CN107663669A - A kind of fragrant artificial lawn fiber and preparation method thereof - Google Patents
A kind of fragrant artificial lawn fiber and preparation method thereof Download PDFInfo
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- CN107663669A CN107663669A CN201610621894.5A CN201610621894A CN107663669A CN 107663669 A CN107663669 A CN 107663669A CN 201610621894 A CN201610621894 A CN 201610621894A CN 107663669 A CN107663669 A CN 107663669A
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- Prior art keywords
- essence
- artificial lawn
- preparation
- lawn fiber
- fragrant artificial
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Classifications
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J13/00—Colloid chemistry, e.g. the production of colloidal materials or their solutions, not otherwise provided for; Making microcapsules or microballoons
- B01J13/02—Making microcapsules or microballoons
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
-
- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
- D01F1/00—General methods for the manufacture of artificial filaments or the like
- D01F1/02—Addition of substances to the spinning solution or to the melt
- D01F1/10—Other agents for modifying properties
-
- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
- D01F6/00—Monocomponent artificial filaments or the like of synthetic polymers; Manufacture thereof
- D01F6/44—Monocomponent artificial filaments or the like of synthetic polymers; Manufacture thereof from mixtures of polymers obtained by reactions only involving carbon-to-carbon unsaturated bonds as major constituent with other polymers or low-molecular-weight compounds
- D01F6/46—Monocomponent artificial filaments or the like of synthetic polymers; Manufacture thereof from mixtures of polymers obtained by reactions only involving carbon-to-carbon unsaturated bonds as major constituent with other polymers or low-molecular-weight compounds of polyolefins
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- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Engineering & Computer Science (AREA)
- Organic Chemistry (AREA)
- General Chemical & Material Sciences (AREA)
- Textile Engineering (AREA)
- Dispersion Chemistry (AREA)
- Manufacturing & Machinery (AREA)
- Life Sciences & Earth Sciences (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Manufacturing Of Micro-Capsules (AREA)
Abstract
The present invention relates to a kind of chinampa manufacturing technology, specifically a kind of fragrant artificial lawn fiber and preparation method thereof.The present invention is made up of essence microcapsule, matrix resin, Masterbatch and auxiliary agent, and its component formed by mass percentage is matrix resin：70~95%, Masterbatch：1~25%, essence microcapsule：0.1~10%, auxiliary agent：0.1~10%, described essence microcapsule is made up of essence, emulsifying agent and wall material, and its component formed by mass percentage is：Wall material：30~80%, essence：10~60%, emulsifying agent：0.01~10%；Preparation method is：After being prepared into essence microcapsule by single or multiple lift wall building method, blending method is recycled to be prepared into fragrant artificial lawn fiber, blending method preparation method includes two steps：Step 1: the preparation of essence microcapsule；Step 2: the preparation of fragrant artificial lawn fiber.
Description
【Technical field】
The present invention relates to chinampa manufacturing technology field, is a kind of fragrant artificial lawn fiber and its system specifically
Preparation Method.
【Background technology】
For various reasons, people like moving and lying fallow on lawn, and due to being influenceed by ecological environment, natural grass
Utilization have significant limitation, use cost is also very high, safeguard it is difficult；Therefore, artificial motion lawn is utilized as
People are of interest.Artificial motion lawn is manufactured using bionics principle, has good simulation quality, its exercise performance, elasticity, pin
Sense, the ball rebound velocity etc. of ball are similar to natural lawn, and influenceed by environment, weather, region it is very small, can it is high and cold,
The extreme climates such as high temperature, plateau area uses.The sixties in last century, European and American developed countries, which have begun to athletic ground indoors, to be made
With artificial motion lawn, by the development of more than 30 years, at present, artificial motion lawn was widely used to various sports places
And Condom.Have been reported that, International Football Union on South Africa world cup in 2010 it is determined that use artificial motion lawn, this decision
Popularization and application that can be to artificial motion lawn are certain to play very big facilitation.
Counting and predict according to authoritative department, the usage amount on the artificial motion lawn in the whole world has reached 200,000,000 square metres at present,
The sports field for having more than 1000 pieces is mated formation artificial motion lawn every year from now on, this numeral does not include also more nonstandard
Quasi- place and Condom, therefore, the application on artificial motion lawn have formd a huge market.
In the manufacture on artificial motion lawn, artificial lawn fiber is its core material, and the performance of artificial lawn fiber is determined
Sport dynamics performance, security performance and the comfort property on motion lawn are determined.From the point of view of the situation of the Searches of Patent Literature, people at present
The research for making motion lawn has focused largely on artificial grass filaments profile --- such as United States Patent (USP) USP 5462778, weaves, the side of mating formation
Method --- such as United States Patent (USP) USP 4381805, USP 6491991, USP 6815059, USP 6955841, performance testing apparatus
--- in United States Patent (USP) USP 6854316, USP 6962073 and preparation technology --- is designed such as European patent EP
1672020, the research to artificial motion lawn material is also few, and the research of the artificial lawn fiber with fragrant breath yet there are no
Report.
Microcapsules technology is that solid, liquid or gaseous matter are wrapped in capsule by one kind using filmogen, forms one
The technology of the individual several microns of small containers to millimeter of diameter, microcapsules have protection something which is in the bag matter exempt from it is influenced by environmental conditions,
The effect of taste, color and smell is shielded, toxicity can be reduced, changes the property or performance of material, extends volatile materials storage
Time, sustained release enter extraneous, function of also isolating immiscible compound etc..At present, microcapsules technology is extensive
Applied to multiple fields such as biological medicine, food, coating, ink, textile, cosmetics, farming and animal husbandries.
【The content of the invention】
It is an object of the invention to overcome the shortcomings of existing artificial motion lawn, there is provided one kind is developed using microcapsules technology
, the fragrant artificial lawn fiber on the artificial motion lawn of manufacture, to meet the needs of market is to simulating sports lawn；The present invention's
Another purpose is to provide a kind of preparation method of described fragrant artificial lawn fiber；Another object of the present invention is to propose
Application of the microcapsules technology in fragrant artificial lawn fiber preparation.
To realize object above, the present invention is achieved through the following technical solutions：
A kind of fragrant artificial lawn fiber, it is made up of essence microcapsule, matrix resin, Masterbatch and auxiliary agent, it presses quality
Percentage form component be：
Matrix resin：70~95%
Masterbatch：1~25%
Essence microcapsule：0.1~10%
Auxiliary agent：0.1~10%
Described essence microcapsule is made up of essence, emulsifying agent and wall material, and its component formed by mass percentage is：
Wall material：30~80%
Essence：10~60%
Emulsifying agent：0.01~10%
It is described composition essence microcapsule wall material for amino resins, epoxy resin, Lauxite, polyurethane, gelatin, I
One or more in uncle's natural gum, styrene maleic anhydride copolymer, cyclodextrin；The essence of the composition essence microcapsule is grass
Any one in odor type, rose scent, Forest Bath odor type, jasmine fragrance, lavender flavor type, fruit flavouring；The composition is fragrant
The emulsifying agent of precise and tiny capsule is neopelex, polyoxyethylene sorbitan fatty acid ester, Sorbitan alcohol ester
One or more in fat acid esters, acrylic homopolymer or copolymer, maleic acid anhydride homopolymer or copolymer.
Described matrix resin is TPO.
Described auxiliary agent is one kind in processing aid and light stabilizer, antioxidant, antistatic additive, dispersant, plasticizer
It is or several.
To realize above goal of the invention, a kind of preparation method of fragrant artificial lawn fiber of the present invention is：By individual layer or
After multilayer wall building method is prepared into essence microcapsule, recycle blending method to be prepared into fragrant artificial lawn fiber, legal system is blended
Preparation Method includes two steps：Step 1: the preparation of essence microcapsule；Step 2: the preparation of fragrant artificial lawn fiber；It has
Body preparation section is：
Step 1
(1) it is emulsified into essence breast in high-speed emulsifying machine effect after mixing essence, emulsifying agent and water according to a certain percentage
Liquid, its component formed by mass percentage are：Wall material be 30~80%, essence be 10~60%, emulsifying agent be 0.01~
10%；
(2) and then essence emulsion is wrapped in wall material using single or multiple lift wall building method and prepares essence microcapsule, its shape
State is spherical, and particle diameter is 0.1~100 μm；
(3) emulsified at a high speed as 100~20000 revs/min using rotating speed in high-speed emulsifying machine and prepare within 1~100 minute essence breast
Liquid；
(4) essence microcapsule and by single or multiple lift wall building method according to following condition is prepared, reaction temperature is 10~90
DEG C, pH value is 1~6,0.1~100 hour time；
Step 2
The blending extrusions such as essence microcapsule, matrix resin, Masterbatch and auxiliary agent are molded so as to prepare fragrant artificial lawn
Fiber, its component formed by mass percentage are：Matrix resin is 70~95%, and Masterbatch is 1~25%, essence microcapsule
For 0.1~10%, auxiliary agent is 0.1~10%；
Wherein, during extrusion molding control temperature be 100~260 DEG C, total drawing ratio be 3~12, oven temperature be 50~
150℃。
To realize above goal of the invention, a kind of preparation method of fragrant artificial lawn fiber of the present invention is：By individual layer or
After multilayer wall building method is prepared into essence microcapsule, finishing method is recycled to be prepared into fragrant artificial lawn fiber, its is specific
Preparation section is：
(1) essence microcapsule, adhesive and water are mixed and made into finishing agent according to certain mass proportioning, it presses quality percentage
Component than composition is：Water 20~80%, essence microcapsule 10~50%, adhesive 5~30%；
(2) it is adhered to artificial turf fiber surface using smearing or compregnate method and is prepared into fragrant artificial turf fiber.
To realize object above, a kind of feature of the preparation method of fragrant artificial lawn fiber of the present invention is microcapsules skill
Application of the art in fragrant artificial lawn fiber preparation.
The positive effect of the present invention is：Can be with the artificial motion lawn manufactured by the fragrant artificial lawn fiber of the present invention
Fragrant breath with natural lawn, odor type can also be adjusted according to demand, and discharge uniform, fragrance remaining time length with fragrance
The characteristics of.
【Embodiment】
A kind of embodiment of fragrant artificial lawn fiber of the present invention presented below and preparation method thereof, provides 3 altogether
Individual embodiment, but the invention is not restricted to the embodiment provided.
Embodiment 1
1. raw material：
(1) careless flavor essence 20kg, neopelex 1kg, urea resin prepolymer 20kg.
(2) essence microcapsule 5kg, acrylic resin 100kg, Masterbatch 5kg, antioxidant 0.5kg, processing aid 1kg.
2. preparation method
First, the preparation of essence microcapsule：
(1) it is newborn under high-speed emulsifying machine effect after careless flavor essence, neopelex and 100kg water are mixed
It is melted into essence emulsion；
(2) and then using single or multiple lift wall building method essence emulsion is wrapped in urea resin prepolymer to prepare essence micro-
Capsule, its form are spherical, and average grain diameter is 10 μm；
(3) emulsified 30 minutes at a high speed as 3000 revs/min using rotating speed in high-speed emulsifying machine and prepare essence emulsion；
(4) essence microcapsule and by single or multiple lift wall building method according to following condition is prepared, reaction temperature is 50 DEG C, pH
It is worth for 4.5, time 30min；
2nd, the preparation of fragrant artificial lawn fiber：
The blending extrusions such as essence microcapsule, matrix resin, Masterbatch and auxiliary agent are molded so as to prepare fragrant artificial lawn
Fiber, wherein, the temperature that controls during extrusion molding is 190 DEG C, and total drawing ratio 5, oven temperature is 50 DEG C.
Prepared fragrant artificial lawn fiber fragrance remaining time can reach more than 3 years.
Embodiment 2
1. raw material：
(1) Rose type essence 20kg, Tween 80 1.5kg, urea resin prepolymer 20kg.
(2) essence microcapsule 5kg, polyvinyl resin 100kg, Masterbatch 5kg, antioxidant 0.5kg, processing aid 1kg.
2. preparation method
First, the preparation of essence microcapsule：
(1) it is emulsified into essence breast in high-speed emulsifying machine effect after Rose type essence, Tween 80 and 120kg water are mixed
Liquid；
(2) and then using single or multiple lift wall building method essence emulsion is wrapped in urea resin prepolymer to prepare essence micro-
Capsule, its form are spherical, and average grain diameter is 15 μm；
(3) emulsified 15 minutes at a high speed as 3000 revs/min using rotating speed in high-speed emulsifying machine and prepare essence emulsion；
(4) essence microcapsule and by single or multiple lift wall building method according to following condition is prepared, reaction temperature is 70 DEG C, pH
It is worth for 4.5, time 60min；
2nd, the preparation of fragrant artificial lawn fiber：
The blending extrusions such as essence microcapsule, matrix resin, Masterbatch and auxiliary agent are molded so as to prepare fragrant artificial lawn
Fiber, wherein, the temperature that controls during extrusion molding is 190 DEG C, and total drawing ratio 5, oven temperature is 50 DEG C.
Prepared fragrant artificial lawn fiber fragrance remaining time can reach more than 3 years.
Embodiment 3
1. raw material：
(1) careless flavor essence 20kg, Span 80 0.5kg, beta-schardinger dextrin 50kg.
(2) essence microcapsule 5kg, adhesive 10kg, deionized water 100kg.
2. preparation method
First, the preparation of essence microcapsule：
(1) it is emulsified into essence breast in high-speed emulsifying machine effect after the water of careless flavor essence, Span 80 and 100kg is mixed
Liquid；
(2) and then essence emulsion is wrapped in beta-schardinger dextrin using single or multiple lift wall building method and prepares essence microcapsule,
Its form is spherical, and average grain diameter is 15 μm；
(3) emulsified 15 minutes at a high speed as 3000 revs/min using rotating speed in high-speed emulsifying machine and prepare essence emulsion；
(4) essence microcapsule and by single or multiple lift wall building method according to following condition is prepared, reaction temperature is 50 DEG C, pH
It is worth for 4, time 60min；
2nd, the preparation of fragrant artificial lawn fiber：
(1) essence microcapsule of above-mentioned preparation, adhesive, deionized water are mixed and made into essence post-finishing agent；
(2) and then by post-finishing agent dip-coating on artificial lawn fiber surface, 80 DEG C of drying prepare fragrant artificial lawn fibre
Dimension.
Prepared fragrant artificial lawn fiber fragrance remaining time can reach more than 3 years.
Claims (6)
- A kind of 1. fragrant artificial lawn fiber, it is characterised in that it is made up of essence microcapsule, matrix resin, Masterbatch and auxiliary agent, Its component formed by mass percentage is：Matrix resin：70~95%, Masterbatch：1~25%, essence microcapsule：0.1~ 10%th, auxiliary agent：0.1~10%.
- 2. a kind of fragrant artificial lawn fiber according to claim 1, it is characterised in that described essence microcapsule is by perfume (or spice) Essence, emulsifying agent and wall material composition, its component formed by mass percentage are：Wall material：30~80%, essence：10~60%, it is newborn Agent：0.01~10%.
- A kind of 3. fragrant artificial lawn fiber according to claim 1 or 2, it is characterised in that the described micro- glue of composition essence The wall material of capsule is that amino resins, epoxy resin, Lauxite, polyurethane, gelatin, gum arabic, maleic anhydride of styrene are common One or more in polymers, cyclodextrin.
- A kind of 4. fragrant artificial lawn fiber according to claim 1 or 2, it is characterised in that the described micro- glue of composition essence The essence of capsule is any one in hay-scented type, rose scent, Forest Bath odor type, jasmine fragrance, lavender flavor type, fruit flavouring Kind.
- A kind of 5. fragrant artificial lawn fiber according to claim 1 or 2, it is characterised in that the described composition essence The emulsifying agent of microcapsules is neopelex, polyoxyethylene sorbitan fatty acid ester, sorbitan-fatty One or more in acid esters, acrylic homopolymer or copolymer, maleic acid anhydride homopolymer or copolymer；Described matrix Resin is TPO；Described auxiliary agent is in processing aid and light stabilizer, antioxidant, antistatic additive, dispersant, plasticizer One or more.
- 6. to realize above goal of the invention, a kind of preparation method of fragrant artificial lawn fiber of the present invention is：Pass through individual layer or more After layer wall building method is prepared into essence microcapsule, blending method is recycled to be prepared into fragrant artificial lawn fiber, prepared by blending method Method includes two steps：Step 1: the preparation of essence microcapsule；Step 2: the preparation of fragrant artificial lawn fiber.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610621894.5A CN107663669A (en) | 2016-07-27 | 2016-07-27 | A kind of fragrant artificial lawn fiber and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610621894.5A CN107663669A (en) | 2016-07-27 | 2016-07-27 | A kind of fragrant artificial lawn fiber and preparation method thereof |
Publications (1)
| Publication Number | Publication Date |
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| CN107663669A true CN107663669A (en) | 2018-02-06 |
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201610621894.5A Pending CN107663669A (en) | 2016-07-27 | 2016-07-27 | A kind of fragrant artificial lawn fiber and preparation method thereof |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN114427148A (en) * | 2022-02-14 | 2022-05-03 | 浙江华东纺织印染有限公司 | Preparation method of Aoli wool |
-
2016
- 2016-07-27 CN CN201610621894.5A patent/CN107663669A/en active Pending
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN114427148A (en) * | 2022-02-14 | 2022-05-03 | 浙江华东纺织印染有限公司 | Preparation method of Aoli wool |
| CN114427148B (en) * | 2022-02-14 | 2023-10-13 | 浙江华东纺织印染有限公司 | Preparation method of Australian wool |
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Application publication date: 20180206 |