CN107723101A - Light chlorimation bubbling agitates method to produce chlorination gutter oil method - Google Patents

Light chlorimation bubbling agitates method to produce chlorination gutter oil method Download PDF

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Publication number
CN107723101A
CN107723101A CN201710362923.5A CN201710362923A CN107723101A CN 107723101 A CN107723101 A CN 107723101A CN 201710362923 A CN201710362923 A CN 201710362923A CN 107723101 A CN107723101 A CN 107723101A
Authority
CN
China
Prior art keywords
kettle
gutter oil
chlorination
production
chlorinated paraffin
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Withdrawn
Application number
CN201710362923.5A
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Chinese (zh)
Inventor
林群祥
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Individual
Original Assignee
Individual
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Individual filed Critical Individual
Priority to CN201710362923.5A priority Critical patent/CN107723101A/en
Publication of CN107723101A publication Critical patent/CN107723101A/en
Withdrawn legal-status Critical Current

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Classifications

    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11C—FATTY ACIDS FROM FATS, OILS OR WAXES; CANDLES; FATS, OILS OR FATTY ACIDS BY CHEMICAL MODIFICATION OF FATS, OILS, OR FATTY ACIDS OBTAINED THEREFROM
    • C11C3/00—Fats, oils, or fatty acids by chemical modification of fats, oils, or fatty acids obtained therefrom
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G73/00—Recovery or refining of mineral waxes, e.g. montan wax
    • C10G73/38—Chemical modification of petroleum
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B13/00—Recovery of fats, fatty oils or fatty acids from waste materials
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B3/00—Refining fats or fatty oils
    • C11B3/001—Refining fats or fatty oils by a combination of two or more of the means hereafter
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B3/00—Refining fats or fatty oils
    • C11B3/008—Refining fats or fatty oils by filtration, e.g. including ultra filtration, dialysis
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B3/00—Refining fats or fatty oils
    • C11B3/10—Refining fats or fatty oils by adsorption
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02W—CLIMATE CHANGE MITIGATION TECHNOLOGIES RELATED TO WASTEWATER TREATMENT OR WASTE MANAGEMENT
    • Y02W30/00—Technologies for solid waste management
    • Y02W30/50—Reuse, recycling or recovery technologies
    • Y02W30/74—Recovery of fats, fatty oils, fatty acids or other fatty substances, e.g. lanolin or waxes

Abstract

Title of the present invention is that Light chlorimation bubbling agitates method to produce chlorination gutter oil method, belong to chlorinated paraffin technical field, in order to improve chlorinated paraffin speed of production, the upper light source of installation in kettle is adopted the technical scheme that based on former 87106851.6 patents are improved with it, the another above bubbler chlorine that installs additional is directly placed into bubbler in 87106851.6 device kettles, gutter oil is boiled, the removal of impurity is gone in layering, debris, moisture content, with activated decoloration after 150 DEG C or so of heating, pass through press filtration again, washed again through superheated water, salt reduction degree, it is layered to put into kettle after water again and reacts, for example traditional thermal chlorination Bubbling method production chlorinated paraffin of production operation, a kind of faster production method is provided.

Description

Light chlorimation bubbling agitates method to produce chlorination gutter oil method
(1) technical field：The present invention relates to a kind of method for producing chlorination gutter oil, category production chlorinated paraffin technology neck Domain.
(2) background technology：" equipment for preparation of paraffin chloride by forced circulating blast method " (former patent No.：87106851.6) its Technical scheme is：Chlorine is sent into the hydrogen chloride gas extraction in reactor space, chlorine and reaction generation, through jet pump and reservoir Groove, it is only absorbed by the water, remaining chlorine drum is pressed into agitation device, such continuous fast reaction.But for producing chlorinated paraffin speed also not Enough ideals, especially produce high chlorinated paraffin product, and to the reaction later stage, speed eases up.
(3) content of the invention：The task of the present invention is based on a kind of improvement to former 87106851.6 patents of invention, there is provided A kind of method of the chlorination gutter oil of production faster, adopts the technical scheme that and installs upper light source in kettle additional, another in its reactor Bubbler in installation, the chlorine supplied by chlorine source are passed directly into bubbler, and bubbling is carried out to reactor material, so are forcing to follow Ring is agitated down along with bubbling improves reaction speed, and gutter oil is boiled, and the removal of impurity, debris, moisture content are removed in layering, is heated With activated decoloration after 150 DEG C or so, then by press filtration, then wash through superheated water, salt reduction degree, then kettle is put into after being layered water Middle reaction, for example traditional thermal chlorination Bubbling method production chlorinated paraffin of production operation.
(4) embodiment：A set of " equipment for preparation of paraffin chloride by forced circulating blast method ", use 500 liters of reactions Kettle, its reactor is interior to install 1000 watts of mercury lamps additional, and existing current bubbler is installed additional again in its reactor.Gutter oil is endured System, the removal of impurity, debris, moisture content are removed in layering, with activated decoloration after 150 DEG C or so of heating, then by press filtration, then through overheat Water is washed, salt reduction degree, then is layered to put into kettle after water and is reacted, for example traditional thermal chlorination Bubbling method production chlorination stone of production operation Wax.
Present invention operation and " equipment for preparation of paraffin chloride by forced circulating blast method " are same.

Claims (1)

1. a kind of Light chlorimation bubbling agitates method to produce chlorination gutter oil method, including chlorine and hydrogen chloride gas is extracted out, chlorination Hydrogen is only absorbed by the water in jet pump and hopper, and remaining chlorine drum is pressed into agitation device, so continuous, it is characterized in that：Kettle is built-in There is light source chlorination chlorine to be directly placed into bubbler in kettle, gutter oil is boiled, the removal of impurity, debris, moisture content are removed in layering, heat With activated decoloration after 150 DEG C or so, then by press filtration, then wash through superheated water, salt reduction degree, then kettle is put into after being layered water Middle reaction, for example traditional thermal chlorination Bubbling method production chlorinated paraffin of production operation.
CN201710362923.5A 2017-05-13 2017-05-13 Light chlorimation bubbling agitates method to produce chlorination gutter oil method Withdrawn CN107723101A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201710362923.5A CN107723101A (en) 2017-05-13 2017-05-13 Light chlorimation bubbling agitates method to produce chlorination gutter oil method

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201710362923.5A CN107723101A (en) 2017-05-13 2017-05-13 Light chlorimation bubbling agitates method to produce chlorination gutter oil method

Publications (1)

Publication Number Publication Date
CN107723101A true CN107723101A (en) 2018-02-23

Family

ID=61201272

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201710362923.5A Withdrawn CN107723101A (en) 2017-05-13 2017-05-13 Light chlorimation bubbling agitates method to produce chlorination gutter oil method

Country Status (1)

Country Link
CN (1) CN107723101A (en)

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN87106851A (en) * 1987-10-06 1988-07-27 林群祥 Equipment for preparation of paraffin chloride by forced circulating blast method
CN105838421A (en) * 2016-04-08 2016-08-10 林群祥 Method for producing chlorinated paraffin through photochlorination bubbling blast method
CN106350216A (en) * 2016-08-25 2017-01-25 林群祥 Chlorinated waste edible oil

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN87106851A (en) * 1987-10-06 1988-07-27 林群祥 Equipment for preparation of paraffin chloride by forced circulating blast method
CN105838421A (en) * 2016-04-08 2016-08-10 林群祥 Method for producing chlorinated paraffin through photochlorination bubbling blast method
CN106350216A (en) * 2016-08-25 2017-01-25 林群祥 Chlorinated waste edible oil

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Application publication date: 20180223