CN107760008A - The preparation method of colour polyurethane material - Google Patents

The preparation method of colour polyurethane material Download PDF

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Publication number
CN107760008A
CN107760008A CN201710947347.0A CN201710947347A CN107760008A CN 107760008 A CN107760008 A CN 107760008A CN 201710947347 A CN201710947347 A CN 201710947347A CN 107760008 A CN107760008 A CN 107760008A
Authority
CN
China
Prior art keywords
pigment
polyurethane material
preparation
colour
reactor
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201710947347.0A
Other languages
Chinese (zh)
Inventor
罗凌
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Guangdong Hua Stick New Material Research Co Ltd
Original Assignee
Guangdong Hua Stick New Material Research Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Guangdong Hua Stick New Material Research Co Ltd filed Critical Guangdong Hua Stick New Material Research Co Ltd
Priority to CN201710947347.0A priority Critical patent/CN107760008A/en
Publication of CN107760008A publication Critical patent/CN107760008A/en
Pending legal-status Critical Current

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Classifications

    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08KUse of inorganic or non-macromolecular organic substances as compounding ingredients
    • C08K3/00Use of inorganic substances as compounding ingredients
    • C08K3/02Elements
    • C08K3/04Carbon
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08KUse of inorganic or non-macromolecular organic substances as compounding ingredients
    • C08K3/00Use of inorganic substances as compounding ingredients
    • C08K3/18Oxygen-containing compounds, e.g. metal carbonyls
    • C08K3/20Oxides; Hydroxides
    • C08K3/22Oxides; Hydroxides of metals
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08KUse of inorganic or non-macromolecular organic substances as compounding ingredients
    • C08K5/00Use of organic ingredients
    • C08K5/0008Organic ingredients according to more than one of the "one dot" groups of C08K5/01 - C08K5/59
    • C08K5/0041Optical brightening agents, organic pigments
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08KUse of inorganic or non-macromolecular organic substances as compounding ingredients
    • C08K3/00Use of inorganic substances as compounding ingredients
    • C08K3/18Oxygen-containing compounds, e.g. metal carbonyls
    • C08K3/20Oxides; Hydroxides
    • C08K3/22Oxides; Hydroxides of metals
    • C08K2003/2237Oxides; Hydroxides of metals of titanium
    • C08K2003/2241Titanium dioxide
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08KUse of inorganic or non-macromolecular organic substances as compounding ingredients
    • C08K3/00Use of inorganic substances as compounding ingredients
    • C08K3/18Oxygen-containing compounds, e.g. metal carbonyls
    • C08K3/20Oxides; Hydroxides
    • C08K3/22Oxides; Hydroxides of metals
    • C08K2003/2265Oxides; Hydroxides of metals of iron
    • C08K2003/2272Ferric oxide (Fe2O3)

Abstract

The invention discloses the preparation method of colour polyurethane material to comprise the following steps:A, choose suitable pigment and determine to be formulated, prepare the pigment prepared;B, the pigment prepared prepares by 0.1% the 0.5% of the percentage by weight of polyurethane material, and dry at a temperature of 100 DEG C 120 DEG C make within 3 hours 2 hours it is standby;C, polyurethane material pours into reactor, and is preheating to 80 DEG C 100 DEG C;C, reactor mixing speed is started in 100 r/min 120r/min, and then control temperature is uniformly added into the ready pigment of step b between 80 DEG C 100 DEG C, mixing time is 1 hour 0.5 hour, forms colour polyurethane finished material.The colour polyurethane material that the inventive method is produced, meet the needs of client is to polyurethane color, produce the polyurethane material that color is needed by client.

Description

The preparation method of colour polyurethane material
Technical field
The present invention relates to a kind of preparation method of new material, more specifically, is related to a kind of colour polyurethane material Preparation method.
Background technology
Polyurethane material made from conventional method, although possessing good toughness, existing polyurethane material is usually Raw material color, mostly yellow or brown.But arranged in pairs or groups therewith in industrial production has a variety of colors using material.It can thus make Influenceed attractive in appearance into aberration.The present invention just needs the polyurethane material of color according to the demand of client, production client.So for The applicability of polyurethane is lifted, meets the needs of various high requests, it is equally significant to create considerable prospect for sales, fixed Good benefit will be created for society and enterprise.
The content of the invention
It is an object of the invention to overcome the deficiencies of the prior art and provide a kind of preparation method of colour polyurethane material, To meet needs that client is required color.
The present invention solve prior art technical scheme be:The preparation method of colour polyurethane material, comprises the following steps:
A, suitable pigment is chosen, and is tuned into the color determination formula of needs in proportion by experiment, and prepares the face prepared Material;
B, the pigment prepared is prepared by the 0.1%-0.5% of the percentage by weight of polyurethane material, and in 100 DEG C -120 DEG C of temperature Lower drying is made standby for -3 hours 2 hours;Pigment can be inorganic pigment or organic pigment, or inorganic pigment and organic pigment Mixture;Wherein described inorganic pigment be inorganic pigment include various metal oxides, chromate, carbonate, sulfate and Sulfide etc.;Described organic pigment is AZOpigments, phthalocyanine color, triaryl methane pigment, polycyclic pigment etc.;
C, polyurethane material pours into reactor, and the temperature for being preheating to 80 DEG C -100 DEG C is standby;
D, the agitator of reactor is started, control mixing speed is in 100 r/min -120r/min, and control temperature is at 80 DEG C -100 Between DEG C, the ready pigment of step b is then uniformly added into, mixing time is -1 hour 0.5 hour, forms colour polyurethane material Expect finished product.
The colour polyurethane material that the inventive method is produced, meets the needs of client is to polyurethane color, production is by visitor Family needs the polyurethane material of color.So for the applicability for lifting polyurethane, meet the needs of various high requests, creation can The prospect for sales of sight is equally significant, fixed to create good benefit for society and enterprise.
Embodiment
Embodiment 1:
The preparation method of colour polyurethane material, comprises the following steps:
A, carbon black and the pigment of titanium white mixing are selected, and is tuned into the gray color formula of needs in proportion by experiment, and is prepared The pigment prepared;
B, the pigment prepared prepares by the 0.2% of the percentage by weight of polyurethane material, and is dried 2 hours at a temperature of 100 DEG C Make standby;
C, polyurethane material pours into reactor, and the temperature for being preheating to 80 DEG C is standby;
D, the agitator of reactor is started, then control mixing speed is uniformly added into 100 r/min, control temperature at 100 DEG C The ready pigment of step b, mixing time are 1 hour, form grey polyurethane material finished product.
Embodiment 2:
The preparation method of colour polyurethane material, comprises the following steps:
A, selective oxidation iron oxide red and cadmium yellow pigment, and the orange color formulas of needs is tuned into by experiment in proportion, and prepare and match somebody with somebody Good pigment;
B, the pigment prepared is prepared by the 0.1%-0.5% of the percentage by weight of polyurethane material, and is dried at a temperature of 120 DEG C Make within 3 hours standby;
C, polyurethane material pours into reactor, and the temperature for being preheating to 100 DEG C is standby;
D, the agitator of reactor is started, then control mixing speed is uniformly added into 120r/min, control temperature at 100 DEG C The ready pigment of step b, mixing time are 1 hour, form orange polyurethane material finished product.
Embodiment 3
The preparation method of colour polyurethane material, comprises the following steps:
A, the pigment of phthalocyanine blue and iron oxide red mixing synthesis is selected, and the purple colors of needs is tuned into by experiment in proportion and matched somebody with somebody Side, and prepare the pigment prepared;
B, the pigment prepared prepares by the 0.2% of the percentage by weight of polyurethane material, and drying 2.5 is small at a temperature of 110 DEG C When make it is standby;
C, polyurethane material pours into reactor, and the temperature for being preheating to 90 DEG C is standby;
D, the agitator of reactor is started, then control mixing speed is uniformly added into step in 110r/min, control temperature at 90 DEG C The ready pigment of rapid b, mixing time are 1 hour, form purple polyurethane material finished product.
The above described is only a preferred embodiment of the present invention, not the structure of the present invention is made any formal Limitation.Any simple modification, equivalent change and modification that every technical spirit according to the present invention is made to above example, In the range of still falling within technical scheme.

Claims (4)

1. the preparation method of colour polyurethane material, it is characterised in that:Comprise the following steps:
A, suitable pigment is chosen, and is tuned into the color determination formula of needs in proportion by experiment, and prepares the face prepared Material;
B, the pigment prepared is prepared by the 0.1%-0.5% of the percentage by weight of polyurethane material, and in 100 DEG C -120 DEG C of temperature Lower drying is made standby for -3 hours 2 hours;
C, polyurethane material pours into reactor, and the temperature for being preheating to 80 DEG C -100 DEG C is standby;
D, the agitator of reactor is started, control mixing speed is in 100 r/min -120r/min, and control temperature is at 80 DEG C -100 Between DEG C, the ready pigment of step b is then uniformly added into, mixing time is -1 hour 0.5 hour, forms colour polyurethane material Expect finished product.
2. the preparation method of colour polyurethane material according to claim 1, it is characterised in that:The pigment is inorganic pigment Or the one or more in organic pigment.
3. the preparation method of colour polyurethane material according to claim 1, it is characterised in that:The pigment is inorganic pigment With the mixture of organic pigment.
4. the preparation method of colour polyurethane material according to claim 1, it is characterised in that:Described inorganic pigment is nothing Machine pigment includes various metal oxides, chromate, carbonate, sulfate and sulfide etc.;Described organic pigment is azo Pigment, phthalocyanine color, triaryl methane pigment, polycyclic pigment etc..
CN201710947347.0A 2017-10-12 2017-10-12 The preparation method of colour polyurethane material Pending CN107760008A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201710947347.0A CN107760008A (en) 2017-10-12 2017-10-12 The preparation method of colour polyurethane material

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201710947347.0A CN107760008A (en) 2017-10-12 2017-10-12 The preparation method of colour polyurethane material

Publications (1)

Publication Number Publication Date
CN107760008A true CN107760008A (en) 2018-03-06

Family

ID=61267148

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201710947347.0A Pending CN107760008A (en) 2017-10-12 2017-10-12 The preparation method of colour polyurethane material

Country Status (1)

Country Link
CN (1) CN107760008A (en)

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103289358A (en) * 2013-05-20 2013-09-11 深圳市沃特新材料股份有限公司 Colorized conductive thermoplastic polyurethane elastomer composite material and preparation method thereof
CN104830047A (en) * 2014-05-09 2015-08-12 晋江国盛新材料科技有限公司 Method of producing moulded body and thin sheet with color TPU foamed particle and sheet material
CN106632966A (en) * 2017-01-17 2017-05-10 广东工业大学 Polyurethane material and preparation method thereof, as well as polyurethane runway aggregates

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103289358A (en) * 2013-05-20 2013-09-11 深圳市沃特新材料股份有限公司 Colorized conductive thermoplastic polyurethane elastomer composite material and preparation method thereof
CN104830047A (en) * 2014-05-09 2015-08-12 晋江国盛新材料科技有限公司 Method of producing moulded body and thin sheet with color TPU foamed particle and sheet material
CN106632966A (en) * 2017-01-17 2017-05-10 广东工业大学 Polyurethane material and preparation method thereof, as well as polyurethane runway aggregates

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
陈侃: "彩色导电可控聚氨酯薄膜的制备与研究", 《中国优秀硕士学位论文全文数据库 工程科技Ⅰ辑》 *

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Application publication date: 20180306