CN107754796B - Hydrothermal stirring equipment for cuprous oxide-titanium dioxide photocatalytic composite material experiment - Google Patents
Hydrothermal stirring equipment for cuprous oxide-titanium dioxide photocatalytic composite material experiment Download PDFInfo
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- CN107754796B CN107754796B CN201710967878.6A CN201710967878A CN107754796B CN 107754796 B CN107754796 B CN 107754796B CN 201710967878 A CN201710967878 A CN 201710967878A CN 107754796 B CN107754796 B CN 107754796B
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- 238000003756 stirring Methods 0.000 title claims abstract description 65
- 239000002131 composite material Substances 0.000 title claims abstract description 22
- GWEVSGVZZGPLCZ-UHFFFAOYSA-N titanium dioxide Inorganic materials O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 title claims abstract description 21
- 230000001699 photocatalysis Effects 0.000 title claims abstract description 20
- 239000004408 titanium dioxide Substances 0.000 title claims abstract description 20
- 238000002474 experimental method Methods 0.000 title claims abstract description 17
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 24
- 238000010438 heat treatment Methods 0.000 claims abstract description 23
- 238000007146 photocatalysis Methods 0.000 claims abstract description 3
- 238000003860 storage Methods 0.000 claims description 8
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical group [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 claims description 7
- 239000008236 heating water Substances 0.000 claims 1
- 238000009434 installation Methods 0.000 abstract description 10
- 239000000463 material Substances 0.000 abstract description 2
- 238000000034 method Methods 0.000 description 8
- 238000002156 mixing Methods 0.000 description 6
- 230000009471 action Effects 0.000 description 3
- 239000003638 chemical reducing agent Substances 0.000 description 3
- 238000000151 deposition Methods 0.000 description 3
- 235000015205 orange juice Nutrition 0.000 description 3
- 230000008569 process Effects 0.000 description 3
- 238000005054 agglomeration Methods 0.000 description 2
- 230000002776 aggregation Effects 0.000 description 2
- 230000015572 biosynthetic process Effects 0.000 description 2
- 238000006243 chemical reaction Methods 0.000 description 2
- 230000001276 controlling effect Effects 0.000 description 2
- 230000007547 defect Effects 0.000 description 2
- 230000004048 modification Effects 0.000 description 2
- 238000012986 modification Methods 0.000 description 2
- 239000000843 powder Substances 0.000 description 2
- 238000002360 preparation method Methods 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- 230000004075 alteration Effects 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000005540 biological transmission Effects 0.000 description 1
- 230000015556 catabolic process Effects 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 238000010276 construction Methods 0.000 description 1
- 229910000365 copper sulfate Inorganic materials 0.000 description 1
- ARUVKPQLZAKDPS-UHFFFAOYSA-L copper(II) sulfate Chemical compound [Cu+2].[O-][S+2]([O-])([O-])[O-] ARUVKPQLZAKDPS-UHFFFAOYSA-L 0.000 description 1
- 239000013078 crystal Substances 0.000 description 1
- 238000006731 degradation reaction Methods 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- 238000000502 dialysis Methods 0.000 description 1
- 238000009826 distribution Methods 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 230000007613 environmental effect Effects 0.000 description 1
- 238000001027 hydrothermal synthesis Methods 0.000 description 1
- 150000002484 inorganic compounds Chemical class 0.000 description 1
- 229910010272 inorganic material Inorganic materials 0.000 description 1
- FDZZZRQASAIRJF-UHFFFAOYSA-M malachite green Chemical compound [Cl-].C1=CC(N(C)C)=CC=C1C(C=1C=CC=CC=1)=C1C=CC(=[N+](C)C)C=C1 FDZZZRQASAIRJF-UHFFFAOYSA-M 0.000 description 1
- 229940107698 malachite green Drugs 0.000 description 1
- 230000007246 mechanism Effects 0.000 description 1
- 239000013081 microcrystal Substances 0.000 description 1
- 239000002245 particle Substances 0.000 description 1
- 238000011056 performance test Methods 0.000 description 1
- 238000000746 purification Methods 0.000 description 1
- 230000001105 regulatory effect Effects 0.000 description 1
- 238000007789 sealing Methods 0.000 description 1
- 239000002904 solvent Substances 0.000 description 1
- 238000006467 substitution reaction Methods 0.000 description 1
- 238000012360 testing method Methods 0.000 description 1
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
- B01J23/70—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of the iron group metals or copper
- B01J23/72—Copper
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J35/00—Catalysts, in general, characterised by their form or physical properties
- B01J35/30—Catalysts, in general, characterised by their form or physical properties characterised by their physical properties
- B01J35/39—Photocatalytic properties
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- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Physical Or Chemical Processes And Apparatus (AREA)
- Mixers Of The Rotary Stirring Type (AREA)
Abstract
The invention discloses hydrothermal stirring equipment for a cuprous oxide-titanium dioxide photocatalytic composite material experiment, which comprises a working box, wherein the top of the inner wall of the working box is fixedly connected with an energy supply output box, two sides of the inner cavity of the energy supply output box are respectively provided with an electromagnetic coil, the bottom of the inner wall of the energy supply output box is fixedly connected with a rotating power box, the bottom of the inner wall of the rotating power box is fixedly connected with an electromagnetic rotating device through an installation frame, and the top of the electromagnetic rotating device is rotatably connected with a telescopic stirrer through a rotating shaft. This hydrothermal agitated vessel for cuprous oxide-titanium dioxide photocatalysis combined material experiments has solved that water heats and the telescopic agitator stirs and experimental article deposits, and the supply of energy and agitator carry out the efficiency that stirs to water when being convenient for water heating have guaranteed that water can the even heating and deposit with deposit the thing and stabilize and deposit, stably carry out the hydrothermal, guarantee the problem of hydrothermal efficiency.
Description
Technical Field
The invention relates to the technical field of photocatalytic composite materials, in particular to hydrothermal stirring equipment for an experiment of a cuprous oxide-titanium dioxide photocatalytic composite material.
Background
The cuprous oxide-titanium dioxide composite material generated by the copper sulfate and the titanium dioxide plays the role of a reducing agent and a template. Scanning electron microscope tests show that the prepared product is several micrometers to dozens of micrometers, and comparison of all samples shows that the particles of the composite material prepared in an orange juice system are small and uniformly distributed, which indicates that orange juice has a regulating and controlling effect on the formation of the composite material. After being subjected to a photocatalytic performance test by malachite green, the composite material prepared by taking the orange juice as the reducing agent has better degradation performance than the composite material prepared by taking Vc as the reducing agent, is green and environment-friendly, has little pollution, can be used as a chemical component to act and participate in reaction under the hydrothermal condition, is a solvent and a mineralizer, and can also be used as a pressure transmission medium; the formation and modification of inorganic compound can be realized by participating in dialysis reaction and controlling physical and chemical factors, etc. the preparation method can be used for preparing single-component micro crystal and preparing double-component or multi-component special compound powder. The method overcomes the inevitable hard agglomeration in certain high-temperature preparation, and the like, and has the characteristics of fine powder (nanometer level), high purity, good dispersibility, uniformity, narrow distribution, no agglomeration, good crystal form, controllable shape, contribution to environmental purification and the like, and the defects of uniform heating and uniform heat supply of water in the conventional hydrothermal method.
Disclosure of Invention
Technical problem to be solved
Aiming at the defects of the prior art, the invention provides hydrothermal stirring equipment for a cuprous oxide-titanium dioxide photocatalytic composite material experiment, which solves the problems that water is heated, a telescopic stirrer is used for stirring and storing experimental articles, the energy is supplied when the water is heated, the efficiency of stirring the water by the stirrer is facilitated, the water can be uniformly heated and the stored articles can be stably stored, the hydrothermal is stably carried out, and the hydrothermal efficiency is ensured.
(II) technical scheme
In order to achieve the purpose, the invention is realized by the following technical scheme: a hydrothermal mixing device for an experiment of a cuprous oxide-titanium dioxide photocatalytic composite material comprises a working box, wherein an energy supply output box is fixedly connected to the top of the inner wall of the working box, electromagnetic coils are respectively arranged on two sides of the inner cavity of the energy supply output box and are electrically connected through a lead, a rotating power box is fixedly connected to the bottom of the inner wall of the energy supply output box, an electromagnetic rotating device is fixedly connected to the bottom of the inner wall of the rotating power box through a mounting frame, the top of the electromagnetic rotating device is rotatably connected with a telescopic stirrer through a rotating shaft, a hydrothermal box is fixedly connected to the top of the outer wall of the energy supply output box, a fixed working frame is fixedly connected to the bottom of the inner wall of the hydrothermal box, supporting frames are fixedly connected to two sides of the top of the fixed working frame, the top of the locking device is provided with a telescopic fixing device;
the telescopic fixing device comprises a first telescopic plate and a second telescopic plate, the left side of the first telescopic plate and the right side of the second telescopic plate are movably connected with one side of the supporting rack respectively, the left side of the second telescopic plate penetrates through the right side of the first telescopic plate and extends into the first telescopic plate, a base is fixedly connected to one side of the top of the inner wall of the first telescopic plate, a clamping rod is rotatably connected to the bottom of the second base, a vertical plate is fixedly connected to the top of the inner wall of the first telescopic plate and located on two sides of the base, a first spring is fixedly connected to one side, opposite to the vertical plate, of the top of the second telescopic plate and two sides of the base, and a clamping groove matched with the clamping rod is formed in the top of the second telescopic plate;
the clamping and locking device comprises a bottom frame, the left side of the bottom frame is fixedly connected with the surface of a supporting rack, a movable rod penetrates through one side of the bottom frame, the movable rod is located on an inner end fixedly connected with movable plate of the bottom frame, the top and the bottom of one side of the movable plate are both fixedly connected with the bottom frame through a second spring, and the movable rod is located on an outer end fixedly connected with clamping head of the bottom frame.
Preferably, the top of the water heating tank is fixedly connected with a closed cover, and one side of the top of the fixed working rack is fixedly connected with a temperature detector.
Preferably, the two sides of the inner wall of the water heating box are both provided with illuminating lamps, and the inner wall of the working box is provided with an electromagnetic heating coil.
Preferably, the electromagnetic rotating device comprises an electromagnetic working box, a power box is fixedly connected to the bottom of the inner wall of the electromagnetic working box, and a power supply is fixedly connected to the bottom of the inner wall of the power box.
Preferably, a main electromagnet core is fixedly connected to the middle position of the top of the inner wall of the electromagnetic work box, a magnetic force rotary installer is fixedly connected to the top of the main electromagnet core, a main coil is sleeved on the outer wall of the main electromagnet core, and the main coil is electrically connected with a power supply.
Preferably, the two sides of the top of the inner wall of the electromagnetic working box are respectively and fixedly connected with an auxiliary electromagnetic core, an auxiliary electromagnetic coil is sleeved on the outer wall of the auxiliary electromagnetic core, and the auxiliary electromagnetic coil is electrically connected with a power supply.
Preferably, the top of the electromagnetic working box is provided with a rotating rack, the bottom of the rotating rack is fixedly connected with a permanent magnet through a magnet mounting rack, and the middle of a cavity of the rotating rack is fixedly connected with a rotating shaft through a mounting rack.
Preferably, telescopic agitator includes the installation base, the installation base rotates through connecting the pivot to be connected with and deposits the stirring cavity, deposit stirring cavity outer wall fixedly connected with stirring fan blade.
Preferably, the inner wall of the storage stirring cavity is provided with a telescopic stirring shaft, and the top end of the telescopic stirring shaft is fixedly connected with an installation unit.
Preferably, the fixed outer wall of flexible (mixing) shaft fixedly connected with time stirring fan blade and folding stirring fan blade, folding stirring fan blade is provided with folding unit.
(III) advantageous effects
The invention provides hydrothermal stirring equipment for an experiment of a cuprous oxide-titanium dioxide photocatalytic composite material. The method has the following beneficial effects:
(1) the hydrothermal stirring device for the cuprous oxide-titanium dioxide photocatalytic composite material experiment, the electromagnetic coil and the electromagnetic heating coil which are arranged in the work box are used for heating, the electromagnetic rotating device in the rotating power box provides power through the main electromagnetic iron core, the main coil, the auxiliary electromagnetic iron core and the auxiliary electromagnetic coil to drive the rotating frame to rotate, thereby drive telescopic agitator and rotate, the stirring cavity of depositing and stirring fan blade of telescopic agitator can stir water, flexible (mixing) shaft drives stirring fan blade, folding stirring fan blade rotates, folding stirring fan blade is folded through folding unit, reached and carried out the purpose of stirring with telescopic agitator that heats water, supply of energy and agitator carry out the efficiency that stirs to water when being convenient for the water heating, guaranteed that water can the even heating.
(2) This hydrothermal agitated vessel for cuprous oxide-titanium dioxide photocatalysis combined material experiments can fix through kelly and draw-in groove through flexible fixing device, and latch device can carry out the rigidity to flexible fixing device through second spring, fly leaf, movable rod and dop, has reached the purpose of depositing experimental article, has guaranteed to steadily to deposit the thing of depositing, stably carries out the hydrothermal, guarantees hydrothermal efficiency.
Drawings
FIG. 1 is a schematic structural view of the present invention as a whole;
FIG. 2 is a schematic structural diagram of an electromagnetic rotating apparatus according to the present invention;
FIG. 3 is a schematic view of the construction of the telescopic stirrer according to the present invention;
FIG. 4 is a schematic structural view of the retractable fixing device of the present invention;
FIG. 5 is a schematic view of the latch mechanism of the present invention.
In the figure: 1 work box, 2 energy supply output box, 3 electromagnetic coil, 4 wire, 5 rotating power box, 6 electromagnetic rotating device, 601 electromagnetic work box, 602 power box, 603 power supply, 604 main electromagnetic core, 605 main coil, 606 magnetic force rotating installation device, 607 auxiliary electromagnetic core, 608 auxiliary electromagnetic coil, 609 rotating frame, 610 magnet installation frame, 611 permanent magnet, 612 installation frame, 613 rotating shaft, 7 water heating box, 8 rotating shaft, 9 telescopic stirrer, 901 installation base, 902 storage stirring cavity, 903 stirring fan blade, 904 telescopic stirring shaft, 905 installation unit, 906 stirring fan blade, 907 folding stirring fan blade, 908 folding unit, 10 fixed work frame, 11 telescopic fixing device, 111 first telescopic plate, riser 112, 113 base, 114 clamping rod, 115 first spring, 116 clamping groove, 117 second telescopic plate, 12 clamping device, 121 bottom frame, 122 second spring, 123 movable plate, 124 movable rod, 125 chuck, 13 support frame, 14 temperature detector, 15 lighting lamp, 16 sealing cover and 17 electromagnetic heating coil.
Detailed Description
The technical solutions in the embodiments of the present invention will be clearly and completely described below with reference to the drawings in the embodiments of the present invention, and it is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all of the embodiments. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.
Referring to fig. 1-5, the present invention provides a technical solution: a hydrothermal mixing device for an experiment of a cuprous oxide-titanium dioxide photocatalytic composite material comprises a working box 1, wherein the top of the inner wall of the working box 1 is fixedly connected with an energy supply output box 2, two sides of the inner cavity of the energy supply output box 2 are respectively provided with an electromagnetic coil 3, the electromagnetic coils 3 are electrically connected through a lead 4, the bottom of the inner wall of the energy supply output box 2 is fixedly connected with a rotating power box 5, the bottom of the inner wall of the rotating power box 5 is fixedly connected with an electromagnetic rotating device 6 through a mounting frame, the top of the electromagnetic rotating device 6 is rotatably connected with a telescopic stirrer 9 through a rotating shaft 8, the top of the outer wall of the energy supply output box 2 is fixedly connected with a hydrothermal box 7, the bottom of the inner wall of the hydrothermal box 7 is fixedly connected with a fixed working frame 10, two sides of, the top of the locking device 12 is provided with a telescopic fixing device 11;
the telescopic fixing device 11 comprises a first telescopic plate 111 and a second telescopic plate 117, the left side of the first telescopic plate 111 and the right side of the second telescopic plate 117 are movably connected with one side of the supporting frame 13 respectively, the left side of the second telescopic plate 117 penetrates through the right side of the first telescopic plate 111 and extends into the first telescopic plate 111, one side of the top of the inner wall of the first telescopic plate 111 is fixedly connected with a base 113, the bottom of the base 113 is rotatably connected with a clamping rod 114, the top of the inner wall of the first telescopic plate 111 and the two sides of the base 113 are fixedly connected with vertical plates 112, one side of the vertical plates 112 opposite to the two sides of the base 113 are fixedly connected with first springs 115, and the top of the second telescopic plate 117 is provided with a clamping groove 116 matched with the clamping rod 114;
the locking device 12 includes a bottom frame 121, a left side of the bottom frame 121 is fixedly connected to a surface of the supporting frame 13, a movable rod 124 penetrates through one side of the bottom frame 121, the movable rod 124 is located on an end fixedly connected to a movable plate 123 inside the bottom frame 121, a top and a bottom of one side of the movable plate 123 are both fixedly connected to the bottom frame 121 through a second spring 122, and the movable rod 124 is located on an end fixedly connected to an external chuck 125 of the bottom frame 121.
The top of the water heating box 7 is fixedly connected with a closed cover 16, and one side of the top of the fixed working frame 10 is fixedly connected with a temperature detector 14.
The two sides of the inner wall of the water heating box 7 are both provided with illuminating lamps 15, and the inner wall of the working box 1 is provided with an electromagnetic heating coil 17.
The electromagnetic rotating device 6 comprises an electromagnetic working box 601, a power box 602 is fixedly connected to the bottom of the inner wall of the electromagnetic working box 601, and a power supply 603 is fixedly connected to the bottom of the inner wall of the power box 602.
The middle position of the top of the inner wall of the electromagnetic working box 601 is fixedly connected with a main electromagnetic core 604, the top of the main electromagnetic core 604 is fixedly connected with a magnetic force rotary installer 606, the outer wall of the main electromagnetic core 604 is sleeved with a main coil 605, and the main coil 605 is electrically connected with a power supply 603.
The two sides of the top of the inner wall of the electromagnetic working box 601 are respectively and fixedly connected with an auxiliary electromagnetic core 607, the outer wall of the auxiliary electromagnetic core 607 is sleeved with an auxiliary electromagnetic coil 608, and the auxiliary electromagnetic coil 608 is electrically connected with the power supply 603.
The top of the electromagnetic working box 601 is provided with a rotating frame 609, the bottom of the rotating frame 609 is fixedly connected with a permanent magnet 611 through a magnet mounting frame 610, and the middle of the cavity of the rotating frame 609 is fixedly connected with a rotating shaft 613 through a mounting frame 612.
The telescopic stirrer 9 comprises a mounting base 901, the mounting base 901 is rotatably connected with a storage stirring cavity 902 through a connecting rotating shaft, and stirring blades 903 are fixedly connected with the outer wall of the storage stirring cavity 902.
Deposit the stirring cavity 902 inner wall and install flexible (mixing) shaft 904, flexible (mixing) shaft 904 top fixedly connected with installation element 905.
The fixed outer wall of the telescopic stirring shaft 904 is fixedly connected with a secondary stirring fan blade 906 and a folding stirring fan blade 907, and the folding stirring fan blade 907 is provided with a folding unit 908.
When the water-saving stirring machine is used, the electromagnetic coil 3 and the electromagnetic heating coil 17 which are installed inside the work box 1 are used for heating, the electromagnetic rotating device 6 in the rotating power box 5 provides power through the main electromagnetic iron core 604, the main coil 605, the auxiliary electromagnetic iron core 607 and the auxiliary electromagnetic coil 608 to drive the rotating rack 609 to rotate, so as to drive the telescopic stirrer 9 to rotate, the storage stirring cavity 902 and the stirring fan blades 903 of the telescopic stirrer 9 can stir water, the telescopic stirring shaft 904 drives the secondary stirring fan blades 906 and the folding stirring fan blades 907 to rotate, the folding stirring fan blades 907 are folded through the folding unit 908, the telescopic fixing device 11 can be fixed through the clamping rod 114 and the clamping groove 116, and the clamping device 12 can fix the position of the telescopic fixing device 11 through the second spring 122, the movable plate 123, the movable rod 124 and the clamping head 125.
It is noted that, herein, relational terms such as first and second, and the like may be used solely to distinguish one entity or action from another entity or action without necessarily requiring or implying any actual such relationship or order between such entities or actions. Also, the terms "comprises," "comprising," or any other variation thereof, are intended to cover a non-exclusive inclusion, such that a process, method, article, or apparatus that comprises a list of elements does not include only those elements but may include other elements not expressly listed or inherent to such process, method, article, or apparatus. Without further limitation. The use of the phrase "comprising one of the elements does not exclude the presence of other like elements in the process, method, article, or apparatus that comprises the element.
Although embodiments of the present invention have been shown and described, it will be appreciated by those skilled in the art that changes, modifications, substitutions and alterations can be made in these embodiments without departing from the principles and spirit of the invention, the scope of which is defined in the appended claims and their equivalents.
Claims (7)
1. The utility model provides a hydrothermal agitated vessel of experimental usefulness of cuprous oxide-titanium dioxide photocatalysis composite, includes work box (1), its characterized in that: the energy supply device is characterized in that an energy supply output box (2) is fixedly connected to the top of the inner wall of the working box (1), electromagnetic coils (3) are arranged on two sides of the inner cavity of the energy supply output box (2) respectively, the electromagnetic coils (3) are electrically connected through a wire (4), a rotary power box (5) is fixedly connected to the bottom of the inner wall of the energy supply output box (2), an electromagnetic rotating device (6) is fixedly connected to the bottom of the inner wall of the rotary power box (5) through a mounting frame, a telescopic stirrer (9) is rotatably connected to the top of the electromagnetic rotating device (6) through a rotating shaft (8), a water heating box (7) is fixedly connected to the top of the outer wall of the energy supply output box (2), a fixed working frame (10) is fixedly connected to the bottom of the inner wall of the water heating box (7, the inner wall of the supporting rack (13) is provided with a locking device (12), and the top of the locking device (12) is provided with a telescopic fixing device (11);
the telescopic fixing device (11) comprises a first telescopic plate (111) and a second telescopic plate (117), the left side of the first expansion plate (111) and the right side of the second expansion plate (117) are respectively movably connected with one side of the supporting frame (13), the left side of the second expansion plate (117) penetrates through the right side of the first expansion plate (111) and extends to the inside of the first expansion plate (111), a base (113) is fixedly connected with one side of the top of the inner wall of the first expansion plate (111), the bottom of the base (113) is rotatably connected with a clamping rod (114), the top of the inner wall of the first expansion plate (111) and two sides of the base (113) are fixedly connected with vertical plates (112), a first spring (115) is fixedly connected with one side of the vertical plate (112) opposite to the two sides of the base (113), the top of the second expansion plate (117) is provided with a clamping groove (116) matched with the clamping rod (114);
the locking device (12) comprises a bottom frame (121), the left side of the bottom frame (121) is fixedly connected with the surface of a supporting rack (13), a movable rod (124) penetrates through one side of the bottom frame (121), one end, located inside the bottom frame (121), of the movable rod (124) is fixedly connected with a movable plate (123), the top and the bottom of one side of the movable plate (123) are fixedly connected with the bottom frame (121) through a second spring (122), and one end, located outside the bottom frame (121), of the movable rod (124) is fixedly connected with a clamping head (125);
the telescopic stirrer (9) comprises a mounting base (901), the mounting base (901) is connected with a storage stirring cavity (902) through a connecting rotating shaft in a rotating mode, stirring blades (903) are fixedly connected to the outer wall of the storage stirring cavity (902), a telescopic stirring shaft (904) is installed on the inner wall of the storage stirring cavity (902), a mounting unit (905) is fixedly connected to the top end of the telescopic stirring shaft (904), a secondary stirring blade (906) and a folding stirring blade (907) are fixedly connected to the outer wall of the telescopic stirring shaft (904), and the folding stirring blade (907) is provided with a folding unit (908).
2. The hydrothermal stirring device for the cuprous oxide-titanium dioxide photocatalytic composite material experiment according to claim 1, wherein: the top of the water heating tank (7) is fixedly connected with a closed cover (16), and one side of the top of the fixed working rack (10) is fixedly connected with a temperature detector (14).
3. The hydrothermal stirring device for the cuprous oxide-titanium dioxide photocatalytic composite material experiment according to claim 1, wherein: the utility model discloses a heating water tank, including hot-water tank (7), heating coil (17), heating coil (15) are all provided with light (15) to hydrothermal case (7) inner wall both sides, electromagnetic heating coil (17) are installed to work box (1) inner wall.
4. The hydrothermal stirring device for the cuprous oxide-titanium dioxide photocatalytic composite material experiment according to claim 1, wherein: the electromagnetic rotating device (6) comprises an electromagnetic working box (601), a power box (602) is fixedly connected to the bottom of the inner wall of the electromagnetic working box (601), and a power supply (603) is fixedly connected to the bottom of the inner wall of the power box (602).
5. The hydrothermal stirring device for the cuprous oxide-titanium dioxide photocatalytic composite material experiment according to claim 4, wherein: the electromagnetic working box is characterized in that a main electromagnetic iron core (604) is fixedly connected to the middle of the top of the inner wall of the electromagnetic working box (601), a magnetic force rotary installer (606) is fixedly connected to the top of the main electromagnetic iron core (604), a main coil (605) is sleeved on the outer wall of the main electromagnetic iron core (604), and the main coil (605) is electrically connected with a power supply (603).
6. The hydrothermal stirring device for the cuprous oxide-titanium dioxide photocatalytic composite material experiment according to claim 5, wherein: electromagnetism work box (601) inner wall top both sides fixedly connected with auxiliary electromagnetic core (607) respectively, auxiliary electromagnetic core (607) outer wall cover is equipped with auxiliary electromagnetic coil (608), auxiliary electromagnetic coil (608) and power supply (603) electric connection.
7. The hydrothermal stirring device for the cuprous oxide-titanium dioxide photocatalytic composite material experiment according to claim 6, wherein: the top of the electromagnetic working box (601) is provided with a rotary rack (609), the bottom of the rotary rack (609) is fixedly connected with a permanent magnet (611) through a magnet mounting rack (610), and the middle of a cavity of the rotary rack (609) is fixedly connected with a rotating shaft (613) through the mounting rack (612).
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| CN201710967878.6A CN107754796B (en) | 2017-10-16 | 2017-10-16 | Hydrothermal stirring equipment for cuprous oxide-titanium dioxide photocatalytic composite material experiment |
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| CN201710967878.6A CN107754796B (en) | 2017-10-16 | 2017-10-16 | Hydrothermal stirring equipment for cuprous oxide-titanium dioxide photocatalytic composite material experiment |
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| CN116251598A (en) * | 2023-04-03 | 2023-06-13 | 黄山学院 | Cu with photocatalytic performance 2 O-Bi 2 O 3 Composite material and preparation method thereof |
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| JP5932629B2 (en) * | 2012-12-25 | 2016-06-08 | 株式会社カジワラ | Stirrer |
| CN204544056U (en) * | 2015-01-25 | 2015-08-12 | 宁波大学 | A kind of magnetic agitation still of improvement |
| CN205886722U (en) * | 2016-07-27 | 2017-01-18 | 重庆洲琪科技发展有限公司 | Magnetic heating stirrer |
| CN106880293A (en) * | 2017-04-13 | 2017-06-23 | 东莞市善为智能电器科技有限公司 | Soft-type agitating device |
| CN107159007A (en) * | 2017-06-20 | 2017-09-15 | 无锡市跨克微营养素有限公司 | High mixing degree powder materials stirring slurry bucket |
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2017
- 2017-10-16 CN CN201710967878.6A patent/CN107754796B/en active Active
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