyde 340-530 parts of recipe requirements amount and start stirring, then Methenamine 17-25 parts are put into, until methenamine is completely dissolved, PH values are surveyed, in PH>Disposably put into after 7.5 The urea of 250-270 parts continues stirring until dissolving, reacts 55-65min, synthesis Lauxite at 59 DEG C -65 DEG C;
2) kneading process:By 1)The Lauxite of middle synthesis is progressively banished into kneader by pipeline, and disposable add is matched somebody with somebody Filler, color masterbatch, curing agent, titanium dioxide, releasing agent, antistatic additive and the plasticizer of square required amount, single direction stirring 15- 30min, make Lauxite, filler and various auxiliary materials and after antistatic additive is sufficiently mixed and disperses, opposite direction is again stirring for above-mentioned It has been sufficiently mixed and each material for disperseing and has been dehydrated 35-50min at 66-77 DEG C simultaneously;
3) drying process:Material after dehydration is 55-70 DEG C in temperature, and 25- is pre-processed under conditions of thickness of feed layer≤5cm 29 minutes, the bed of material, which is realized, to be turned over, and temperature gradually rises to 91-95 DEG C of progress dry materials 77-87 minute, and the bed of material is realized second Turn over, be progressively segmented through 35-50 minutes under the conditions of 67-85 DEG C and be cooled to normal temperature;
4) pulverizing process:Material after drying process crushes under 3600 revs/min of crushing speed is less than 1mm for diameter Irregular coarse powder material;
5) ball milling and screening:Coarse powder material is 29-35 revs/min in rotational speed of ball-mill and material ball ratio is 1:Ball milling 6-8 under conditions of 2 Hour, ball milling is diameter<The spherical fine powder of 76 purposes;
6) granulating working procedure and whole grain process:Step 5)In spherical fine powder by mechanical means roughing be irregular piece, Bar or grain, piece, bar or grain after roughing are further through crushing with whole grain into the material containing certain powder ratio;
7) mix, pack:The thing grain identical to model, performance is consistent mixed, it is dispersed 2 hours after pack.
Embodiment
With reference to embodiment, to a kind of Antistatic resin sand preparation technology provided by the invention, it is described in detail.
Embodiment
A kind of Antistatic resin sand preparation technology of the present embodiment, comprises the following steps:
1) Lauxite is synthesized:Prepare 280 parts of urea, 490 parts of formaldehyde, 27 parts of methenamine by the weight proportion of recipe requirements. First disposably put into 430 parts of the formaldehyde of recipe requirements amount and start stirring, then put into 19 parts of methenamine, until methenamine It is completely dissolved, PH values is surveyed, in PH>The urea of disposable 270 parts of input continues stirring until dissolving, at 65 DEG C after 7.5 55min is reacted, synthesizes Lauxite;
2) kneading process:By 1)The Lauxite of middle synthesis is progressively banished into kneader by pipeline, and disposable add is matched somebody with somebody Filler, color masterbatch, curing agent, titanium dioxide, releasing agent, antistatic additive and the plasticizer of square required amount, single direction stirring 19min, make Lauxite, filler and various auxiliary materials and after antistatic additive is sufficiently mixed and disperses, opposite direction is again stirring for above-mentioned It has been sufficiently mixed and each material for disperseing and has been dehydrated 39min at 77 DEG C simultaneously;
3) drying process:Material after dehydration is 59 DEG C in temperature, is pre-processed 29 minutes under conditions of thickness of feed layer≤5cm, The bed of material, which is realized, to be turned over, and temperature gradually rises to 91 DEG C and carries out dry materials 77 minutes, and the bed of material is realized second and turned over, 85 DEG C of conditions Lower be progressively segmented through 35 minutes is cooled to normal temperature;
4) pulverizing process:Material after drying process crushes under 3600 revs/min of crushing speed is less than 1mm for diameter Irregular coarse powder material;
5) ball milling and screening:Coarse powder material is 29 revs/min in rotational speed of ball-mill and material ball ratio is 1:Ball milling 8 hours, ball under conditions of 2 Grind as diameter<The spherical fine powder of 76 purposes;
6) granulating working procedure and whole grain process:Step 5)In spherical fine powder by mechanical means roughing be irregular piece, bar Or grain, piece, bar or grain after roughing are further through crushing with whole grain into the material containing certain powder ratio;
7) mix, pack:The thing grain identical to model, performance is consistent mixed, it is dispersed 2 hours after pack.

Claims (1)

  1. A kind of 1. Antistatic resin sand preparation technology, it is characterised in that:Comprise the following steps:
    1) Lauxite is synthesized:Prepare urea 250-290 parts, formaldehyde 470-530 parts, Wu Luotuo by the weight proportion of recipe requirements Product 17-28 parts, first disposably put into formaldehyde 340-530 parts of recipe requirements amount and start stirring, then put into methenamine 17-25 parts, until methenamine is completely dissolved, PH values are surveyed, in PH>7.5 the urine of rear disposable input 250-270 parts Element continues stirring until dissolving, reacts 55-65min, synthesis Lauxite at 59 DEG C -65 DEG C;
    2) kneading process:By 1)The Lauxite of middle synthesis is progressively banished into kneader by pipeline, and disposable add is matched somebody with somebody Filler, color masterbatch, curing agent, titanium dioxide, releasing agent, antistatic additive and the plasticizer of square required amount, single direction stirring 15- 30min, make Lauxite, filler and various auxiliary materials and after antistatic additive is sufficiently mixed and disperses, opposite direction is again stirring for above-mentioned It has been sufficiently mixed and each material for disperseing and has been dehydrated 35-50min at 66-77 DEG C simultaneously;
    3) drying process:Material after dehydration is 55-70 DEG C in temperature, and 25- is pre-processed under conditions of thickness of feed layer≤5cm 29 minutes, the bed of material, which is realized, to be turned over, and temperature gradually rises to 91-95 DEG C of progress dry materials 77-87 minute, and the bed of material is realized second Turn over, be progressively segmented through 35-50 minutes under the conditions of 67-85 DEG C and be cooled to normal temperature;
    4) pulverizing process:Material after drying process crushes under 3600 revs/min of crushing speed is less than 1mm for diameter Irregular coarse powder material;
    5) ball milling and screening:Coarse powder material is 29-35 revs/min in rotational speed of ball-mill and material ball ratio is 1:Ball milling 6-8 is small under conditions of 2 When, ball milling is diameter<The spherical fine powder of 76 purposes;
    6) granulating working procedure and whole grain process:Step 5)In spherical fine powder by mechanical means roughing be irregular piece, Bar or grain, piece, bar or grain after roughing are further through crushing with whole grain into the material containing certain powder ratio;
    7) mix, pack:The thing grain identical to model, performance is consistent mixed, it is dispersed 2 hours after pack.
CN201610729008.0A 2016-08-26 2016-08-26 A kind of Antistatic resin sand preparation technology Pending CN107774887A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201610729008.0A CN107774887A (en) 2016-08-26 2016-08-26 A kind of Antistatic resin sand preparation technology

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201610729008.0A CN107774887A (en) 2016-08-26 2016-08-26 A kind of Antistatic resin sand preparation technology

Publications (1)

Publication Number Publication Date
CN107774887A true CN107774887A (en) 2018-03-09

Family

ID=61438840

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201610729008.0A Pending CN107774887A (en) 2016-08-26 2016-08-26 A kind of Antistatic resin sand preparation technology

Country Status (1)

Country Link
CN (1) CN107774887A (en)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108526385A (en) * 2018-04-12 2018-09-14 盐城仁创砂业科技有限公司 A kind of elimination electrostatic precoated sand and preparation method thereof

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108526385A (en) * 2018-04-12 2018-09-14 盐城仁创砂业科技有限公司 A kind of elimination electrostatic precoated sand and preparation method thereof
CN108526385B (en) * 2018-04-12 2019-11-01 盐城仁创砂业科技有限公司 A kind of elimination electrostatic precoated sand and preparation method thereof

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Application publication date: 20180309