CN107764968A - Casting alloy product quality detection method - Google Patents

Casting alloy product quality detection method Download PDF

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Publication number
CN107764968A
CN107764968A CN201710868111.8A CN201710868111A CN107764968A CN 107764968 A CN107764968 A CN 107764968A CN 201710868111 A CN201710868111 A CN 201710868111A CN 107764968 A CN107764968 A CN 107764968A
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China
Prior art keywords
sample
product quality
casting alloy
alloy product
detection method
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Pending
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CN201710868111.8A
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Chinese (zh)
Inventor
臧永伟
李光
车立志
赵瑞敏
罗映东
陈渝
邹学通
汤顺荣
何维聪
孙荣亮
李永生
龙文再
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Yunnan Yunlv Ruixin Aluminum Co Ltd
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Yunnan Yunlv Ruixin Aluminum Co Ltd
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Priority to CN201710868111.8A priority Critical patent/CN107764968A/en
Publication of CN107764968A publication Critical patent/CN107764968A/en
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    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N33/00Investigating or analysing materials by specific methods not covered by groups G01N1/00 - G01N31/00
    • G01N33/20Metals
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N33/00Investigating or analysing materials by specific methods not covered by groups G01N1/00 - G01N31/00
    • G01N33/20Metals
    • G01N33/202Constituents thereof
    • G01N33/2022Non-metallic constituents
    • G01N33/2025Gaseous constituents

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  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Food Science & Technology (AREA)
  • Medicinal Chemistry (AREA)
  • Physics & Mathematics (AREA)
  • Analytical Chemistry (AREA)
  • Biochemistry (AREA)
  • General Health & Medical Sciences (AREA)
  • General Physics & Mathematics (AREA)
  • Immunology (AREA)
  • Pathology (AREA)
  • Sampling And Sample Adjustment (AREA)
  • Investigating And Analyzing Materials By Characteristic Methods (AREA)

Abstract

The invention discloses a kind of casting alloy product quality detection method, the casting alloy product quality detection method, comprise the following steps:S1:By furnace alloying to molten condition, during refining, contained using sampling instrument from the furnace and take alloy liquid sample;S2:The alloy liquid sample in the sampling instrument is poured into mould and cooled down to generate detection sample;S3;Detect the product quality of the detection sample.Casting alloy product quality detection method according to embodiments of the present invention, contained by using sampling instrument in alloy solution refining process and take alloy and generation is detected into sample, staff can predict the quality of casting alloy product by detecting the product quality of sample.

Description

Casting alloy product quality detection method
Technical field
The present invention relates to casting alloy production technical field, more particularly to a kind of casting alloy product quality detection method.
Background technology
, it is necessary to which strictly the dregginess in control aluminium alloy solution and air content are (main during Production of casting Al alloys For hydrogen content), the two directly affects product pinhole rate grade, and the physical and chemical index that product pinhole rate is client to be paid close attention to the most it One, directly affect product qualification rate.During Production of casting Al alloys, pinhole rate is examined generally to be carried out with solid articles sampling Experiment, and be difficult to test by process product aluminium liquid.In this mode, if solid articles sample pinhole rate is unqualified It can result in the unqualified of whole batch finished product, it is difficult to before finished product comes out improve the remedial measure of pinhole rate, Zhi Neng Finished solid sample pin hole experimental result could judge whether whole batch products are qualified after coming out.Finished product so will be greatly increased not Qualification rate risk, process of rework add energy resource consumption and operating personnel's labor intensity and production cost etc., are unfavorable for giving birth to The energy-saving and clean manufacturing of production process.
The content of the invention
It is contemplated that at least solves one of technical problem present in prior art.Therefore, the present invention proposes a kind of casting Alloy product quality determining method is made, the casting alloy product quality detection method can effectively predict casting alloy product Quality.
Casting alloy product quality detection method according to embodiments of the present invention, comprises the following steps:
S1:By furnace alloying to molten condition, during refining, contained using sampling instrument from the furnace Take alloy liquid sample;
S2:The alloy liquid sample in the sampling instrument is poured into mould and cooled down to generate detection sample;
S3;Detect the product quality of the detection sample.
Casting alloy product quality detection method according to embodiments of the present invention, by using sampling instrument in alloy solution Contained during refining process and take alloy and generation is detected into sample, staff can predict casting by detecting the product quality of sample Make the quality of alloy product.
In certain embodiments, step S3 also comprises the following steps:
Q1:The surface crystallization situation for detecting sample is observed to detect air content, the dregginess of the detection sample.
In certain embodiments, also include in S3 steps:
Q2:Multiple sections are cut out on the detection sample;
Q3:The section crystalline condition for detecting sample is observed to detect air content, the dregginess of the detection sample.
Specifically, in step s3, according to the surface crystallization situation of the detection sample and the prediction casting of section crystalline condition Make air content, the dregginess of alloy product.
In certain embodiments, also comprise the following steps before step S1:
S0:The sampling instrument and the mould are preheated.
In some optional embodiments, the alloy is aluminium alloy.
In certain embodiments, the alloy liquid sample generates the detection sample by natural cooling in step s 2 Product.
In certain embodiments, the sampling instrument is nonmetallic materials.
The additional aspect and advantage of the present invention will be set forth in part in the description, and will partly become from the following description Obtain substantially, or recognized by the practice of the present invention.
Brief description of the drawings
The above-mentioned and/or additional aspect and advantage of the present invention will become in the description from combination accompanying drawings below to embodiment Substantially and it is readily appreciated that, wherein:
Fig. 1 is the casting alloy product quality detection method schematic flow sheet of the embodiment of the present invention.
Embodiment
Embodiments of the invention are described below in detail, the example of the embodiment is shown in the drawings, wherein from beginning to end Same or similar label represents same or similar element or the element with same or like function.Below with reference to attached The embodiment of figure description is exemplary, is only used for explaining the present invention, and is not considered as limiting the invention.
The specific steps of casting alloy product quality detection method according to embodiments of the present invention are described below with reference to Fig. 1.
As shown in figure 1, casting alloy product quality detection method according to embodiments of the present invention, comprises the following steps:
S1:By furnace alloying to molten condition, during refining, contained using sampling instrument from furnace and take conjunction Golden liquid sample;S2:Alloy liquid sample in sampling instrument is poured into mould and cooled down to generate detection sample;S3;Detection Detect the product quality of sample.
It is understood that furnace alloying is to molten condition, it is aluminium alloy by process product during refining Body takes out part and imported in mould, and after alloy liquid cools down generation detection sample completely, the quality of detection detection sample can be with The alloy solution of furnace is prejudged in the quality as final products.If testing result is satisfied the criteria, the conjunction in furnace Gold solution is used directly for casting.But if testing result is not inconsistent standardization, that is to say, that detection sample is the qualified production in portion Product, it is believed that the alloy solution existing defects in furnace, it is impossible to be directly used in casting.Staff can with according to testing result, Working condition, raw material components to furnace etc. adjust, and are then repeating above-mentioned detecting step.The casting of the embodiment of the present invention The quality of casting alloy product can be predicted by making alloy product quality determining method so that staff can adjust smelting in time Parameter, so as to improve the qualification rate of product, probability of doing over again is reduced, saves prime cost.
Casting alloy product quality detection method according to embodiments of the present invention, by using sampling instrument in alloy solution Contained during refining process and take alloy and generation is detected into sample, staff can predict casting by detecting the product quality of sample Make the quality of alloy product.
In certain embodiments, step S3 also comprises the following steps:Q1:The surface crystallization situation of observation detection sample is to examine Survey air content, the dregginess of detection sample.It should be noted that the form of surface crystallization being capable of reaction detection to a certain extent The air content and dregginess of sample outer surface, and detect sample surfaces crystalline condition can represent to a certain extent casting close The surface crystallization situation of golden product.Therefore, staff can predict casting by detecting air content and the dregginess of sample The air content and dregginess of alloy product, so as to reach the purpose of prediction casting alloy product quality.
In certain embodiments, also include in S3 steps:Q2:Multiple sections are cut out on detection sample;Q3:Observation inspection The section crystalline condition of test sample product is to detect sample air content, dregginess.It should be noted that the form of section crystallization can be The air content and dregginess of reaction detection sample interior to a certain extent, and sample in cross section crystalline condition is detected to a certain degree On can represent casting alloy product inside crystalline condition.Therefore, staff can be by detecting the air content of sample The air content of casting alloy product and dregginess are predicted with dregginess, so as to reach the mesh of prediction casting alloy product quality 's.
Advantageously, multiple sections not of uniform size, different, direction is different are cut off on detection sample.So can be with The representativeness in section is improved, improves the accuracy of casting alloy product quality forecast.
Advantageously, in step s3, closed according to the surface crystallization situation of detection sample and the prediction casting of section crystalline condition Air content, the dregginess of golden product.Thus, it is possible to improve the accuracy of casting alloy product quality forecast.Certainly in this hair Only it can predict that casting alloy produces by the surface crystallization that detects sample or section crystalline condition in bright other embodiment Air content, the dregginess of product.
In certain embodiments, also comprise the following steps before step S1:
S0:Sampling instrument and mould are preheated.It should be noted that if sampling instrument carries steam, then The hydrogen content of alloy solution can be increased in sampling process, the quality of casting alloy product is had adverse effect on.Band in mould There is steam not only to influence to detect the crystallization degree of sample, prevent it from the quality of reacting alloy solution exactly, and closing Easily exploded in the cooling procedure of gold solution, endanger personal safety.In summary, sampling instrument and mould are preheated It can not only avoid sampling instrument from influenceing the quality of alloy solution, reduce the forecasting inaccuracy exactness of final product quality, be also prevented from Exploded in alloy solution cooling procedure, improve security.
In some optional embodiments, alloy is aluminium alloy.The matter of the casting alloy product of certain embodiment of the present invention Quantity measuring method can also detect other alloy product quality, such as titanium alloy etc..
In certain embodiments, alloy liquid sample generates detection sample by natural cooling in step s 2.It can manage Solution, alloy liquid sample natural cooling production detection sample can reduce cost, in addition, the detection sample of natural cooling generation Product can react air content and dregginess in alloy solution to greatest extent, so as to be lifted to casting alloy product quality forecast Accuracy.
In certain embodiments, sampling instrument is nonmetallic materials.It is understood that if sampling instrument utilizes metal Material is made, and is easily aligned gold solution and produces pollution, and then influences the product quality of casting alloy product.Thus, using by non- Sampling instrument made of metal material can reduce pollution of the sampling instrument to alloy solution, ensure the degree of purity of alloy solution.
The casting alloy product quality detection method of a specific embodiment of the invention is described below.
The casting alloy product quality detection method of the present embodiment comprises the following steps:
P1:Sampling instrument and mould are preheated so that the two keeps drying.
P2:During the refining of alloy liquid, contained using sampling instrument from furnace and take alloy liquid sample;
P3:Alloy liquid sample in sampling instrument is poured into mould and cooled down to generate detection sample;
P4:The surface crystallization situation of observation detection sample detects air content, the dregginess of sample to detect.
P5:Multiple sections are cut out on detection sample;
P6:The section crystalline condition of observation detection sample detects air content, the dregginess of sample to detect.
P7:Air content, the dregginess of surface crystallization situation and section crystalline condition prediction casting alloy product.
The casting alloy quality product detection method of the present embodiment, sampling, cooling excessively to process product (alloy solution), Detection sample is ultimately generated, by observing detection sample surfaces and section crystalline condition, can effectively predict that the batch process produces Whether pinhole rate of the product (alloy solution) when as final finished be qualified, and staff can be according to prediction result, in process The middle remedial measure implemented to alloy solution, greatly improves final products qualification rate.
In the description of this specification, reference term " one embodiment ", " some embodiments ", " example ", " specifically show The description of example " or " some examples " etc. means specific features, structure, material or the spy for combining the embodiment or example description Point is contained at least one embodiment or example of the present invention.In this manual, to the schematic representation of above-mentioned term not Necessarily refer to identical embodiment or example.Moreover, specific features, structure, material or the feature of description can be any One or more embodiments or example in combine in an appropriate manner.
Although an embodiment of the present invention has been shown and described, it will be understood by those skilled in the art that:Not In the case of departing from the principle and objective of the present invention a variety of change, modification, replacement and modification can be carried out to these embodiments, this The scope of invention is limited by claim and its equivalent.

Claims (8)

1. a kind of casting alloy product quality detection method, it is characterised in that comprise the following steps:
S1:By furnace alloying to molten condition, during refining, contained using sampling instrument from the furnace and take conjunction Golden liquid sample;
S2:The alloy liquid sample in the sampling instrument is poured into mould and cooled down to generate detection sample;
S3;Detect the product quality of the detection sample.
2. casting alloy product quality detection method according to claim 1, it is characterised in that step S3 also includes as follows Step:
Q1:The surface crystallization situation for detecting sample is observed to detect air content, the dregginess of the detection sample.
3. casting alloy product quality detection method according to claim 1 or 2, it is characterised in that in S3 steps also Including:
Q2:Multiple sections are cut out on the detection sample;
Q3:The section crystalline condition for detecting sample is observed to detect air content, the dregginess of the detection sample.
4. casting alloy product quality detection method according to claim 3, it is characterised in that in step s3, according to The surface crystallization situation of the detection sample and air content, the dregginess of section crystalline condition prediction casting alloy product.
5. casting alloy product quality detection method according to claim 1, it is characterised in that also include before step S1 Following steps:
S0:The sampling instrument and the mould are preheated.
6. casting alloy product quality detection method according to claim 1, it is characterised in that the alloy closes for aluminium Gold.
7. casting alloy product quality detection method according to claim 1, it is characterised in that the conjunction in step s 2 Golden liquid sample generates the detection sample by natural cooling.
8. casting alloy product quality detection method according to claim 1, it is characterised in that the sampling instrument is non- Metal material.
CN201710868111.8A 2017-09-22 2017-09-22 Casting alloy product quality detection method Pending CN107764968A (en)

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN111893302A (en) * 2020-06-23 2020-11-06 洛阳双瑞万基钛业有限公司 Point type process and device for detecting carbon value of titanium sponge by quickly reducing titanium tetrachloride
CN114280266A (en) * 2021-12-27 2022-04-05 河南省产品质量监督检验院 Product quality detection method and detection device

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CN103160640A (en) * 2013-02-26 2013-06-19 河北钢铁股份有限公司邯郸分公司 Method of dynamically detecting contents of manganese, phosphorus and sulphur of slag in converter steelmaking process
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Patent Citations (3)

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CN101576498A (en) * 2009-06-23 2009-11-11 中国船舶重工集团公司第十二研究所 Method for analyzing and detecting alloying elements in beryllium-aluminum alloy
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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN111893302A (en) * 2020-06-23 2020-11-06 洛阳双瑞万基钛业有限公司 Point type process and device for detecting carbon value of titanium sponge by quickly reducing titanium tetrachloride
CN114280266A (en) * 2021-12-27 2022-04-05 河南省产品质量监督检验院 Product quality detection method and detection device

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Application publication date: 20180306