CN107747108A - A kind of device and method of the concentration of electrolyte of detection in real time - Google Patents
A kind of device and method of the concentration of electrolyte of detection in real time Download PDFInfo
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- CN107747108A CN107747108A CN201711167141.2A CN201711167141A CN107747108A CN 107747108 A CN107747108 A CN 107747108A CN 201711167141 A CN201711167141 A CN 201711167141A CN 107747108 A CN107747108 A CN 107747108A
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- electrolyte
- concentration
- temperature
- voltage
- detection
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- 239000003792 electrolyte Substances 0.000 title claims abstract description 96
- 238000001514 detection method Methods 0.000 title claims abstract description 42
- 238000000034 method Methods 0.000 title claims abstract description 23
- 238000005868 electrolysis reaction Methods 0.000 claims abstract description 22
- 230000005540 biological transmission Effects 0.000 claims description 6
- 230000005611 electricity Effects 0.000 claims description 3
- 239000007788 liquid Substances 0.000 claims description 2
- 230000006641 stabilisation Effects 0.000 abstract description 2
- 238000011105 stabilization Methods 0.000 abstract description 2
- 239000012267 brine Substances 0.000 description 6
- HPALAKNZSZLMCH-UHFFFAOYSA-M sodium;chloride;hydrate Chemical compound O.[Na+].[Cl-] HPALAKNZSZLMCH-UHFFFAOYSA-M 0.000 description 6
- 239000000243 solution Substances 0.000 description 5
- 238000000354 decomposition reaction Methods 0.000 description 3
- 235000013399 edible fruits Nutrition 0.000 description 3
- ZAMOUSCENKQFHK-UHFFFAOYSA-N Chlorine atom Chemical compound [Cl] ZAMOUSCENKQFHK-UHFFFAOYSA-N 0.000 description 2
- 229910052801 chlorine Inorganic materials 0.000 description 2
- 239000000460 chlorine Substances 0.000 description 2
- 238000007689 inspection Methods 0.000 description 2
- 239000012266 salt solution Substances 0.000 description 2
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 238000011897 real-time detection Methods 0.000 description 1
- 235000015598 salt intake Nutrition 0.000 description 1
- 150000003839 salts Chemical class 0.000 description 1
- 238000004659 sterilization and disinfection Methods 0.000 description 1
- 238000006467 substitution reaction Methods 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C25—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
- C25B—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES FOR THE PRODUCTION OF COMPOUNDS OR NON-METALS; APPARATUS THEREFOR
- C25B15/00—Operating or servicing cells
- C25B15/02—Process control or regulation
-
- C—CHEMISTRY; METALLURGY
- C25—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
- C25B—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES FOR THE PRODUCTION OF COMPOUNDS OR NON-METALS; APPARATUS THEREFOR
- C25B1/00—Electrolytic production of inorganic compounds or non-metals
- C25B1/01—Products
- C25B1/24—Halogens or compounds thereof
- C25B1/26—Chlorine; Compounds thereof
-
- C—CHEMISTRY; METALLURGY
- C25—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
- C25B—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES FOR THE PRODUCTION OF COMPOUNDS OR NON-METALS; APPARATUS THEREFOR
- C25B15/00—Operating or servicing cells
- C25B15/08—Supplying or removing reactants or electrolytes; Regeneration of electrolytes
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Electrochemistry (AREA)
- Materials Engineering (AREA)
- Metallurgy (AREA)
- Organic Chemistry (AREA)
- Automation & Control Theory (AREA)
- Inorganic Chemistry (AREA)
- Water Treatment By Electricity Or Magnetism (AREA)
Abstract
The invention provides a kind of device of the concentration of electrolyte of detection in real time, including constant-current supply, electrolytic anode, electrolysis cathode, electrolytic cell and voltage check device, the electrolytic anode and the electrolysis cathode to electrically connect with constant-current supply respectively；Electrolyte is loaded with the electrolytic cell, the electrolytic anode and the electrolysis cathode are respectively protruding into the electrolyte, and the both ends of the voltage check device electrically connect with the electrolytic anode and the electrolysis cathode respectively.Present invention also offers a kind of method of the concentration of electrolyte of detection in real time.Apparatus and method provided by the invention are simple and practical, time saving and energy saving, can be widely used for the detection of various concentration of electrolytes, detect the concentration level of electrolyte in real time, ensure the qualified stabilization of concentration of electrolysate.
Description
Technical field
The invention belongs to Concentration Detection field, more particularly to a kind of device of concentration of electrolyte of detection in real time and side
Method.
Background technology
During electrolysis unit electrolytic brine prepares liquor natrii hypochloritis, the concentration and its stability of salt solution are very heavy
Will.Brine strength is too high, can cause salt consumption increase, and cost increases；Brine strength is too low, and effective chlorine density can be reduced substantially, meeting
Power consumption is caused to increase；Brine strength is unstable, then liquor natrii hypochloritis's effective chlorine density for producing can be caused unstable, and then
Disinfection Effect when influenceing to use.Brine strength must be controlled under a stable, suitable concentration conditions, can just given birth to
Output is qualified and the liquor natrii hypochloritis of stay in grade.Therefore, detect that the concentration of salt solution is particularly significant in time.
The content of the invention
In order to solve the above-mentioned technical problem, the present invention provides a kind of device of the concentration of electrolyte of detection in real time, including constant current
Power supply, electrolytic anode, electrolysis cathode, electrolytic cell and voltage check device, the electrolytic anode and electrolysis cathode difference
Electrically connected with constant-current supply；Electrolyte is loaded with the electrolytic cell, the electrolytic anode and the electrolysis cathode are respectively protruding into
In the electrolyte, the both ends of the voltage check device electrically connect with the electrolytic anode and the electrolysis cathode respectively.
Further, described device also include the processor that is connected with the voltage check device and with the processor
The warning device of connection；The processor is used to judge whether concentration of electrolyte is qualified, and sends alarm signal according to judged result
Cease to the warning device.
Further, the processor includes：
Voltage module：The voltage detecting result sent for receiving voltage detection means；
Judge module：For judging whether concentration of electrolyte is qualified according to voltage detecting result, and it will determine that result is sent
To alarm module；
Alarm module：For after the judged result of judge module transmission is received, deciding whether to give birth to according to judged result
Warning device is sent into warning message, and by warning message.
Further, described device also includes temperature-detecting device, and the temperature-detecting device is stretched into the electrolyte.
Further, the processor also includes thermal module；
The thermal module is used for the temperature detection result for receiving temperature-detecting device transmission；
The judge module is used to judge whether concentration of electrolyte is qualified according to temperature detection result and voltage detecting result,
And it will determine that result is sent to alarm module.
Further, the judge module judges concentration of electrolyte whether qualified detailed process includes：First determine whether temperature
Spend whether testing result allows in temperature range positioned at electrolyte, if it is not, then sending temperature determination result to warning device；Such as
Fruit is, then according to c=k1U+k2T+B calculates concentration of electrolyte c, wherein, k1For voltage coefficient, U is the voltage of detection, k2For temperature
Coefficient is spent, t is the temperature of detection, and B is corrected parameter；Then c value is judged whether in the range of the certified concentration of electrolyte,
And concentration judged result is sent to warning device.
The present invention also provides a kind of method of the concentration of electrolyte of detection in real time, including：Detect the voltage of electrolytic circuit；Will inspection
Survey voltage qualified voltage corresponding with the electrolyte of certified concentration to be analyzed, judge that the concentration of electrolyte in electrolytic cell is
It is no qualified.
Further, methods described also includes：Detect the temperature of electrolyte, and the temperature and electrolytic circuit for passing through electrolyte
Voltage judge whether the concentration of electrolyte in electrolytic cell qualified jointly.
Further, it is described " electricity in electrolytic cell to be judged by the temperature of electrolyte and the voltage of electrolytic circuit jointly
Solution liquid concentration it is whether qualified " detailed process include：First determine whether electrolyte temperature whether positioned at electrolyte permission temperature range
It is interior, if it is not, then showing that electrolyte temperature has been over allowed band, it is necessary to adjust in time；If it is, according to c=k1U
+k2T+B calculates concentration of electrolyte c, wherein, k1For voltage coefficient, U is the voltage of detection, k2For temperature coefficient, t is the temperature of detection
Degree, B is corrected parameter；Then judge c value whether in the range of the certified concentration of electrolyte.
Compared with prior art, the beneficial effects of the present invention are：
Apparatus and method provided by the invention are simple and practical, time saving and energy saving, can be widely used for the inspection of various concentration of electrolytes
Survey, detect the concentration level of electrolyte in real time, ensure the qualified stabilization of concentration of electrolysate.
Brief description of the drawings
Fig. 1 is the structural representation of the device of the real-time detection concentration of electrolyte of the present invention；
Fig. 2 is the structural representation of the processor of the present invention；
Wherein：1 constant-current supply, 2 electrolytic anodes, 3 electrolysis cathodes, 4 electrolytic cells, 5 voltage check devices, 6 temperature detections dress
Put, 7 processors, 701 voltage modules, 702 judge modules, 703 alarm modules, 704 thermal modules.
Embodiment
To be easy to understand the technical means, the inventive features, the objects and the advantages of the present invention, with reference to
Specific embodiment, the present invention is expanded on further.
Embodiment 1
A kind of device of the concentration of electrolyte of detection in real time, as shown in figure 1, cloudy including constant-current supply 1, electrolytic anode 2, electrolysis
Pole 3, electrolytic cell 4 and voltage check device 5, electrolytic anode 2 are connected with the positive pole of constant-current supply 1, electrolysis cathode 3 and Constant Electric Current
The negative pole in source 1 connects, and electrolyte is housed in electrolytic cell 4, electrolytic anode 2 and electrolysis cathode 3 are stretched into the electrolyte, voltage
The both ends of detection means 5 electrically connect with electrolytic anode 2 and electrolysis cathode 3 respectively.
In electrolytic process, concentration of electrolyte is different, and its electrical conductivity also correspondingly changes；Concentration of electrolyte is low, its
Electrical conductivity is low；Concentration of electrolyte is high, and its electrical conductivity is also correspondingly high.
In the present embodiment, voltage check device 5 is connected in parallel in electrolytic circuit.It is permanent during device work provided by the invention
Stream power supply 1 can export constant Faradaic current, therefore concentration of electrolyte is higher, then the voltage that voltage check device 5 detects
It is lower；Concentration of electrolyte is lower, then the voltage that voltage check device 5 detects is higher.What voltage check device 5 detected
The voltage of electrolytic circuit can directly react the size of concentration of electrolyte, and staff can adjust electrolyte on this basis
Concentration, the qualified purpose for stablizing electrolytically generated solution is prepared so as to reach.On the basis of Faradaic current keeps constant, survey first
The allowed band of the decomposition voltage gone out under the concentration of electrolyte for preparing qualified solution, then observes voltage detecting in electrolytic process
The voltage that device 5 determines, if voltage value, higher than the upper limit for allowing voltage, now concentration of electrolyte is relatively low in electrolytic cell 4, needs
To increase the concentration of electrolyte using the methods of adding electrolytic salt；If voltage value is less than the lower limit for allowing voltage, now
In electrolytic cell concentration of electrolyte it is higher, it is necessary to using plus reduce the concentration of electrolyte the methods of water.
In the present embodiment, constant-current supply 1 can select constant-current supply of the in the market often with brand and model.
In the present embodiment, as shown in figure 1, being additionally provided with temperature-detecting device 6 in device, the temperature detection of temperature-detecting device 6
Part is stretched into the electrolyte.When being changed due to electrolyte temperature, the decomposition voltage of the electrolyte of same concentrations also can
Change.Temperature-detecting device 6 detects the temperature of electrolyte, for excluding influence of the temperature to decomposition voltage, so as to accurate
Judge the concentration of electrolyte.
Embodiment 2
A kind of device of the concentration of electrolyte of detection in real time, as different from Example 1, as shown in Fig. 2 described device is also wrapped
Include the processor 7 being connected with the voltage check device 5 and the warning device being connected with the processor 7；
The processor 7 includes：
Voltage module 701：The voltage detecting result sent for receiving voltage detection means 5；
Thermal module 704：For receiving the temperature detection result of the transmission of temperature-detecting device 6；
Judge module 702：For judging whether concentration of electrolyte is qualified according to temperature detection result and voltage detecting result,
And it will determine that result is sent to alarm module 703；Judging concentration of electrolyte, whether qualified detailed process includes：First determine whether temperature
Spend whether testing result allows in temperature range positioned at electrolyte, if it is not, then sending temperature determination result to warning device；Such as
Fruit is, then according to c=k1U+k2T+B calculates concentration of electrolyte c, wherein, k1For voltage coefficient, U is the voltage of detection, k2For temperature
Coefficient is spent, t is the temperature of detection, and B is corrected parameter；Then c value is judged whether in the range of the certified concentration of electrolyte,
And concentration judged result is sent to warning device；
Alarm module 703：For after the judged result of the transmission of judge module 702 is received, being determined according to judged result
Warning message whether is generated, and warning message is sent to warning device.
In the present embodiment, can be automatically by temperature detection knot due to being provided with processor 7 and warning device in device
Fruit and voltage detecting result obtain the concentration value of electrolyte, and exceed permission temperature range and concentration beyond qualified dense in temperature
Warning reminding staff is carried out when spending scope, both can effectively mitigate the workload of staff, is also prevented from work mistake
Generation, improve the efficiency and accuracy of Concentration Testing by mistake.
In the present embodiment, voltage coefficient k1, temperature coefficient k2, corrected parameter B numerical value all in accordance with electrolyte species come
It is determined that.For example electrolytic brine prepares the electrolysis system of liquor natrii hypochloritis, k1=-1.9, k2=-0.3, B=13.8.
In the present embodiment, warning device includes at least one of indicator lamp and buzzer.Once the temperature of electrolyte
Exceed the bound of certified concentration, corresponding indicator lamp flicker, buzzer hair beyond the scope or concentration of electrolyte for allowing temperature
Go out sound, play a part of timely and effective prompting staff.For ease of staff's quick discriminating concentration of electrolyte situation,
Concentration indicator lamp can set two, the respectively higher indicator lamp of concentration and the relatively low indicator lamp of concentration.Equally, temperature indicator
Temperature drift indicator lamp and the relatively low indicator lamp of temperature two can be set.
Embodiment 3
A kind of method of the concentration of electrolyte of detection in real time, including：Detect the voltage of electrolytic circuit and the temperature of electrolyte；Sentence
Whether the temperature of disconnected electrolyte is in the permission temperature range of the electrolyte, if it is not, then showing the temperature of electrolyte
Temperature allowed range is exceeded, it is necessary to adjust in time；If it is, according to c=k1U+k2T+B calculates concentration of electrolyte c, wherein,
k1For voltage coefficient, U is the voltage of detection, k2For temperature coefficient, t is the temperature of detection, and B is corrected parameter；Then judge c's
Whether value is in the range of the certified concentration of electrolyte.
Finally it should be noted that the above embodiments are merely illustrative of the technical solutions of the present invention and it is unrestricted, although reference
The present invention is described in detail for preferred embodiment, it will be understood by those within the art that, can be to the present invention's
Technical scheme is modified or equivalent substitution, and without departing from the spirit and scope of technical solution of the present invention, it all should cover
Among scope of the presently claimed invention.
Claims (9)
1. a kind of device of the concentration of electrolyte of detection in real time, it is characterised in that described device includes constant-current supply (1), electrolysis sun
Pole (2), electrolysis cathode (3), electrolytic cell (4) and voltage check device (5), the electrolytic anode (2) and the electrolysis cathode
(3) electrically connected respectively with the constant-current supply (1)；Be loaded with electrolyte in the electrolytic cell (4), the electrolytic anode (2) and
The electrolysis cathode (3) is respectively protruding into the electrolyte, and the both ends of the voltage check device (5) are positive with the electrolysis respectively
Pole (2) and the electrolysis cathode (3) electrical connection.
2. device according to claim 1, it is characterised in that described device also includes and the voltage check device (5)
The processor (7) of connection and the warning device being connected with the processor (7)；The processor (7) is used to judge electrolyte
Whether concentration is qualified, and sends warning message to the warning device according to judged result.
3. device according to claim 2, it is characterised in that the processor (7) includes：
Voltage module (701)：The voltage detecting result sent for receiving voltage detection means (5)；
Judge module (702)：For judging whether concentration of electrolyte is qualified according to voltage detecting result, and it will determine that result is sent
Give alarm module (703)；
Alarm module (703)：For after the judged result of judge module (702) transmission is received, being determined according to judged result
Warning message whether is generated, and warning message is sent to warning device.
4. device according to claim 1, it is characterised in that described device also includes temperature-detecting device (6), the temperature
Degree detection means (6) is stretched into the electrolyte.
5. device according to claim 4, it is characterised in that the processor (7) also includes thermal module (704)；
The thermal module (704) is used for the temperature detection result for receiving temperature-detecting device (6) transmission；
The judge module (702) is used to judge whether concentration of electrolyte closes according to temperature detection result and voltage detecting result
Lattice, and will determine that result is sent to alarm module (703).
6. device according to claim 5, it is characterised in that whether the judge module (702) judges concentration of electrolyte
Qualified detailed process includes：First determine whether temperature detection result allows in temperature range positioned at electrolyte, if it is not, then
Temperature determination result is sent to warning device；If it is, according to c=k1U+k2T+B calculates concentration of electrolyte c, wherein, k1For
Voltage coefficient, U be detection voltage, k2For temperature coefficient, t is the temperature of detection, and B is corrected parameter；Then judging c value is
It is no in the range of the certified concentration of electrolyte, and send concentration judged result to warning device.
A kind of 7. method of the concentration of electrolyte of detection in real time, it is characterised in that methods described includes：Detect the electricity of electrolytic circuit
Pressure；Detection voltage qualified voltage corresponding with the electrolyte of certified concentration is analyzed, judges the electrolysis in electrolytic cell
Whether liquid concentration is qualified.
8. according to the method for claim 7, it is characterised in that methods described also includes：The temperature of electrolyte is detected, and is led to
The temperature of electrolyte and the voltage of electrolytic circuit are crossed to judge whether the concentration of electrolyte in electrolytic cell is qualified jointly.
9. according to the method for claim 8, it is characterised in that described " to pass through the temperature of electrolyte and the electricity of electrolytic circuit
Press and judge whether the concentration of electrolyte in electrolytic cell qualified jointly " detailed process include：First determining whether electrolyte temperature is
It is no to allow positioned at electrolyte in temperature range, if it is not, then showing that electrolyte temperature has been over allowed band, it is necessary in time
Adjustment；If it is, according to c=k1U+k2T+B calculates concentration of electrolyte c, wherein, k1For voltage coefficient, U is the voltage of detection,
k2For temperature coefficient, t is the temperature of detection, and B is corrected parameter；Then judge whether c value is located at the certified concentration of electrolyte
In the range of.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201711167141.2A CN107747108A (en) | 2017-11-21 | 2017-11-21 | A kind of device and method of the concentration of electrolyte of detection in real time |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201711167141.2A CN107747108A (en) | 2017-11-21 | 2017-11-21 | A kind of device and method of the concentration of electrolyte of detection in real time |
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| CN107747108A true CN107747108A (en) | 2018-03-02 |
Family
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| CN201711167141.2A Pending CN107747108A (en) | 2017-11-21 | 2017-11-21 | A kind of device and method of the concentration of electrolyte of detection in real time |
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Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111060655A (en) * | 2019-12-28 | 2020-04-24 | 安徽正熹标王新能源有限公司 | Battery is electrolyte selective examination device for production line |
| CN112251775A (en) * | 2020-10-23 | 2021-01-22 | 珠海格力电器股份有限公司 | Control method and control device of electrolysis device and electrolysis device |
| CN112725858A (en) * | 2020-12-02 | 2021-04-30 | 西比里电机技术(苏州)有限公司 | State detection method for thermoelectric chemical oxidation system |
| CN113030225A (en) * | 2021-03-10 | 2021-06-25 | 哈尔滨工程大学 | Judgment and automatic response method for molten salt purification end point |
| CN113046762A (en) * | 2021-03-10 | 2021-06-29 | 哈尔滨工程大学 | Method for judging and automatically responding electrodeposition endpoint of uranium dioxide in molten salt system |
| CN113671373A (en) * | 2021-07-27 | 2021-11-19 | 三门三友科技股份有限公司 | Electrolytic process monitoring system and method in electrolytic cell with self-checking function |
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Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111060655A (en) * | 2019-12-28 | 2020-04-24 | 安徽正熹标王新能源有限公司 | Battery is electrolyte selective examination device for production line |
| CN112251775A (en) * | 2020-10-23 | 2021-01-22 | 珠海格力电器股份有限公司 | Control method and control device of electrolysis device and electrolysis device |
| CN112725858A (en) * | 2020-12-02 | 2021-04-30 | 西比里电机技术(苏州)有限公司 | State detection method for thermoelectric chemical oxidation system |
| CN113030225A (en) * | 2021-03-10 | 2021-06-25 | 哈尔滨工程大学 | Judgment and automatic response method for molten salt purification end point |
| CN113046762A (en) * | 2021-03-10 | 2021-06-29 | 哈尔滨工程大学 | Method for judging and automatically responding electrodeposition endpoint of uranium dioxide in molten salt system |
| CN113671373A (en) * | 2021-07-27 | 2021-11-19 | 三门三友科技股份有限公司 | Electrolytic process monitoring system and method in electrolytic cell with self-checking function |
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