CN107739580A - A kind of preparation method of high viscosity armor band - Google Patents
A kind of preparation method of high viscosity armor band Download PDFInfo
- Publication number
- CN107739580A CN107739580A CN201711119996.8A CN201711119996A CN107739580A CN 107739580 A CN107739580 A CN 107739580A CN 201711119996 A CN201711119996 A CN 201711119996A CN 107739580 A CN107739580 A CN 107739580A
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- China
- Prior art keywords
- parts
- binding agent
- high viscosity
- preparation
- armor band
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Classifications
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
- C09J163/00—Adhesives based on epoxy resins; Adhesives based on derivatives of epoxy resins
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
- C09J11/00—Features of adhesives not provided for in group C09J9/00, e.g. additives
- C09J11/02—Non-macromolecular additives
- C09J11/06—Non-macromolecular additives organic
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
- C09J163/00—Adhesives based on epoxy resins; Adhesives based on derivatives of epoxy resins
- C09J163/10—Epoxy resins modified by unsaturated compounds
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2201/00—Properties
- C08L2201/02—Flame or fire retardant/resistant
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2201/00—Properties
- C08L2201/08—Stabilised against heat, light or radiation or oxydation
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
- C09J2203/00—Applications of adhesives in processes or use of adhesives in the form of films or foils
- C09J2203/302—Applications of adhesives in processes or use of adhesives in the form of films or foils for bundling cables
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
- C09J2400/00—Presence of inorganic and organic materials
- C09J2400/10—Presence of inorganic materials
- C09J2400/14—Glass
- C09J2400/143—Glass in the substrate
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Laminated Bodies (AREA)
- Compositions Of Macromolecular Compounds (AREA)
Abstract
A kind of preparation method of high viscosity armor band, including following operating procedure：（1）Fiberglass adhesive tape is put into 70 75 DEG C of hot water, isothermal holding 35 hours, on external coating after binding agent A, is put into baking oven and dries；（2）Step will be passed through（1）The fiberglass adhesive tape external coating binding agent B of processing, after naturally dry handles 50 60min, airtight package, finished product.High viscosity armor band produced by the present invention, easy to use, odorless, nontoxic, nonflammable, high insulation, it can complete in 5 7min to solidify load-bearing, especially it has excellent adhesion strength, and weatherability is strong, service life length, greatly improves the quality of armor band.
Description
Technical field
The invention belongs to armor band preparing technical field, and in particular to a kind of preparation method of high viscosity armor band.
Background technology
Armor band be by special glass fibre be woven into high intensity, high-elastic structure fabric, then braiding belt surface
Coat water cure high-molecular compound Er System into a kind of fiberglass product.It, which has, meets water rapid curing, easy to operate and application
The features such as scope is wide, the works bending strength and tensile strength that are formed after solidification be high, nonpoisonous and tasteless non-stimulated, water-fast corrosion resistant
Erosion.Armor band can be wrapped up directly on cable accessory or cable, form the machine of high intensity outer jacket, energy reinforced joint and cable
Tool is protected.Armor band of the prior art, low there is adhesion strength, especially weatherability can not meet requirement, life-span
The defects of short.
The content of the invention
In order to solve the above-mentioned technical problem, the present invention provides a kind of preparation method of high viscosity armor band.
The present invention is achieved by the following technical solutions.
A kind of preparation method of high viscosity armor band, including following operating procedure：
（1）Fiberglass adhesive tape is put into 70-75 DEG C of hot water, isothermal holding 3-5 hours, on external coating after binding agent A,
It is put into baking oven and dries, wherein binding agent A is made up of the component of following parts by weight：Amino tetrafunctional epoxy resin 45-53 parts, gather
First and second aldehyde 34-39 parts of vinyl alcohol contracting, ethanol 15-19 parts, Deferoxamine 3-8 parts, D-ALPHA-Hydroxypropionic acid methyl esters 6-8 parts；
（2）Step will be passed through（1）After the fiberglass adhesive tape external coating binding agent B of processing, naturally dry processing 50-60min,
Airtight package, wherein finished product, binding agent B are made up of the component of following parts by weight：Lignin 34-39 parts, epoxy vinyl
Fat resin 42-46 parts, Potassium Hydrogen Phthalate 11-16 parts, δ-dodecalactone 2-4 parts, water 22-27 parts.
Specifically, above-mentioned steps（1）In, binding agent A is made of following methods：By amino tetrafunctional epoxy resin and second
After alcohol mixing, continue addition, polyvinyl formal acetal, Deferoxamine, D-ALPHA-Hydroxypropionic acid methyl esters thereto, be mixed evenly, be made
Binding agent A.
Specifically, the volume fraction of above-mentioned ethanol is 90-95%.
Specifically, above-mentioned steps（1）In, the temperature of drying is 55-60 DEG C.
Specifically, above-mentioned steps（2）In, binding agent B is made of following methods：By Potassium Hydrogen Phthalate, lignin
Add into water, after persistently stirring 35min using 400r/min rotating speed, continue to add thereto epoxy vinyl fat resin,
δ-dodecalactone, continue after stirring 20min, binding agent B is made.
Technical scheme more than, the beneficial effects of the invention are as follows：
High viscosity armor band produced by the present invention, easy to use, odorless, nontoxic, nonflammable, high insulation, 5-7min are interior
Solidification load-bearing is completed, especially it has excellent adhesion strength, and weatherability is strong, service life length, greatly improves armor
The quality of band.Wherein, the present invention coats binding agent A on fiberglass adhesive tape now, and binding agent A can play increasing as intermediate layer
The effect of strong adhesive force of the binding agent B on armor band so that armor band is torn again before curing in the case of operating mistake
Under, binding agent is not in the phenomenon to come off, while binding agent A can also play the protective action to fiberglass adhesive tape, lifting
The weatherability of armor band；Bonding B has excellent adhesive property, and adhesion strength is high, is not easy to be oxidized, greatly extends armour
The service life of first band.
Embodiment
In order to make the purpose , technical scheme and advantage of the present invention be clearer, following examples are carried out to the present invention
It is further described.It should be appreciated that specific embodiment party example described herein is not used to limit only to explain the present invention
The fixed present invention.
Embodiment 1
A kind of preparation method of high viscosity armor band, including following operating procedure：
（1）Fiberglass adhesive tape is put into 70 DEG C of hot water, isothermal holding 3 hours, on external coating after binding agent A, be put into
Dried in baking oven, wherein binding agent A is made up of the component of following parts by weight：45 parts of amino tetrafunctional epoxy resin, polyvinyl alcohol
Contract 34 parts of the first and second aldehyde, 15 parts of ethanol, 3 parts of Deferoxamine, 6 parts of D-ALPHA-Hydroxypropionic acid methyl esters；
（2）Step will be passed through（1）It is close after the fiberglass adhesive tape external coating binding agent B of processing, naturally dry processing 50min
Closure fills, and finished product, wherein binding agent B are made up of the component of following parts by weight：34 parts of lignin, epoxy vinyl fat resin
42 parts, 11 parts of Potassium Hydrogen Phthalate, 2 parts of δ-dodecalactone, 22 parts of water.
Specifically, above-mentioned steps（1）In, binding agent A is made of following methods：By amino tetrafunctional epoxy resin and second
After alcohol mixing, continue addition, polyvinyl formal acetal, Deferoxamine, D-ALPHA-Hydroxypropionic acid methyl esters thereto, be mixed evenly, be made
Binding agent A.
Specifically, the volume fraction of above-mentioned ethanol is 90%.
Specifically, above-mentioned steps（1）In, the temperature of drying is 55 DEG C.
Specifically, above-mentioned steps（2）In, binding agent B is made of following methods：By Potassium Hydrogen Phthalate, lignin
Add into water, after persistently stirring 35min using 400r/min rotating speed, continue to add thereto epoxy vinyl fat resin,
δ-dodecalactone, continue after stirring 20min, binding agent B is made.
Armor band in the present embodiment, for normal use after 1 year, its adhesion strength still has 14kg/cm2。
Embodiment 2
A kind of preparation method of high viscosity armor band, including following operating procedure：
（1）Fiberglass adhesive tape is put into 73 DEG C of hot water, isothermal holding 4 hours, on external coating after binding agent A, be put into
Dried in baking oven, wherein binding agent A is made up of the component of following parts by weight：48 parts of amino tetrafunctional epoxy resin, polyvinyl alcohol
Contract 37 parts of the first and second aldehyde, 17 parts of ethanol, 5 parts of Deferoxamine, 7 parts of D-ALPHA-Hydroxypropionic acid methyl esters；
（2）Step will be passed through（1）It is close after the fiberglass adhesive tape external coating binding agent B of processing, naturally dry processing 55min
Closure fills, and finished product, wherein binding agent B are made up of the component of following parts by weight：36 parts of lignin, epoxy vinyl fat resin
44 parts, 13 parts of Potassium Hydrogen Phthalate, 3 parts of δ-dodecalactone, 25 parts of water.
Specifically, above-mentioned steps（1）In, binding agent A is made of following methods：By amino tetrafunctional epoxy resin and second
After alcohol mixing, continue addition, polyvinyl formal acetal, Deferoxamine, D-ALPHA-Hydroxypropionic acid methyl esters thereto, be mixed evenly, be made
Binding agent A.
Specifically, the volume fraction of above-mentioned ethanol is 93%.
Specifically, above-mentioned steps（1）In, the temperature of drying is 58 DEG C.
Specifically, above-mentioned steps（2）In, binding agent B is made of following methods：By Potassium Hydrogen Phthalate, lignin
Add into water, after persistently stirring 35min using 400r/min rotating speed, continue to add thereto epoxy vinyl fat resin,
δ-dodecalactone, continue after stirring 20min, binding agent B is made.
Armor band in the present embodiment, for normal use after 1 year, its adhesion strength still has 15kg/cm2。
Embodiment 3
A kind of preparation method of high viscosity armor band, including following operating procedure：
（1）Fiberglass adhesive tape is put into 75 DEG C of hot water, isothermal holding 5 hours, on external coating after binding agent A, be put into
Dried in baking oven, wherein binding agent A is made up of the component of following parts by weight：53 parts of amino tetrafunctional epoxy resin, polyvinyl alcohol
Contract 39 parts of the first and second aldehyde, 19 parts of ethanol, 8 parts of Deferoxamine, 8 parts of D-ALPHA-Hydroxypropionic acid methyl esters；
（2）Step will be passed through（1）It is close after the fiberglass adhesive tape external coating binding agent B of processing, naturally dry processing 60min
Closure fills, and finished product, wherein binding agent B are made up of the component of following parts by weight：39 parts of lignin, epoxy vinyl fat resin
46 parts, 16 parts of Potassium Hydrogen Phthalate, 4 parts of δ-dodecalactone, 27 parts of water.
Specifically, above-mentioned steps（1）In, binding agent A is made of following methods：By amino tetrafunctional epoxy resin and second
After alcohol mixing, continue addition, polyvinyl formal acetal, Deferoxamine, D-ALPHA-Hydroxypropionic acid methyl esters thereto, be mixed evenly, be made
Binding agent A.
Specifically, the volume fraction of above-mentioned ethanol is 95%.
Specifically, above-mentioned steps（1）In, the temperature of drying is 60 DEG C.
Specifically, above-mentioned steps（2）In, binding agent B is made of following methods：By Potassium Hydrogen Phthalate, lignin
Add into water, after persistently stirring 35min using 400r/min rotating speed, continue to add thereto epoxy vinyl fat resin,
δ-dodecalactone, continue after stirring 20min, binding agent B is made.
Armor band in the present embodiment, for normal use after 1 year, its adhesion strength still has 18kg/cm2。
It should be noted that the above embodiments are merely illustrative of the technical solutions of the present invention and it is unrestricted.Although with reference to compared with
The present invention is described in detail good embodiment, it will be understood by those within the art that, can be to the technology of invention
Scheme is modified or equivalent substitution, and without departing from the scope of technical solution of the present invention, it all should cover the power in the present invention
In sharp claimed range.
Claims (5)
1. a kind of preparation method of high viscosity armor band, it is characterised in that including following operating procedure：
（1）Fiberglass adhesive tape is put into 70-75 DEG C of hot water, isothermal holding 3-5 hours, on external coating after binding agent A,
It is put into baking oven and dries, wherein binding agent A is made up of the component of following parts by weight：Amino tetrafunctional epoxy resin 45-53 parts, gather
First and second aldehyde 34-39 parts of vinyl alcohol contracting, ethanol 15-19 parts, Deferoxamine 3-8 parts, D-ALPHA-Hydroxypropionic acid methyl esters 6-8 parts；
（2）Step will be passed through（1）After the fiberglass adhesive tape external coating binding agent B of processing, naturally dry processing 50-60min,
Airtight package, wherein finished product, binding agent B are made up of the component of following parts by weight：Lignin 34-39 parts, epoxy vinyl
Fat resin 42-46 parts, Potassium Hydrogen Phthalate 11-16 parts, δ-dodecalactone 2-4 parts, water 22-27 parts.
A kind of 2. preparation method of high viscosity armor band according to claim 1, it is characterised in that above-mentioned steps（1）In,
Binding agent A is made of following methods：After amino tetrafunctional epoxy resin is mixed with ethanol, continue addition, poly- second thereto
The first and second aldehyde of enol contracting, Deferoxamine, D-ALPHA-Hydroxypropionic acid methyl esters, are mixed evenly, binding agent A are made.
A kind of 3. preparation method of high viscosity armor band according to claim 2, it is characterised in that the volume of above-mentioned ethanol
Fraction is 90-95%.
A kind of 4. preparation method of high viscosity armor band according to claim 1, it is characterised in that above-mentioned steps（1）In,
The temperature of drying is 55-60 DEG C.
A kind of 5. preparation method of high viscosity armor band according to claim 1, it is characterised in that above-mentioned steps（2）In,
Binding agent B is made of following methods：Potassium Hydrogen Phthalate, lignin are added into water, using 400r/min rotating speed
After persistently stirring 35min, continue to add epoxy vinyl fat resin, δ-dodecalactone thereto, continue after stirring 20min, system
Obtain binding agent B.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201711119996.8A CN107739580A (en) | 2017-11-14 | 2017-11-14 | A kind of preparation method of high viscosity armor band |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201711119996.8A CN107739580A (en) | 2017-11-14 | 2017-11-14 | A kind of preparation method of high viscosity armor band |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN107739580A true CN107739580A (en) | 2018-02-27 |
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ID=61234566
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201711119996.8A Pending CN107739580A (en) | 2017-11-14 | 2017-11-14 | A kind of preparation method of high viscosity armor band |
Country Status (1)
| Country | Link |
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| CN (1) | CN107739580A (en) |
Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101338167A (en) * | 2007-08-13 | 2009-01-07 | 张一平 | Curable adhesive tape for blocking Leakage, and repairing and protecting cable |
-
2017
- 2017-11-14 CN CN201711119996.8A patent/CN107739580A/en active Pending
Patent Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101338167A (en) * | 2007-08-13 | 2009-01-07 | 张一平 | Curable adhesive tape for blocking Leakage, and repairing and protecting cable |
Non-Patent Citations (1)
| Title |
|---|
| 李子东等: "《现代胶粘技术手册》", 31 January 2002, 新时代出版社 * |
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Application publication date: 20180227 |