CN107751258A - A kind of processing method of long-acting slow release type mosquito expelling plaster - Google Patents
A kind of processing method of long-acting slow release type mosquito expelling plaster Download PDFInfo
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- CN107751258A CN107751258A CN201711073868.4A CN201711073868A CN107751258A CN 107751258 A CN107751258 A CN 107751258A CN 201711073868 A CN201711073868 A CN 201711073868A CN 107751258 A CN107751258 A CN 107751258A
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- mosquito
- expelling plaster
- mosquito expelling
- slow release
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02A—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
- Y02A50/00—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE in human health protection, e.g. against extreme weather
- Y02A50/30—Against vector-borne diseases, e.g. mosquito-borne, fly-borne, tick-borne or waterborne diseases whose impact is exacerbated by climate change
Abstract
The invention discloses a kind of processing method of long-acting slow release type mosquito expelling plaster, it is related to mosquito repellent product technical field, comprises the following steps：(1) the structure structure of mosquito expelling plaster, the preparation of (2) mosquito-dispelling tablet, the processing of (3) mosquito expelling plaster.The first use time of the made mosquito expelling plaster of the present invention is 10 days, can form diameter 2.5m guard circle when in use；And only mosquito is produced and walks quickly and keeps away effect, does not produce killing action, so as to improve its safety in utilization, though to avoid effectively killing the defects of mosquito can damage human body existing for conventional mosquito repellent product simultaneously.
Description
Technical field：
The present invention relates to mosquito repellent product technical field, and in particular to a kind of processing method of long-acting slow release type mosquito expelling plaster.
Background technology：
Arrive whenever summer, bite by mosquitos worry can also come at the appointed time.Bite by mosquitos not only influences the sleep of people, can also
Trigger swelling and pain, itch, especially perplex child.Therefore, people, which seek various methods, carries out mosquito repellent.Traditional mosquito-repellent incense, mosquito-dispelling tablet lead to
Cross burning and mode of heating release mosquito component, people suck after mosquito repellent gas for a long time can trigger uncomfortable, and this drive
Mosquito mode short run effect is significantly, it is necessary to frequently using just can guarantee that repelling effect.Mosquito-repellent spray will directly be driven by spray pattern
Mosquito composition is held into air to play repelling effect, but can only short time mosquito repellent, the mosquito component content in a denier air declines,
Mosquito will attack again；And it can cause allergy after part mosquito-repellent spray contact skin, not be suitable for infant and skin is easy
The crowd of allergy.
In recent years, mosquito expelling plaster is widely used with its convenience.But effective mosquito component master in conventional mosquito expelling plaster
If chemical agent, and more spirituosity, essence etc. are to the component of skin irritatin；And portioned product is in order to prevent mosquito component from becoming
Matter, also added preservative, and safety in utilization is extremely low.In addition, the mosquito repellent effectiveness time of mosquito expelling plaster it is shorter, it is necessary to timing change,
Otherwise repelling effect can not normally be played.
The content of the invention：
The technical problems to be solved by the invention are to provide that a kind of safe to use, service life is long and repelling effect
The processing method of good long-acting slow release type mosquito expelling plaster.
The technical problems to be solved by the invention are realized using following technical scheme：
A kind of processing method of long-acting slow release type mosquito expelling plaster, comprises the following steps：
(1) the structure structure of mosquito expelling plaster：Mosquito expelling plaster includes paste section and carries medicine portion, and the paste section is by gum base fabric, load
Medicine connects cloth and adhesive film is made, and carries medicine portion and is made up of non-woven fabrics and mosquito-dispelling tablet, and adhesive film is attached at the back side of gum base fabric, the back of the body
The front of matrix cloth, which is provided with, pastes hook side, and the front for carrying medicine connection cloth is provided with the stickup matte to match with pasting hook side, carries medicine
Connection cloth is attached on non-woven fabrics by sewing mode；
(2) preparation of mosquito-dispelling tablet：Culicifuge is added into carrier, is sent into after being sufficiently mixed in tablet press machine, through tablet press machine pressure
Into thickness 3-5mm thin slice, mosquito-dispelling tablet is produced；
(3) processing of mosquito expelling plaster：Load medicine connection cloth is attached on non-woven fabrics using sewing machine is automated, and will be pasted with
The gum base fabric of adhesive film by paste hook side with carry medicine be connected cloth stickup matte adhesive effect stickup is formed on non-woven fabrics
Portion, recycle automatic packaging machine that made mosquito-dispelling tablet is packaged into non-woven fabrics and carry medicine portion to be formed, produce mosquito expelling plaster, it is finally right
Mosquito expelling plaster carries out plastics package.
Rounded, the oval or regular polygonized structure of the thin slice.
The culicifuge is by mass ratio 5:3:2:1:0.5 tea tree ethereal oil, P-Cymene, Chinese ilex essential oil, black pepper essential oil,
Cordate houttuynia essential oil mixes.
The mass ratio of the culicifuge and carrier is 5-10:35-45.
The raw material of the following parts by weight of carrier is made：Sensor Chip CM 5 sodium 25-35 parts, cation guar gum 5-10
Part, trimethylol-propane trimethacrylate 1-5 parts, rilanit special 1-5 parts, polyaluminium sulfate 1-5 parts, N- methylols third
Acrylamide 0.5-3 parts, gamma-polyglutamic acid 0.5-3 parts, potassium peroxydisulfate 0.01-0.05 parts, butyl titanate 0.005-0.01 parts.
Its preparation method comprises the following steps：
(1) deionized water is added dropwise until being completely dissolved into Sensor Chip CM 5 sodium under stirring, recycles dust technology regulation
PH value is heated to 60-70 DEG C of insulated and stirred to 3-4, detects a pH value every 5min, dilute nitre is added when pH value is more than 4
Acid so that pH value control in 3-4, when system pH in 15min continually and steadily in 3-4 when add N hydroxymethyl acrylamide, after
It is continuous to be heated to reflux state insulated and stirred 2-5h, trimethylol-propane trimethacrylate and potassium peroxydisulfate are added, again
Flowed back insulated and stirred 1-3h, and gained mixture is sent into spray dryer when naturally cooling to less than 50 DEG C, dries gained particle
Micro mist is made through micronizer, produces water-based glucan-acrylic resin compound；
(2) molten condition insulated and stirred is heated to after mixing cation guar gum, gamma-polyglutamic acid and butyl titanate
1-3h, to weight boiling water such as gained solid additions when naturally cooling to less than 70 DEG C, and it is heated to reflux state insulated and stirred 10-
15min, gained mixture is concentrated to reach 60-70% to solid content, is finally sent into freeze drier, dries gained solid warp
Micro mist is made in micronizer, produces modified guar；
(3) into above-mentioned made water-based glucan-acrylic resin compound add modified guar, rilanit special and
Polyaluminium sulfate, it is sufficiently mixed, produces carrier.
The gamma-polyglutamic acid is selected from food-grade gamma-polyglutamic acid.
The rilanit special passes through modification, and its specific method of modifying is：First rilanit special is heated to melting
State insulated and stirred 3-5min, adds trihydroxymethylpropanyltri diglycidyl ether and HPMA, continues to be heated to
110-120 DEG C of insulated and stirred 0.5-2h, gained mixture are cooled to 0-5 DEG C of insulation with 5 DEG C/min cooling rate and stand 1-2h,
Produce modified hydrogenated castor oil.
The mass ratio of the rilanit special, trihydroxymethylpropanyltri diglycidyl ether and HPMA is 5-
10:0.5-3:0.5-3。
The beneficial effects of the invention are as follows：
(1) present invention is built by the structure of the mosquito expelling plaster, makes made mosquito expelling plaster when in use only need to be by its adhesive film
Just it could be adhered to using position after tearing；And by paste hook side and paste matte setting, realize using rear paste section with
The separation in medicine portion is carried, non-woven fabrics and mosquito-dispelling tablet can be further separated into by carrying medicine portion, be handled so as to the classification of rubbish；Simultaneously using viscous
Detachable annexation between patch portion and load medicine portion, position is used to mosquito expelling plaster in a manner of by changing paste section
Move；
(2) present invention is improved using peace using five kinds of plants essential oils as culicifuge on the basis of its repelling effect is ensured
Quan Xing, wherein tea tree ethereal oil, P-Cymene, Patchouli essential oil, black pepper essential oil, the mode that is applied in combination of cordate houttuynia essential oil do not exist
This area discloses, especially using Patchouli essential oil, black pepper essential oil, cordate houttuynia essential oil as mosquito component application；
(3) present invention to control the rate of release of plants essential oil, and passes through slow releasing function to make carrier loaded culicifuge by oneself
To realize the long-acting use of mosquito expelling plaster, effectiveness existing for common mosquito expelling plaster or other mosquito repellent products is avoided to use the problem of short；Together
When make to maintain relatively low essential oil concentration in the use environment air of mosquito expelling plaster by its distinctive slow releasing function, keep driving for a long time
Mosquito effect, prevent mosquito from being attacked again because essential oil concentration reduces suddenly；
(4) the first use time of the made mosquito expelling plaster of the present invention is 10 days, can form diameter 2.5m's when in use
Guard circle；And only mosquito is produced and walks quickly and keeps away effect, does not produce killing action, so as to improve its safety in utilization, to avoid often
Though the defects of effectively killing mosquito existing for rule mosquito repellent product but human body can be damaged simultaneously.
Brief description of the drawings：
Fig. 1 is the structural representation of mosquito expelling plaster of the present invention；
Wherein：1- gum base fabrics；2- carries medicine connection cloth；3- adhesive films；4- non-woven fabrics；5- mosquito-dispelling tablets；6- pastes hook side；7-
Paste matte.
Embodiment：
In order that the technical means, the inventive features, the objects and the advantages of the present invention are easy to understand, tie below
Conjunction is specifically illustrating and embodiment, and the present invention is expanded on further.
Embodiment 1
The processing of long-acting slow release type mosquito expelling plaster：
(1) the structure structure of mosquito expelling plaster：As shown in figure 1, mosquito expelling plaster includes paste section and carries medicine portion, the paste section is by carrying on the back
Matrix cloth 1, load medicine connection cloth 2 and adhesive film 3 are made, and carry medicine portion and are made up of non-woven fabrics 4 and mosquito-dispelling tablet 5, adhesive film is attached at the back of the body
The back side of matrix cloth, the front of gum base fabric, which is provided with, pastes hook side 6, and the front of load medicine connection cloth is provided with to match with pasting hook side
Stickup matte 7, carry medicine connection cloth be attached to by sewing mode on non-woven fabrics；
(2) preparation of mosquito-dispelling tablet：5g culicifuges are added into 35g carriers, are sent into after being sufficiently mixed in tablet press machine, through tabletting
Machine is pressed into thickness 5mm thin slice, produces mosquito-dispelling tablet；
(3) processing of mosquito expelling plaster：Load medicine connection cloth is attached on non-woven fabrics using sewing machine is automated, and will be pasted with
The gum base fabric of adhesive film by paste hook side with carry medicine be connected cloth stickup matte adhesive effect stickup is formed on non-woven fabrics
Portion, recycle automatic packaging machine that made mosquito-dispelling tablet is packaged into non-woven fabrics and carry medicine portion to be formed, produce mosquito expelling plaster, it is finally right
Mosquito expelling plaster carries out plastics package.
Culicifuge is by mass ratio 5:3:2:1:0.5 tea tree ethereal oil, P-Cymene, Chinese ilex essential oil, black pepper essential oil, fish raw meat
Careless essential oil mixes.
The preparation of carrier：
(1) deionized water is added dropwise until being completely dissolved into 35g Sensor Chip CM 5 sodium under stirring, recycles dust technology to adjust
PH value is saved to 3-4, and is heated to 60-70 DEG C of insulated and stirred, a pH value is detected every 5min, is added when pH value is more than 4 dilute
Nitric acid so that pH value control in 3-4, when system pH in 15min continually and steadily in 3-4 when add 3gN- methylol acryloyls
Amine, continue to be heated to reflux state insulated and stirred 3h, add 5g trimethylol-propane trimethacrylates and 0.05g over cures
Sour potassium, flowed back insulated and stirred 2h again, and gained mixture is sent into spray dryer when naturally cooling to less than 50 DEG C, dries institute
Obtain particle and micro mist is made through micronizer, produce water-based glucan-acrylic resin compound；
(2) it is heated to after mixing 8g cation guar gums, 1g food-grades gamma-polyglutamic acid and 0.005g butyl titanates
Molten condition insulated and stirred 2h, to weight boiling water such as gained solid additions when naturally cooling to less than 70 DEG C, and it is heated to flowing back
State insulated and stirred 15min, gained mixture is concentrated to reach 60-70% to solid content, is finally sent into freeze drier, does
Micro mist is made through micronizer in dry gained solid, produces modified guar；
(3) modified guar, 3g rilanit specials are added into above-mentioned made water-based glucan-acrylic resin compound
With 2g polyaluminium sulfates, it is sufficiently mixed, produces carrier.
Embodiment 2
The processing of long-acting slow release type mosquito expelling plaster：
(1) the structure structure of mosquito expelling plaster：As shown in figure 1, mosquito expelling plaster includes paste section and carries medicine portion, the paste section is by carrying on the back
Matrix cloth 1, load medicine connection cloth 2 and adhesive film 3 are made, and carry medicine portion and are made up of non-woven fabrics 4 and mosquito-dispelling tablet 5, adhesive film is attached at the back of the body
The back side of matrix cloth, the front of gum base fabric, which is provided with, pastes hook side 6, and the front of load medicine connection cloth is provided with to match with pasting hook side
Stickup matte 7, carry medicine connection cloth be attached to by sewing mode on non-woven fabrics；
(2) preparation of mosquito-dispelling tablet：5g culicifuges are added into 45g carriers, are sent into after being sufficiently mixed in tablet press machine, through tabletting
Machine is pressed into thickness 5mm thin slice, produces mosquito-dispelling tablet；
(3) processing of mosquito expelling plaster：Load medicine connection cloth is attached on non-woven fabrics using sewing machine is automated, and will be pasted with
The gum base fabric of adhesive film by paste hook side with carry medicine be connected cloth stickup matte adhesive effect stickup is formed on non-woven fabrics
Portion, recycle automatic packaging machine that made mosquito-dispelling tablet is packaged into non-woven fabrics and carry medicine portion to be formed, produce mosquito expelling plaster, it is finally right
Mosquito expelling plaster carries out plastics package.
Culicifuge is by mass ratio 5:3:2:1:0.5 tea tree ethereal oil, P-Cymene, Chinese ilex essential oil, black pepper essential oil, fish raw meat
Careless essential oil mixes.
The preparation of carrier：
(1) deionized water is added dropwise until being completely dissolved into 30g Sensor Chip CM 5 sodium under stirring, recycles dust technology to adjust
PH value is saved to 3-4, and is heated to 60-70 DEG C of insulated and stirred, a pH value is detected every 5min, is added when pH value is more than 4 dilute
Nitric acid so that pH value control in 3-4, when system pH in 15min continually and steadily in 3-4 when add 3gN- methylol acryloyls
Amine, continue to be heated to reflux state insulated and stirred 3h, add 3g trimethylol-propane trimethacrylates and 0.05g over cures
Sour potassium, flowed back insulated and stirred 2h again, and gained mixture is sent into spray dryer when naturally cooling to less than 50 DEG C, dries institute
Obtain particle and micro mist is made through micronizer, produce water-based glucan-acrylic resin compound；
(2) heated after mixing 10g cation guar gums, 2g food-grades gamma-polyglutamic acid and 0.005g butyl titanates
To molten condition insulated and stirred 3h, to weight boiling water such as gained solid additions when naturally cooling to less than 70 DEG C, and it is heated to back
Stream mode insulated and stirred 15min, gained mixture is concentrated to reach 60-70% to solid content, is finally sent into freeze drier,
Dry gained solid and micro mist is made through micronizer, produce modified guar；
(3) modified guar, 2g rilanit specials are added into above-mentioned made water-based glucan-acrylic resin compound
With 2g polyaluminium sulfates, it is sufficiently mixed, produces carrier.
Embodiment 3
The processing of long-acting slow release type mosquito expelling plaster：
(1) the structure structure of mosquito expelling plaster：As shown in figure 1, mosquito expelling plaster includes paste section and carries medicine portion, the paste section is by carrying on the back
Matrix cloth 1, load medicine connection cloth 2 and adhesive film 3 are made, and carry medicine portion and are made up of non-woven fabrics 4 and mosquito-dispelling tablet 5, adhesive film is attached at the back of the body
The back side of matrix cloth, the front of gum base fabric, which is provided with, pastes hook side 6, and the front of load medicine connection cloth is provided with to match with pasting hook side
Stickup matte 7, carry medicine connection cloth be attached to by sewing mode on non-woven fabrics；
(2) preparation of mosquito-dispelling tablet：5g culicifuges are added into 35g carriers, are sent into after being sufficiently mixed in tablet press machine, through tabletting
Machine is pressed into thickness 5mm thin slice, produces mosquito-dispelling tablet；
(3) processing of mosquito expelling plaster：Load medicine connection cloth is attached on non-woven fabrics using sewing machine is automated, and will be pasted with
The gum base fabric of adhesive film by paste hook side with carry medicine be connected cloth stickup matte adhesive effect stickup is formed on non-woven fabrics
Portion, recycle automatic packaging machine that made mosquito-dispelling tablet is packaged into non-woven fabrics and carry medicine portion to be formed, produce mosquito expelling plaster, it is finally right
Mosquito expelling plaster carries out plastics package.
Culicifuge is by mass ratio 5:3:2:1:0.5 tea tree ethereal oil, P-Cymene, Chinese ilex essential oil, black pepper essential oil, fish raw meat
Careless essential oil mixes.
The preparation of carrier：
(1) deionized water is added dropwise until being completely dissolved into 35g Sensor Chip CM 5 sodium under stirring, recycles dust technology to adjust
PH value is saved to 3-4, and is heated to 60-70 DEG C of insulated and stirred, a pH value is detected every 5min, is added when pH value is more than 4 dilute
Nitric acid so that pH value control in 3-4, when system pH in 15min continually and steadily in 3-4 when add 3gN- methylol acryloyls
Amine, continue to be heated to reflux state insulated and stirred 3h, add 5g trimethylol-propane trimethacrylates and 0.05g over cures
Sour potassium, flowed back insulated and stirred 2h again, and gained mixture is sent into spray dryer when naturally cooling to less than 50 DEG C, dries institute
Obtain particle and micro mist is made through micronizer, produce water-based glucan-acrylic resin compound；
(2) it is heated to after mixing 8g cation guar gums, 1g food-grades gamma-polyglutamic acid and 0.005g butyl titanates
Molten condition insulated and stirred 2h, to weight boiling water such as gained solid additions when naturally cooling to less than 70 DEG C, and it is heated to flowing back
State insulated and stirred 15min, gained mixture is concentrated to reach 60-70% to solid content, is finally sent into freeze drier, does
Micro mist is made through micronizer in dry gained solid, produces modified guar；
(3) modified guar, 3g rilanit specials are added into above-mentioned made water-based glucan-acrylic resin compound
With 2g polyaluminium sulfates, it is sufficiently mixed, produces carrier.
The modification of rilanit special：8g rilanit specials are first heated to molten condition insulated and stirred 5min, add 2g
Trihydroxymethylpropanyltri diglycidyl ether and 0.5g HPMAs, continue to be heated to 110-120 DEG C of insulated and stirred 1h, institute
Obtain mixture and 0-5 DEG C of insulation standing 2h is cooled to 5 DEG C/min cooling rate, produce modified hydrogenated castor oil.
Embodiment 4
The processing of long-acting slow release type mosquito expelling plaster：
(1) the structure structure of mosquito expelling plaster：As shown in figure 1, mosquito expelling plaster includes paste section and carries medicine portion, the paste section is by carrying on the back
Matrix cloth 1, load medicine connection cloth 2 and adhesive film 3 are made, and carry medicine portion and are made up of non-woven fabrics 4 and mosquito-dispelling tablet 5, adhesive film is attached at the back of the body
The back side of matrix cloth, the front of gum base fabric, which is provided with, pastes hook side 6, and the front of load medicine connection cloth is provided with to match with pasting hook side
Stickup matte 7, carry medicine connection cloth be attached to by sewing mode on non-woven fabrics；
(2) preparation of mosquito-dispelling tablet：5g culicifuges are added into 45g carriers, are sent into after being sufficiently mixed in tablet press machine, through tabletting
Machine is pressed into thickness 5mm thin slice, produces mosquito-dispelling tablet；
(3) processing of mosquito expelling plaster：Load medicine connection cloth is attached on non-woven fabrics using sewing machine is automated, and will be pasted with
The gum base fabric of adhesive film by paste hook side with carry medicine be connected cloth stickup matte adhesive effect stickup is formed on non-woven fabrics
Portion, recycle automatic packaging machine that made mosquito-dispelling tablet is packaged into non-woven fabrics and carry medicine portion to be formed, produce mosquito expelling plaster, it is finally right
Mosquito expelling plaster carries out plastics package.
Culicifuge is by mass ratio 5:3:2:1:0.5 tea tree ethereal oil, P-Cymene, Chinese ilex essential oil, black pepper essential oil, fish raw meat
Careless essential oil mixes.
The preparation of carrier：
(1) deionized water is added dropwise until being completely dissolved into 30g Sensor Chip CM 5 sodium under stirring, recycles dust technology to adjust
PH value is saved to 3-4, and is heated to 60-70 DEG C of insulated and stirred, a pH value is detected every 5min, is added when pH value is more than 4 dilute
Nitric acid so that pH value control in 3-4, when system pH in 15min continually and steadily in 3-4 when add 3gN- methylol acryloyls
Amine, continue to be heated to reflux state insulated and stirred 3h, add 3g trimethylol-propane trimethacrylates and 0.05g over cures
Sour potassium, flowed back insulated and stirred 2h again, and gained mixture is sent into spray dryer when naturally cooling to less than 50 DEG C, dries institute
Obtain particle and micro mist is made through micronizer, produce water-based glucan-acrylic resin compound；
(2) heated after mixing 10g cation guar gums, 2g food-grades gamma-polyglutamic acid and 0.005g butyl titanates
To molten condition insulated and stirred 3h, to weight boiling water such as gained solid additions when naturally cooling to less than 70 DEG C, and it is heated to back
Stream mode insulated and stirred 15min, gained mixture is concentrated to reach 60-70% to solid content, is finally sent into freeze drier,
Dry gained solid and micro mist is made through micronizer, produce modified guar；
(3) modified guar, 2g rilanit specials are added into above-mentioned made water-based glucan-acrylic resin compound
With 2g polyaluminium sulfates, it is sufficiently mixed, produces carrier.
The modification of rilanit special：10g rilanit specials are first heated to molten condition insulated and stirred 5min, add 3g
Trihydroxymethylpropanyltri diglycidyl ether and 1g HPMAs, continue to be heated to 110-120 DEG C of insulated and stirred 2h, gained
Mixture is cooled to 0-5 DEG C of insulation with 5 DEG C/min cooling rate and stands 2h, produces modified hydrogenated castor oil.
Reference examples 1
The processing of long-acting slow release type mosquito expelling plaster：
(1) the structure structure of mosquito expelling plaster：As shown in figure 1, mosquito expelling plaster includes paste section and carries medicine portion, the paste section is by carrying on the back
Matrix cloth 1, load medicine connection cloth 2 and adhesive film 3 are made, and carry medicine portion and are made up of non-woven fabrics 4 and mosquito-dispelling tablet 5, adhesive film is attached at the back of the body
The back side of matrix cloth, the front of gum base fabric, which is provided with, pastes hook side 6, and the front of load medicine connection cloth is provided with to match with pasting hook side
Stickup matte 7, carry medicine connection cloth be attached to by sewing mode on non-woven fabrics；
(2) preparation of mosquito-dispelling tablet：5g culicifuges are added into 35g carriers, are sent into after being sufficiently mixed in tablet press machine, through tabletting
Machine is pressed into thickness 5mm thin slice, produces mosquito-dispelling tablet；
(3) processing of mosquito expelling plaster：Load medicine connection cloth is attached on non-woven fabrics using sewing machine is automated, and will be pasted with
The gum base fabric of adhesive film by paste hook side with carry medicine be connected cloth stickup matte adhesive effect stickup is formed on non-woven fabrics
Portion, recycle automatic packaging machine that made mosquito-dispelling tablet is packaged into non-woven fabrics and carry medicine portion to be formed, produce mosquito expelling plaster, it is finally right
Mosquito expelling plaster carries out plastics package.
Culicifuge is by mass ratio 5:3:2:1:0.5 tea tree ethereal oil, P-Cymene, Chinese ilex essential oil, black pepper essential oil, fish raw meat
Careless essential oil mixes.
The preparation of carrier：
(1) deionized water is added dropwise until being completely dissolved into 35g Sensor Chip CM 5 sodium under stirring, recycles dust technology to adjust
PH value is saved to 3-4, and is heated to 60-70 DEG C of insulated and stirred, a pH value is detected every 5min, is added when pH value is more than 4 dilute
Nitric acid so that pH value control in 3-4, when system pH in 15min continually and steadily in 3-4 when add 3gN- methylol acryloyls
Amine, continue to be heated to reflux state insulated and stirred 3h, add 5g trimethylol-propane trimethacrylates and 0.05g over cures
Sour potassium, flowed back insulated and stirred 2h again, and gained mixture is sent into spray dryer when naturally cooling to less than 50 DEG C, dries institute
Obtain particle and micro mist is made through micronizer, produce water-based glucan-acrylic resin compound；
(2) 8g cation guar gums, 3g hydrogenation castors are added into above-mentioned made water-based glucan-acrylic resin compound
Sesame oil and 2g polyaluminium sulfates, are sufficiently mixed, produce carrier.
Reference examples 2
The processing of long-acting slow release type mosquito expelling plaster：
(1) the structure structure of mosquito expelling plaster：As shown in figure 1, mosquito expelling plaster includes paste section and carries medicine portion, the paste section is by carrying on the back
Matrix cloth 1, load medicine connection cloth 2 and adhesive film 3 are made, and carry medicine portion and are made up of non-woven fabrics 4 and mosquito-dispelling tablet 5, adhesive film is attached at the back of the body
The back side of matrix cloth, the front of gum base fabric, which is provided with, pastes hook side 6, and the front of load medicine connection cloth is provided with to match with pasting hook side
Stickup matte 7, carry medicine connection cloth be attached to by sewing mode on non-woven fabrics；
(2) preparation of mosquito-dispelling tablet：5g culicifuges are added into 35g carriers, are sent into after being sufficiently mixed in tablet press machine, through tabletting
Machine is pressed into thickness 5mm thin slice, produces mosquito-dispelling tablet；
(3) processing of mosquito expelling plaster：Load medicine connection cloth is attached on non-woven fabrics using sewing machine is automated, and will be pasted with
The gum base fabric of adhesive film by paste hook side with carry medicine be connected cloth stickup matte adhesive effect stickup is formed on non-woven fabrics
Portion, recycle automatic packaging machine that made mosquito-dispelling tablet is packaged into non-woven fabrics and carry medicine portion to be formed, produce mosquito expelling plaster, it is finally right
Mosquito expelling plaster carries out plastics package.
Culicifuge is by mass ratio 5:3:2:1:0.5 tea tree ethereal oil, P-Cymene, Chinese ilex essential oil, black pepper essential oil, fish raw meat
Careless essential oil mixes.
The preparation of carrier：
(1) it is heated to after mixing 8g cation guar gums, 1g food-grades gamma-polyglutamic acid and 0.005g butyl titanates
Molten condition insulated and stirred 2h, to weight boiling water such as gained solid additions when naturally cooling to less than 70 DEG C, and it is heated to flowing back
State insulated and stirred 15min, gained mixture is concentrated to reach 60-70% to solid content, is finally sent into freeze drier, does
Micro mist is made through micronizer in dry gained solid, produces modified guar；
(2) modified guar, 3g rilanit specials and 2g polyaluminium sulfates are added into 35g Sensor Chip CM 5 sodium, is filled
Divide mixing, produce carrier.
Reference examples 3
With the load in the made macromolecular sustained-release carrier A alternate embodiments 1 of patent CN201010262410.5 embodiments 1
Body.
Reference examples 4
With the blue or green essential oil in eucalyptus leaf essential oil, dried orange peel essential oil, Peppermint essential oil replacement winter embodiment 1, black pepper essential oil, cordate houttuynia
Essential oil.
Embodiment 5
1st, acute oral toxicity test is carried out to the made mosquito-dispelling tablet of embodiment 1-4, reference examples 1-4.
Experimental animal：Regular grade SD rats, body weight 180-200g, male and female half and half, every group 10.
Test method：Rat Septal curfew eats before experiment, can't help water, using the mode that feeds, poisoning dosage 5000mg/kg, connects
Continuous observation 14 days, the performance of record animal poisoning and death condition；After off-test, survival rats are put to death, dissection checks.
Result of the test：Experiment rat no abnormality seen in 14 day observation period, also no abnormality seen after dissection.
Conclusion (of pressure testing)：The acute oral toxicity test result of mosquito-dispelling tablet is LD50＞ 5000mg/kg are nontoxic.
2nd, skin contact toxicity test is carried out to the made mosquito-dispelling tablet of embodiment 1-4, reference examples 1-4
Experimental animal：New zealand rabbit, body weight 2.5-2.8kg, male and female half and half, every group 3.
Test method：24h before experiment, rabbit backbone both sides hair is cut, skin must not be damaged.Unhairing scope 3cm ×
3cm, mosquito-dispelling tablet is dissolved in after water and takes 2ml to be coated on the skin of unhairing of side, rinsed after smearing 4h with water, daily smearing 1 time, continuously
Smear 14 days.Result is observed, blank control is used as using opposite side skin of unhairing.
Result of the test：Smeared for examination rabbit on the side skin of unhairing of mosquito-dispelling tablet and erythema and oedema phenomenon do not occur.
Conclusion (of pressure testing)：Mosquito-dispelling tablet belongs to nonirritant to the stimulus intensity of rabbit.
3rd, repelling effect test is carried out to the made mosquito expelling plaster of embodiment 1-4, reference examples 1-4
Test mosquito kind：Aedes albopictus, the female adult mosquito do not sucked blood for 4-5 days after emergence.
Test method：The clear glass room that two lengths are 2.5m is set, passes through glass between two glass chambers
Pipeline is together with glass pipe diameter 25cm；Mosquito expelling plaster is placed in the centre position inside a glass chamber wherein, and by 500
Aedes albopictus is put into this glass chamber, and situation is walked quickly and kept away in observation.
Result of the test：Mosquito expelling plaster of the present invention reaches 100% to the rate of walking quickly and keeping away of aedes albopictus, killing rate 0.
Conclusion (of pressure testing)：Mosquito expelling plaster of the present invention has excellent effect of walking quickly and keeping away to mosquito, does not produce killing action.
4th, long-acting mosquito-driving measure of merit is carried out to the made mosquito expelling plaster of embodiment 1-4, reference examples 1-4
Test method：The clear glass room that length is 2.5m is set, and one is set directly per face on glass chamber
Footpath 3cm air-vent, mosquito repellent is adhered on into the centre position inside glass chamber, determine the essential oil volatilization in glass chamber inner air
Gas concentration.
Result of the test：As shown in table 1.
Conclusion (of pressure testing)：The made mosquito expelling plasters of 1-4 of the embodiment of the present invention have long-acting slow-release repelling effect, and embodiment 1, implementation
The long-acting slow-release effect of example 2 is slightly weaker than embodiment 3, embodiment 4.
The long-acting mosquito-driving effect of the made mosquito expelling plaster of the present invention of table 1
The general principle and principal character and advantages of the present invention of the present invention has been shown and described above.The technology of the industry
Personnel are it should be appreciated that the present invention is not limited to the above embodiments, and the simply explanation described in above-described embodiment and specification is originally
The principle of invention, without departing from the spirit and scope of the present invention, various changes and modifications of the present invention are possible, these changes
Change and improvement all fall within the protetion scope of the claimed invention.The claimed scope of the invention by appended claims and its
Equivalent thereof.
Claims (7)
- A kind of 1. processing method of long-acting slow release type mosquito expelling plaster, it is characterised in that：Comprise the following steps：(1) the structure structure of mosquito expelling plaster：Mosquito expelling plaster includes paste section and carries medicine portion, and the paste section is connected by gum base fabric, load medicine Connect cloth and adhesive film is made, carry medicine portion and be made up of non-woven fabrics and mosquito-dispelling tablet, adhesive film is attached at the back side of gum base fabric, gum base The front of cloth, which is provided with, pastes hook side, and the front for carrying medicine connection cloth is provided with the stickup matte to match with pasting hook side, carries medicine connection Cloth is attached on non-woven fabrics by sewing mode；(2) preparation of mosquito-dispelling tablet：Culicifuge is added into carrier, is sent into after being sufficiently mixed in tablet press machine, thickness is pressed into through tablet press machine 3-5mm thin slice is spent, produces mosquito-dispelling tablet；(3) processing of mosquito expelling plaster：Load medicine connection cloth is attached on non-woven fabrics using sewing machine is automated, and stickup will be pasted with The gum base fabric of film by paste hook side with carry medicine be connected cloth stickup matte adhesive effect paste section is formed on non-woven fabrics, then Made mosquito-dispelling tablet is packaged into non-woven fabrics using automatic packaging machine and carries medicine portion to be formed, mosquito expelling plaster is produced, finally to mosquito repellent Exchange premium row plastics package.
- 2. the processing method of long-acting slow release type mosquito expelling plaster according to claim 1, it is characterised in that：The thin slice is in circle The polygonized structure of shape, ellipse or rule.
- 3. the processing method of long-acting slow release type mosquito expelling plaster according to claim 1, it is characterised in that：The culicifuge is by matter Measure ratio 5:3:2:1:0.5 tea tree ethereal oil, P-Cymene, Chinese ilex essential oil, black pepper essential oil, cordate houttuynia essential oil mix.
- 4. the processing method of long-acting slow release type mosquito expelling plaster according to claim 1, it is characterised in that：The culicifuge is with carrying The mass ratio of body is 5-10:35-45.
- 5. the processing method of long-acting slow release type mosquito expelling plaster according to claim 1, it is characterised in that：The carrier weighs as follows The raw material of amount number is made：Sensor Chip CM 5 sodium 25-35 parts, cation guar gum 5-10 parts, trimethylol propane trimethyl Acrylate 1-5 parts, rilanit special 1-5 parts, polyaluminium sulfate 1-5 parts, N hydroxymethyl acrylamide 0.5-3 parts, γ-poly- paddy Propylhomoserin 0.5-3 parts, potassium peroxydisulfate 0.01-0.05 parts, butyl titanate 0.005-0.01 parts.
- 6. the processing method of long-acting slow release type mosquito expelling plaster according to claim 5, it is characterised in that：Its preparation method includes Following steps：(1) deionized water is added dropwise until being completely dissolved into Sensor Chip CM 5 sodium under stirring, recycles dust technology regulation pH value To 3-4, and be heated to 60-70 DEG C of insulated and stirred, every 5min detect a pH value, added when pH value is more than 4 dust technology with Make pH value control in 3-4, when system pH in 15min continually and steadily in 3-4 when add N hydroxymethyl acrylamide, continue plus Heat adds trimethylol-propane trimethacrylate and potassium peroxydisulfate, flowed back again to reflux state insulated and stirred 2-5h Insulated and stirred 1-3h, gained mixture are sent into spray dryer when naturally cooling to less than 50 DEG C, dry gained particle through super Micro mist is made in atomizer, produces water-based glucan-acrylic resin compound；(2) molten condition insulated and stirred 1- is heated to after mixing cation guar gum, gamma-polyglutamic acid and butyl titanate 3h, to weight boiling water such as gained solid additions when naturally cooling to less than 70 DEG C, and it is heated to reflux state insulated and stirred 10- 15min, gained mixture is concentrated to reach 60-70% to solid content, is finally sent into freeze drier, dries gained solid warp Micro mist is made in micronizer, produces modified guar；(3) modified guar, rilanit special and polymerization are added into above-mentioned made water-based glucan-acrylic resin compound Aluminum sulfate, it is sufficiently mixed, produces carrier.
- 7. the processing method of long-acting slow release type mosquito expelling plaster according to claim 6, it is characterised in that：γ-the polyglutamic Acid is selected from food-grade gamma-polyglutamic acid.
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108914592A (en) * | 2018-07-02 | 2018-11-30 | 汪涛 | A kind of dacron afterfinish softening agent |
| CN111202059A (en) * | 2020-02-24 | 2020-05-29 | 青岛农业大学 | Slow-release carrier for liquid fumigant and sex attractant and preparation and use methods thereof |
| CN112715523A (en) * | 2020-12-25 | 2021-04-30 | 成都彩虹电器（集团）股份有限公司 | Natural plant essential oil mosquito-repellent product and preparation method thereof |
Citations (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1915015A (en) * | 2005-08-17 | 2007-02-21 | 郭正贤 | Method for preparing extractive material for preventing and driving mosquito away, and paste for preventing and driving mosquito away produced from extractive material |
| EP1919279A1 (en) * | 2005-09-02 | 2008-05-14 | Evergreen Land Limited | Material controllingly releasing a liquid active substance by evaporation and a mosquito repellent bracelet comprising said material |
| CN101317566A (en) * | 2007-06-04 | 2008-12-10 | 常州市第四制药厂有限公司 | Mosquito driving paster |
| CN101926746A (en) * | 2010-08-25 | 2010-12-29 | 邱日辉 | Polymer controlled release long-acting mosquito repellent product and preparation method thereof |
| CN201947840U (en) * | 2011-01-24 | 2011-08-31 | 刘敏 | Mosquito expelling sticker |
| CN102771910A (en) * | 2012-07-09 | 2012-11-14 | 昆山市周市惠宏服装厂 | Novel anti-mosquito T-shirt |
| CN202800438U (en) * | 2012-09-13 | 2013-03-20 | 杨丹 | Schoolbag with mosquito repelling ring |
| CN103876322A (en) * | 2012-12-20 | 2014-06-25 | 王斌 | Mosquito-repellent breathable clothing |
-
2017
- 2017-11-05 CN CN201711073868.4A patent/CN107751258A/en active Pending
Patent Citations (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1915015A (en) * | 2005-08-17 | 2007-02-21 | 郭正贤 | Method for preparing extractive material for preventing and driving mosquito away, and paste for preventing and driving mosquito away produced from extractive material |
| EP1919279A1 (en) * | 2005-09-02 | 2008-05-14 | Evergreen Land Limited | Material controllingly releasing a liquid active substance by evaporation and a mosquito repellent bracelet comprising said material |
| CN101317566A (en) * | 2007-06-04 | 2008-12-10 | 常州市第四制药厂有限公司 | Mosquito driving paster |
| CN101926746A (en) * | 2010-08-25 | 2010-12-29 | 邱日辉 | Polymer controlled release long-acting mosquito repellent product and preparation method thereof |
| CN201947840U (en) * | 2011-01-24 | 2011-08-31 | 刘敏 | Mosquito expelling sticker |
| CN102771910A (en) * | 2012-07-09 | 2012-11-14 | 昆山市周市惠宏服装厂 | Novel anti-mosquito T-shirt |
| CN202800438U (en) * | 2012-09-13 | 2013-03-20 | 杨丹 | Schoolbag with mosquito repelling ring |
| CN103876322A (en) * | 2012-12-20 | 2014-06-25 | 王斌 | Mosquito-repellent breathable clothing |
Non-Patent Citations (1)
| Title |
|---|
| 裘炳毅 等编: "《现代化妆品科学与技术•下》", 31 March 2016, 中国轻工业出版社 * |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108914592A (en) * | 2018-07-02 | 2018-11-30 | 汪涛 | A kind of dacron afterfinish softening agent |
| CN111202059A (en) * | 2020-02-24 | 2020-05-29 | 青岛农业大学 | Slow-release carrier for liquid fumigant and sex attractant and preparation and use methods thereof |
| CN112715523A (en) * | 2020-12-25 | 2021-04-30 | 成都彩虹电器（集团）股份有限公司 | Natural plant essential oil mosquito-repellent product and preparation method thereof |
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