CN107699208A - Engine coolant and preparation method thereof - Google Patents
Engine coolant and preparation method thereof Download PDFInfo
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- CN107699208A CN107699208A CN201710227367.0A CN201710227367A CN107699208A CN 107699208 A CN107699208 A CN 107699208A CN 201710227367 A CN201710227367 A CN 201710227367A CN 107699208 A CN107699208 A CN 107699208A
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- engine coolant
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09K—MATERIALS FOR MISCELLANEOUS APPLICATIONS, NOT PROVIDED FOR ELSEWHERE
- C09K5/00—Heat-transfer, heat-exchange or heat-storage materials, e.g. refrigerants; Materials for the production of heat or cold by chemical reactions other than by combustion
- C09K5/20—Antifreeze additives therefor, e.g. for radiator liquids
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Abstract
The invention discloses a kind of engine coolant and preparation method thereof, the component and each component mass percent of engine coolant are as follows：PH adjusting agent：0.5% 3.0%；2 thylhexoic acids：0.3% 2.0%；Sodium benzoate：0.3% 1.0%；Terephthalic acid (TPA)：0.3% 1.0%；Organic ternary carboxylic acid：0.5% 2.0%；BTA：0.1% 0.5%；Antioxidant：0.2% 1.0%；Defoamer：0.001% 0.1%；Pigment：0.001% 0.1%；Surplus is ethylene glycol, amounts to 100%.The present invention has low freezing point, high boiling feature; defoaming effect is good; and use organic carboxyl acid technology; improve its protecting effect to the various metals of engine-cooling system; solves the problems such as silicate-type coolant causes coolant inhibitor reduced capability, scale-preventing performance to weaken because of itself gel polymerisation simultaneously, so as to effectively extend engine and engine coolant service life.
Description
Technical field
The present invention relates to a kind of engine coolant and preparation method thereof.
Background technology
At present, engine coolant of the prior art is using silicate-type coolant, and it is because of itself gel polymerisation
And coolant inhibitor reduced capability, scale-preventing performance is caused to weaken.
The content of the invention
The technical problems to be solved by the invention are the defects of overcoming prior art, there is provided a kind of engine coolant, it
With low freezing point, high boiling feature, defoaming effect is good, and uses organic carboxyl acid technology, improves it to engine cool
The protecting effect of the various metals of system, while solve silicate-type coolant and cause coolant inhibitor because of itself gel polymerisation
The problems such as reduced capability, scale-preventing performance weaken, so as to effectively extend engine and engine coolant service life.
In order to solve the above technical problems, the technical scheme is that：A kind of engine coolant, its component and each
Constituent mass percentage is as follows：
PH adjusting agent：0.5%-3.0%；
2 ethyl hexanoic acid：0.3%-2.0%；
Sodium benzoate：0.3%-1.0%；
Terephthalic acid (TPA)：0.3%-1.0%；
Organic ternary carboxylic acid：0.5%-2.0%；
BTA：0.1%-0.5%；
Antioxidant：0.2%-1.0%；
Defoamer：0.001%-0.1%；
Pigment：0.001%-0.1%；
Surplus is ethylene glycol, amounts to 100%.
Further, its component and each component mass percent are as follows：
PH adjusting agent：1.0%-2.0%；
2 ethyl hexanoic acid：0.5%-1.5%；
Sodium benzoate：0.4%-0.8%；
Terephthalic acid (TPA)：0.4%-0.8%；
Organic ternary carboxylic acid：1.0%-1.5%；
BTA：0.2%-0.4%；
Antioxidant：0.25%-0.5%；
Defoamer：0.005%-0.05%；
Pigment：0.01%-0.08%；
Surplus is ethylene glycol, amounts to 100%.
Further, its component and each component mass percent are as follows：
PH adjusting agent：1.5%；
2 ethyl hexanoic acid：1.0%；
Sodium benzoate：0.5%；
Terephthalic acid (TPA)：0.5%；
Organic ternary carboxylic acid：1.2%；
BTA：0.25%；
Antioxidant：0.3%；
Defoamer：0.01%；
Pigment：0.05%；
Surplus is ethylene glycol, amounts to 100%.
The pH adjusting agent is sodium hydroxide.
Further, the organic ternary carboxylic acid is 2,4,6- tri- (amino caproyl) -1,3,5-triazines.
Further, the pigment is at least one of fluorescein, fluorescein, ZTH red, true yellow, ethereal blue.
Present invention also offers a kind of preparation method of engine coolant, the step of method in contain：
(a) pH adjusting agent is dissolved in appropriate deionized water, solution A is obtained after being sufficiently stirred；
(b) pigment is dissolved in appropriate deionized water, obtains solution B；
(c) by 2 ethyl hexanoic acid, sodium benzoate, terephthalic acid (TPA), organic ternary carboxylic acid, BTA, antioxidant and
Solution A is added in ethylene glycol, and solution C is obtained after being sufficiently stirred；
(d) defoamer and solution B are added in solution C, required engine coolant is obtained after being sufficiently stirred.
Further, in described step (c), solution C is obtained after being sufficiently stirred under 40-50 DEG C of temperature environment.
Further, in described step (c), the time being sufficiently stirred is 30min.
Further, in described step (d), 5~10min is sufficiently stirred at normal temperatures.
After employing above-mentioned technical proposal, engine coolant prepared by the present invention has low freezing point, high boiling feature,
Defoaming effect is good, and uses organic carboxyl acid technology, improves its protecting effect to the various metals of engine-cooling system, together
When solve silicate-type coolant cause because of itself gel polymerisation coolant inhibitor reduced capability, scale-preventing performance weaken etc.
Problem, so as to effectively extend engine and engine coolant service life.
Embodiment
In order that present disclosure is easier to be clearly understood, below according to specific embodiment, the present invention is made into
One step is described in detail.
Embodiment one
A kind of engine coolant, its component and each component mass percent are as follows：
PH adjusting agent：0.5%；
2 ethyl hexanoic acid：0.3%；
Sodium benzoate：0.3%；
Terephthalic acid (TPA)：0.3%；
Organic ternary carboxylic acid：0.5%；
BTA：0.1%；
Antioxidant：0.2%；
Defoamer：0.001%；
Pigment：0.001%；
Surplus is ethylene glycol, amounts to 100%.
The pH adjusting agent is sodium hydroxide.
The organic ternary carboxylic acid is 2,4,6- tri- (amino caproyl) -1,3,5- triazines.
The pigment is the red mixture of fluorescein, fluorescein, ZTH.
Contain in a kind of the step of preparation method of engine coolant：
(a) pH adjusting agent is dissolved in appropriate deionized water, solution A is obtained after being sufficiently stirred；
(b) pigment is dissolved in appropriate deionized water, obtains solution B；
(c) by 2 ethyl hexanoic acid, sodium benzoate, terephthalic acid (TPA), organic ternary carboxylic acid, BTA, antioxidant and
Solution A is added in ethylene glycol, and solution C is obtained after being sufficiently stirred；
(d) defoamer and solution B are added in solution C, required engine coolant is obtained after being sufficiently stirred.
In described step (c), solution C is obtained after being sufficiently stirred under 40-50 DEG C of temperature environment.
In described step (c), the time being sufficiently stirred is 30min.
In described step (d), 5~10min is sufficiently stirred at normal temperatures.
Embodiment two
A kind of engine coolant, its component and each component mass percent are as follows：
PH adjusting agent：3.0%；
2 ethyl hexanoic acid：2.0%；
Sodium benzoate：1.0%；
Terephthalic acid (TPA)：1.0%；
Organic ternary carboxylic acid：2.0%；
BTA：0.5%；
Antioxidant：1.0%；
Defoamer：0.1%；
Pigment：0.1%；
Surplus is ethylene glycol, amounts to 100%.
The pH adjusting agent is sodium hydroxide.
The organic ternary carboxylic acid is 2,4,6- tri- (amino caproyl) -1,3,5- triazines.
The pigment is fluorescein.
Contain in a kind of the step of preparation method of engine coolant：
(a) pH adjusting agent is dissolved in appropriate deionized water, solution A is obtained after being sufficiently stirred；
(b) pigment is dissolved in appropriate deionized water, obtains solution B；
(c) by 2 ethyl hexanoic acid, sodium benzoate, terephthalic acid (TPA), organic ternary carboxylic acid, BTA, antioxidant and
Solution A is added in ethylene glycol, and solution C is obtained after being sufficiently stirred；
(d) defoamer and solution B are added in solution C, required engine coolant is obtained after being sufficiently stirred.
In described step (c), solution C is obtained after being sufficiently stirred under 50 DEG C of temperature environment.
In described step (c), the time being sufficiently stirred is 30min.
In described step (d), 10min is sufficiently stirred at normal temperatures.
Embodiment three
A kind of engine coolant, its component and each component mass percent are as follows：
PH adjusting agent：1.0%%；
2 ethyl hexanoic acid：0.5%；
Sodium benzoate：0.4%；
Terephthalic acid (TPA)：0.4%；
Organic ternary carboxylic acid：1.0%；
BTA：0.2%；
Antioxidant：0.25%；
Defoamer：0.005%；
Pigment：0.01%；
Surplus is ethylene glycol, amounts to 100%.
The organic ternary carboxylic acid is 2,4,6- tri- (amino caproyl) -1,3,5- triazines.
The pigment is that ZTH is red.
Contain in a kind of the step of preparation method of engine coolant：
(a) pH adjusting agent is dissolved in appropriate deionized water, solution A is obtained after being sufficiently stirred；
(b) pigment is dissolved in appropriate deionized water, obtains solution B；
(c) by 2 ethyl hexanoic acid, sodium benzoate, terephthalic acid (TPA), organic ternary carboxylic acid, BTA, antioxidant and
Solution A is added in ethylene glycol, and solution C is obtained after being sufficiently stirred；
(d) defoamer and solution B are added in solution C, required engine coolant is obtained after being sufficiently stirred.
In described step (c), solution C is obtained after being sufficiently stirred under 40 DEG C of temperature environment.
In described step (c), the time being sufficiently stirred is 30min.
In described step (d), 5min is sufficiently stirred at normal temperatures.
Example IV
A kind of engine coolant, its component and each component mass percent are as follows：
PH adjusting agent：2.0%；
2 ethyl hexanoic acid：1.5%；
Sodium benzoate：0.8%；
Terephthalic acid (TPA)：0.8%；
Organic ternary carboxylic acid：1.5%；
BTA：0.4%；
Antioxidant：0.5%；
Defoamer：0.05%；
Pigment：0.08%；
Surplus is ethylene glycol, amounts to 100%.
The organic ternary carboxylic acid is 2,4,6- tri- (amino caproyl) -1,3,5- triazines.
The pigment is fluorescein, the mixture of fluorescein.
Contain in a kind of the step of preparation method of engine coolant：
(a) pH adjusting agent is dissolved in appropriate deionized water, solution A is obtained after being sufficiently stirred；
(b) pigment is dissolved in appropriate deionized water, obtains solution B；
(c) by 2 ethyl hexanoic acid, sodium benzoate, terephthalic acid (TPA), organic ternary carboxylic acid, BTA, antioxidant and
Solution A is added in ethylene glycol, and solution C is obtained after being sufficiently stirred；
(d) defoamer and solution B are added in solution C, required engine coolant is obtained after being sufficiently stirred.
In described step (c), solution C is obtained after being sufficiently stirred under 40-50 DEG C of temperature environment.
In described step (c), the time being sufficiently stirred is 30min.
In described step (d), 8min is sufficiently stirred at normal temperatures.
Embodiment five
A kind of engine coolant, its component and each component mass percent are as follows：
PH adjusting agent：1.5%；
2 ethyl hexanoic acid：1.0%；
Sodium benzoate：0.5%；
Terephthalic acid (TPA)：0.5%；
Organic ternary carboxylic acid：1.2%；
BTA：0.25%；
Antioxidant：0.3%；
Defoamer：0.01%；
Pigment：0.05%；
Surplus is ethylene glycol, amounts to 100%.
The pH adjusting agent is sodium hydroxide.
The organic ternary carboxylic acid is 2,4,6- tri- (amino caproyl) -1,3,5- triazines.
The pigment is true yellow, the mixture of ethereal blue.
Contain in a kind of the step of preparation method of engine coolant：
(a) pH adjusting agent is dissolved in appropriate deionized water, solution A is obtained after being sufficiently stirred；
(b) pigment is dissolved in appropriate deionized water, obtains solution B；
(c) by 2 ethyl hexanoic acid, sodium benzoate, terephthalic acid (TPA), organic ternary carboxylic acid, BTA, antioxidant and
Solution A is added in ethylene glycol, and solution C is obtained after being sufficiently stirred；
(d) defoamer and solution B are added in solution C, required engine coolant is obtained after being sufficiently stirred.
In described step (c), solution C is obtained after being sufficiently stirred under 45 DEG C of temperature environment.
In described step (c), the time being sufficiently stirred is 30min.
In described step (d), 7min is sufficiently stirred at normal temperatures.
Embodiment six
A kind of engine coolant, its component and each component mass percent are as follows：
PH adjusting agent：1.8%；
2 ethyl hexanoic acid：1.2%；
Sodium benzoate：0.6%；
Terephthalic acid (TPA)：0.7%；
Organic ternary carboxylic acid：1.3%；
BTA：0.3%；
Antioxidant：0.6%；
Defoamer：0.05%；
Pigment：0.05%；
Surplus is ethylene glycol, amounts to 100%.
The pH adjusting agent is sodium hydroxide.
The organic ternary carboxylic acid is 2,4,6- tri- (amino caproyl) -1,3,5- triazines.
The pigment is ethereal blue.
Contain in a kind of the step of preparation method of engine coolant：
(a) pH adjusting agent is dissolved in appropriate deionized water, solution A is obtained after being sufficiently stirred；
(b) pigment is dissolved in appropriate deionized water, obtains solution B；
(c) by 2 ethyl hexanoic acid, sodium benzoate, terephthalic acid (TPA), organic ternary carboxylic acid, BTA, antioxidant and
Solution A is added in ethylene glycol, and solution C is obtained after being sufficiently stirred；
(d) defoamer and solution B are added in solution C, required engine coolant is obtained after being sufficiently stirred.
In described step (c), solution C is obtained after being sufficiently stirred under 40-50 DEG C of temperature environment.
In described step (c), the time being sufficiently stirred is 30min.
In described step (d), 5~10min is sufficiently stirred at normal temperatures.
The engine coolant that more than prepared by six embodiments, finds in actual use, and freezing point is relatively low, boiling
Point is higher, and defoaming effect is good, improves its protecting effect to the various metals of engine-cooling system, while solves silicate
Type coolant cause because of itself gel polymerisation coolant inhibitor reduced capability, scale-preventing performance weaken the problems such as, engine and
The service life of engine coolant is extended.
Particular embodiments described above, the technical problems to be solved by the invention, technical scheme and beneficial effect are entered
Further description is gone, should be understood that the specific embodiment that the foregoing is only the present invention, be not used to limit
The system present invention, within the spirit and principles of the invention, any modification, equivalent substitution and improvements done etc., should be included in
Within protection scope of the present invention.
Claims (10)
1. a kind of engine coolant, it is characterised in that its component and each component mass percent is as follows：
PH adjusting agent：0.5%-3.0%；
2 ethyl hexanoic acid：0.3%-2.0%；
Sodium benzoate：0.3%-1.0%；
Terephthalic acid (TPA)：0.3%-1.0%；
Organic ternary carboxylic acid：0.5%-2.0%；
BTA：0.1%-0.5%；
Antioxidant：0.2%-1.0%；
Defoamer：0.001%-0.1%；
Pigment：0.001%-0.1%；
Surplus is ethylene glycol, amounts to 100%.
2. engine coolant according to claim 1, it is characterised in that its component and each component mass percent is such as
Under：
PH adjusting agent：1.0%-2.0%；
2 ethyl hexanoic acid：0.5%-1.5%；
Sodium benzoate：0.4%-0.8%；
Terephthalic acid (TPA)：0.4%-0.8%；
Organic ternary carboxylic acid：1.0%-1.5%；
BTA：0.2%-0.4%；
Antioxidant：0.25%-0.5%；
Defoamer：0.005%-0.05%；
Pigment：0.01%-0.08%；
Surplus is ethylene glycol, amounts to 100%.
3. engine coolant according to claim 1, it is characterised in that its component and each component mass percent is such as
Under：
PH adjusting agent：1.5%；
2 ethyl hexanoic acid：1.0%；
Sodium benzoate：0.5%；
Terephthalic acid (TPA)：0.5%；
Organic ternary carboxylic acid：1.2%；
BTA：0.25%；
Antioxidant：0.3%；
Defoamer：0.01%；
Pigment：0.05%；
Surplus is ethylene glycol, amounts to 100%.
4. engine coolant according to claim 1, it is characterised in that：The pH adjusting agent is sodium hydroxide.
5. engine coolant according to claim 1, it is characterised in that：The organic ternary carboxylic acid is 2,4,6- tri-
(amino caproyl) -1,3,5- triazines.
6. engine coolant according to claim 1, it is characterised in that：The pigment is fluorescein, fluorescein, ZTH
At least one of red, true yellow, ethereal blue.
7. the preparation method of a kind of engine coolant as any one of claim 1 to 6, it is characterised in that method
Contain in step：
(a) pH adjusting agent is dissolved in appropriate deionized water, solution A is obtained after being sufficiently stirred；
(b) pigment is dissolved in appropriate deionized water, obtains solution B；
(c) by 2 ethyl hexanoic acid, sodium benzoate, terephthalic acid (TPA), organic ternary carboxylic acid, BTA, antioxidant and solution A
It is added in ethylene glycol, solution C is obtained after being sufficiently stirred；
(d) defoamer and solution B are added in solution C, required engine coolant is obtained after being sufficiently stirred.
8. preparation method according to claim 7, it is characterised in that：In described step (c), in 40-50 DEG C of temperature
Solution C is obtained after being sufficiently stirred under degree environment.
9. preparation method according to claim 7, it is characterised in that：In described step (c), time for being sufficiently stirred
For 30min.
10. preparation method according to claim 7, it is characterised in that：In described step (d), at normal temperatures fully
Stir 5~10min.
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| Application Number | Priority Date | Filing Date | Title |
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| CN201710227367.0A CN107699208A (en) | 2017-04-10 | 2017-04-10 | Engine coolant and preparation method thereof |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710227367.0A CN107699208A (en) | 2017-04-10 | 2017-04-10 | Engine coolant and preparation method thereof |
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Family
ID=61169504
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109652023A (en) * | 2018-12-29 | 2019-04-19 | 中国船舶重工集团公司第七八研究所 | A kind of solar energy heat conducting medium and preparation method |
| CN111978932A (en) * | 2020-07-09 | 2020-11-24 | 纯牌科技股份有限公司 | Organic corrosion inhibition cooling liquid and preparation method thereof |
| CN112940692A (en) * | 2021-01-25 | 2021-06-11 | 广东石油化工学院 | Thermal management system fluid composition |
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| CN105602533A (en) * | 2015-12-17 | 2016-05-25 | 长春德联化工有限公司 | Good corrosion inhibition engine liquid coolant and preparation method thereof |
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| DE19547499A1 (en) * | 1995-11-10 | 1997-05-15 | Hyundai Motor Co Ltd | Engine coolant composition with low depletion rate |
| RU2182585C2 (en) * | 2000-05-15 | 2002-05-20 | Сахно Николай Витальевич | Cooling liquid |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN109652023A (en) * | 2018-12-29 | 2019-04-19 | 中国船舶重工集团公司第七八研究所 | A kind of solar energy heat conducting medium and preparation method |
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| CN111978932A (en) * | 2020-07-09 | 2020-11-24 | 纯牌科技股份有限公司 | Organic corrosion inhibition cooling liquid and preparation method thereof |
| CN112940692A (en) * | 2021-01-25 | 2021-06-11 | 广东石油化工学院 | Thermal management system fluid composition |
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Application publication date: 20180216 |