CN107707674A - The monitoring method and system of a kind of nuclear magnetic resonance chemical analyser - Google Patents
The monitoring method and system of a kind of nuclear magnetic resonance chemical analyser Download PDFInfo
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- CN107707674A CN107707674A CN201711077404.0A CN201711077404A CN107707674A CN 107707674 A CN107707674 A CN 107707674A CN 201711077404 A CN201711077404 A CN 201711077404A CN 107707674 A CN107707674 A CN 107707674A
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- spectrometer
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- H—ELECTRICITY
- H04—ELECTRIC COMMUNICATION TECHNIQUE
- H04L—TRANSMISSION OF DIGITAL INFORMATION, e.g. TELEGRAPHIC COMMUNICATION
- H04L67/00—Network arrangements or protocols for supporting network services or applications
- H04L67/01—Protocols
- H04L67/02—Protocols based on web technology, e.g. hypertext transfer protocol [HTTP]
- H04L67/025—Protocols based on web technology, e.g. hypertext transfer protocol [HTTP] for remote control or remote monitoring of applications
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N24/00—Investigating or analyzing materials by the use of nuclear magnetic resonance, electron paramagnetic resonance or other spin effects
- G01N24/08—Investigating or analyzing materials by the use of nuclear magnetic resonance, electron paramagnetic resonance or other spin effects by using nuclear magnetic resonance
-
- H—ELECTRICITY
- H04—ELECTRIC COMMUNICATION TECHNIQUE
- H04L—TRANSMISSION OF DIGITAL INFORMATION, e.g. TELEGRAPHIC COMMUNICATION
- H04L67/00—Network arrangements or protocols for supporting network services or applications
- H04L67/01—Protocols
-
- H—ELECTRICITY
- H04—ELECTRIC COMMUNICATION TECHNIQUE
- H04L—TRANSMISSION OF DIGITAL INFORMATION, e.g. TELEGRAPHIC COMMUNICATION
- H04L69/00—Network arrangements, protocols or services independent of the application payload and not provided for in the other groups of this subclass
- H04L69/16—Implementation or adaptation of Internet protocol [IP], of transmission control protocol [TCP] or of user datagram protocol [UDP]
- H04L69/163—In-band adaptation of TCP data exchange; In-band control procedures
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- Physics & Mathematics (AREA)
- Signal Processing (AREA)
- Computer Networks & Wireless Communication (AREA)
- High Energy & Nuclear Physics (AREA)
- General Physics & Mathematics (AREA)
- Biochemistry (AREA)
- General Health & Medical Sciences (AREA)
- Analytical Chemistry (AREA)
- Immunology (AREA)
- Pathology (AREA)
- Chemical & Material Sciences (AREA)
- Computer Security & Cryptography (AREA)
- Life Sciences & Earth Sciences (AREA)
- Health & Medical Sciences (AREA)
- Magnetic Resonance Imaging Apparatus (AREA)
Abstract
The monitoring method and system of a kind of nuclear magnetic resonance chemical analyser, first, monitoring host computer connection instrument controlling client obtain spectrometer information data, are uploaded onto the server after being organized into spectrometer state parameter information and experiment parameter information；The information received is stored in database by server according to corresponding relation；Corresponding data is obtained after mobile terminal connection server and authentication.The method and system of the present invention, fully utilize existing network technology resource, solve inconvenience and the inefficiency problem of nuclear magnetic resonance spectrometer acquisition of information, user is set to be in the status information that can in laboratory obtains nuclear magnetic resonance spectrometer, be advantageous to allow user more easily to understand spectrometer situation, reasonability and whole efficiency that spectrometer uses are improved, the difficulty of management is reduced, is easy to spectrometer of controlling risk and safeguard.
Description
Technical field
The present invention relates to nuclear magnetic resonance chemical analyser field, the monitoring method of particularly a kind of nuclear magnetic resonance chemical analyser and it is
System.
Background technology
Nuclear magnetic resonance chemical analyser device is to analyze the analysis of the magnetically of material using the difference of different Elements Atom nulcear properties
Instrument.This instrument is widely used in the structure determination of compound, quantitative analysis and zoological research etc., is technical requirements
Height, strongly professional high-end scientific instrument.It is that user enters to carry out acquisition to nuclear magnetic resonance spectrometer status information or experiment information
A kind of primary demand of traveling wave spectrum experiment.
At present, the Host control software of nuclear magnetic resonance chemical analyser device can realize instrument state information and experiment information
Acquisition, but need to use personnel that main frame is operated and checked at laboratory scene, the acquisition modes of this information are deposited
In obvious not convenient property, it is necessary to which user pays more times and management cost, can not directly understand in remaining place
To spectrometer or the situation of experiment, it is impossible to fully using existing network technology resource, more potential efficiency may be brought
The problems such as low and risk control.
The content of the invention
It is a primary object of the present invention to overcome drawbacks described above of the prior art, proposition is a kind of to improve what spectrometer used
Reasonability and whole efficiency, the difficulty of management is reduced, the monitoring of nuclear magnetic resonance chemical analyser be easy to control risk and safeguarded
Method and system.
The present invention adopts the following technical scheme that：
A kind of monitoring method of nuclear magnetic resonance chemical analyser, it is characterised in that：First, monitoring host computer connection instrument controlling client
End obtains spectrometer information data, is uploaded onto the server after being organized into spectrometer state parameter information and experiment parameter information；Server
The information received is stored in by database according to corresponding relation；Corresponding data is obtained after mobile terminal connection server and authentication.
Preferably, the monitoring host computer is established TCP with the instrument controlling client and is connected, in units of once connecting,
Send communication to wrap and wait the confirmation of the instrument controlling client, if time-out does not confirm, retransmit, until reaching expired times
The upper limit；If confirming, the instrument controlling client actively returns to the communication comprising the spectrometer information data and wrapped to the prison
Control main frame.
Preferably, the monitoring host computer is established HTTP with the server and is connected, by the nuclear magnetic resonance chemical analyser state
Information and experiment information are encoded into string format and are uploaded to the server using URL codings or JSON.
Preferably, the corresponding relation is the unique identifier that the instrument controlling client is pre-set.
Preferably, the spectrometer state parameter information is including the use of person, running situation, rotating speed, temperature, remaining liquid nitrogen water
Flat, remaining liquid helium is horizontal and water lock is put down.
Preferably, the experiment parameter information includes pulse train, sample, solvent, Current Scan number, total scanning time
Number, experimental data path, experiment submission time and scheduled time.
A kind of monitoring system of nuclear magnetic resonance chemical analyser, it is characterised in that：Including
Monitoring host computer, establish and connect with instrument controlling client and server, for sending control command and receiving spectrometer
Information data, and uploaded onto the server after spectrometer information data is organized into spectrometer state parameter information and experiment parameter information；
Instrument controlling client, on nuclear magnetic resonance spectrometer, for receiving control command and sending spectrometer information data；
Server, the spectrometer state parameter information received and experiment parameter information are stored in by data according to corresponding relation
Storehouse；
Mobile terminal, established by connection server and realized far with associating for nuclear magnetic resonance chemical analyser with receiving corresponding data
Range monitoring.
Preferably, the monitoring host computer includes interactive module, communication module and control module, the interactive module and control mould
Block is connected to provide patterned user interface；The communication module is used to send control command and receives spectrometer Information Number
According to；The control module is connected with communication module so that spectrometer information data is organized into spectrometer state parameter information and experiment parameter
After information, uploaded onto the server by communication module.
Preferably, the server, which is provided with, is used to receive the data that the monitoring host computer uploads and is deposited into database
Receiving module and the enquiry module that data query is carried out for providing mobile terminal.
Preferably, the mobile terminal include be used for provide diversified graphic display interface display module, for please
Seek the request module of data needed for obtaining, for operation of the offer to information, modification, deletion, the pipe for auditing user's application information
Manage module and user's registration is provided and applies for the subscription authentication module of the interface function of authority.
From the above-mentioned description of this invention, compared with prior art, the present invention has the advantages that：
The method and system of the present invention, fully using existing network technology resource, solves nuclear magnetic resonance spectrometer information
The inconvenience of acquisition and inefficiency problem, user is set to be in the status information that can in laboratory obtains nuclear magnetic resonance spectrometer,
Be advantageous to allow user more easily to understand spectrometer situation, improve reasonability and whole efficiency that spectrometer uses, reduce management
Difficulty, be easy to spectrometer of controlling risk and safeguard.
Brief description of the drawings
Fig. 1 is present system composition figure；
Fig. 2 is monitoring host computer of the present invention composition figure；
Fig. 3 is mobile terminal module figure of the present invention；
Fig. 4 is the inventive method flow chart；
Wherein：10th, monitoring host computer, 11, interactive module, 12, communication module, 13, control module, 20, NMR spectrum
Instrument, 21, instrument controlling client, 30, server, 31, receiving module, 32, enquiry module, 40, mobile terminal, 41, display mould
Block, 42, request module, 43, information management module, 44, subscription authentication module.
Embodiment
Below by way of embodiment, the invention will be further described.
Referring to figs. 1 to Fig. 4, a kind of monitoring method of nuclear magnetic resonance chemical analyser, comprise the following steps：
S1 monitoring host computers 10 are established TCP with the instrument controlling client 21 of nuclear magnetic resonance chemical analyser 20 and are connected, once to connect
Unit is connected in, communication is sent and wraps and wait the confirmation of instrument controlling client 21, the communication bag includes essential information (such as communication bag
Size and verification and) and real data (such as instrument state sets data and experiment information to set data), if time-out does not confirm,
Then retransmit, if until reaching expired times upper limit confirms that instrument controlling client 21, which actively returns, includes spectrometer information data
Communication wrap to monitoring host computer 10, the spectrometer information data reads from nuclear magnetic resonance chemical analyser 20, and it includes instrument parameter data
Bag and experiment parameter packet etc..
S2 monitoring host computers 10 are established HTTP with server 30 and are connected, and spectrometer state parameter information and experiment parameter information are adopted
String format is encoded into URL codings or JSON, then uploads onto the server 30.The spectrometer state parameter information can include making
User, running situation (idle, tuning, lock field, shimming, experiment, mistake), rotating speed, temperature, remaining liquid helium be horizontal, remaining liquid nitrogen
Level, water lock level values etc., experiment parameter information can include pulse train, sample, solvent, Current Scan number, total scanning time
Number, experimental data path, experiment submission time and scheduled time etc..
S3 servers 30 receive the upload request of monitoring host computer 10, and the information received is stored in into number according to corresponding relation
According to storehouse.The corresponding relation is the unique identifier that instrument controlling client 21 is pre-set.Follow-up step needs user to this
Unique identifier is applied, by the relation that user and nuclear magnetic resonance chemical analyser 20 are established after examination ＆ verification.
Corresponding data is obtained after the connection server 30 of S4 mobile terminals 40 and authentication.User is connected by mobile terminal 40 and taken
Be engaged in device 30, register and apply establishing corresponding relation with the nuclear magnetic resonance spectrometer of required monitoring, after being audited by keeper confirm be
It is no to pass through.The data of the resolution server 30 of mobile terminal 40 return and display, it is remote to the state of nuclear magnetic resonance spectrometer so as to realize
Range monitoring, user only need just obtain desired information without being in laboratory by mobile terminal 40.
Referring to figs. 1 to Fig. 3, a kind of monitoring system of nuclear magnetic resonance chemical analyser, including
Monitoring host computer 10, including interactive module 11, communication module 12 and control module 13, the interactive module 11 and control mould
Block 13 is connected to provide patterned user interface；The communication module 12 is used to establish TCP with instrument controlling client 21
Connection to instrument controlling client 21 to send control command and receives spectrometer information data, and it is established HTTP with server 30 and connected
Connect.The control module 13 is connected with communication module 12 so that spectrometer information data is organized into spectrometer state parameter information and experiment ginseng
After number information, 30 are uploaded onto the server by communication module 12, uploaded format can be by information needed by URL codings or
The character string of JSON codings.
Instrument controlling client 21, in nuclear magnetic resonance spectrometer, for receiving control command and sending spectrometer Information Number
According to.
Server 30, including receiving module 31 and enquiry module 32.The receiving module 31 will receive according to corresponding relation
Spectrometer state parameter information and experiment parameter information deposit database, the corresponding relation can be that instrument controlling client 21 is pre-
The unique identifier first set.The receiving module 31 may include reception spectrometer state parameter information and experiment parameter information, and
Renewal or the routine interface for deleting data.The enquiry module 32 is used to provide the progress data query of mobile terminal 40.The inquiry mould
Block 32 needs the authentication procedure to user, after server 30 receives legitimate request, by spectrometer state parameter information and
Experiment parameter information is returned with general format string, is parsed by mobile terminal 40.Customer volume or data volume compared with
In the case of big, the server architecture of the separation such as data storage server, user's storage server can be used.Server software
Administrator Info's operate interface (such as upload or delete the essential information of spectrometer, tax power is carried out to user) is also provided, intactly
Realize the management function to the condition monitoring of nuclear magnetic resonance chemical analyser 20.
Mobile terminal 40, established by connection server 30 and associated with nuclear magnetic resonance chemical analyser 20 to realize long-range prison
Control.It includes display module 41, request module 42, information management module 43 and subscription authentication module 44 etc..The display module 41
For providing diversified graphic display interface, user is facilitated to check data.The request module 42 is used for for service
The query interface that device 30 provides, carry out HTTP request, data needed for acquisition.The information management module 43 is used to provide keeper couple
The functions such as the operation of device information, modification, deletion, examination ＆ verification user's application.The subscription authentication module 44 is used to provide user's registration
With the interface function of application authority.
For nuclear magnetic resonance spectrometer in the present invention to need monitoring and obtaining the instrument of data, it carries instrument controlling client
21 can realize hardware data signal acquisition.Monitoring host computer 10 is the main frame for being provided with control software, with instrument controlling visitor
Family end 21 carries out TCP communication and obtains information needed data.Mobile terminal 40 can be that the mobile communication such as tablet personal computer, mobile phone is set
It is standby, HTTP can be established with server 30 by communications such as WIFI, 4G, 3G and be connected, mobile terminal 40 can pass through
Register and apply establishing with the nuclear magnetic resonance chemical analyser of required monitoring 20 and associate, there is provided keeper's register function, to spectrum
Instrument information, user profile (including mandate) etc. is operated.
The embodiment of the present invention is above are only, but the design concept of the present invention is not limited thereto, it is all to utilize this
Conceive the change that unsubstantiality is carried out to the present invention, the behavior for invading the scope of the present invention all should be belonged to.
Claims (10)
- A kind of 1. monitoring method of nuclear magnetic resonance chemical analyser, it is characterised in that：First, monitoring host computer connection instrument controlling client Spectrometer information data is obtained, is uploaded onto the server after being organized into spectrometer state parameter information and experiment parameter information；Server root The information received is stored in database according to corresponding relation；Corresponding data is obtained after mobile terminal connection server and authentication.
- A kind of 2. monitoring method of nuclear magnetic resonance chemical analyser as claimed in claim 1, it is characterised in that：The monitoring host computer with The instrument controlling client establishes TCP connections, in units of once connecting, sends communication and wraps and wait the instrument controlling visitor The confirmation at family end, if time-out does not confirm, retransmit, until reaching the expired times upper limit；If confirm, the instrument controlling client End actively returns to the communication comprising the spectrometer information data and wrapped to the monitoring host computer.
- A kind of 3. monitoring method of nuclear magnetic resonance chemical analyser as claimed in claim 1, it is characterised in that：The monitoring host computer with The server establishes HTTP connections, the nuclear magnetic resonance chemical analyser status information and experiment information are encoded using URL or JSON is encoded into string format and is uploaded to the server.
- A kind of 4. monitoring method of nuclear magnetic resonance chemical analyser as claimed in claim 1, it is characterised in that：The corresponding relation is The unique identifier that the instrument controlling client is pre-set.
- A kind of 5. monitoring method of nuclear magnetic resonance chemical analyser as claimed in claim 1, it is characterised in that：The spectrometer state ginseng Number information includes user, running situation, rotating speed, temperature, remaining liquid nitrogen horizontal, remaining liquid helium level and water lock and put down.
- A kind of 6. monitoring method of nuclear magnetic resonance chemical analyser as claimed in claim 1, it is characterised in that：The experiment parameter letter Breath include pulse train, sample, solvent, Current Scan number, total scanning times, experimental data path, test submission time and Scheduled time.
- A kind of 7. monitoring system of nuclear magnetic resonance chemical analyser, it is characterised in that：IncludingMonitoring host computer, establish and connect with instrument controlling client and server, for sending control command and receiving spectrometer information Data, and uploaded onto the server after spectrometer information data is organized into spectrometer state parameter information and experiment parameter information；Instrument controlling client, on nuclear magnetic resonance spectrometer, for receiving control command and sending spectrometer information data；Server, the spectrometer state parameter information received and experiment parameter information are stored in by database according to corresponding relation；Mobile terminal, established by connection server and realize long-range prison with associating for nuclear magnetic resonance chemical analyser to receive corresponding data Control.
- A kind of 8. monitoring system of nuclear magnetic resonance chemical analyser as described in right 7, it is characterised in that：The monitoring host computer includes handing over Mutual module, communication module and control module, the interactive module are connected with control module to provide patterned user interface； The communication module is used to send control command and receives spectrometer information data；The control module is connected with communication module with by spectrometer After information data is organized into spectrometer state parameter information and experiment parameter information, uploaded onto the server by communication module.
- A kind of 9. monitoring system of nuclear magnetic resonance chemical analyser as claimed in claim 7, it is characterised in that：The server is provided with For receiving data that the monitoring host computer uploads and being deposited into the receiving module of database and enter for providing mobile terminal The enquiry module of row data query.
- A kind of 10. monitoring system of nuclear magnetic resonance chemical analyser as claimed in claim 7, it is characterised in that：The mobile terminal Including the display module for providing diversified graphic display interface, the request module for data needed for acquisition request, use In operation of the offer to information, modification, deletion, the management module for auditing user's application information and provide user's registration and applying right The subscription authentication module of the interface function of limit.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
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| CN201711077404.0A CN107707674A (en) | 2017-11-06 | 2017-11-06 | The monitoring method and system of a kind of nuclear magnetic resonance chemical analyser |
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| Application Number | Priority Date | Filing Date | Title |
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| CN201711077404.0A CN107707674A (en) | 2017-11-06 | 2017-11-06 | The monitoring method and system of a kind of nuclear magnetic resonance chemical analyser |
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| CN107707674A true CN107707674A (en) | 2018-02-16 |
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| CN201711077404.0A Pending CN107707674A (en) | 2017-11-06 | 2017-11-06 | The monitoring method and system of a kind of nuclear magnetic resonance chemical analyser |
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108845279A (en) * | 2018-05-03 | 2018-11-20 | 厦门大学 | A kind of permanent magnetism low field miniaturization nuclear magnetic resonance chemical analyser field frequency interlock system and method |
| CN111178209A (en) * | 2019-12-20 | 2020-05-19 | 凯思轩达医疗科技无锡有限公司 | Nuclear magnetic resonance interaction processing method and device and nuclear magnetic resonance interaction system |
| CN114355262A (en) * | 2022-01-10 | 2022-04-15 | 厦门大学 | Integrated coupling system and method for parahydrogen hyperpolarization small nuclear magnetic resonance spectrometer |
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| CN114355262A (en) * | 2022-01-10 | 2022-04-15 | 厦门大学 | Integrated coupling system and method for parahydrogen hyperpolarization small nuclear magnetic resonance spectrometer |
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