CN107669705A - A kind of Colla Corii Asini bead and preparation method thereof - Google Patents
A kind of Colla Corii Asini bead and preparation method thereof Download PDFInfo
- Publication number
- CN107669705A CN107669705A CN201710918808.1A CN201710918808A CN107669705A CN 107669705 A CN107669705 A CN 107669705A CN 201710918808 A CN201710918808 A CN 201710918808A CN 107669705 A CN107669705 A CN 107669705A
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- Prior art keywords
- donkey
- corii asini
- colla corii
- hide gelatin
- asini bead
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K35/00—Medicinal preparations containing materials or reaction products thereof with undetermined constitution
- A61K35/12—Materials from mammals; Compositions comprising non-specified tissues or cells; Compositions comprising non-embryonic stem cells; Genetically modified cells
- A61K35/36—Skin; Hair; Nails; Sebaceous glands; Cerumen; Epidermis; Epithelial cells; Keratinocytes; Langerhans cells; Ectodermal cells
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K35/00—Medicinal preparations containing materials or reaction products thereof with undetermined constitution
- A61K35/56—Materials from animals other than mammals
- A61K35/618—Molluscs, e.g. fresh-water molluscs, oysters, clams, squids, octopus, cuttlefish, snails or slugs
Abstract
The invention provides a kind of Colla Corii Asini bead and preparation method thereof, preparation method of the present invention is that donkey-hide gelatin block will be allowed fully to be heated to soften and then make 0.4-0.6mm particle；Then in dehumidifying, sterilizing drying to 13% moisture content；By the clam meal after dehumidifying, sterilizing and Colla Corii Asini bead particle 1:2 ratio is well mixed, and is heated to 90 110 DEG C afterwards, donkey-hide gelatin granule is sufficiently mixed thermally equivalent with clam meal, is become 1.0 1.5mm pearl after donkey-hide gelatin granule expanded by heating, weed out irregular Colla Corii Asini bead and clam meal, receive to obtain Colla Corii Asini bead.Colla Corii Asini bead particle produced by the present invention is smaller, purity is higher, effect is more preferable, mouthfeel is more comfortable, does not glue clam meal substantially, while overall process uses production line balance, improves production efficiency.
Description
Technical field
The present invention relates to a kind of prepared slices of Chinese crude drugs technical field, and in particular to the preparation technology of prepared slices of Chinese crude drugs Colla Corii Asini bead.
Technical background
The method of conventionally produced " Colla Corii Asini bead ", according to the Pharmacopoeia of People's Republic of China 2015 edition rule of page 176
Fixed, the production of the prepared slices of Chinese crude drugs " Colla Corii Asini bead " is to take donkey-hide gelatin softened by baking, is cut into 1cm or so fourth, scalds beading with clam meal, during the interior sugar-free heart
Take out, weed out clam meal, cool.This product is in spherical, surface brown color or canescence, and with white powder, body is light, matter is crisp, disconnected
Face is hollow or cellular, and faint yellow to brown, gas is micro-, the micro- sweet tea of taste, and moisture content must not cross 10.0% with medicinal material, total ash with medicinal material not
4.0% must be crossed.Following defect be present in the Colla Corii Asini bead produced using the methods and techniques in pharmacopeia：1st, Colla Corii Asini bead particle is larger, grain
Footpath is typically in 6-7mm, and because Colla Corii Asini bead particle diameter is larger, so the clam meal being bonded on Colla Corii Asini bead is on the high side, the purity of Colla Corii Asini bead is natural
It can be affected, assimilation effect is poor when people take.2nd, the clam meal being bonded on Colla Corii Asini bead is on the high side, and particle is thicker.People exist
May feel that when taking in the container for brew Colla Corii Asini bead has many deep, and mouthfeel is poor when taking, and causes people to receive journey to it
Degree is limited.3rd, the clam meal on Colla Corii Asini bead is more, and particle more slightly cause product design unsightly, shade deviation, be unfavorable for packing.4、
Traditional Colla Corii Asini bead is substantially that manual method makes, and every pot can only fry 200-300g, produce the amount of being not easy.
In order to solve the above problems, China Patent No. is：201210147945.7 patent of invention just propose a kind of donkey-hide gelatin
Pearl and preparation method thereof, mainly there are following steps：1) clam meal is placed in machine for stir-frying Chinese medicine and is heated to 120-125 DEG C, it is then natural
Be cooled to 70-120 DEG C it is standby；2) donkey-hide gelatin block is embedded in and made popular in standby clam meal 5-10 minutes, make donkey-hide gelatin block fully heated
Soften；3) the donkey-hide gelatin block of heated softening is placed on stress on machine, latticed or eye donkey-hide gelatin block is formed, then by net
The donkey-hide gelatin block of trellis or eye, which is positioned in container, allows its natural cooling to be hardened, and the donkey-hide gelatin block after being hardened is put into granulator
It is interior, granulator is rotated, latticed or eye donkey-hide gelatin block is worn into particle in machine；4）Clam meal is beaten carefully, is heated to
120-125 DEG C, be cooled to 20-50 DEG C it is standby；5) clam meal after cooling and standby donkey-hide gelatin granule are pressed 1:3-5 ratio is mixed
Close uniformly, be placed in containers for future use；6) heater is opened, is heated to 70-100 DEG C, the donkey-hide gelatin granule mixed and clam meal is slow
Slowly it is placed in funnel, Colla Corii Asini bead particle and clam meal is sufficiently mixed thermally equivalent, become 1.5- after the expansion of Colla Corii Asini bead particles by heat
2mm pearl, weeds out clam meal, receives to obtain Colla Corii Asini bead, completes the preparation process of Colla Corii Asini bead.
Found in actual production process, if heating process clam meal is meticulous, clam meal can mist formation in a device, so as to escape
Go out equipment, whole workshop diffuses dust, influences plant personnel health and environmental protection；The inequality if clam meal can conduct heat when excessively thick
It is even, the heated deficiency of donkey-hide gelatin block is caused, influences the quality of donkey-hide gelatin block.Secondly the production technology is by donkey-hide gelatin block when heating donkey-hide gelatin block
It is embedded in clam meal, when 70-90 DEG C of clam meal temperature, is not easy to soften donkey-hide gelatin block because temperature is too low, when temperature is at 110-120 DEG C
Shi Wendu is too high easily to make donkey-hide gelatin block be carbonized, hence in so that the control in actual mechanical process to temperature is very strict so that behaviour
Make difficulty raising.All used manually using the operation being embedded in donkey-hide gelatin block in clam meal simultaneously, although the output increased of single,
It is or the batch production of continuous-flow type can not be realized, therefore production efficiency is low.
The content of the invention
The problem to be solved in the present invention aiming at more than deficiency and provide a kind of particle is smaller, purity is higher, effect more
Well, mouthfeel is more comfortable, the Colla Corii Asini bead of substantially not viscous clam meal, and its preparation method.Its technical scheme is as follows：
A kind of preparation method of Colla Corii Asini bead is as follows：
1）The clam meal of 60 mesh to 70 mesh is placed in machine for stir-frying Chinese medicine and is heated to 100-110 DEG C, appropriate donkey-hide gelatin block is then put into, allows
Donkey-hide gelatin block is fully heated to soften；
2）After the donkey-hide gelatin block of heated softening is separated with clam meal, put into equipment, make 0.4-0.6mm particle；
3) clam meal is beaten carefully at least 120 mesh, the thinner mouthfeel to Colla Corii Asini bead is better, when clam meal mesh number occurs less than 120
Puckery mouth, knocks the bad mouthfeel such as tooth, in dehumidifying, sterilizing drying to 13% moisture content；
4）By the clam meal after dehumidifying, sterilizing and Colla Corii Asini bead particle 1:2 ratio is well mixed（The too low Colla Corii Asini bead of ratio is inter-adhesive
Into cake, the too high dust that produces of ratio influences operation, environmental protection）, insert containers for future use；
5）Microwave sterilization heater is opened, is heated to 90-110 DEG C, the donkey-hide gelatin granule mixed and clam meal are placed into flowing water makees
The specialty of industry, which is fried, processs in the microwave machine for stir-frying Chinese medicine of Colla Corii Asini bead, donkey-hide gelatin granule and clam meal is sufficiently mixed thermally equivalent, donkey-hide gelatin granule by
Become 1.0-1.5mm pearl after thermal expansion, weed out irregular Colla Corii Asini bead and clam meal, receive to obtain Colla Corii Asini bead, complete the system of Colla Corii Asini bead
Standby process.
Further optimal technical scheme is in the present invention：Step 1）Described in heating-up temperature be 105 DEG C；Step 2）Middle institute
It is 0.5mm to state particle diameter.
Compared with prior art, the invention has the advantages that：
1st, this inventive method first allows donkey-hide gelatin block fully to be become by heat on the premise of raw material donkey-hide gelatin block, auxiliary material clam meal are all constant
It is soft, then by the donkey-hide gelatin block used device of heated softening, make 0.5mm particle, then donkey-hide gelatin block is pelletized again, passed through
" Colla Corii Asini bead " of modernization process output, particle diameter 1.0-1.5mm smaller compared with traditional handicraft Colla Corii Asini bead particle can be fully when being heated
Expanded, water content is reduced between 4.0-6.0%, and purity is higher, while realizes the production of streamlined, improves production efficiency, drop
Low cost of labor.
2nd, product particle of the present invention is smaller, particle diameter 1.0-1.5mm, its substantially not viscous clam meal and ashes, in spherical, table
Face brown color, body are light, matter is crisp, frangible, surface mesoporous or cellular, and mouthfeel is more comfortable, are so more conducive to people and take, are easy to inhale
Receive, effect is more preferable.
3rd, it is industrial production to change manual production, and pollution is reduced, and quality is secure, and product is easy to upper amount, has good warp
Ji value and social value.
4th, the substantially not viscous clam meal of product of the present invention and ashes, good appearance, color is bright, more conducively packs.
5th, the present invention is not required to donkey-hide gelatin block being manually embedded in clam meal, so as to realize that streamlined produces, improves production efficiency, subtracts
It is few artificial, cost-effective.
6th, clam meal is beaten carefully to 60-70 mesh in this hair, powder is formed in heating process if just avoiding crossing detailed rules and regulations
Mist, while reduce heating-up temperature, excessively it is thick then can uneven heating also improve heating-up temperature simultaneously and cause energy waste.
Embodiment
Technical scheme is described further with reference to embodiment, but the present invention is not limited in following reality
Apply example.
Embodiment one
The present embodiment Colla Corii Asini bead, is made according to the following steps：
1）The clam meal of 60 mesh to 70 mesh is placed in machine for stir-frying Chinese medicine and heats 100 DEG C, allows its leading high-temperature sterilization to sterilize；Then input is suitable
The donkey-hide gelatin block of amount, allow donkey-hide gelatin block is fully heated after being mixed with clam meal to soften.
2) the donkey-hide gelatin block of heated softening is separated with clam meal, donkey-hide gelatin block is then placed on stress on machine, form grid
Shape donkey-hide gelatin block, each sizing grid 2-3mm, grid donkey-hide gelatin block thickness 1-2mm, then latticed donkey-hide gelatin block is placed in container and allowed
Its natural cooling is hardened, and the donkey-hide gelatin block after being hardened is put into granulator, is rotated granulator, is made latticed donkey-hide gelatin block in machine
0.5-1.0mm particle is worn into, is then rolled out automatically out of machine, takes in containers for future use., will be by when making latticed donkey-hide gelatin block
The soft donkey-hide gelatin block of thermal change is placed on the machine with gear or rack, allows its heated donkey-hide gelatin block to soften by gear or rack, this
When donkey-hide gelatin block on form strip impression, the donkey-hide gelatin block with strip impression is then changed into direction by gear or rack again, this
When donkey-hide gelatin block on form grid；
3) clam meal is beaten carefully to 120 mesh, the thinner mouthfeel to Colla Corii Asini bead is better, when clam meal mesh number occur less than 120 it is puckery
Mouthful, the bad mouthfeel such as tooth is knocked, in dehumidifying, sterilizing drying to 13% moisture content；
4）By the clam meal after dehumidifying, sterilizing and step 2）In obtained donkey-hide gelatin granule 1:2 ratio is well mixed（Ratio too low Ah
Glue bead is inter-adhesive to influence operation, environmental protection into cake, the too high dust that produces of ratio）, insert containers for future use；
5) microwave sterilization heater is opened, is heated to 90 DEG C, the donkey-hide gelatin granule mixed and clam meal are placed into continuous productive process
Specialty is fried in the microwave machine for stir-frying Chinese medicine for processing Colla Corii Asini bead, donkey-hide gelatin granule is sufficiently mixed thermally equivalent with clam meal, donkey-hide gelatin granule is heated swollen
Size becomes 1.0-1.5mm pearl after swollen, is observed by peep hole, after largely pearl is formed, slowly allows it to roll out, weeds out not
The Colla Corii Asini bead and clam meal of rule, must to meet NF standard be in class ball-type so as to receiving, and surface brown color, body are light, matter is crisp, easy
Broken, surface mesoporous or cavernous Colla Corii Asini bead.
Embodiment two：
This implementation Colla Corii Asini bead, is made according to the following steps：
1) clam meal of 60 mesh to 70 mesh is placed in machine for stir-frying Chinese medicine and is heated to 110 DEG C, allow its leading high-temperature sterilization to sterilize；Then put into
Appropriate donkey-hide gelatin block, allow donkey-hide gelatin block is fully heated after being mixed with clam meal to soften.
2) the donkey-hide gelatin block of heated softening is separated with clam meal, donkey-hide gelatin block is then placed on stress on machine, form grid
Shape donkey-hide gelatin block, each sizing grid 2-3mm, latticed donkey-hide gelatin block thickness 1-2mm, then latticed donkey-hide gelatin block is placed in container
Its natural cooling is allowed to be hardened, the donkey-hide gelatin block after being hardened is put into granulator, is rotated granulator, is made latticed donkey-hide gelatin block in machine
0.4-0.6mm particle is inside worn into, is then rolled out automatically out of machine, takes in containers for future use；When making latticed donkey-hide gelatin block,
Latticed mould is installed on machine, the donkey-hide gelatin block of heated softening is placed in punching press on mould, formed on donkey-hide gelatin block latticed；
3) clam meal is beaten carefully to 130 mesh, is heated to 110 DEG C, allow its leading high-temperature sterilization sterilization, and removal moisture drying is within 13%
Moisture content；
4) by the clam meal after cooling and step 2）In get out standby donkey-hide gelatin granule by 0.5:1 ratio is well mixed, and is inserted
Containers for future use；
5) microwave sterilization heater is opened, is heated to 110 DEG C, the donkey-hide gelatin granule mixed and clam meal are placed into continuous productive process
Specialty fry and process in the microwave machine for stir-frying Chinese medicine of Colla Corii Asini bead, donkey-hide gelatin granule is sufficiently mixed thermally equivalent with clam meal, donkey-hide gelatin granule is heated
Size becomes 1.0-1.5mm pearl after expansion, is observed by peep hole, after largely pearl is formed, slowly allows it to roll out, weeds out
Irregular Colla Corii Asini bead and clam meal, must to meet NF standard be in class ball-type so as to receiving, and surface brown color, body are light, matter is crisp, easy
Broken, surface mesoporous or cavernous Colla Corii Asini bead.
Embodiment three：
The present embodiment Colla Corii Asini bead, is made according to the following steps：
1) clam meal of 60 mesh to 70 mesh is placed in machine for stir-frying Chinese medicine and is heated to 105 DEG C, allow its leading high-temperature sterilization to sterilize；Then put into
Appropriate donkey-hide gelatin block, allow donkey-hide gelatin block is fully heated after being mixed with clam meal to soften.
2) the donkey-hide gelatin block of heated softening is separated with clam meal, donkey-hide gelatin block is then placed on stress on machine, form grid
Shape donkey-hide gelatin block, each sizing grid 2-3mm, latticed donkey-hide gelatin block thickness 1-2mm, then latticed donkey-hide gelatin block is placed in container
Its natural cooling is allowed to be hardened, the donkey-hide gelatin block after being hardened is put into granulator, is rotated granulator, is made latticed donkey-hide gelatin block in machine
0.5-0.6mm particle is inside worn into, is then rolled out automatically out of machine, takes in containers for future use；When making latticed donkey-hide gelatin block,
Latticed mould is installed on machine, the donkey-hide gelatin block of heated softening is placed in punching press on mould, formed on donkey-hide gelatin block latticed；
3) clam meal is beaten carefully to 125 mesh, is heated to 110 DEG C, allow its leading high-temp sterilizing；And dry to 13% moisture.
4）By the clam meal after cooling and step 2）In obtained donkey-hide gelatin granule by 0.5:1 ratio is well mixed, and inserts appearance
It is standby in device；
5) microwave sterilization heater is opened, is heated to 90-120 DEG C, the donkey-hide gelatin granule mixed and clam meal are placed into flowing water makees
The specialty of industry, which is fried, processs in the microwave machine for stir-frying Chinese medicine of Colla Corii Asini bead, donkey-hide gelatin granule and clam meal is sufficiently mixed thermally equivalent, donkey-hide gelatin granule by
Become 1.0-1.5mm pearl after thermal expansion, observed by peep hole, after largely pearl is formed, slowly allow it to roll out, weed out not
The Colla Corii Asini bead and clam meal of rule, must to meet NF standard be in class ball-type so as to receiving, and surface brown color, body are light, matter is crisp, easy
Broken, surface mesoporous or cavernous Colla Corii Asini bead.
Claims (4)
1. a kind of preparation method of Colla Corii Asini bead, it is characterised in that this method comprises the following steps：
1）The clam meal of 60 mesh to 70 mesh is placed in machine for stir-frying Chinese medicine and is heated to 100-110 DEG C, appropriate donkey-hide gelatin block is then put into, allows
Donkey-hide gelatin block is fully heated to soften；
2）After the donkey-hide gelatin block of heated softening is separated with clam meal, put into equipment, make 0.4mm -0.6mm particle；
3) clam meal is beaten carefully at least 120 mesh, in dehumidifying, sterilizing drying to 13% moisture content；
4）By the clam meal after dehumidifying, sterilizing and Colla Corii Asini bead particle 1:2 ratio is well mixed, and inserts containers for future use；
5）Microwave sterilization heater is opened, is heated to 90-110 DEG C, the donkey-hide gelatin granule mixed and clam meal are placed into flowing water makees
The specialty of industry, which is fried, processs in the microwave machine for stir-frying Chinese medicine of Colla Corii Asini bead, donkey-hide gelatin granule and clam meal is sufficiently mixed thermally equivalent, donkey-hide gelatin granule by
Become 1.0-1.5mm pearl after thermal expansion, weed out irregular Colla Corii Asini bead and clam meal, receive to obtain Colla Corii Asini bead.
A kind of 2. preparation method of Colla Corii Asini bead according to claim 1, it is characterised in that step 1）Described in heating-up temperature
For 105 DEG C.
A kind of 3. preparation method of Colla Corii Asini bead according to claim 1, it is characterised in that step 2）Described in particle diameter
For 0.5mm.
A kind of 4. Colla Corii Asini bead, it is characterised in that：The Colla Corii Asini bead is made using the method described in any one of claim 1-3.
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| CN201710918808.1A CN107669705B (en) | 2017-09-30 | 2017-09-30 | Donkey-hide gelatin beads and preparation method thereof |
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Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108578234A (en) * | 2018-04-19 | 2018-09-28 | 四川御致药业有限公司 | A kind of Colla Corii Asini bead bulking equipment and technique |
| CN110448573A (en) * | 2019-07-18 | 2019-11-15 | 山东东阿国胶堂阿胶药业有限公司 | A kind of Colla Corii Asini bead processing unit (plant) and Colla Corii Asini bead processing technology is processed using the device |
| CN111714518A (en) * | 2020-08-13 | 2020-09-29 | 贵州苗立克中药科技有限公司 | Preparation method of donkey-hide gelatin beads and donkey-hide gelatin beads prepared by method |
| CN112956533A (en) * | 2021-03-24 | 2021-06-15 | 重庆海王生物工程有限公司 | Donkey-hide gelatin milk tea and preparation process thereof |
| CN113632915A (en) * | 2021-08-10 | 2021-11-12 | 安徽盛安堂药业有限公司 | Stir-frying process for donkey-hide gelatin beads |
| CN114948999A (en) * | 2022-04-25 | 2022-08-30 | 广州至信药业股份有限公司 | Preparation method of donkey-hide gelatin beads |
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Cited By (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108578234A (en) * | 2018-04-19 | 2018-09-28 | 四川御致药业有限公司 | A kind of Colla Corii Asini bead bulking equipment and technique |
| CN110448573A (en) * | 2019-07-18 | 2019-11-15 | 山东东阿国胶堂阿胶药业有限公司 | A kind of Colla Corii Asini bead processing unit (plant) and Colla Corii Asini bead processing technology is processed using the device |
| CN111714518A (en) * | 2020-08-13 | 2020-09-29 | 贵州苗立克中药科技有限公司 | Preparation method of donkey-hide gelatin beads and donkey-hide gelatin beads prepared by method |
| CN111714518B (en) * | 2020-08-13 | 2023-06-16 | 贵州苗立克中药科技有限公司 | Preparation method of donkey-hide gelatin beads and donkey-hide gelatin beads prepared by method |
| CN112956533A (en) * | 2021-03-24 | 2021-06-15 | 重庆海王生物工程有限公司 | Donkey-hide gelatin milk tea and preparation process thereof |
| CN113632915A (en) * | 2021-08-10 | 2021-11-12 | 安徽盛安堂药业有限公司 | Stir-frying process for donkey-hide gelatin beads |
| CN114948999A (en) * | 2022-04-25 | 2022-08-30 | 广州至信药业股份有限公司 | Preparation method of donkey-hide gelatin beads |
| CN114948999B (en) * | 2022-04-25 | 2023-12-12 | 广州至信药业股份有限公司 | Preparation method of donkey-hide gelatin beads |
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