CN107754727A - A kind of Intelligent high-pressure kettle being heated evenly for being used to prepare nano material - Google Patents

A kind of Intelligent high-pressure kettle being heated evenly for being used to prepare nano material Download PDF

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Publication number
CN107754727A
CN107754727A CN201711230963.0A CN201711230963A CN107754727A CN 107754727 A CN107754727 A CN 107754727A CN 201711230963 A CN201711230963 A CN 201711230963A CN 107754727 A CN107754727 A CN 107754727A
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CN
China
Prior art keywords
kettle
magazine
fixed
heated evenly
nano material
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CN201711230963.0A
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Chinese (zh)
Inventor
冯云
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Naga Taehye Long Xin Mstar Technology Ltd
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Naga Taehye Long Xin Mstar Technology Ltd
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Priority to CN201711230963.0A priority Critical patent/CN107754727A/en
Publication of CN107754727A publication Critical patent/CN107754727A/en
Withdrawn legal-status Critical Current

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    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J3/00Processes of utilising sub-atmospheric or super-atmospheric pressure to effect chemical or physical change of matter; Apparatus therefor
    • B01J3/002Component parts of these vessels not mentioned in B01J3/004, B01J3/006, B01J3/02 - B01J3/08; Measures taken in conjunction with the process to be carried out, e.g. safety measures
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J3/00Processes of utilising sub-atmospheric or super-atmospheric pressure to effect chemical or physical change of matter; Apparatus therefor
    • B01J3/02Feed or outlet devices therefor
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J3/00Processes of utilising sub-atmospheric or super-atmospheric pressure to effect chemical or physical change of matter; Apparatus therefor
    • B01J3/04Pressure vessels, e.g. autoclaves
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B82NANOTECHNOLOGY
    • B82YSPECIFIC USES OR APPLICATIONS OF NANOSTRUCTURES; MEASUREMENT OR ANALYSIS OF NANOSTRUCTURES; MANUFACTURE OR TREATMENT OF NANOSTRUCTURES
    • B82Y30/00Nanotechnology for materials or surface science, e.g. nanocomposites
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B82NANOTECHNOLOGY
    • B82YSPECIFIC USES OR APPLICATIONS OF NANOSTRUCTURES; MEASUREMENT OR ANALYSIS OF NANOSTRUCTURES; MANUFACTURE OR TREATMENT OF NANOSTRUCTURES
    • B82Y40/00Manufacture or treatment of nanostructures

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  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Nanotechnology (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Physics & Mathematics (AREA)
  • Condensed Matter Physics & Semiconductors (AREA)
  • General Physics & Mathematics (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Composite Materials (AREA)
  • Materials Engineering (AREA)
  • Manufacturing & Machinery (AREA)
  • Physical Or Chemical Processes And Apparatus (AREA)

Abstract

The present invention relates to a kind of Intelligent high-pressure kettle being heated evenly for being used to prepare nano material,Including base,Top plate,Charging mechanism,Water injection pipe,Kettle cover,Kettle,Controller,Discharge nozzle,Elevating mechanism,Two pillars and at least two legs,Reaction tank and at least two heating arrangements are provided with kettle,Heating arrangements include infrared lamp,Framework,Connecting rod,First motor,Two fix bars,Driving wheel and fixing axle,Charging mechanism includes hopper,Magazine and expects pipe,Material controlling block is provided with magazine,Coil,Magnet,Control assembly and two springs,This adds quantitative pharmacy response for preparing during the Intelligent high-pressure kettle being heated evenly of nano material is realized toward reaction tank by charging mechanism,Prevent medicament deficiency or excessive,Moreover,Infrared lamp is set to swing back and forth by heating arrangements,Heat radiation is carried out from different directions,Ensure that the aqueous solution in reaction tank is heated evenly,So as to be advantageous to the preparation of nano material and production.

Description

A kind of Intelligent high-pressure kettle being heated evenly for being used to prepare nano material
Technical field
It is more particularly to a kind of to be used to preparing being heated evenly for nano material the present invention relates to new material production equipment field Intelligent high-pressure kettle.
Background technology
Nano material refers in three dimensions at least one everywhere in nano-scale (0.1- as a kind of new material 100nm) or by the material that they are formed as elementary cell, this is about as much as what 10-100 atom was arranged closely together Yardstick, at present the preparation method of nano material mainly have vapor phase method, liquid phase method and solid phase method, wherein liquid phase method is divided into colloidal sol and coagulated again These four modes of glue method, the precipitation method, hydro-thermal method and microemulsion method, and hydro-thermal method has and some high temperature can be overcome to prepare can not keep away Hard aggregation, the powder exempted from are thin, purity is high, good dispersion, narrowly distributing, crystal formation are good, controlled shape and to be advantageous to the depollution of environment etc. excellent Gesture, therefore by the accreditation and popularization of people.
Hydro-thermal method is primarily referred to as under certain temperature and pressure, with the water in the high-temperature high-voltage reaction environment in autoclave As reaction medium, a kind of inorganic preparation method for making material be reacted in the solution.Under hydrothermal conditions, water can conduct A kind of chemical constituent works and participates in reaction, is both solvent and mineralizer, while is also used as pressure transmission medium.But Be existing autoclave mainly by the aqueous solution in electric furnace heating kettle body, and in heating process, the position of electric furnace Immobilize, cause to fix the heating location of the aqueous solution, the aqueous solution relies solely on flowing to realize heat transfer, causes water-soluble Uneven heating is even everywhere for liquid, influences the reaction in autoclave, and moreover, existing autoclave fails when adding pharmacy response Realization accurately quantitatively controls, and medicament addition is excessive, easily causes the waste of raw material, medicament addition is very few, then can cause to receive The yield of rice material declines, and then causes existing autoclave practicality to reduce.
The content of the invention
The technical problem to be solved in the present invention is:For overcome the deficiencies in the prior art, there is provided one kind is used to prepare nanometer The Intelligent high-pressure kettle being heated evenly of material.
The technical solution adopted for the present invention to solve the technical problems is:It is a kind of to be used to prepare being heated evenly for nano material Intelligent high-pressure kettle, including base, top plate, charging mechanism, water injection pipe, kettle cover, kettle, controller, discharge nozzle, lift Structure, two pillars and at least two legs, two pillars are separately fixed at the both ends of base, and the top plate is erected at two pillars On, the leg is circumferentially evenly distributed on the lower section of kettle, and the kettle is fixed on the top of base, the kettle cover by leg The top of kettle is arranged on, the elevating mechanism is arranged on the lower section of top plate, and the elevating mechanism is connected with kettle cover, described Charging mechanism is arranged on the side of elevating mechanism, and the water injection pipe is arranged on the opposite side of elevating mechanism, set in the water injection pipe There is the first valve, the discharge nozzle is arranged on the bottom of kettle, is provided with the second valve in the discharge nozzle, the controller is fixed Wherein on a pillar;
Reaction tank and at least two heating arrangements are provided with the kettle, the heating arrangements are circumferentially evenly distributed on reaction The periphery in pond, the heating arrangements include infrared lamp, framework, connecting rod, the first motor, two fix bars, driving wheel and fixation Axle, two fix bars are separately positioned on the both sides of the first motor, and first motor is fixed by the inwall of fix bar and kettle Connection, first motor are connected with driving wheel, and the fixing axle is fixed on the remote circle centre position of driving wheel, the fixation Axle is arranged in framework, and one end of the connecting rod and the inwall of kettle are hinged, and the other end of the connecting rod and one end of framework are consolidated Fixed connection, the infrared lamp are fixed on the other end of framework;
The charging mechanism includes hopper, magazine and expects pipe, and the magazine is fixed on the top of kettle cover, and the magazine leans on The inwall of the side of nearly elevating mechanism is provided with through hole, and one end of the expects pipe is connected by through hole with magazine, the expects pipe The other end connects with reaction tank, and the hopper is fixed on the top of magazine, and the hopper connects with magazine;
Material controlling block, coil, magnet, control assembly and two springs are provided with the magazine, two springs are separately positioned on The both sides of the lower section of material controlling block, the material controlling block are fixedly connected by spring with the bottom of magazine, and the coil is arranged on material controlling In block, the magnet is fixed on the bottom of magazine, and the control assembly is arranged on the top of material block.
Preferably, medicament is entered in feeding pipe by the through hole of magazine for convenience, the vertical cross-section of the material controlling block Be shaped as right-angled trapezium, two bases in the right-angled trapezium section bear against the inwall of the both sides of magazine, the right angle The underlying waist of trapezoid cross section is horizontally disposed with, and the waist above in the right-angled trapezium section is set diagonally downward.
Preferably, in order to realize the automatic addition of medicament, the material controlling component includes swash plate, sprue and pole, described Swash plate is located at the top of material controlling block, and the swash plate is obliquely installed, and the swash plate is fixed on the side of the close elevating mechanism of magazine Inwall on, the sprue is fixed on the top of material controlling block by pole, and the sprue is located at the remote elevating mechanism of swash plate The top of one end.
Preferably, in order to by controlling the lifting number of material controlling block to realize the quantitative control of medicament, the material controlling block Lower section is provided with montant and counter, and the counter is fixed on the lower section of montant by montant.
Preferably, in order to realize the lifting of kettle cover, the elevating mechanism includes the second motor, the second drive shaft and set Pipe, second motor are fixed on the lower section of top plate, and second motor and the second drive shaft are connected, second driving The periphery of axle is provided with external screw thread, and described sleeve pipe is set in the second drive shaft, is provided with internal thread in described sleeve pipe, in described sleeve pipe Internal thread match with the external screw thread in the second drive shaft, described sleeve pipe is fixed on the top of kettle cover.
Preferably, in order to ensure that kettle cover smoothly lifts, the elevating mechanism also includes retainer ring and two suspension rods, two Individual suspension rod is separately positioned on the both sides of retainer ring, and the retainer ring is fixed on the lower section of top plate, the Fixing shrink ring by suspension rod It is located on sleeve pipe.
Preferably, in order to ensure the driving force of the second motor, second motor is DC servo motor.
Preferably, for the ease of addition medicament and the aqueous solution, the shape of the water injection pipe and the shape of hopper are loudspeaker Shape.
Preferably, for the ease of operation, the controller is provided with display screen, loudspeaker and some control buttons.
Preferably, for the ease of remote-control communication, the controller is interior to be provided with bluetooth.
The invention has the advantages that the Intelligent high-pressure kettle being heated evenly for being used to prepare nano material passes through charging Mechanism adds quantitative pharmacy response in realizing toward reaction tank, medicament deficiency or excessive is prevented, with traditional feeding mechanism phase Than the feeding mechanism is simple in construction, and function is reliable, moreover, infrared lamp is swung back and forth by heating arrangements, from difference Direction carry out heat radiation, ensure reaction tank in the aqueous solution be heated evenly, so as to be advantageous to the preparation of nano material and production, Compared with traditional heating arrangements, the heating arrangements are heated using infrared ray, and the thermal efficiency is high, power density is big and heating is fast Speed, so that the practicality of equipment is improved.
Brief description of the drawings
The present invention is further described with reference to the accompanying drawings and examples.
Fig. 1 is the structural representation for being used to prepare the Intelligent high-pressure kettle being heated evenly of nano material of the present invention;
Fig. 2 is the top view for being used to prepare the kettle of the Intelligent high-pressure kettle being heated evenly of nano material of the present invention;
Fig. 3 is the structure for being used to prepare the heating arrangements of the Intelligent high-pressure kettle being heated evenly of nano material of the present invention Schematic diagram;
Fig. 4 is the structure for being used to prepare the feeding mechanism of the Intelligent high-pressure kettle being heated evenly of nano material of the present invention Schematic diagram;
Fig. 5 is the structure for being used to prepare the elevating mechanism of the Intelligent high-pressure kettle being heated evenly of nano material of the present invention Schematic diagram;
In figure:1. base, 2. top plates, 3. water injection pipes, 4. kettle covers, 5. kettlies, 6. controllers, 7. discharge nozzles, 8. pillars, 9. Leg, 10. first valves, 11. second valves, 12. reaction tanks, 13. infrared lamps, 14. frameworks, 15. connecting rods, 16. first electricity Machine, 17. fix bars, 18. driving wheels, 19. fixing axles, 20. hoppers, 21. magazines, 22. expects pipes, 23. through holes, 24. material controlling blocks, 25. coil, 26. magnet, 27. springs, 28. swash plates, 29. sprues, 30. poles, 31. montants, 32. counters, 33. second electricity Machine, 34. second drive shafts, 35. sleeve pipes, 36. retainer rings, 37. suspension rods, 38. display screens, 39. loudspeakers, 40. control buttons.
Embodiment
In conjunction with the accompanying drawings, the present invention is further explained in detail.These accompanying drawings are simplified schematic diagram, only with Illustration illustrates the basic structure of the present invention, therefore it only shows the composition relevant with the present invention.
As shown in figure 1, a kind of Intelligent high-pressure kettle being heated evenly for being used to prepare nano material, including base 1, top plate 2nd, charging mechanism, water injection pipe 3, kettle cover 4, kettle 5, controller 6, discharge nozzle 7, elevating mechanism, two pillars 8 and at least two Pin 9, two pillars 8 are separately fixed at the both ends of base 1, and the top plate 2 is erected on two pillars 8, and the leg 9 is circumferential The even lower section for being distributed in kettle 5, the kettle 5 are fixed on the top of base 1 by leg 9, and the kettle cover 4 is arranged on kettle 5 Top, the elevating mechanism is arranged on the lower section of top plate 2, and the elevating mechanism is connected with kettle cover 4, the charging mechanism The side of elevating mechanism is arranged on, the water injection pipe 3 is arranged on the opposite side of elevating mechanism, first is provided with the water injection pipe 3 Valve 10, the discharge nozzle 7 are arranged on the bottom of kettle 5, and the second valve 11 is provided with the discharge nozzle 7, and the controller 6 is solid It is scheduled on one of pillar 8;
In the reactor, kettle 5 is supported by leg 9, the height and position of fixed kettle 5, top plate 2 is fixed using pillar 8 Position, consequently facilitating the height and position of fixed elevating mechanism, the lifting of kettle cover 4 is can control by elevating mechanism, is easy to observe Inside kettle 5, the side above kettle cover 4, the accurate addition of dosing is realized by charging mechanism, above kettle cover 4 Opposite side adds the aqueous solution by water injection pipe 3, using the operation of the control device of controller 6 on pillar 8, after completion of the reaction, The second valve 11 is opened, finished product is flowed out from discharge nozzle 7.
As Figure 2-3, the heating arrangements of reaction tank 12 and at least two, the heating arrangements week are provided with the kettle 5 To the periphery for being evenly distributed on reaction tank 12, the heating arrangements include infrared lamp 13, framework 14, connecting rod 15, the first motor 16th, two fix bars 17, driving wheel 18 and fixing axle 19, two fix bars 22 are separately positioned on the both sides of the first motor 16, institute State the first motor 16 to be fixedly connected with the inwall of kettle 5 by fix bar 17, first motor 16 connects with the transmission of driving wheel 18 Connect, the fixing axle 19 is fixed on the remote circle centre position of driving wheel 18, and the fixing axle 19 is arranged in framework 14, the connecting rod 15 one end and the inwall of kettle 5 are hinged, and the other end of the connecting rod 15 is fixedly connected with one end of framework 14, the infrared lamp Pipe 13 is fixed on the other end of framework 14;
Inside kettle 5, realized by multiple heating arrangements of the periphery of reaction tank 12 and kettle 5 is internally heated, heated In mechanism, drive driving wheel 18 to rotate by the first motor 16, the driver framework 14 of fixing axle 19 on driving wheel 18 is carried out backswing It is dynamic, reaction tank 12 is heated so that infrared lamp 13 swings back and forth, infrared lamp fluorescent tube transmitting infrared ray, carries out radiation biography Heat, heat is transmitted by electromagnetic wave, make the molecule in the aqueous solution in reaction tank 12 that " resonance " occur with atom, produce strong shake Dynamic and rotation, and the temperature rise for causing the aqueous solution is rotated and rotates, reaching the purpose of heating, infrared lamp 13 swings back and forth, Heated from different directions, ensure that the aqueous solution is heated evenly, so as to be advantageous to being smoothed out for reaction.
As shown in figure 4, the charging mechanism includes hopper 20, magazine 21 and expects pipe 22, the magazine 21 is fixed on kettle cover 4 Top, the inwall of the side of the close elevating mechanism of the magazine 21 is provided with through hole 23, and one end of the expects pipe 22 passes through Through hole 23 connects with magazine 21, and the other end of the expects pipe 22 connects with reaction tank 12, and the hopper 20 is fixed on magazine 21 Top, the hopper 20 connect with magazine 21;
Material controlling block 24, coil 25, magnet 26, control assembly and two springs 27, two springs are provided with the magazine 21 27 are separately positioned on the both sides of the lower section of material controlling block 24, and the material controlling block 24 is fixed by the bottom of spring 27 and magazine 21 to be connected Connect, the coil 25 is arranged in material controlling block 24, and the magnet 26 is fixed on the bottom of magazine 21, and the control assembly is arranged on Expect the top of block.
In charging mechanism, medicament is entered in magazine 21 by hopper 20, in magazine 21, is increased with the amount of medicament, The pressure of material controlling block 24 is increased, pressure is more than the elastic force of spring 27, is gradually reduced material controlling block 24, through hole 23 exposes, medicament Glided along the surface of material controlling block 24, enter feeding pipe 22 from through hole 23, then entered by expects pipe 22 in reaction tank 12, and in medicine When agent is entered in feeding pipe 22, material controlling component prevents medicament from continuing to fall on material controlling block 24, expects on material controlling block 24 as medicament flows into The amount of pipe 22 increases, and the pressure suffered by material controlling block 24 reduces, and the elastic force of spring 27 is more than pressure, material controlling block 24 is increased, blocks logical Hole 23, now material controlling component medicament is dropped down onto the surface of material controlling block 24 under continuing, so circulation, realize gradually quantitatively adding for medicament Add, when no longer needing to add medicament, be powered to coil 25, produce magnetic, it is mutually exclusive between magnet 26 and coil 25, make magnetic Iron 26 produces upward active force to coil 25, support material controlling block 24, prevents material controlling block 24 from continuing to decline.
As shown in figure 4, the vertical cross-section of the material controlling block 24 is shaped as right-angled trapezium, the two of the right-angled trapezium section Individual base bears against the inwall of the both sides of magazine 21, and the underlying waist in the right-angled trapezium section is horizontally disposed with, described The waist above in right-angled trapezium section is set diagonally downward.
The vertical cross-section of material controlling block 24 is set using the shape of right-angled trapezium, two bottom plates is born against in magazine 21 On the inwall of both sides, prevent from dropping in gap of the medicament between material controlling block 24 and the inwall of magazine 21, while also help medicament Along the inclined waist slide downward of right-angled trapezium.
As shown in figure 4, the material controlling component includes swash plate 28, sprue 29 and pole 30, the swash plate 28 is located at material controlling block 24 top, the swash plate 28 are obliquely installed, and the swash plate 28 is fixed on the inwall of the side of the close elevating mechanism of magazine 21 On, the sprue 29 is fixed on the top of material controlling block 24 by pole 30, and the sprue 29 is located at the remote lift of swash plate 28 The top of one end of structure.
When accumulating excessive medicament on material controlling block 24, material controlling block 24 declines, and pole 30 can be driven to decline, and makes sprue 29 The space blocked between brace and the inwall of expects pipe 22, prevent medicament from continuing to fall on material controlling block 24, the medicament on material controlling block 24 When very few, spring 27 promotes material controlling block 24, material controlling block 24 is increased, so that sprue 29 rises, is easy to medicament from swash plate 28 It is slipped on material controlling block 24.
Preferably, in order to by controlling the lifting number of material controlling block 24 to realize the quantitative control of medicament, the material controlling block 24 lower section is provided with montant 31 and counter 32, and the counter 32 is fixed on the lower section of montant 31 by montant 31.
During the decline of material controlling block 24, the bottom that counter 32 touches magazine 21 is once counted, due to material controlling In 24 each lifting process of block, the quality that the medicament of expects pipe 22 is flowed into from through hole 23 immobilizes, therefore when count value reaches special During fixed number, the total amount for the medicament for representing to flow into expects pipe 22 from through hole 23 reaches reaction and required, now can be by coil 25 It is powered, material controlling block 24 is increased, prevents from continuing to continue to add medicament toward in reaction tank 12.
As shown in figure 5, the elevating mechanism includes the second motor 33, the second drive shaft 34 and sleeve pipe 35, second electricity Machine 33 is fixed on the lower section of top plate 2, and second motor 33 is connected with the second drive shaft 34, second drive shaft 34 Periphery is provided with external screw thread, and described sleeve pipe 35 is set in the second drive shaft 34, and internal thread, described sleeve pipe are provided with described sleeve pipe 35 Internal thread in 35 matches with the external screw thread in the second drive shaft 34, and described sleeve pipe 35 is fixed on the top of kettle cover 4.
Second motor 33 is run, and is driven the second drive shaft 34 to rotate, the external screw thread in the second drive shaft 34 is acted on set Internal thread in pipe 35, and then drive sleeve pipe 35 to lift, realize the rise and fall of kettle cover 4.
Preferably, in order to ensure that kettle cover 4 smoothly lifts, the elevating mechanism also includes retainer ring 36 and two suspension rods 37, two suspension rods 37 are separately positioned on the both sides of retainer ring 36, and the retainer ring 36 is fixed under top plate 2 by suspension rod 37 Side, the retainer ring 36 are set on sleeve pipe 35.The retainer ring 36 fixed using position secures the lifting track of sleeve pipe 35, makes Sleeve pipe 35 is along fixed direction, so as to ensure that kettle cover 4 smoothly lifts.
Preferably, using DC servo motor driving force it is strong the characteristics of, in order to ensure the driving force of the second motor 33, institute It is DC servo motor to state the second motor 33.
Preferably, it is for the ease of addition medicament and the aqueous solution, the shape of the water injection pipe 3 and the shape of hopper 20 It is tubaeform.
Preferably, for the ease of operation, the controller 6 is provided with display screen 38, loudspeaker 39 and some controls and pressed Key 40.By the operation information of the observable autoclave of display screen 38, control button 40 can carry out the setting of relevant parameter, work as reaction After the completion of, utilize the sounding reminding people of loudspeaker 39.
Preferably, the characteristics of can carrying out wireless data transmission using bluetooth, for the ease of remote-control communication, the controller Bluetooth is provided with 6.
The autoclave controls whether medicament falls in material controlling block 24 in use, by the material controlling component in magazine 21 Top, when the medicament on material controlling block 24 is enough, material controlling block 24 declines, and prevents from continuing to add medicament using material controlling component, when During medicament deficiency on material controlling block 24, material controlling block 24 rises, and medicament is fallen above material controlling block 24 using material controlling component, is easy to past Addition medicament, is counted by counter 32, realizes quantitative control in reaction tank 12, moreover, in the periphery of reaction tank 12, Drive infrared lamp 13 to swing back and forth using heating arrangements, carry out heat radiation from different directions, ensure the water in reaction tank 12 Solution is heated evenly, and is advantageous to the progress of reaction.
Compared with prior art, the Intelligent high-pressure kettle being heated evenly for being used to prepare nano material passes through charging mechanism Quantitative pharmacy response is added in realizing toward reaction tank 12, prevents medicament deficiency or excessive, compared with traditional feeding mechanism, The feeding mechanism is simple in construction, and function is reliable, moreover, infrared lamp 13 is swung back and forth by heating arrangements, from difference Direction carry out heat radiation, ensure reaction tank 12 in the aqueous solution be heated evenly, so as to be advantageous to the preparation of nano material and life Production, compared with traditional heating arrangements, the heating arrangements are heated using infrared ray, and the thermal efficiency is high, power density is big and rises It is warm rapid, so that the practicality of equipment is improved.
It is complete by above-mentioned description, relevant staff using the above-mentioned desirable embodiment according to the present invention as enlightenment Various changes and amendments can be carried out without departing from the scope of the technological thought of the present invention' entirely.The technology of this invention Property scope is not limited to the content on specification, it is necessary to determines its technical scope according to right.

Claims (10)

1. a kind of Intelligent high-pressure kettle being heated evenly for being used to prepare nano material, it is characterised in that including base (1), top Plate (2), charging mechanism, water injection pipe (3), kettle cover (4), kettle (5), controller (6), discharge nozzle (7), elevating mechanism, two branch Post (8) and at least two legs (9), two pillars (8) are separately fixed at the both ends of base (1), and the top plate (2) is erected at two On individual pillar (8), the leg (9) is circumferentially evenly distributed on the lower section of kettle (5), and the kettle (5) is fixed by leg (9) In the top of base (1), the kettle cover (4) is arranged on the top of kettle (5), and the elevating mechanism is arranged under top plate (2) Side, the elevating mechanism are connected with kettle cover (4), and the charging mechanism is arranged on the side of elevating mechanism, the water injection pipe (3) opposite side of elevating mechanism is arranged on, is provided with the first valve (10) in the water injection pipe (3), the discharge nozzle (7) is arranged on The bottom of kettle (5), the discharge nozzle (7) is interior to be provided with the second valve (11), and the controller (6) is fixed therein a pillar (8) on;
Reaction tank (12) and at least two heating arrangements are provided with the kettle (5), the heating arrangements are circumferentially evenly distributed on The periphery of reaction tank (12), the heating arrangements include infrared lamp (13), framework (14), connecting rod (15), the first motor (16), Two fix bars (17), driving wheel (18) and fixing axle (19), two fix bars (17) are separately positioned on the first motor (16) Both sides, first motor (16) are fixedly connected by fix bar (17) with the inwall of kettle (5), first motor (16) with Driving wheel (18) is connected, and the fixing axle (19) is fixed on the remote circle centre position of driving wheel (18), the fixing axle (19) Be arranged in framework (14), one end of the connecting rod (15) and the inwall of kettle (5) are hinged, the other end of the connecting rod (15) and One end of framework (14) is fixedly connected, and the infrared lamp (13) is fixed on the other end of framework (14);
The charging mechanism includes hopper (20), magazine (21) and expects pipe (22), and the magazine (21) is fixed on the upper of kettle cover (4) Side, the inwall of the side of the close elevating mechanism of the magazine (21) are provided with through hole (23), and one end of the expects pipe (22) leads to Cross through hole (23) to connect with magazine (21), the other end of the expects pipe (22) connects with reaction tank (12), and the hopper (20) is solid The top of magazine (21) is scheduled on, the hopper (20) connects with magazine (21);
It is provided with material controlling block (24), coil (25), magnet (26), control assembly and two springs (27) in the magazine (21), two Individual spring (27) is separately positioned on the both sides of the lower section of material controlling block (24), and the material controlling block (24) passes through spring (27) and magazine (21) bottom is fixedly connected, and the coil (25) is arranged in material controlling block (24), and the magnet (26) is fixed on magazine (21) Bottom, the control assembly is arranged on the top of material controlling block (24).
2. the Intelligent high-pressure kettle as claimed in claim 1 that be heated evenly for being used to prepare nano material, it is characterised in that institute The right-angled trapezium that is shaped as of the vertical cross-section of material controlling block (24) is stated, two bases in the right-angled trapezium section bear against magazine (21) inwall of both sides, the underlying waist in the right-angled trapezium section are horizontally disposed with, the position in the right-angled trapezium section Waist in top is set diagonally downward.
3. the Intelligent high-pressure kettle as claimed in claim 1 that be heated evenly for being used to prepare nano material, it is characterised in that institute Stating material controlling component includes swash plate (28), sprue (29) and pole (30), and the swash plate (28) is located at the top of material controlling block (24), institute State swash plate (28) to be obliquely installed, the swash plate (28) is fixed on the inwall of the side of the close elevating mechanism of magazine (21), institute The top that sprue (29) is fixed on material controlling block (24) by pole (30) is stated, the sprue (29) is located at the remote liter of swash plate (28) The top of one end of descending mechanism.
4. the Intelligent high-pressure kettle as claimed in claim 1 that be heated evenly for being used to prepare nano material, it is characterised in that institute The lower section for stating material controlling block (24) is provided with montant (31) and counter (32), and the counter (32) is fixed on perpendicular by montant (31) The lower section of bar (31).
5. the Intelligent high-pressure kettle as claimed in claim 1 that be heated evenly for being used to prepare nano material, it is characterised in that institute Stating elevating mechanism includes the second motor (33), the second drive shaft (34) and sleeve pipe (35), and second motor (33) is fixed on top The lower section of plate (2), second motor (33) are connected with the second drive shaft (34), the periphery of second drive shaft (34) Provided with external screw thread, described sleeve pipe (35) is set in the second drive shaft (34), and internal thread, the set are provided with described sleeve pipe (35) Internal thread in pipe (35) matches with the external screw thread in the second drive shaft (34), and described sleeve pipe (35) is fixed on kettle cover (4) Top.
6. the Intelligent high-pressure kettle as claimed in claim 5 that be heated evenly for being used to prepare nano material, it is characterised in that institute Stating elevating mechanism also includes retainer ring (36) and two suspension rods (37), and two suspension rods (37) are separately positioned on the two of retainer ring (36) Side, the retainer ring (36) are fixed on the lower section of top plate (2) by suspension rod (37), and the retainer ring (36) is set in sleeve pipe (35) On.
7. the Intelligent high-pressure kettle as claimed in claim 5 that be heated evenly for being used to prepare nano material, it is characterised in that institute It is DC servo motor to state the second motor (33).
8. the Intelligent high-pressure kettle as claimed in claim 1 that be heated evenly for being used to prepare nano material, it is characterised in that institute It is tubaeform to state the shape of water injection pipe (3) and the shape of hopper (20).
9. the Intelligent high-pressure kettle as claimed in claim 1 that be heated evenly for being used to prepare nano material, it is characterised in that institute State controller (6) and be provided with display screen (38), loudspeaker (39) and some control buttons (40).
10. the Intelligent high-pressure kettle as claimed in claim 1 that be heated evenly for being used to prepare nano material, it is characterised in that Bluetooth is provided with the controller (6).
CN201711230963.0A 2017-11-29 2017-11-29 A kind of Intelligent high-pressure kettle being heated evenly for being used to prepare nano material Withdrawn CN107754727A (en)

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109966987A (en) * 2019-04-09 2019-07-05 江苏中砼新材料科技有限公司 It is a kind of for producing the energy-saving agitating device of concrete antifreezer

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109966987A (en) * 2019-04-09 2019-07-05 江苏中砼新材料科技有限公司 It is a kind of for producing the energy-saving agitating device of concrete antifreezer

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