CN107764971A - Based on the method to the quick property test evaluation of oil-gas Layer alkali - Google Patents
Based on the method to the quick property test evaluation of oil-gas Layer alkali Download PDFInfo
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- CN107764971A CN107764971A CN201610679576.4A CN201610679576A CN107764971A CN 107764971 A CN107764971 A CN 107764971A CN 201610679576 A CN201610679576 A CN 201610679576A CN 107764971 A CN107764971 A CN 107764971A
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- salt solution
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- gas layer
- value
- rock core
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- 239000003513 alkali Substances 0.000 title claims abstract description 18
- 238000000034 method Methods 0.000 title claims abstract description 14
- 238000011156 evaluation Methods 0.000 title claims abstract description 11
- 238000012360 testing method Methods 0.000 title claims abstract description 9
- 239000012266 salt solution Substances 0.000 claims abstract description 34
- 239000011435 rock Substances 0.000 claims abstract description 18
- 230000035699 permeability Effects 0.000 claims abstract description 17
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 6
- FAPWRFPIFSIZLT-UHFFFAOYSA-M Sodium chloride Chemical compound [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 claims abstract description 4
- 238000002347 injection Methods 0.000 claims abstract description 4
- 239000007924 injection Substances 0.000 claims abstract description 4
- 238000002360 preparation method Methods 0.000 claims abstract description 4
- 239000011780 sodium chloride Substances 0.000 claims abstract description 4
- 230000006641 stabilisation Effects 0.000 claims description 3
- 238000011105 stabilization Methods 0.000 claims description 3
- 238000009738 saturating Methods 0.000 claims 1
- 230000000903 blocking effect Effects 0.000 abstract description 9
- 239000012530 fluid Substances 0.000 abstract description 7
- 239000002734 clay mineral Substances 0.000 abstract description 6
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 abstract description 5
- 239000007789 gas Substances 0.000 description 38
- 239000005416 organic matter Substances 0.000 description 17
- VNWKTOKETHGBQD-UHFFFAOYSA-N methane Chemical group C VNWKTOKETHGBQD-UHFFFAOYSA-N 0.000 description 6
- 230000015572 biosynthetic process Effects 0.000 description 4
- 125000002887 hydroxy group Chemical group [H]O* 0.000 description 4
- 238000011084 recovery Methods 0.000 description 3
- 241000196324 Embryophyta Species 0.000 description 2
- OTMSDBZUPAUEDD-UHFFFAOYSA-N Ethane Chemical compound CC OTMSDBZUPAUEDD-UHFFFAOYSA-N 0.000 description 2
- 238000005516 engineering process Methods 0.000 description 2
- 238000004519 manufacturing process Methods 0.000 description 2
- 238000011160 research Methods 0.000 description 2
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 1
- 239000004215 Carbon black (E152) Substances 0.000 description 1
- 238000004458 analytical method Methods 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 239000000090 biomarker Substances 0.000 description 1
- 229910052799 carbon Inorganic materials 0.000 description 1
- 239000003518 caustics Substances 0.000 description 1
- 239000004568 cement Substances 0.000 description 1
- 238000003776 cleavage reaction Methods 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 238000005553 drilling Methods 0.000 description 1
- 239000000446 fuel Substances 0.000 description 1
- 238000010438 heat treatment Methods 0.000 description 1
- 229930195733 hydrocarbon Natural products 0.000 description 1
- 150000002430 hydrocarbons Chemical class 0.000 description 1
- 229910052500 inorganic mineral Inorganic materials 0.000 description 1
- 239000011859 microparticle Substances 0.000 description 1
- 239000011707 mineral Substances 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 239000003345 natural gas Substances 0.000 description 1
- 230000007935 neutral effect Effects 0.000 description 1
- 239000003129 oil well Substances 0.000 description 1
- 238000001556 precipitation Methods 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 230000007017 scission Effects 0.000 description 1
- 239000000243 solution Substances 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
Classifications
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N15/00—Investigating characteristics of particles; Investigating permeability, pore-volume or surface-area of porous materials
- G01N15/08—Investigating permeability, pore-volume, or surface area of porous materials
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N33/00—Investigating or analysing materials by specific methods not covered by groups G01N1/00 - G01N31/00
- G01N33/24—Earth materials
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- Life Sciences & Earth Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Health & Medical Sciences (AREA)
- Analytical Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Pathology (AREA)
- Immunology (AREA)
- General Physics & Mathematics (AREA)
- General Health & Medical Sciences (AREA)
- Biochemistry (AREA)
- Physics & Mathematics (AREA)
- Geology (AREA)
- Medicinal Chemistry (AREA)
- Food Science & Technology (AREA)
- Remote Sensing (AREA)
- General Life Sciences & Earth Sciences (AREA)
- Environmental & Geological Engineering (AREA)
- Dispersion Chemistry (AREA)
- Investigating Or Analyzing Non-Biological Materials By The Use Of Chemical Means (AREA)
Abstract
The invention discloses a kind of method based on to the quick property test evaluation of oil-gas Layer alkali, the preparation of different pH value salt solution, according to actual conditions, pH value is raised step by step since the pH value of stratum water, afterbody salt solution pH value can be set to 12, the rock core vacuumizing saturation first order salt solution that will be chosen, and 20 ~ 24h is soaked, under conditions of less than critical flow velocity, the stable permeability K of rock core is measured with first order salt solution1, second level salt solution is injected, soaks 20 ~ 24h, under conditions of less than critical flow velocity, the stable permeability K of rock core is measured with second level salt solution2, change the rank of injection salt solution, until measuring the steady seepage rate K of the rock core after afterbody saline treatmentn.This method is tested by the quick property of the alkali to oil-gas Layer, obtains accurate numerical value, after can preventing high ph-values fluid from entering oil-gas Layer, the structure for causing oil-gas Layer CLAY MINERALS AND THEIR SIGNIFICANCE and silicious gangue is destroyed, the problem of so as to cause the blocking of oil-gas Layer to damage.
Description
Technical field
The present invention relates to a kind of method, more particularly, to a kind of method based on to the quick property test evaluation of oil-gas Layer alkali.
Background technology
Oil gas is the gas from oil well out with oil, and main component is methane, ethane etc..As fuel and chemical industry
Raw material.Oil-gas generation has following condition, first, to see organic matter quantity in source bed number, commonly referred to as " organic matter is rich
Degree ".The organic carbon content wherein remained is mainly determined, to determine an area whether there is source bed, how many source bed, and it
Be divided into by certain standard, medium and poor source bed, carry out evaluation of classification.Second, to see organic in source bed
The quality of matter quality, commonly referred to as " organic matter type ".According to biological source, the kerogen of Oil source bed is divided into three major types.
The first kind is sapropelic organic matters, and biological source is mainly the plankton in water, is I type kerogens, and category is top-quality
Organic matter.Second class is rotten plant type organic matter, and biological source is mainly higher plant, is type III kerogen, belongs to second-rate
Organic matter.3rd class is mixed type organic matter therebetween, is II type kerogens, is the preferable organic matter of quality.It is real
Room is tested by the analysis result to sample, a regional organic matter type is determined by certain standard, to the quality of organic matter
Make evaluation.3rd, it is gentle to see whether organic matter has generated oil, commonly referred to as " maturity of organic matter ", when possessing
The organic matter of certain amount and quality is changed into after oil under certain conditions.In other words, if not possessing generation oil
" duration and degree of heating ", organic matter at most, be desirably also without what real value.So the maturity of research organic matter is critically important
A ring.The information that analyze data is provided, the temperature course that organic matter undergoes in underground can be reflected indirectly.According to these numbers
According to, maturity be divided into immature, oil generation peak, moisture, dry gas (dry gas refers to that its origin cause of formation is relevant with oil, and containing ethane with
On heavy hydrocarbon it is seldom, the flammable natural gas of methane content more than 95%.It is close with this as the composition of biogas and coal-type gas, but
The origin cause of formation is different, shoulds be regarded as a different matter.) etc. four-stage.What stage of ripeness evaluation organic matter is in, and people can be told on some ground
Area is advantageous for oil prospecting or gas finding.4th, to see that the oil of generation or gas are from that source bed, commonly referred to as " oil sources
Contrast ".I.e. after oil gas is found, oil gas and oil source rock are carried out pair with " fingerprint compound " (or biomarker)
Than, explore the affiliation between oil source rock and oil gas, research institute's generation it is oily it is gentle be from that source bed.It is not difficult to think
As, there is provided the source bed of oil sources is more, and oil sources is abundanter, to forming oil gas field just advantageously.Do not have in existing recovery process
Have and these infringements are tested, damaged after causing oil-gas Layer exploitation a period of time so that production efficiency is affected.Ground
Layer water pH value is typically in neutral or alkalescent, and the pH value of most of drilling fluids is between 8 ~ 12, the caustic waterflooding in secondary oil recovery
Also there is higher pH value.After high ph-values fluid enters oil-gas Layer, the knot of oil-gas Layer CLAY MINERALS AND THEIR SIGNIFICANCE and silicious gangue will be caused
Structure destroys（Mainly release microparticles after clay mineral cleavage and cement dissolving）, so as to cause the blocking of oil-gas Layer to damage；This
Outside, substantial amounts of hydroxyl can generate insoluble matter with some divalence sun from combination, cause the blocking of oil-gas Layer to damage.
The content of the invention
It is an object of the invention to overcome in above-mentioned existing recovery process not test these infringements, oil gas is caused
Layer damages after exploitation a period of time so that the problem of production efficiency is affected, devises a kind of be based on to oil-gas Layer alkali
The method of quick property test evaluation, this method are tested by the quick property of the alkali to oil-gas Layer, obtain accurate numerical value, can prevent
After high ph-values fluid enters oil-gas Layer, the structure for causing oil-gas Layer CLAY MINERALS AND THEIR SIGNIFICANCE and silicious gangue is destroyed, so as to cause oil
The blocking infringement of gas-bearing formation；Substantial amounts of hydroxyl can generate insoluble matter with some divalence sun from combination, cause the blocking of oil-gas Layer
The problem of infringement, occurs.
The purpose of the present invention is achieved through the following technical solutions：Based on the method to the quick property test evaluation of oil-gas Layer alkali, bag
Include following steps：
（1）The preparation of different pH value salt solution, according to actual conditions, pH value is raised step by step, finally since the pH value of stratum water
One-level salt solution pH value can be set to 12；
（2）The rock core vacuumizing saturation first order salt solution that will be chosen, and 20 ~ 24h is soaked, under conditions of less than critical flow velocity,
The stable permeability K of rock core is measured with first order salt solution1；
（3）Second level salt solution is injected, 20 ~ 24h is soaked, under conditions of less than critical flow velocity, rock core is measured with second level salt solution
Stable permeability K2；
（4）Change the rank of injection salt solution, repeat the（3）Step, until the stabilization of the rock core after measuring afterbody saline treatment
Permeability Kn, pHi-1The permeability K of salt solutioni-1With pHiThe permeability K of salt solutioniBetween meet relational expression
Illustrate alkali has occurred quick, then pHi-1As critical pH.
The quick property of alkali refers to that alkali lye reacts after entering stratum with the quick mineral of alkali in stratum and formation fluid, produces precipitation
Or particulate is discharged, the phenomenon for declining in-place permeability.
In summary, the beneficial effects of the invention are as follows：This method is tested by the quick property of the alkali to oil-gas Layer, obtains standard
True numerical value, after can preventing high ph-values fluid from entering oil-gas Layer, the knot of oil-gas Layer CLAY MINERALS AND THEIR SIGNIFICANCE and silicious gangue will be caused
Structure destroys, so as to cause the blocking of oil-gas Layer to damage；Substantial amounts of hydroxyl can generate insoluble matter with some divalence sun from combination,
The problem of causing the blocking of oil-gas Layer to damage.
Embodiment
With reference to embodiment, the present invention is described in further detail, but embodiments of the present invention are not limited only to
This.
Embodiment：
Based on the method to the quick property test evaluation of oil-gas Layer alkali, comprise the following steps：
（1）The preparation of different pH value salt solution, according to actual conditions, pH value is raised step by step, finally since the pH value of stratum water
One-level salt solution pH value can be set to 12；
（2）The rock core vacuumizing saturation first order salt solution that will be chosen, and 20 ~ 24h is soaked, under conditions of less than critical flow velocity,
The stable permeability K of rock core is measured with first order salt solution1；
（3）Second level salt solution is injected, 20 ~ 24h is soaked, under conditions of less than critical flow velocity, rock core is measured with second level salt solution
Stable permeability K2；
（4）Change the rank of injection salt solution, repeat the（3）Step, until the stabilization of the rock core after measuring afterbody saline treatment
Permeability Kn, pHi-1The permeability K of salt solutioni-1With pHiThe permeability K of salt solutioniBetween meet relational expression
Illustrate alkali has occurred quick, then pHi-1As critical pH.
This method is tested by the quick property of the alkali to oil-gas Layer, is obtained accurate numerical value, can be prevented high ph-values fluid
Into after oil-gas Layer, the structure for causing oil-gas Layer CLAY MINERALS AND THEIR SIGNIFICANCE and silicious gangue is destroyed, so as to cause the blocking of oil-gas Layer
Infringement；Substantial amounts of hydroxyl can generate insoluble matter with some divalence sun from combination, the problem of causing the blocking of oil-gas Layer to damage
Occur.
It is described above, be only presently preferred embodiments of the present invention, any formal limitation not done to the present invention, it is every according to
Any simply modification, the equivalent variations substantially made according to the technology of the present invention, method to above example, each fall within the present invention
Protection domain within.
Claims (1)
1. based on the method to the quick property test evaluation of oil-gas Layer alkali, it is characterised in that comprise the following steps：
（1）The preparation of different pH value salt solution, according to actual conditions, pH value is raised step by step, finally since the pH value of stratum water
One-level salt solution pH value can be set to 12；
（2）The rock core vacuumizing saturation first order salt solution that will be chosen, and 20 ~ 24h is soaked, under conditions of less than critical flow velocity,
The stable permeability K of rock core is measured with first order salt solution1；
（3）Second level salt solution is injected, 20 ~ 24h is soaked, under conditions of less than critical flow velocity, rock core is measured with second level salt solution
Stable permeability K2；
（4）Change the rank of injection salt solution, repeat the and 3. walk, until the stabilization of the rock core after measuring afterbody saline treatment is oozed
Saturating rate Kn, pHi-1The permeability K of salt solutioni-1With pHiThe permeability K of salt solutioniBetween meet relational expression
Illustrate alkali has occurred quick, then pHi-1As critical pH.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610679576.4A CN107764971A (en) | 2016-08-17 | 2016-08-17 | Based on the method to the quick property test evaluation of oil-gas Layer alkali |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610679576.4A CN107764971A (en) | 2016-08-17 | 2016-08-17 | Based on the method to the quick property test evaluation of oil-gas Layer alkali |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN107764971A true CN107764971A (en) | 2018-03-06 |
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201610679576.4A Withdrawn CN107764971A (en) | 2016-08-17 | 2016-08-17 | Based on the method to the quick property test evaluation of oil-gas Layer alkali |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109580454A (en) * | 2019-01-05 | 2019-04-05 | 中国海洋石油集团有限公司 | A method of compact reservoir Fluid Sensitivity is tested with pressure oscillation method |
-
2016
- 2016-08-17 CN CN201610679576.4A patent/CN107764971A/en not_active Withdrawn
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109580454A (en) * | 2019-01-05 | 2019-04-05 | 中国海洋石油集团有限公司 | A method of compact reservoir Fluid Sensitivity is tested with pressure oscillation method |
| CN109580454B (en) * | 2019-01-05 | 2022-02-08 | 中国海洋石油集团有限公司 | Method for testing fluid sensitivity of tight reservoir by using pressure oscillation method |
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| PB01 | Publication | ||
| PB01 | Publication | ||
| WW01 | Invention patent application withdrawn after publication | ||
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Application publication date: 20180306 |