CN107717765B - A kind of grinding wheel and preparation method thereof applied to the grinding of ceramic insertion core concentricity - Google Patents

A kind of grinding wheel and preparation method thereof applied to the grinding of ceramic insertion core concentricity Download PDF

Info

Publication number
CN107717765B
CN107717765B CN201711070211.2A CN201711070211A CN107717765B CN 107717765 B CN107717765 B CN 107717765B CN 201711070211 A CN201711070211 A CN 201711070211A CN 107717765 B CN107717765 B CN 107717765B
Authority
CN
China
Prior art keywords
grinding
grinding wheel
insertion core
ceramic insertion
preparation
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Active
Application number
CN201711070211.2A
Other languages
Chinese (zh)
Other versions
CN107717765A (en
Inventor
叶腾飞
曹剑锋
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Zhengzhou Research Institute for Abrasives and Grinding Co Ltd
Original Assignee
Zhengzhou Research Institute for Abrasives and Grinding Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Zhengzhou Research Institute for Abrasives and Grinding Co Ltd filed Critical Zhengzhou Research Institute for Abrasives and Grinding Co Ltd
Priority to CN201711070211.2A priority Critical patent/CN107717765B/en
Publication of CN107717765A publication Critical patent/CN107717765A/en
Application granted granted Critical
Publication of CN107717765B publication Critical patent/CN107717765B/en
Active legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Classifications

    • BPERFORMING OPERATIONS; TRANSPORTING
    • B24GRINDING; POLISHING
    • B24DTOOLS FOR GRINDING, BUFFING OR SHARPENING
    • B24D18/00Manufacture of grinding tools or other grinding devices, e.g. wheels, not otherwise provided for
    • B24D18/0072Manufacture of grinding tools or other grinding devices, e.g. wheels, not otherwise provided for using adhesives for bonding abrasive particles or grinding elements to a support, e.g. by gluing
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B24GRINDING; POLISHING
    • B24DTOOLS FOR GRINDING, BUFFING OR SHARPENING
    • B24D18/00Manufacture of grinding tools or other grinding devices, e.g. wheels, not otherwise provided for
    • B24D18/0009Manufacture of grinding tools or other grinding devices, e.g. wheels, not otherwise provided for using moulds or presses
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B24GRINDING; POLISHING
    • B24DTOOLS FOR GRINDING, BUFFING OR SHARPENING
    • B24D3/00Physical features of abrasive bodies, or sheets, e.g. abrasive surfaces of special nature; Abrasive bodies or sheets characterised by their constituents
    • B24D3/02Physical features of abrasive bodies, or sheets, e.g. abrasive surfaces of special nature; Abrasive bodies or sheets characterised by their constituents the constituent being used as bonding agent
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B24GRINDING; POLISHING
    • B24DTOOLS FOR GRINDING, BUFFING OR SHARPENING
    • B24D3/00Physical features of abrasive bodies, or sheets, e.g. abrasive surfaces of special nature; Abrasive bodies or sheets characterised by their constituents
    • B24D3/34Physical features of abrasive bodies, or sheets, e.g. abrasive surfaces of special nature; Abrasive bodies or sheets characterised by their constituents characterised by additives enhancing special physical properties, e.g. wear resistance, electric conductivity, self-cleaning properties
    • B24D3/342Physical features of abrasive bodies, or sheets, e.g. abrasive surfaces of special nature; Abrasive bodies or sheets characterised by their constituents characterised by additives enhancing special physical properties, e.g. wear resistance, electric conductivity, self-cleaning properties incorporated in the bonding agent

Landscapes

  • Engineering & Computer Science (AREA)
  • Mechanical Engineering (AREA)
  • Manufacturing & Machinery (AREA)
  • Polishing Bodies And Polishing Tools (AREA)

Abstract

A kind of preparation method of the grinding wheel applied to the grinding of ceramic insertion core concentricity, belong to optical fiber connecting material Ultraprecision Machining field and includes the following steps: that (1) phenol-formaldehyde resin modified liquid, zirconia hollow microsphere and the calcirm-fluoride after dilution are added in ethyl acetate, 50 DEG C -90 DEG C of stirrings 1-3 hours, sodium chloride solution is added, 75-85 DEG C of heating 45-90nin obtains block mixture, and modified polyimide resin is added, ball milling, sieving obtain bonding agent;(2) bonding agent obtained by diamond and step (1) is weighed according to mass ratio for the ratio of 1:(3-8), sieving is suppressed in 280 DEG C -360 DEG C, 5MPa-15MPa, and the dwell time is 30-80 minutes, obtains grinding layer;(3) grinding layer is adhered on fluorine silicone rubber, fluorine silicone rubber is adhered on grinding wheel base body, obtain grinding wheel semi-finished product;(4) the inlet port and outlet port of grinding wheel semi-finished product carry out chamfering to get.

Description

A kind of grinding wheel and preparation method thereof applied to the grinding of ceramic insertion core concentricity
Technical field
The invention belongs to optical fiber connecting material Ultra-precision Turning fields, and in particular to one kind is applied to ceramic insertion core concentricity Grinding wheel of grinding and preparation method thereof.
Background technique
Ceramic insertion core is that a kind of high accuracy circular cylinder special type zirconia ceramics of precise centering in optical fiber connector plug is former Part, hardness is high, and fusing point is high, and grinding difficulty is larger.The outer circles and outer surface smoothness requirements of such workpiece are high, It is just able to satisfy the fixation of optical fiber, meets the matching requirements of production and application.0.1 μm of < of outer circle finish Ra generally is required, concentricity It is required that≤1 μm.
It is mainly at present ceramic bond diamond abrasive grinding wheel for the grinding wheel of this outer circles processing.But adding There are problems that following three during work: one, Ra0.1 is not achieved in outer round surface finish part in batch production process.Two, outer 1 μm of circle concentricity >;Three, single-grain grinding is processed, the thimble fracture frequency is higher, about grinds 400 lock pins with regard to broken needle;For Grinding is threaded, broken string phenomenon is serious, about grinding 10-13 group lock pin, just will appear broken string.Problem above not only influences product Quality, and cause production cost higher, production efficiency is lower.
Technique of Vitrified Diamond Wheels intensity is high, resistance to grinding heat, long service life, but is being ground hard and crisp oxidation , but can be higher due to matching hardness when zircon ceramic lock pin, and cause the self-sharpening of grinding wheel bad, it is easy to appear above-mentioned three spoken of A problem.
Summary of the invention
The present invention is directed to the hardness of ceramic insertion core material, intensity, and requires to meet ceramic insertion core concentricity, invention A kind of grinding wheel applied to the grinding of ceramic insertion core concentricity, the grinding wheel are resin anchoring agent diamond grinding wheel, and self-sharpening is good, grinding It is sharp, final abrasive product finish ra < 0.08, be ground out lock pin concentricity reach 0.3 μm hereinafter, and grinding wheel using Cheng Zhong, no matter take single-grain grinding or threading grinding, all will not broken needle broken string, be finally reached and meet the same of quality requirement When, production efficiency is improved, processing cost is reduced.The present invention also provides a kind of sand applied to the grinding of ceramic insertion core concentricity simultaneously The preparation method of wheel.
Based on above-mentioned purpose, the present invention is adopted the following technical scheme that:
(1) phenol-formaldehyde resin modified liquid, zirconia hollow microsphere and the calcirm-fluoride after dilution are added in ethyl acetate, 50 DEG C -90 DEG C stirring 1-3 hours, sodium chloride solution is added, 75-85 DEG C of heating 45-90nin obtains block mixture, and modification is added Polyimide resin, ball milling, sieving obtain bonding agent;
(2) bonding agent obtained by diamond and step (1) is weighed according to mass ratio for the ratio of 1:(3-8), sieving, It is suppressed in 280 DEG C -360 DEG C, 5MPa-15MPa, the dwell time is 30-80 minutes, obtains grinding layer;
(3) grinding layer is adhered on fluorine silicone rubber, fluorine silicone rubber is adhered on grinding wheel base body, obtain grinding wheel half at Product;
(4) the inlet port and outlet port of grinding wheel semi-finished product carry out chamfering to get.
Preferably, the phenol-formaldehyde resin modified liquid in the step (1) after dilution, zirconia hollow microsphere, the matter of calcirm-fluoride Amount is than being 1:(18 ~ 22): (28 ~ 32), the weight of modified polyimide resin are the 1.5-2 of the block mixture weight after drying Times
Preferably, the phenol-formaldehyde resin modified liquid after diluting described in the step (1) refers to changing according to 1:20 mass ratio Property the dilution that carries out of phenolic resin and cresols, the concentration of the sodium chloride solution is 40-50wt%, sodium chloride solution plus Entering amount is phenol-formaldehyde resin modified liquid after dilution, 2 ~ 8 times of zirconia hollow microsphere and calcirm-fluoride gross weight.
Preferably, zirconia hollow microsphere partial size is 50 μm -65 μm, and ball wall is broken with a thickness of 5 μm -9 μm;Calcirm-fluoride is point It analyses pure, it is desirable that median particle diameter D50 is 60 μm, and D95 is no more than 100 μm;The partial size of modified polyimide resin powder is 24 μm of -48 μ m。
Diamond is nickel plating diamond in the step (2) and granularity is -1500 mesh of 100 mesh.
The above-mentioned preparation method grinding wheel obtained applied to the grinding of ceramic insertion core concentricity.
The grinding wheel is followed successively by grinding wheel base body, transition zone and grinding layer from inside to outside, and grinding layer ring width is 5-25mm, transition Layer is fluorine silicone rubber, and the width of fluorine silicone rubber is 5-25mm, and grinding wheel base body is stainless steel base, and grinding wheel overall thickness is 25- 100mm, grinding wheel diameter 75-250mm.
It is a kind of applied to ceramic insertion core concentricity grinding grinding wheel include grinding wheel base body, transition zone and grinding layer, the sand Wheel matrix is stainless steel base;Transition zone is fluorine silicone rubber, and grinding layer is made of abrasive material, bonding agent;Abrasive material is diamond, in conjunction with Agent is modified polyimide resin powder, phenol-formaldehyde resin modified liquid, composite ceramics microballoon pore creating material, calcirm-fluoride pore creating material etc..It is described Abrasive material, bonding agent by mixing sieving, hot-forming at the grinding layer with ablation, carried out with grinding wheel transition zone it is be bonded, Form the grinding wheel for being applied to the grinding of this ceramic insertion core concentricity.
Grinding wheel base body of the present invention is stainless steel base.This material has good hardness and strength, makes in high revolving speed It in the process, is unlikely to deform, can guarantee good machining accuracy, be easy to carry out turnery processing, it can be according to mating grinding machine need It asks, is processed into different shapes.For grinding wheel base body, the non-corrosive in the case where there is grinding fluid grinding.
Abrasive diamond abrasive material of the present invention, according to the grinding allowance of workpiece, diamond grit range can be chosen most Thick 100 mesh, most thin 1500 mesh and median particle size range.
Modified polyimide resin powder of the present invention, particle size range are 24 μm -48 μm.
Functional stuffing of the present invention is zirconia hollow microsphere, and partial size is 50 μm -65 μm.Ball wall fracture with a thickness of 5 μm- 9μm.Calcirm-fluoride is that analysis is pure, it is desirable that median particle diameter D50 is 60 μm.D95 is no more than 100 μm.
Original creation part of the invention is, according to the hardness of ceramic lock pin based on zirconium oxide, density, concentricity requires etc., specially Devise the grinding wheel structure that can reach this requirement, grinding wheel formula and emery wheel making technique, especially in conjunction with the manufacturing process of agent, To be initiated in industry.Transition zone selects fluorine silicone rubber, not only has excellent high temperature resistance, but also have good cementability Can, the elasticity having matches the grinding force with grinding wheel layer in grinding well, can be according to grinding force size, phase occurs for elasticity It should change, suitability is fine, thus while guaranteeing sharp grinding, and can make that there is certain elasticity when wheel grinding, it is not easy Broken needle broken string, finally obtains the grinding wheel that can be used in the grinding of ceramic insertion core concentricity.
Beneficial effects of the present invention:
The manufacture of bonding agent of the present invention, using three steps, inorganic material colloid is made in the first step, and second step is made corresponding multiple Close bonding agent, the method that third step uses ball milling sieving.The selection or manufacture craft no matter this bonding agent is formulated, can Guarantee that bonding agent is uniformly mixed, calcirm-fluoride and zirconia hollow microsphere pore creating material can reach 90% or more pore-creating effect, can It improves grinding wheel sharpness and holds bits ability, and in use without finishing.
The high self-sharpening nickel plating diamond that diamond in the present invention is chosen, diamond itself possess the more of similar polycrystal A corner angle, and have both shape retention and sharpness, it can be good at processing concentricity at 1 μm, smoothness requirements are in Ra0.3 Workpiece below.
Intermediate layer of the present invention uses fluorine silicone rubber, has certain elasticity, while having with corresponding intensity, is being ground When elastic deformation self can occur to adjust grinding wheel for the grinding force of workpiece according to the hardness of material, can process different big Small workpiece, while meeting the work pieces process requirement of size surplus, the phenomenon that broken needle or broken string are avoided in grinding.
This grinding wheel is designed using the structure of edge chamfer, can guarantee there is certain buffering when workpiece is fed, The contact area for increasing charging, can guarantee that lock pin concentricity consistency, concentricity reach 0.3 micron of requirement below, meanwhile, Also the appearance of broken needle broken string phenomenon is effectively prevented.
Detailed description of the invention
Fig. 1 is the SEM figure of wheel grinding layer made from embodiment 1;The effect of hollow sphere is obvious as can be seen from Figure 1, makes Increased number of stomata is generated inside grinding layer, there can not only be good heat spreading function in grinding process, and there are enough appearances It considers space to be worth doing, to prevent grinding wheel obstruction from causing to generate scratch to workpiece surface, can be good at promoting grinding skin finish and table Face quality.
Fig. 2 is the SEM figure of wheel grinding layer made from embodiment 2;Point of the diamond in bonding agent as can be seen from Figure 2 Cloth is uniform, and is oxidized zirconium tiny balloon around diamond and wraps up well, forms thin-walled after hollow ball fractured, can reduce knot Mixture intensity makes grinding layer have better self-sharpening, which thereby enhances grinding efficiency and sharpness, final to improve the outer of workpiece Circle concentricity.
Fig. 3 is the structural schematic diagram of grinding wheel produced by the present invention;
In Fig. 3,1 is grinding wheel base body, and 2 be transition zone, and 3 be grinding layer,
X is grinding layer ring width, and X range is 5-25mm;
α is chamfering degree, and α range is 8 ° -25 °;
Y is transition zone width, and Y range is 5-25mm;
T is grinding wheel overall thickness, T range 25-100mm;
D is grinding wheel diameter, and D range is 75-250mm;
Grinding layer is stone layer;
Transition zone is fluorosilicone rubber layer.
Specific embodiment
Below in conjunction with specific embodiment, further details of the technical solution of the present invention, but protection model of the invention It encloses and is not limited thereto.
Calcirm-fluoride is that analysis is pure in following embodiments, it is desirable that median particle diameter D50 is 60 μm, and D95 is no more than 100 μm;Mixing Cresols is ordinary commercial products.Phenol-formaldehyde resin modified is the PF3032 of Shengquan Group Co. Ltd., Jinan's production, flowing length Degree is 15-50mm, Rockwell hardness 20-40HRB, tensile strength 20-60MPa.Zirconia hollow microsphere is commercial goods, grain Diameter is 50 μm -65 μm.Ball wall is broken with a thickness of 5 μm -9 μm.Calcirm-fluoride is that analysis is pure, it is desirable that median particle diameter D50 is 60 μm.D95 No more than 100 μm.Modified polyimide resin is the PI001, tensile strength 65- of Qinyang Tian Yi Chemical Co., Ltd. production 85MPa, Rockwell hardness 40-70HRB, partial size are 24 μm -48 μm.Diamond is nickel plating diamond, flies Meng's diamond purchased from Henan Industrial Co., Ltd.Cresols be the meta position of cresols, contraposition, the three kinds of Cresol Isomeric Compounds in ortho position mixture, be common commercially available Product.
Embodiment 1
A kind of preparation method of the grinding wheel applied to the grinding of ceramic insertion core concentricity, includes the following steps:
(1) phenol-formaldehyde resin modified liquid, zirconia hollow microsphere and the calcirm-fluoride 1:20:30 in mass ratio after dilution are added In ethyl acetate, the quality of ethyl acetate is phenol-formaldehyde resin modified liquid, zirconia hollow microsphere and the calcirm-fluoride three after dilution 5 times of total weight, 50 DEG C stirred in water bath 3 hours, the sodium chloride solution of 45wt% is added, and (additional amount of sodium chloride solution is 5 times of phenol-formaldehyde resin modified liquid, zirconia hollow microsphere and calcirm-fluoride three's total weight after dilution), 80 DEG C of heating 60min, Dry block mixture is obtained, it is sub- that modified polyamides is added according to block mixture and 1 ︰ 2 of modified polyimide resin mass ratio Polyimide resin, ball milling sieve with 100 mesh sieve net and obtain bonding agent, wherein the phenol-formaldehyde resin modified liquid after the dilution refers to according to 1: The dilution of cresols progress is added into phenol-formaldehyde resin modified for 20 mass ratioes;
(2) ratio for being 1:5 according to mass ratio by bonding agent obtained by diamond and step (1) that granularity is 280 mesh 120 mesh screens are crossed in weighing, are suppressed in 280 DEG C, 10MPa, and the dwell time is 60 minutes, obtains grinding layer;
(3) grinding layer is adhered on fluorine silicone rubber, fluorine silicone rubber is adhered on grinding wheel base body, obtain grinding wheel half at Product;
(4) unified in order in grinding, guarantee that the concentricity of workpiece and lock pin process continuity and size end to end Property, as shown in Figure 1, the inlet port and outlet port of grinding wheel semi-finished product are carried out chamfering, chamfering degree α is 8 ° -25 °, and length is 2mm-15mm, the grinding wheel are followed successively by 3 layers of grinding wheel base body 1, transition zone 2 and grinding from inside to outside, and 3 ring width X of grinding layer is 5- 25mm, transition zone 2 are fluorine silicone rubber, and the width Y of fluorine silicone rubber is 5-25mm, and grinding wheel base body 1 is stainless steel base, grinding wheel total thickness Degree T is 25-100mm, and grinding wheel diameter D is 75-250mm.
Embodiment 2
A kind of preparation method of the grinding wheel applied to the grinding of ceramic insertion core concentricity, includes the following steps:
(1) phenol-formaldehyde resin modified liquid, zirconia hollow microsphere and the calcirm-fluoride 1:20:30 in mass ratio after dilution are added In ethyl acetate, the quality of ethyl acetate is phenol-formaldehyde resin modified liquid, zirconia hollow microsphere and the calcirm-fluoride three after dilution 3 times of total weight, 90 DEG C stirred in water bath 1 hour, the sodium chloride solution of 50wt% is added, and (additional amount of sodium chloride solution is 8 times of phenol-formaldehyde resin modified liquid, zirconia hollow microsphere and calcirm-fluoride three's total weight after dilution), 75 DEG C of heating water baths 90min obtains block mixture, and modified polyamides is added according to block mixture and 1 ︰ 1.5 of modified polyimide resin mass ratio Imide resin, ball milling, cross 1200 mesh screens obtain bonding agent, wherein the phenol-formaldehyde resin modified liquid after the dilution refer to according to The dilution of cresols progress is added into phenol-formaldehyde resin modified for 1:20 mass ratio;
(2) ratio for being 1:3 according to mass ratio by bonding agent obtained by diamond and step (1) that granularity is 100 mesh 120 mesh screens are crossed in weighing, are suppressed in 320 DEG C, 15MPa, and the dwell time is 30 minutes, obtains grinding layer;
(3) grinding layer is adhered on fluorine silicone rubber, fluorine silicone rubber is adhered on grinding wheel base body, obtain grinding wheel half at Product;
(4) unified in order in grinding, guarantee that the concentricity of workpiece and lock pin process continuity and size end to end Property, as shown in Figure 1, the inlet port and outlet port of grinding wheel semi-finished product are carried out chamfering, chamfering degree α is 8 ° -25 °, and length is 2mm-15mm, the grinding wheel are followed successively by 3 layers of grinding wheel base body 1, transition zone 2 and grinding from inside to outside, and 3 ring width X of grinding layer is 5- 25mm, transition zone 2 are fluorine silicone rubber, and the width Y of fluorine silicone rubber is 5-25mm, and grinding wheel base body 1 is stainless steel base, grinding wheel total thickness Degree T is 25-100mm, and grinding wheel diameter D is 75-250mm.
Embodiment 3
A kind of preparation method of the grinding wheel applied to the grinding of ceramic insertion core concentricity, includes the following steps:
(1) phenol-formaldehyde resin modified liquid, zirconia hollow microsphere and the calcirm-fluoride 1:18:32 in mass ratio after dilution are added (quality of ethyl acetate is phenol-formaldehyde resin modified liquid, zirconia hollow microsphere and the fluorine after dilution in mass fraction ethyl acetate Change 8 times of calcium three total weight), 70 DEG C stirred in water bath 2 hours, the sodium chloride solution ((sodium chloride solution of 40wt% is added Additional amount be phenol-formaldehyde resin modified liquid after dilution, 2 times of zirconia hollow microsphere and calcirm-fluoride three's total weight)), 85 DEG C heating water bath 45min, obtains dry block mixture, according to 1 ︰ of block mixture and modified polyimide resin mass ratio 2 are added modified polyimide resin, and ball milling sieves with 100 mesh sieve net and obtains bonding agent, wherein the modified phenolic resin after the dilution Rouge liquid refers to the dilution that cresols progress is added into phenol-formaldehyde resin modified according to 1:20 mass ratio;
It (2) is that bonding agent obtained by 100 mesh diamonds and step (1) claims according to the ratio that mass ratio is 1:8 by granularity Weight crosses 120 mesh screens, suppresses in 360 DEG C, 5MPa, and the dwell time is 80 minutes, obtains grinding layer;
(3) grinding layer is adhered on fluorine silicone rubber, fluorine silicone rubber is adhered on grinding wheel base body, obtain grinding wheel half at Product;
(4) unified in order in grinding, guarantee that the concentricity of workpiece and lock pin process continuity and size end to end Property, as shown in figure 3, the inlet port and outlet port of grinding wheel semi-finished product are carried out chamfering, chamfering degree α is 8 ° -25 °, and length is 2mm-15mm, the grinding wheel are followed successively by 3 layers of grinding wheel base body 1, transition zone 2 and grinding from inside to outside, and 3 ring width X of grinding layer is 5- 25mm, transition zone 2 are fluorine silicone rubber, and the width Y of fluorine silicone rubber is 5-25mm, and grinding wheel base body 1 is stainless steel base, grinding wheel total thickness Degree T is 25-100mm, and grinding wheel diameter D is 75-250mm.
It is tested on single-grain grinding grinding machine with grinding wheel made from embodiment 1, experimental technique parameter and effect are as follows Shown in table 1, workpiece grinding allowance is 0.3mm as shown in Table 1, and the grinding wheel single depth of cut is 0.003mm, and grinding wheel speed is 2600rpm, under conditions of X-direction is 40.00mm/min, gained grinding wheel can be in a finishing period grinding 180 in embodiment 1 The ceramic insertion core of a diameter 2.0mm is ground final concentricity between 0.010-0.025mm, fully meets and is more than this work The concentricity industry processing request of part.Wheel grinding effect made from embodiment 2, embodiment 3 and embodiment 1 are identical.
Table 1
It should be noted last that: technical solution of the present invention that the above embodiments are only illustrative and not limiting is any right The equivalent replacement and do not depart from the modification of spirit and scope of the invention or locally replace that the present invention carries out, should all cover in this hair Within bright protective scope of the claims.

Claims (7)

1. a kind of preparation method of the grinding wheel applied to the grinding of ceramic insertion core concentricity, which comprises the steps of:
(1) phenol-formaldehyde resin modified liquid, zirconia hollow microsphere and the calcirm-fluoride after dilution are added in ethyl acetate, 50 DEG C- 90 DEG C stirring 1-3 hours, sodium chloride solution is added, 75-85 DEG C of heating 45-90min obtains block mixture, and modified gather is added Imide resin, ball milling, sieving obtain bonding agent;
(2) bonding agent obtained by diamond and step (1) is weighed according to the ratio that mass ratio is 1:3-8, sieving, 280 DEG C -360 DEG C, 5MPa-15MPa compacting, dwell time are 30-80 minutes, obtain grinding layer;
(3) grinding layer is adhered on fluorine silicone rubber, fluorine silicone rubber is adhered on grinding wheel base body, obtain grinding wheel semi-finished product;
(4) the inlet port and outlet port of grinding wheel semi-finished product carry out chamfering to get.
2. being applied to the preparation method of the grinding wheel of ceramic insertion core concentricity grinding according to claim 1, which is characterized in that institute State the phenol-formaldehyde resin modified liquid in step (1) after dilution, zirconia hollow microsphere, calcirm-fluoride mass ratio be 1:18 ~ 22:28 ~ 32, the weight of modified polyimide resin is 1.5-2 times of the block mixture weight after drying.
3. being applied to the preparation method of the grinding wheel of ceramic insertion core concentricity grinding according to claim 1, which is characterized in that institute Phenol-formaldehyde resin modified liquid after stating dilution described in step (1) refers to mixed according to the phenol-formaldehyde resin modified and cresols of 1:20 mass ratio The dilution carried out is closed, the concentration of the sodium chloride solution is 40-50wt%, and the additional amount of sodium chloride solution is the modification after dilution 2 ~ 8 times of liquid phenolic resin, zirconia hollow microsphere and calcirm-fluoride gross weight.
4. being applied to the preparation method of the grinding wheel of ceramic insertion core concentricity grinding according to claim 2, which is characterized in that oxygen Changing zirconium tiny balloon partial size is 50 μm -65 μm, and ball wall is broken with a thickness of 5 μm -9 μm;Calcirm-fluoride is that analysis is pure, it is desirable that median particle diameter D50 is 60 μm, and D95 is no more than 100 μm;The partial size of modified polyimide resin powder is 24 μm -48 μm.
5. being applied to the preparation method of the grinding wheel of ceramic insertion core concentricity grinding according to claim 1, which is characterized in that institute State that diamond in step (2) is nickel plating diamond and granularity is -1500 mesh of 100 mesh.
6. utilizing the grinding wheel for being applied to the grinding of ceramic insertion core concentricity made from any preparation method of claim 1 to 5.
7. it is according to claim 6 applied to ceramic insertion core concentricity grinding grinding wheel, which is characterized in that the grinding wheel by Interior to be followed successively by grinding wheel base body, transition zone and grinding layer to outer, grinding layer ring width is 5-25mm, and transition zone is fluorine silicone rubber, fluorine silicon The width of rubber is 5-25mm, and grinding wheel base body is stainless steel base, and grinding wheel overall thickness is 25-100mm, grinding wheel diameter 75- 250mm。
CN201711070211.2A 2017-11-03 2017-11-03 A kind of grinding wheel and preparation method thereof applied to the grinding of ceramic insertion core concentricity Active CN107717765B (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201711070211.2A CN107717765B (en) 2017-11-03 2017-11-03 A kind of grinding wheel and preparation method thereof applied to the grinding of ceramic insertion core concentricity

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201711070211.2A CN107717765B (en) 2017-11-03 2017-11-03 A kind of grinding wheel and preparation method thereof applied to the grinding of ceramic insertion core concentricity

Publications (2)

Publication Number Publication Date
CN107717765A CN107717765A (en) 2018-02-23
CN107717765B true CN107717765B (en) 2019-04-05

Family

ID=61222496

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201711070211.2A Active CN107717765B (en) 2017-11-03 2017-11-03 A kind of grinding wheel and preparation method thereof applied to the grinding of ceramic insertion core concentricity

Country Status (1)

Country Link
CN (1) CN107717765B (en)

Families Citing this family (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108747877B (en) * 2018-06-15 2022-06-14 江苏赛扬精工科技有限责任公司 Self-sharpening hard alloy cutter polishing grinding wheel and preparation method thereof
CN109015425B (en) * 2018-06-26 2019-12-20 郑州磨料磨具磨削研究所有限公司 Resin binder grinding wheel and preparation method thereof
CN113414643A (en) * 2021-06-19 2021-09-21 贵州航箭电子产品有限公司 Grinding method of rectangular electric connector

Citations (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB546697A (en) * 1941-01-24 1942-07-27 A C Wickman Ltd Improvements in or relating to bonded abrasive bodies
EP0433692A2 (en) * 1989-11-23 1991-06-26 Toyoda Koki Kabushiki Kaisha Segmentee grinding wheel
CN1461687A (en) * 2002-05-27 2003-12-17 吴诺顿株式会社 Abrasive wheel for grinding
CN201371422Y (en) * 2008-09-17 2009-12-30 桂林矿产地质研究院 Diamond grinding wheel and grinding equipment using same
CN101693356A (en) * 2009-07-24 2010-04-14 扬中市江南砂布有限公司 High-efficiency extra strength alloy steel moderate grinding abrasive band and detection method thereof
CN102501186A (en) * 2011-11-02 2012-06-20 广东奔朗新材料股份有限公司 Wear-resistant diamond polishing grinder and production method thereof
CN105598833A (en) * 2015-12-31 2016-05-25 厉志安 Novel disc type flexible grinding wheel machining tool

Patent Citations (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB546697A (en) * 1941-01-24 1942-07-27 A C Wickman Ltd Improvements in or relating to bonded abrasive bodies
EP0433692A2 (en) * 1989-11-23 1991-06-26 Toyoda Koki Kabushiki Kaisha Segmentee grinding wheel
CN1461687A (en) * 2002-05-27 2003-12-17 吴诺顿株式会社 Abrasive wheel for grinding
CN201371422Y (en) * 2008-09-17 2009-12-30 桂林矿产地质研究院 Diamond grinding wheel and grinding equipment using same
CN101693356A (en) * 2009-07-24 2010-04-14 扬中市江南砂布有限公司 High-efficiency extra strength alloy steel moderate grinding abrasive band and detection method thereof
CN102501186A (en) * 2011-11-02 2012-06-20 广东奔朗新材料股份有限公司 Wear-resistant diamond polishing grinder and production method thereof
CN105598833A (en) * 2015-12-31 2016-05-25 厉志安 Novel disc type flexible grinding wheel machining tool

Also Published As

Publication number Publication date
CN107717765A (en) 2018-02-23

Similar Documents

Publication Publication Date Title
CN107717765B (en) A kind of grinding wheel and preparation method thereof applied to the grinding of ceramic insertion core concentricity
CN104999365B (en) Sapphire wafer abrasive polishing method
CN104191385B (en) Ferromagnetism diamond abrasive prepared by a kind of wet method
CN105538174B (en) A kind of emery wheel block and preparation method thereof, buffing wheel
CN104985537B (en) A kind of composition metal resin anchoring agent diamond grinding wheel
CZ2004633A3 (en) Porous grinding tool and process for producing thereof
CN108115546B (en) A kind of honing stone and its preparation method and application
CN104290199B (en) Diamond cutting tool with composite structure plating and preparation method thereof
CN105856089A (en) Grinding composite body and preparation method thereof
CN1646267A (en) Metal-coated abrasives, grinding wheel using metal-coated abrasives and method of producing metal-coated abrasives
CN105437091B (en) A kind of stainless steel cross grinding macro pore resin bonding agent extra hard material grinding wheel and preparation method thereof
CN103320775A (en) Magnetic abrasive preparation method
CN104947095B (en) A kind of chemical plating fluid and chemical plating method for preparing nickel plating thorn diamond abrasive grain
CN108747877A (en) A kind of self-sharpening hard alloy cutter buffing wheel and preparation method thereof
CN106753241B (en) Magnetic abrasive and preparation method thereof
CN103991041A (en) Method for preparing ceramic bond CBN grinding wheel with high spherical porosity and ultrafine particle size
CN102218537A (en) Method for manufacturing pre-deformation line diamond line saw through powder metallurgy
CN108789189A (en) A kind of preparation process of brazed multilayer diamond tool
CN109590915A (en) A kind of cymbal type resin wheel and preparation method thereof
CN106737256A (en) A kind of Nano diamond grinding tool pellet preparation method of use wet mixing method
CN107628809A (en) A kind of microcosmic stratiform interlocking nanocrystalline ceramics corundum abrasive and preparation method thereof
CN103529002B (en) The observation procedure of micro-crack and hole in a kind of carbon/carbon compound material
Wang et al. Performance on lapping quartz glass by UV curing fixed abrasive pad with Gr2O3-diamond composite abrasives
CN104760146A (en) Composite fixed abrasive saw line for multi-line cutting and preparation method thereof
CN106891271B (en) A kind of stainless steel cut grinding wheel and preparation method thereof

Legal Events

Date Code Title Description
PB01 Publication
PB01 Publication
SE01 Entry into force of request for substantive examination
SE01 Entry into force of request for substantive examination
GR01 Patent grant
GR01 Patent grant